[Federal Register Volume 90, Number 105 (Tuesday, June 3, 2025)]
[Proposed Rules]
[Pages 23483-23489]
From the Federal Register Online via the Government Publishing Office [www.gpo.gov]
[FR Doc No: 2025-09983]


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DEPARTMENT OF JUSTICE

Drug Enforcement Administration

21 CFR Part 1310

[Docket No. DEA-1189]


Designation of Propionyl Chloride as a List I Chemical

AGENCY: Drug Enforcement Administration, Department of Justice.

ACTION: Notice of proposed rulemaking.

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SUMMARY: The Drug Enforcement Administration is proposing the control 
of propionyl chloride as a list I chemical under the Controlled 
Substances Act (CSA). The Drug Enforcement Administration finds that 
propionyl chloride is used in the illicit manufacture of the controlled 
substances fentanyl, fentanyl analogues and fentanyl-related 
substances, and is important to the manufacture of these substances. In 
the respective synthetic pathways in which it is used to manufacture 
those substances, it is a replacement for propionic anhydride, which is 
currently a list I chemical. If finalized, the proposed rule would 
subject handlers of propionyl chloride to the chemical regulatory 
provisions of the CSA and its implementing regulations. This proposed 
rulemaking does not establish a threshold for domestic and 
international transactions of propionyl chloride. As such, all 
transactions of propionyl chloride, regardless of size, shall be 
regulated. In addition, chemical mixtures containing propionyl chloride 
are not exempt from regulatory requirements at any concentration. 
Therefore, all transactions of chemical mixtures containing any 
quantity of propionyl chloride shall be regulated pursuant to the CSA. 
Although no automatic exemption is available, manufacturers may submit 
an application for exemption.

DATES: Comments must be submitted electronically or postmarked on or 
before July 3, 2025. Commenters should be aware that the electronic 
Federal Docket Management System will not accept any comments after 
11:59 p.m. Eastern Time on the last day of the comment period.

ADDRESSES: To ensure proper handling of comments, please reference 
``Docket No. DEA-1189'' on all electronic and written correspondence, 
including any attachments.
     Electronic comments: The Drug Enforcement Administration 
encourages that all comments be submitted electronically through the 
Federal eRulemaking Portal which provides the ability to type short 
comments directly into the comment field on the web page or attach a 
file for lengthier comments. Please go to http://www.regulations.gov 
and follow the online instructions at that site for submitting 
comments. Upon completion of your submission, you will receive a 
Comment Tracking Number for your comment. Please be aware that 
submitted comments are not instantaneously available for public view on 
Regulations.gov. If you have received a Comment Tracking Number, your 
comment has been successfully submitted and there is no need to 
resubmit the same comment.
     Paper comments: Paper comments that duplicate electronic 
submissions are not necessary. Should you wish to mail a paper comment, 
in lieu of an electronic comment, it should be sent via regular or 
express mail to: Drug Enforcement Administration, Attn: DEA Federal 
Register Representative/DPW,

[[Page 23484]]

8701 Morrissette Drive, Springfield, Virginia 22152.
     Paperwork Reduction Act Comments: All comments concerning 
collections of information under the Paperwork Reduction Act must be 
submitted to the Office of Information and Regulatory Affairs, OMB, 
Attention: Desk Officer for DOJ, Washington, DC 20503. Please state 
that your comment refers to Docket No. DEA-1189.

FOR FURTHER INFORMATION CONTACT: Terrence L. Boos, Drug and Chemical 
Evaluation Section, Diversion Control Division, Drug Enforcement 
Administration; Telephone: (571) 362-3249. As required by 5 U.S.C. 
553(b)(4), a summary of this rule may be found in the docket for this 
rulemaking at www.regulations.gov.

SUPPLEMENTARY INFORMATION:

Posting of Public Comments

    Please note that all comments received in response to this docket 
are considered part of the public record. DEA will make comments 
available for public inspection online at http://www.regulations.gov. 
Such information includes personal or business identifiers (such as 
name, address, state or Federal identifiers, etc.) voluntarily 
submitted by the commenter. Generally, all information voluntarily 
submitted by the commenter, unless clearly marked as Confidential 
Information in the method described below, will be publicly posted. 
Comments may be submitted anonymously. The Freedom of Information Act 
applies to all comments received.
    Commenters submitting comments which include personal identifying 
information (PII), confidential, or proprietary business information 
that the commenter does not want made publicly available should submit 
two copies of the comment. One copy must be marked ``CONTAINS 
CONFIDENTIAL INFORMATION'' and should clearly identify all PII or 
business information the commenter does not want to be made publicly 
available, including any supplemental materials. DEA will review this 
copy, including the claimed PII and confidential business information, 
in its consideration of comments. The second copy should be marked ``TO 
BE PUBLICLY POSTED'' and must have all claimed confidential PII and 
business information already redacted. DEA will post only the redacted 
comment on http://www.regulations.gov for public inspection.
    For easy reference, an electronic copy of this document and 
supplemental information to this proposed scheduling action are 
available at http://www.regulations.gov.

Legal Authority

    The Controlled Substances Act (CSA) gives the Attorney General the 
authority to specify, by regulation, chemicals as list I chemicals.\1\ 
A ``list I chemical'' is a chemical that is used in manufacturing a 
controlled substance in violation of the CSA and is important to the 
manufacture of the controlled substance.\2\ The current list of all 
listed chemicals is published at 21 CFR 1310.02. Pursuant to 28 CFR 
0.100(b), the Attorney General has delegated his authority to designate 
list I chemicals to the Administrator of DEA (Administrator). DEA 
regulations set forth the process by which DEA may add a chemical as a 
listed chemical. As set forth in 21 CFR 1310.02(c), the agency may do 
so by publishing a final rule in the Federal Register following a 
published notice of proposed rulemaking (NPRM) with at least 30 days 
for public comments.
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    \1\ 21 U.S.C. 802(34).
    \2\ Id.
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Background

    The clandestine manufacture of fentanyl, fentanyl analogues, and 
fentanyl-related substances remains extremely concerning as the 
distribution of illicit fentanyl, fentanyl analogues, and fentanyl-
related substances continues to drive drug-related overdose deaths in 
the United States. Fentanyl is a synthetic opioid and was first 
synthesized in Belgium in the late 1950s. Fentanyl was introduced into 
medical practice and is approved for medical practitioners in the 
United States to prescribe lawfully for anesthesia and analgesia. Yet, 
due to its pharmacological effects, fentanyl can be used as a 
substitute for heroin, oxycodone, and other opioids in opioid dependent 
individuals. Therefore, despite its currently accepted medical use in 
treatment in the United States, DEA controls fentanyl as a schedule II 
controlled substance due to its high potential for abuse and the 
possibility that abuse may lead to severe psychological or physical 
dependence.\3\ Moreover, there are a substantial number of fentanyl 
analogues and fentanyl-related substances that are being distributed on 
the illicit drug market despite DEA's actions adding them as schedule I 
controlled substances. Illicit manufacturers attempt to utilize 
unregulated precursor chemicals to evade law enforcement detection and 
precursor chemical controls in order to manufacture fentanyl, fentanyl 
analogues, and fentanyl-related substances. This strategy allows for 
the synthesis of a variety of fentanyl analogues and fentanyl-related 
substances by making slight modifications to the core fentanyl 
structure while maintaining the same synthetic methodology used to 
synthesize fentanyl, fentanyl analogues, and fentanyl-related 
substances.
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    \3\ 21 U.S.C. 812(c) Schedule II(b)(6) and 21 CFR 1308.12(c).
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    The unlawful trafficking of fentanyl, fentanyl analogues, and 
fentanyl-related substances in the United States continues to pose an 
imminent hazard to the public safety. Since 2012, fentanyl has shown a 
dramatic increase in the illicit drug supply as a single substance, in 
mixtures with other illicit drugs (i.e., heroin, cocaine, and 
methamphetamine), and in forms that mimic pharmaceutical preparations 
including prescription opiates.\4\
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    \4\ National Drug Threat Assessment 2024, Drug Enforcement 
Administration, May 2024.
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    DEA has noted a significant increase in overdoses and overdose 
fatalities from fentanyl, fentanyl analogues, and fentanyl-related 
substances in the United States in recent years. According to the 
Centers for Disease Control and Prevention (CDC), opioids, mainly 
synthetic opioids (which include fentanyl), are predominantly 
responsible for drug overdose deaths in recent years. According to CDC 
WONDER,\5\ drug-induced overdose deaths involving synthetic opioids 
(excluding methadone) in the United States increased from 36,359 in 
2019 to 56,516 in 2020 to 70,601 in 2021, and 73,838 in 2022. Based on 
provisional data, the predicted number of drug overdose deaths 
involving synthetic opioids (excluding methadone) in the United States 
for the 12 months ending March 2024 is 70,972 individuals, or 
approximately 70 percent of all drug-induced overdose deaths for that 
time period.\6\ The increase in overdose fatalities involving synthetic 
opioids coincides with a dramatic increase in law enforcement 
encounters of fentanyl, fentanyl analogues, and fentanyl-related

[[Page 23485]]

substances. According to the National Forensic Laboratory Information 
System (NFLIS-Drug),\7\ reports from forensic laboratories of drug 
items containing fentanyl, fentanyl analogues, and fentanyl-related 
substances increased dramatically since 2014, as shown in Table 1.
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    \5\ Centers for Disease Control and Prevention, National Center 
for Health Statistics. National Vital Statistics System, Provisional 
Mortality on CDC WONDER Online Database. Data are from the final 
Multiple Cause of Death Files, 2018-2022, and from provisional data 
for years 2022-2024, as compiled from data provided by the 57 vital 
statistics jurisdictions through the Vital Statistics Cooperative 
Program. Accessed at http://wonder.cdc.gov/mcd-icd10-provisional.html on August 16, 2024.
    \6\ Ahmad FB, Cisewski JA, Rossen LM, Sutton P. Provisional drug 
overdose death counts. National Center for Health Statistics. 2024. 
Accessed at https://www.cdc.gov/nchs/nvss/vsrr/drug-overdose-data.htm on August 16, 2024.
    \7\ The National Forensic Laboratory Information System (NFLIS-
Drug) is a national forensic laboratory reporting system that 
systematically collects results from drug chemistry analyses 
conducted by Federal, State and local forensic laboratories in the 
United States. While NFLIS-Drug data is not direct evidence of 
abuse, it can lead to an inference that a drug has been diverted and 
abused. See 76 FR 77330, 77332 (December 12, 2011). NFLIS-Drug data 
was queried on December 14, 2023.

             Table 1--Annual Reports of Fentanyl and Select Fentanyl Analogues and Fentanyl-Related Substances Identified in Drug Encounters
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                              Year                                 2014     2015     2016     2017     2018      2019       2020       2021       2022
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Annual Fentanyl Reports........................................    5,554   15,461   37,155   61,644   89,974    108,138    126,042    165,486    168,768
Annual Reports of select fentanyl analogues and fentanyl-             78    2,317    7,624   21,981   16,177     20,918      7,804     26,468     29,919
 related substances............................................
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Role of Propionyl Chloride in the Synthesis of Fentanyl

    Fentanyl, fentanyl analogues, and fentanyl-related substances are 
not naturally occurring substances. As such, the manufacture of these 
substances requires them to be produced through synthetic organic 
chemistry. Synthetic organic chemistry is the process in which a new 
organic molecule is created through a series of chemical reactions, 
which involve precursor chemicals. Through chemical reactions, the 
chemical structures of precursor chemicals are modified in a desired 
fashion. These chemical reaction sequences, also known as synthetic 
pathways, are designed to create a desired substance. Several synthetic 
pathways to fentanyl, fentanyl analogues, and fentanyl-related 
substances have been identified in clandestine laboratory settings; 
these include the original ``Janssen method,'' the ``Siegfried 
method,'' and the ``Gupta method.'' In response to the illicit 
manufacture of fentanyl, fentanyl analogues, and fentanyl-related 
substances using these methods, DEA controlled N-phenethyl-4-piperidone 
(NPP); \8\ N-(1-benzylpiperidin-4-yl)-N-phenylpropionamide 
(benzylfentanyl) and its salts; \9\ N-phenylpiperidin-4-amine (4-
anilinopiperidine) including its amides, halides, carbamates, salts, 
and any combination thereof; \10\ and 4-piperidone (piperidin-4-one) 
including its acetals, amides, carbamates, salts, and salts of acetals, 
amides, and carbamates, and any combination thereof \11\ as list I 
chemicals. DEA also controls 4-anilino-N-phenethylpiperidine (ANPP) 
\12\ and N-phenyl-N-(piperidin-4-yl)propionamide (norfentanyl) \13\ as 
schedule II immediate precursors under the CSA.
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    \8\ Control of a Chemical Precursor Used in the Illicit 
Manufacture of Fentanyl as a List I Chemical, 72 FR 20039 (Apr. 23, 
2007).
    \9\ Designation of Benzylfentanyl and 4-Anilinopiperidine, 
Precursor Chemicals Used in the Illicit Manufacture of Fentanyl, as 
List I Chemicals, 85 FR 20822 (Apr. 15, 2020).
    \10\ Designation of Benzylfentanyl and 4-Anilinopiperidine, 
Precursor Chemicals Used in the Illicit Manufacture of Fentanyl, as 
List I Chemicals, 85 FR 20822 (Apr. 15, 2020).); See Also 
Designation of Halides of 4-Anilinopiperidine as List 1 Chemicals, 
88 FR 74352 (Oct. 31, 2023).
    \11\ Designation of 4-Piperidone as a List I Chemical, 88 FR 
21902-21910 (Apr. 12, 2023).
    \12\ Control of Immediate Precursor Used in the Illicit 
Manufacture of Fentanyl as a Schedule II Controlled Substance, 75 FR 
37295 (June 29, 2010).
    \13\ Control of the Immediate Precursor Norfentanyl Used in the 
Illicit Manufacture of Fentanyl as a Schedule II Controlled 
Substance, 85 FR 21320 (Apr. 17, 2020).
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Propionyl Chloride

    The original published synthetic pathway to fentanyl, known as the 
Janssen method, involves the list I chemical benzylfentanyl and 
schedule II immediate precursor norfentanyl. In this synthetic pathway, 
benzylfentanyl, a list I chemical under the CSA,\14\ is synthesized by 
reacting propionyl chloride with 4-anilino-1-benzylpiperidine, which is 
then converted to norfentanyl, the schedule II immediate precursor in 
this synthetic pathway.\15\ Norfentanyl is then subjected to one simple 
chemical reaction to complete the synthesis of fentanyl. This synthetic 
pathway can also be easily modified to produce fentanyl analogues and 
fentanyl-related substances. Propionyl chloride also serves as a 
precursor chemical in the Siegfried method. In this synthetic pathway, 
propionyl chloride is reacted with ANPP,\16\ the schedule II immediate 
precursor in the Siegfried method, to complete the synthesis of 
fentanyl. This synthetic pathway can also be easily modified to produce 
fentanyl analogues and fentanyl-related substances. In addition to the 
Janssen and Siegfried methods, clandestine manufacturers are using 
other methods to synthesize fentanyl, one of which is known as the 
Gupta method. In this synthetic pathway, 4-piperidone, a list I 
chemical under the CSA, is used to synthesize 4-anilinopiperidine, 
another list I chemical under the CSA,\17\ which serves as an 
alternative precursor chemical to NPP, a list I chemical, in the 
synthesis of ANPP, a schedule II immediate precursor albeit through a 
different synthetic process. The resulting ANPP is reacted with 
propionyl chloride to manufacture the schedule II controlled substance, 
fentanyl. This synthetic pathway can also be easily modified to produce 
fentanyl analogues and fentanyl-related substances.
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    \14\ See footnote 10.
    \15\ See footnote 13.
    \16\ See footnote 12.
    \17\ Designation of Benzylfentanyl and 4-Anilinopiperidine, 
Precursor Chemicals Used in the Illicit Manufacture of Fentanyl, as 
List I Chemicals, 85 FR 20822 (May 15, 2020).
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    Propionyl chloride is attractive to illicit manufacturers because 
there is a lack of regulations on this chemical, it is readily 
available from chemical suppliers, and it can be easily used in many 
known synthetic pathways used in the illicit manufacture of fentanyl, 
fentanyl analogues, and fentanyl-related substances.

Information Gathered by DEA Concerning Propionyl Chloride

    On October 12, 2023, DEA published in the Federal Register an 
Advance Notice of Proposed Rulemaking (ANPRM) \18\ in anticipation of 
proposing to designate propionyl chloride as a list I chemical. The 
ANPRM invited interested persons to submit information related to 
current uses of propionyl chloride (other than for the synthesis of 
fentanyl) in order to properly determine the effect such a proposed 
action would have on legitimate industry.
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    \18\ Propionyl Chloride, 88 FR 70610 (Oct. 12, 2023).
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    DEA solicited input from all potentially affected parties 
regarding: (1) The types of legitimate industries using propionyl 
chloride; (2) the legitimate uses, legitimate needs and quantity

[[Page 23486]]

produced, used, and distributed of propionyl chloride; (3) the size of 
the domestic market for propionyl chloride; (4) the number of 
manufacturers of propionyl chloride; (5) the number of distributors of 
propionyl chloride; (6) the level of import and export of propionyl 
chloride; (7) the potential burden that controlling propionyl chloride 
as a list I chemical may have on any legitimate industry and trade; (8) 
the potential number of individuals/firms that may be adversely 
affected by such regulatory controls (particularly with respect to the 
impact on small businesses); and (9) any other information on the 
manner of manufacturing, distribution, consumption, storage, disposal, 
and uses of propionyl chloride by industry and others. DEA invited all 
interested parties to provide any information on any legitimate uses of 
propionyl chloride in industry, commerce, academia, research and 
development, or other applications. DEA sought both quantitative and 
qualitative data.

Comments

    DEA received six responses to the ANPRM. Three of the comments were 
in support of the control of propionyl chloride as a list I chemical, 
while three comments offered potential problems with controlling 
propionyl chloride.
    Relevant to solicitations (1) and (2), three commenters stated that 
propionyl chloride has potential use as a reagent for chemical 
synthesis processes, including in the natural product syntheses of N-
deoxymilitarinone A and torrubiellone B, potential pharmaceutical 
development, resin/materials development, and agricultural chemicals. 
One of the commenters stated that it may have uses for the medical 
field, without providing additional detail. While one of the comments 
provided patent numbers and a published letter to support the existence 
of these potential uses, there were no details allowing DEA to identify 
the existence or extent of the actual use of propionyl chloride for 
these purposes.
    Relevant to solicitation (7), two commenters stated that 
controlling propionyl chloride as a list I chemical is likely to have a 
burden on legitimate industry and trade in that it will make the 
chemical more expensive and difficult to access for chemical and 
pharmaceutical research labs and will ``impact researchers greatly.'' A 
third commenter stated that distributors, manufacturers, importers, and 
exporters of propionyl would be required to pay DEA registration fees 
if propionyl chloride is placed in list I. Another commenter, however, 
stated that it may primarily be used by ``personnel who would already 
possess any documentation needed to obtain it.''
    Relevant to solicitation (8), one commenter stated that PubChem 
lists 43 vendors currently offering to supply propionyl chloride.

Regulation of Propionyl Chloride as a List I Chemical

    The CSA, specifically 21 U.S.C. 802(34), and its implementing 
regulations at 21 CFR 1310.02(c), provide the Attorney General with the 
authority to specify, by regulation, additional precursor or essential 
chemicals as listed chemicals if they are used in the manufacture of 
controlled substances in violation of the CSA. Recent law enforcement 
encounters indicate propionyl chloride is being used in the illicit 
manufacture of the schedule II controlled substance fentanyl. This 
proposed rule would regulate propionyl chloride as a list I chemical 
because DEA finds that propionyl chloride is used in the illicit 
manufacture of the controlled substance fentanyl, and is important to 
the manufacture of the controlled substance fentanyl because it can be 
used as a replacement for the list I chemical propionic anhydride in 
its respective synthetic pathways which are used in the illicit 
manufacture of fentanyl.

Chemical Mixtures of Propionyl Chloride

    This proposed rulemaking, if finalized, would specify that chemical 
mixtures containing propionyl chloride would not be exempt from 
regulatory requirements at any concentration, unless an application for 
exemption of a chemical mixture is submitted by a propionyl chloride 
manufacturer and the application is reviewed and accepted by DEA under 
21 CFR 1310.13. The control of chemical mixtures containing any amount 
of propionyl chloride is necessary to prevent the extraction, 
isolation, and use of propionyl chloride in the illicit manufacture of 
fentanyl. This proposed rule would modify the Table of Concentration 
Limits in 21 CFR 1310.12(c) to reflect the fact that chemical mixtures 
containing any amount of propionyl chloride are subject to the CSA 
chemical control provisions.

Exemption by Application Process

    DEA has implemented an application process to exempt mixtures from 
the requirements of the CSA and its implementing regulations.\19\ Under 
the application process, manufacturers may submit an application for 
exemption for those mixtures that do not qualify for automatic 
exemption. Exemption status can be granted if DEA determines that the 
mixture is formulated in such a way that it cannot be easily used in 
the illicit production of a controlled substance and that the listed 
chemical cannot be readily recovered.\20\
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    \19\ 21 CFR 1310.13.
    \20\ 21 CFR U.S.C. 802(39)(A)(vi).
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Requirements for Handling List I Chemicals

    If this rule is finalized as proposed, propionyl chloride will be 
subject to all of the regulatory controls and administrative, civil, 
and criminal sanctions applicable to the manufacture, distribution, 
importing, and exporting of list I chemicals. Upon publication of a 
final rule, persons potentially handling propionyl chloride, including 
regulated chemical mixtures containing propionyl chloride, will be 
required to comply with list I chemical regulations, including the 
following:
    1. Registration. Any person who manufactures, distributes, imports, 
or exports propionyl chloride, including chemical mixtures containing 
propionyl chloride, or proposes to engage in the manufacture, 
distribution, importation, or exportation of propionyl chloride, 
including chemical mixtures containing propionyl chloride, must obtain 
a registration pursuant to 21 U.S.C. 822, 823, 957, and 958. 
Regulations describing registration for list I chemical handlers are 
set forth in 21 CFR part 1309. DEA regulations require separate 
registrations for manufacturing, distributing, importing, and exporting 
of list I chemicals. 21 CFR 1309.21. Further, a separate registration 
is required for each principal place of business at one general 
physical location where list I chemicals are manufactured, distributed, 
imported, or exported by a person. 21 U.S.C. 822(e)(1) and 21 CFR 
1309.23(a).
    DEA notes that under the CSA, ``warehousemen'' are not required to 
register and may lawfully possess list I chemicals, if the possession 
of those chemicals is in the usual course of business or employment. 
Under DEA implementing regulations, the warehouse in question must 
receive the list I chemical from a DEA registrant and shall only 
distribute the list I chemical back to the DEA registrant and 
registered location from which it was received. A warehouse that 
distributes list I chemicals to persons other than the registrant and 
registered location from

[[Page 23487]]

which they were obtained is conducting distribution activities and is 
required to register as such.
    Upon publication of a final rule, any person manufacturing, 
distributing, importing, or exporting propionyl chloride or a chemical 
mixture containing propionyl chloride would become subject to the 
registration requirement under the CSA. DEA recognizes, however, that 
it is not possible for persons who are subject to the registration 
requirements to immediately complete and submit an application for 
registration, and for DEA to immediately issue registrations for those 
activities. Therefore, to allow any continued legitimate commerce in 
propionyl chloride or a chemical mixture containing propionyl chloride, 
DEA is proposing to establish in 21 CFR 1310.09, a temporary exemption 
from the registration requirement for persons desiring to engage in 
activities with propionyl chloride or a chemical mixture containing 
propionyl chloride, provided that DEA receives a properly completed 
application for registration or application for exemption of a chemical 
mixture under 21 CFR 1310.13 on or before 30 days after publication of 
a final rule implementing regulations regarding propionyl chloride. The 
temporary exemption for such persons will remain in effect until DEA 
takes final action on their application for registration or application 
for exemption of a chemical mixture.
    The temporary exemption applies solely to the registration 
requirement; all other chemical control requirements, including 
recordkeeping and reporting, would become effective on the effective 
date of the final rule. This is necessary because a delay in regulating 
these transactions could result in increased diversion of chemicals 
desirable to drug traffickers.
    Additionally, the temporary exemption for registration does not 
suspend applicable federal criminal laws relating to propionyl 
chloride, nor does it supersede State or local laws or regulations. All 
handlers of propionyl chloride must comply with applicable State and 
local requirements in addition to the CSA regulatory controls.
    2. Records and Reports. Every DEA registrant would be required to 
maintain records and submit reports with respect to propionyl chloride 
pursuant to 21 U.S.C. 830 and in accordance with 21 CFR 1310.04 and 
1310.05. Pursuant to 21 CFR 1310.04, a record must be kept for two 
years after the date of a transaction involving a listed chemical, 
provided the transaction is a regulated transaction.
    Each regulated bulk manufacturer of a listed chemical will be 
required to submit manufacturing, inventory, and use data on an annual 
basis. 21 CFR 1310.05(d). Existing standard industry reports containing 
the required information are acceptable, provided the information is 
separate or readily retrievable from the report.
    The CSA and its implementing regulations require that each 
regulated person must report to DEA any regulated transaction involving 
an extraordinary quantity of a listed chemical, an uncommon method of 
payment or delivery, or any other circumstance that the regulated 
person believes may indicate that the listed chemical will be used in 
violation of subchapter I of the CSA. In addition, regulated persons 
must report any proposed regulated transaction with a person whose 
description or other identifying characteristics DEA has previously 
furnished to the regulated person, any unusual or excessive loss or 
disappearance of a listed chemical under the control of the regulated 
person, and any in-transit loss in which the regulated person is the 
supplier. 21 U.S.C. 830(b) and 21 CFR 1310.05(a) and (b).
    3. Importation and Exportation. All importation and exportation of 
propionyl chloride or a chemical mixture containing propionyl chloride 
would need to be done in compliance with 21 U.S.C. 957, 958, and 971 
and in accordance with 21 CFR part 1313.
    4. Security. All applicants and registrants would be required to 
provide effective controls against theft and diversion of list I 
chemicals in accordance with 21 CFR 1309.71-1309.73.
    5. Administrative Inspection. Places, including factories, 
warehouses, or other establishments and conveyances, where registrants 
or other regulated persons may lawfully hold, manufacture, distribute, 
or otherwise dispose of a list I chemical or where records relating to 
those activities are maintained, are controlled premises as defined in 
21 U.S.C. 880(a) and 21 CFR 1316.02(c). The CSA allows for 
administrative inspections of these controlled premises as provided in 
21 CFR part 1316, subpart A. 21 U.S.C. 880.
    6. Liability. Any activity involving propionyl chloride not 
authorized by, or in violation of, the CSA, would be unlawful, and 
would subject the person to administrative, civil, and/or criminal 
action.

Regulatory Analyses

Executive Orders 12866, 1356, and 14192 (Regulatory Review)

    DEA has determined that this rulemaking is not a ``significant 
regulatory action'' under section 3(f) of Executive Order (E.O.) 12866, 
Regulatory Planning and Review. Accordingly, this proposed rule has not 
been submitted to the Office of Management and Budget for review. This 
proposed rule has been drafted and reviewed in accordance with E.O. 
12866, ``Regulatory Planning and Review,'' section 1(b), Principles of 
Regulation and E.O. 13563, ``Improving Regulation and Regulatory 
Review,'' section 1(b), General Principles of Regulation. DEA 
scheduling actions are not subject to E.O. 14192, ``Unleashing 
Prosperity Through Deregulation.''
    DEA is proposing the control of propionyl chloride as a list I 
chemical under the CSA. DEA finds that propionyl chloride is used in 
the illicit manufacture of the controlled substances fentanyl, fentanyl 
analogues and fentanyl-related substances, and is important to the 
manufacture of these substances. The replacement chemical for propionyl 
chloride in the respective pathways is already a list I chemical. If 
finalized, the proposed rule would subject handlers of propionyl 
chloride to the chemical regulatory provisions of the CSA and its 
implementing regulations. This proposed rulemaking does not establish a 
threshold for domestic and international transactions of propionyl 
chloride. As such, all transactions of propionyl chloride, regardless 
of size, shall be regulated. In addition, chemical mixtures containing 
propionyl chloride are not exempt from regulatory requirements at any 
concentration. Therefore, all transactions of chemical mixtures 
containing any quantity of propionyl chloride shall be regulated 
pursuant to the CSA. If finalized as proposed, propionyl chloride will 
be subject to all of the regulatory control and administrative, civil, 
and criminal sanctions applicable to the manufacture, distribution, 
importing, and exporting of list I chemicals.
    DEA evaluated the cost of this proposed rule. Due to many unknowns, 
DEA is unable to provide an estimated cost of this proposed rule; 
however, DEA believes the cost will not be significant and will be far 
below the E.O. 12866 3(f)(1) threshold.
    Propionyl chloride is used for the legitimate manufacturing of 
pharmaceutical fentanyl as well as clandestinely synthesized illicit 
fentanyl. DEA has searched information

[[Page 23488]]

in the public domain for legitimate uses of propionyl chloride and has 
not documented a legitimate commercial or industrial use for propionyl 
chloride other than as an intermediary chemical in the production of 
fentanyl. DEA welcomes any comments related to the uses of propionyl 
chloride in the legitimate marketplace.
    The primary costs associated with this proposed rule would be the 
annual registration fee for list I chemicals ($3,699 for manufacturers 
and $1,850 for distributors, importers, and exporters). DEA has 
identified 20 domestic distributors of propionyl chloride. Three are 
already registered to handle list I chemicals, and this rule will not 
have impacts on their operations. The remaining distributors will need 
to register with DEA and employ security and handling processes to 
continue supplying propionyl chloride. For the nonregistered suppliers, 
it is difficult to estimate the amount of propionyl chloride that they 
distribute. It is also common for these chemical distributors to have 
items in their catalog while not actually having any material level of 
sales. Hence, DEA expects the quantities of propionyl chloride 
distributed by nonregistered distributors is much smaller compared to 
the registered distributors. If this proposed rule is finalized, these 
distributors are expected to choose the least cost option, and stop 
selling propionyl chloride, rather than incur the registration cost. 
DEA expects that the cost of foregone sales is small; and thus, the 
cost of this proposed rule is minimal. DEA welcomes any public comment 
regarding this estimate.
    In summary, DEA conducted a qualitative analysis of this proposed 
rule. DEA believes any manufacturer or distributor that uses propionyl 
chloride for legitimate pharmaceutical fentanyl production already 
would be registered with DEA and have all security and other handling 
processes in place, such that this regulation would result in minimal 
cost to those entities. Therefore, any potential cost as a result of 
this regulation is minimal.

Executive Order 12988, Civil Justice Reform

    This proposed regulation meets the applicable standards set forth 
in sections 3(a) and 3(b)(2) of E.O. 12988 Civil Justice Reform to 
eliminate drafting errors and ambiguity, minimize litigation, provide a 
clear legal standard for affected conduct, and promote simplification 
and burden reduction.

Executive Order 13132, Federalism

    This proposed rulemaking does not have federalism implications 
warranting the application of E.O. 13132. The proposed rule does not 
have substantial direct effects on the States, on the relationship 
between the national Government and the States, or the distribution of 
power and responsibilities among the various levels of government.

Executive Order 13175, Consultation and Coordination With Indian Tribal 
Governments

    This proposed rule does not have tribal implications warranting the 
application of E.O. 13175. This proposed rule does not have substantial 
direct effects on one or more Indian tribes, on the relationship 
between the Federal government and Indian tribes, or on the 
distribution of power and responsibilities between the Federal 
government and Indian tribes.

Regulatory Flexibility Act

    The Acting Administrator, in accordance with the Regulatory 
Flexibility Act, 5 U.S.C. 601-612, has reviewed this rule and by 
approving it, certifies that it will not have a significant economic 
impact on a substantial number of small entities.
    As discussed above, if finalized as proposed, propionyl chloride 
and chemical mixtures containing propionyl chloride will be subject to 
all of the regulatory controls and administrative, civil, and criminal 
sanctions applicable to the manufacture, distribution, importing, and 
exporting of list I chemicals. If finalized, it will affect all 
business activities that handle propionyl chloride including 
manufacturers, distributors, importers, and exporters. DEA identified 
20 domestic suppliers, 17 (85 percent) of which are not registered with 
DEA to handle list I chemicals. All non-registered entities will be 
affected by this rule and are small entities based on Small Business 
Administration classification for Other Chemical and Allied Products 
Merchant Wholesalers (NAICS classification code 424690).\21\
---------------------------------------------------------------------------

    \21\ U.S. Small Business Administration, Table of size 
standards, Version March 2023, Effective: March 17, 2023, https://www.sba.gov/sites/sbagov/files/2023-.
---------------------------------------------------------------------------

    There are 8,804 small entities under 424690 Other Chemical and 
Allied Products Merchant Wholesalers.\22\ The number of small entities 
affected by this proposed rule is 0.19 percent of all the small 
businesses in this industry.\23\ Based on these factors, DEA projects 
that this rule, if promulgated, will not result in a significant 
economic impact on a substantial number of small entities.
---------------------------------------------------------------------------

    \22\ 2021 SUSB Annual Data Tables by Establishment Industry, 
https://www.census.gov/data/tables/2021/econ/susb/2021-susb-annual.html, accessed: 1/9/2024.
    \23\ Assuming all of the 17 non-registered suppliers are small 
businesses, the percent of small businesses affected by this rule is 
17/8,804 = 0.19%.
---------------------------------------------------------------------------

Unfunded Mandates Reform Act of 1995

    On the basis of information contained in the ``Regulatory 
Flexibility Act'' section above, DEA has determined and certifies 
pursuant to the Unfunded Mandates Reform Act of 1995 (UMRA), 2 U.S.C. 
1501 et seq., that this action would not result in any Federal mandate 
that may result ``in the expenditure by State, local, and tribal 
governments, in the aggregate, or by the private sector, of 
$100,000,000 or more (adjusted for inflation) in any one year . . . .'' 
Therefore, neither a Small Government Agency Plan nor any other action 
is required under provisions of UMRA.

Paperwork Reduction Act of 1995

    This action does not impose any new or revised ``collection[s] of 
information'' as defined by the Paperwork Reduction Act of 1995, 44 
U.S.C. 3502(3).

List of Subjects in 21 CFR Part 1310

    Administrative practice and procedure, Drug traffic control, 
Reporting and recordkeeping requirements.

    For the reasons set out above, DEA proposes to amend 21 CFR part 
1310 as follows:

PART 1310--RECORDS AND REPORTS OF LISTED CHEMICALS AND CERTAIN 
MACHINES; IMPORTATION AND EXPORTATION OF CERTAIN MACHINES

0
1. The authority citation for part 1310 continues to read as follows:

    Authority:  21 U.S.C. 802, 827(h), 830, 871(b), 890.

0
2. In Sec.  1310.02, add paragraph (a)(40) to read as follows:


Sec.  1310.02  Substances covered.

* * * * *
    (a) * * *
* * * * *

 
 
 
(40) Propionyl chloride.........................................   8337
 

* * * * *
0
3. In Sec.  1310.04:
0
a. Redesignate paragraphs (g)(1)(xviii) and (g)(1)(xix) as paragraphs 
(g)(1)(xix) and (g)(1)(xx), respectively; and

[[Page 23489]]

0
b. Add new paragraph (g)(1)(xviii) to read as follows:


Sec.  1310.04  Maintenance of records.

* * * * *
    (g) * * *
    (1) * * *
    (xviii) Propionyl chloride
* * * * *
0
4. In Sec.  1310.09 add paragraph (t) to read as follows:


Sec.  1310.09  Temporary exemption from registration.

* * * * *
    (t)(1) Each person required under 21 U.S.C. 822 and 21 U.S.C. 957 
to obtain a registration to manufacture, distribute, import, or export 
propionyl chloride, including regulated chemical mixtures pursuant to 
Sec.  1310.12, is temporarily exempted from the registration 
requirement, provided that DEA receives a properly completed 
application for registration or application for exemption for a 
chemical mixture containing propionyl chloride pursuant to Sec.  
1310.13 on or before 30 days after the publication of a rule finalizing 
this action. The exemption would remain in effect for each person who 
has made such application until the Administration has approved or 
denied that application. This exemption applies only to registration; 
all other chemical control requirements set forth in the Act and parts 
1309, 1310, 1313, and 1316 of this chapter remain in full force and 
effect.
    (2) Any person who manufactures, distributes, imports, or exports a 
chemical mixture containing propionyl chloride whose application for 
exemption is subsequently denied by DEA must obtain a registration with 
DEA. A temporary exemption from the registration requirement will also 
be provided for those persons whose application for exemption is 
denied, provided that DEA receives a properly completed application for 
registration on or before 30 days following the date of official DEA 
notification that the application for exemption has been denied. The 
temporary exemption for such persons would remain in effect until DEA 
takes final action on their registration application.
0
5. In 1310.12, amend the table in paragraph (c) by adding in 
alphabetical order an entry for ``propionyl chloride'' to read as 
follows:


Sec.  1310.12  Exempt chemical mixtures.

* * * * *
    (c) * * *

                                          Table of Concentration Limits
----------------------------------------------------------------------------------------------------------------
                                             DEA
                                           chemical
                                             code           Concentration               Special conditions
                                            number
----------------------------------------------------------------------------------------------------------------
                                                List I Chemicals
----------------------------------------------------------------------------------------------------------------
 
                                                  * * * * * * *
Propionyl chloride......................       8337  Not exempt at any           Chemical mixtures containing
                                                      concentration.              any amount of propionyl
                                                                                  chloride are not exempt.
 
                                                  * * * * * * *
----------------------------------------------------------------------------------------------------------------

* * * * *

Signing Authority

    This document of the Drug Enforcement Administration was signed on 
May 25, 2025, by Acting Administrator Robert J. Murphy. That document 
with the original signature and date is maintained by DEA. For 
administrative purposes only, and in compliance with requirements of 
the Office of the Federal Register, the undersigned DEA Federal 
Register Liaison Officer has been authorized to sign and submit the 
document in electronic format for publication, as an official document 
of DEA. This administrative process in no way alters the legal effect 
of this document upon publication in the Federal Register.

Heather Achbach,
Federal Register Liaison Officer, Drug Enforcement Administration.
[FR Doc. 2025-09983 Filed 6-2-25; 8:45 am]
BILLING CODE 4410-09-P