[Federal Register Volume 61, Number 165 (Friday, August 23, 1996)]
[Proposed Rules]
[Pages 43501-43515]
From the Federal Register Online via the Government Publishing Office [www.gpo.gov]
[FR Doc No: 96-21628]


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ENVIRONMENTAL PROTECTION AGENCY
40 CFR Parts 60, 63, 260, 261, 264, 265, 266, 270 and 271

[FRL-5558-5]
RIN 2050-AF01


Hazardous Waste Combustors; Revised Standards; Proposed Rule--
Notice of Data Availability and Request for Comments

AGENCY: Environmental Protection Agency (EPA).

ACTION: Notice of data availability and request for comments.

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SUMMARY: This document is a notice of availability and invitation for 
comment on the following information pertaining to the proposed revised 
standards for hazardous waste combustors (61 FR 17358 (April 19, 
1996)): Reports from an independent peer review of technical aspects of 
the rule; additional analyses of various fuel oils to be used to 
establish a specification to exclude comparable fuels; and information 
on a synthesis gas process and product gas specifications that was 
inadvertently not included in the docket.
    Readers should note that only comments about new information 
discussed in this document will be considered during the comment 
period. Issues related to the April 19, 1996 proposed rule that are not 
directly affected by the documents or data referenced in this Notice of 
Data Availability are not open for further comment.

DATES: Written comments on the peer review reports, the new comparable 
fuels analyses, and the synthesis gas process and product information 
must be submitted by September 23, 1996.

ADDRESSES: Commenters must send an original and two copies of their 
comments referencing Docket Number F-96-RCSP-FFFFF to: RCRA Docket 
Information Center, Office of Solid Waste (5305G), U.S. Environmental 
Protection Agency Headquarters (EPA, HQ), 401 M Street, S.W., 
Washington, D.C. 20460. Comments may also be submitted electronically 
through the Internet to: [email protected]. Comments in 
electronic format should also be identified by the docket number F-96-
RCSP-FFFFF. All electronic comments must be submitted as an ASCII file 
avoiding the use of special characters and any form of encryption. 
Commenters should not submit electronically any confidential business 
information (CBI). An original and two copies of the CBI must be 
submitted under separate cover to: RCRA CBI Document Control Officer, 
OSW (5305W), 401 M Street, SW, Washington D.C. 20460. For other 
information regarding submitting comments electronically, viewing the 
comments received, and supporting information, please refer to the 
proposed rule (61 FR 17358 (April 19, 1996)). The RCRA Information 
Center is located at Crystal Gateway One, 1235 Jefferson Davis Highway, 
First Floor, Arlington, Virginia and is open for public inspection and 
copying of supporting information for RCRA rules from 9:00

[[Page 43502]]

am to 4:00 pm Monday through Friday, except for Federal holidays. The 
public must make an appointment to view docket materials by calling 
(703) 603-9230. The public may copy a maximum of 100 pages from any 
regulatory document at no cost. Additional copies cost $0.15 per page.

FOR FURTHER INFORMATION CONTACT: For general information, call the RCRA 
Hotline at 1-800-424-9346 or TDD 1-800-553-7672 (hearing impaired) 
including directions on how to access electronically some of the 
documents and data referred to in this notice via EPA's Cleanup 
Information Bulletin Board System (CLU-IN). The CLU-IN modem access 
phone number is 301-589-8366 or Telnet to clu-in.epa.gov for Internet 
access. Callers within the Washington Metropolitan Area must dial 703-
412-9810 or TDD 703-412-3323 (hearing impaired). The RCRA Hotline is 
open Monday-Friday, 9:00 a.m. to 6:00 p.m., Eastern Standard Time. For 
other information on this notice, contact Shiva Garg (5302W), Office of 
Solid Waste, 401 M Street, S.W., Washington, DC 20460, phone (703) 308-
8459, e-mail: [email protected].

SUPPLEMENTARY INFORMATION: On April 19, 1996, EPA proposed revised 
standards for hazardous waste combustors (i.e., incinerators and cement 
and lightweight aggregate kilns that burn hazardous waste). See 61 FR 
17358. The Agency originally established a 60-day comment period, but 
later extended it to 120 days (61 FR 27038 (May 30, 1996)). The last 
date for receipt of comments on the Federal Register notice of April 
19, 1996 continues to remain August 19, 1996.
    The Agency is today providing notice and opportunity to comment on 
the following additional information pertaining to the proposed rule: 
(1) Reports from an independent peer review of technical aspects of the 
rule; (2) additional analyses of various fuel oils to be used to 
establish a specification to exclude comparable fuels; and (3) 
information on a synthesis gas process and product gas specifications 
that was inadvertently not included in the docket.

Peer Review Reports

    As part of the rule development process, the Agency initiated a 
peer review of the proposed rule, preamble and relevant supporting 
background documents in three subject areas of the rule: engineering, 
risk assessment and economic analysis. The review panel members were 
tasked with conducting a comprehensive and critical review of the 
proposed rule in their designated subject areas, addressing a set of 
questions pertaining to the technical basis of the approaches adopted 
by the Agency, and providing comments and/or recommendations where 
warranted. Each subject area panel prepared a summary report 
highlighting the key points of discussion, including the consensus 
reports or the dissenting opinions. Copies of the peer review panel 
report of each subject area and individual review comments of each 
panel member are available in the docket.

Comparable Fuel Specification

    As part of the proposed comparable fuel specification, EPA used a 
benchmark approach to develop a series of technical specifications that 
would allow hazardous waste similar in composition to a commercially 
available fossil fuel to be excluded under RCRA when burned. One of 
these specifications included the Agency's proposal to limit the 
Appendix VIII, Part 261, constituents in comparable fuels 1 to 
those found in the benchmark fossil fuel. As discussed in the preamble 
of the proposal (61 FR 17461), EPA was unable to analyze for some 
compounds on the Appendix VIII list because either an analytical method 
was not available or could not be identified in time for initial 
analysis. Those compounds were not listed in the proposed 
specifications published on April 19, 1996.
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    \1\ The specification would also include two metals that are 
identified in Clean Air Act section 112(b) as hazardous air 
pollutants: cobalt and manganese. See 61 FR 17460.
---------------------------------------------------------------------------

    EPA has subsequently been able to identify methods for analyzing 
some additional Appendix VIII compounds and is presenting a proposed 
specification level or detection limit for these compounds. These 
compounds are listed in today's notice and also can be found, along 
with the analytical methods, in the Draft Technical Support Document 
for HWC MACT Standards, Addendum to Volume VI: Development of 
Comparable Fuels Specifications, August 1996. EPA invites comment on 
today's new individual specifications, as well as the composite 
specifications, and the analytical methods used in EPA's new analysis.
    In addition, we want to clarify the rationale for proposing 
comparable fuel specification limits for total halogens and total 
nitrogen. Although neither total halogens nor total nitrogen are listed 
on Appendix VIII, Part 261 (or proposed for Appendix X), we believe 
that they should be limited to ensure that halogenated and nitrated 
products of incomplete combustion (PICs) from burning excluded waste 
would not be emitted at higher levels than from burning benchmark 
fossil fuel. Halogenated and nitrated organic compounds can pose a 
particular hazard to human health and the environment.

Synthesis Gas Comparable Fuel Exclusion

    In discussing the exclusion of synthesis gas (syngas) fuel in the 
proposed rule, EPA referenced a Molten Metals Technology (MMT) letter 
that presented data on the MMT syngas process, including relevant 
specifications. See preamble discussion at 61 FR 17465. In placing the 
MMT information in the docket, an attachment to the letter containing 
the data was inadvertently not placed in the docket until late in the 
comment period. EPA has since received a request to extend the comment 
period pertaining only to the syngas exclusion to allow adequate time 
to review this attachment and provide comment on the syngas exclusion. 
In response to this request, EPA is granting 30 days from the 
publication date of this notice to comment on the proposed syngas fuel 
exclusion.

Appendix--Comparable Fuel Constituent and Physical Specifications

    Note 1: All numbers in the tables of this appendix are expressed 
to two significant figures.

 Table 1.--Detection and Detection Limit Values for a Possible Gasoline 
                              Specification                             
------------------------------------------------------------------------
                                                               Maximum  
                                      Concentration limit     detection 
           Chemical name             (mg/kg at 10,000 Btu/   limit (mg/ 
                                              lb)                kg)    
------------------------------------------------------------------------
1,1,1-Trichloroethane..............  Non-detect...........         34   

[[Page 43503]]

                                                                        
1,1,2-Trichloro-1,2,2-               Non-detect...........         30   
 trifluoroethane.                                                       
1,1-Dichloro-1-propene.............  Non-detect...........         30   
1,1-Dichloroethane.................  Non-detect...........         34   
1,2,3,4,6,7,8-Heptachlorodibenzo-p-  Non-detect...........          8.8 
 dioxin.                                                                
1,2,3,4,6,7,8-Heptachlorodibenzo-p-  Non-detect...........          8.8 
 furan.                                                                 
1,2,3,4-Tetrachlorobenzene.........  Non-detect...........         14   
1,2,3,5-Tetrachlorobenzene.........  Non-detect...........         14   
1,2,3,6,7,8-Hexachlorodibenzo-p-     Non-detect...........          8.8 
 dioxin.                                                                
1,2,3,6,7,8-Hexachlorodibenzo-p-     Non-detect...........          8.8 
 furan.                                                                 
1,2,3,7,8-Pentachlorodibenzo-p-      Non-detect...........          8.8 
 dioxin.                                                                
1,2,3,7,8-Pentachlorodibenzo-p-      Non-detect...........          8.8 
 furan.                                                                 
1,2,3-Trichlorobenzene.............  Non-detect...........         14   
1,2-Dichloroethane.................  Non-detect...........         34   
1,2-Dichloropropane................  Non-detect...........         34   
1,3-Dichloro-2-propanol............  Non-detect...........         30   
1,3-Dichloropropane................  Non-detect...........         30   
1,3-Propane sultone................  Non-detect...........         14   
1-Chloronaphthalene................  Non-detect...........         14   
2,2-Dichloropropane................  Non-detect...........         30   
2,3,4,5-Tetrachlorophenol..........  Non-detect...........         14   
2,3,4-Trichlorophenol..............  Non-detect...........         14   
2,3,5-Trichlorophenol..............  Non-detect...........         14   
2,3,6-Trichlorophenol..............  Non-detect...........         14   
2,3,7,8-Tetrachlorodibenzo-p-dioxin  Non-detect...........          3.5 
2,3,7,8-Tetrachlorodibenzo-p-furan.  Non-detect...........          3.5 
2,3-Dichloro-1-propene.............  Non-detect...........         30   
2,3-Dichlorophenol.................  Non-detect...........         14   
2,4-D..............................  Non-detect...........          7.0 
2,5-Dichlorophenol.................  Non-detect...........         14   
2-Fluoroacetamide..................  Non-detect...........         14   
2-Methylnaphthalene................  1200.................  ............
2-Nitropropane.....................  Non-detect...........         30   
3,3'-Dimethoxybenzidine............  Non-detect...........         14   
3,4-Dichlorophenol.................  Non-detect...........         14   
3,5-Dichlorophenol.................  Non-detect...........         14   
3-/4-Chlorophenol..................  Non-detect...........         14   
3-Nitroaniline.....................  Non-detect...........        670   
4,4'-methylene-bis(2-chloroaniline)  Non-detect...........         14   
4-Aminopyrridine...................  Non-detect...........         14   
4-Chlorophenyl phenyl ether........  Non-detect...........        670   
6-Propyl-2-thiouracil..............  Non-detect...........         14   
Acenaphthene.......................  Non-detect...........        670   
Acetone cyanohydrin................  Non-detect...........         14   
Allyl alcohol......................  Non-detect...........         30   
Ammonium vanadate..................  Non-detect...........         32   
Anthracene.........................  Non-detect...........        670   
Arochlor-1016......................  Non-detect...........          1.4 
Arochlor-1221......................  Non-detect...........          1.4 
Arochlor-1232......................  Non-detect...........          1.4 
Arochlor-1242......................  Non-detect...........          1.4 
Arochlor-1248......................  Non-detect...........          1.4 
Arochlor-1254......................  Non-detect...........          1.4 
Arochlor-1260......................  Non-detect...........          1.4 
Arsenic acid.......................  Non-detect...........          0.27
Arsenic pentoxide..................  Non-detect...........          0.22
Arsenic trioxide...................  Non-detect...........          0.19
Barium Cyanide.....................  Non-detect...........          3.7 
Benzal chloride....................  Non-detect...........         14   
Benzenethiol.......................  Non-detect...........         30   
Benzyl chloride....................  Non-detect...........         14   
Bis(2-chloroethoxy)methane.........  Non-detect...........        670   
Bis(2-chloroethyl)ether............  Non-detect...........        670   
Bis(2-ethylhexyl)phthalate.........  Non-detect...........        670   
Bromide............................  Non-detect...........          5.0 
Bromodichloromethane...............  Non-detect...........         34   
Calcium Cyanide....................  Non-detect...........          1.8 
Calcium chromate...................  Non-detect...........          4.2 
Chlordane..........................  Non-detect...........         14   
Chloride...........................  6.2..................  ............

[[Page 43504]]

                                                                        
Chloroethane.......................  Non-detect...........         34   
Copper Cyanide.....................  Non-detect...........          1.7 
Cyanide............................  Non-detect...........          1.0 
Cyanogen Bromide...................  Non-detect...........          6.6 
Cyanogen Chloride..................  Non-detect...........        100   
Di-selenium-tetra-sulfide..........  Non-detect...........        830   
Dibenzofuran.......................  Non-detect...........        670   
Dibromochloromethane...............  Non-detect...........         34   
Endosulfan I.......................  Non-detect...........          1.4 
Endosulfan II......................  Non-detect...........          1.4 
Endothal...........................  Non-detect...........         14   
Endrin.............................  Non-detect...........          1.4 
Endrin aldehyde....................  Non-detect...........          1.4 
Endrin ketone......................  Non-detect...........          1.4 
Epichlorohydrin....................  Non-detect...........         30   
Ethyl carbamate....................  Non-detect...........         14   
Ethylene glycol monoethyl ether....  Non-detect...........         14   
Ethylenethiourea (2-                 Non-detect...........         14   
 Imidazolidinethione).                                                  
Fluoride...........................  Non-detect...........          3.0 
Heptachlor.........................  Non-detect...........          1.4 
Heptachlor epoxide.................  Non-detect...........          2.8 
Lead acetate.......................  Non-detect...........         13   
Lead phosphate.....................  Non-detect...........          9.2 
MNNG (N-Methyl-N-nitroso-N'-         Non-detect...........         14   
 nitroguanidine).                                                       
Methomyl...........................  Non-detect...........          7.0 
N-Nitrosodiphenylamine.............  Non-detect...........        670   
Nickel Cyanide.....................  Non-detect...........          3.5 
Nickel carbonyl....................  Non-detect...........          8.2 
Nicotine...........................  Non-detect...........         14   
Octachlorodibenzodioxin............  Non-detect...........         18   
Octachlorodibenzofuran.............  Non-detect...........         18   
Osmium tetraoxide..................  Non-detect...........         41   
Phenanthrene.......................  Non-detect...........        670   
Phenylthiourea.....................  Non-detect...........          7.0 
Potassium Cyanide..................  Non-detect...........          2.5 
Potassium Silver Cyanide...........  Non-detect...........          2.9 
Propargyl alcohol..................  Non-detect...........         30   
Pyrene.............................  Non-detect...........        670   
Selenium dioxide...................  Non-detect...........          0.20
Selenium sulfide...................  Non-detect...........          0.31
Silver Cyanide.....................  Non-detect...........          2.6 
Silvex.............................  Non-detect...........          7.0 
Strychnine.........................  Non-detect...........         14   
Tetra-selenium-tetra-sulfide.......  Non-detect...........       1600   
Tetraethyl lead....................  Non-detect...........         11   
Thallium acetate...................  Non-detect...........         18   
Thallium carbonate.................  Non-detect...........         16   
Thallium chloride..................  Non-detect...........         17   
Thallium nitrate...................  Non-detect...........         18   
Thallium oxide.....................  Non-detect...........         15   
Thallium sulfate...................  Non-detect...........         17   
Thioacetamide......................  Non-detect...........          7.0 
Thiofanox..........................  Non-detect...........         14   
Thiourea...........................  Non-detect...........          7.0 
Toluene-2,4-diamine................  Non-detect...........          7.0 
Toluene-2,6-diamine................  Non-detect...........          7.0 
Vanadium pentoxide.................  Non-detect...........         18   
Zinc Cyanide.......................  Non-detect...........          2.3 
Zinc phosphide.....................  Non-detect...........          0.37
alpha-BHC..........................  Non-detect...........          1.4 
beta-BHC...........................  Non-detect...........          1.4 
delta-BHC..........................  Non-detect...........          1.4 
gamma-BHC (Lindane)................  Non-detect...........          1.4 
m-Dinitrobenzene...................  Non-detect...........        670   
p-Toluidine........................  Non-detect...........         14   
trans-1,3-Dichloropropene..........  Non-detect...........         34   
------------------------------------------------------------------------



[[Page 43505]]



 Table 2.--Detection and Detection Limit Values for a Possible Number 2 
                         Fuel Oil Specification                         
------------------------------------------------------------------------
                                                               Maximum  
                                      Concentration limit     detection 
           Chemical name             (mg/kg at 10,000 Btu/   limit (mg/ 
                                              lb)                kg)    
------------------------------------------------------------------------
1,1,1-Trichloroethane..............  Non-detect...........         34   
1,1,2-Trichloro-1,2,2-               Non-detect...........         30   
 trifluoroethane.                                                       
1,1-Dichloro-1-propene.............  Non-detect...........         30   
1,1-Dichloroethane.................  Non-detect...........         34   
1,2,3,4,6,7,8-Heptachlorodibenzo-p-  Non-detect...........         75   
 dioxin.                                                                
1,2,3,4,6,7,8-Heptachlorodibenzo-p-  Non-detect...........         75   
 furan.                                                                 
1,2,3,4-Tetrachlorobenzene.........  Non-detect...........        100   
1,2,3,5-Tetrachlorobenzene.........  Non-detect...........        100   
1,2,3,6,7,8-Hexachlorodibenzo-p-     Non-detect...........         75   
 dioxin.                                                                
1,2,3,6,7,8-Hexachlorodibenzo-p-     Non-detect...........         75   
 furan.                                                                 
1,2,3,7,8-Pentachlorodibenzo-p-      Non-detect...........         75   
 dioxin.                                                                
1,2,3,7,8-Pentachlorodibenzo-p-      Non-detect...........         75   
 furan.                                                                 
1,2,3-Trichlorobenzene.............  Non-detect...........        100   
1,2-Dichloroethane.................  Non-detect...........         34   
1,2-Dichloropropane................  Non-detect...........         34   
1,3-Dichloro-2-propanol............  Non-detect...........         30   
1,3-Dichloropropane................  Non-detect...........         30   
1,3-Propane sultone................  Non-detect...........        100   
1-Chloronaphthalene................  Non-detect...........        100   
2,2-Dichloropropane................  Non-detect...........         30   
2,3,4,5-Tetrachlorophenol..........  Non-detect...........        100   
2,3,4-Trichlorophenol..............  Non-detect...........        100   
2,3,5-Trichlorophenol..............  Non-detect...........        100   
2,3,6-Trichlorophenol..............  Non-detect...........        100   
2,3,7,8-Tetrachlorodibenzo-p-dioxin  Non-detect...........         30   
2,3,7,8-Tetrachlorodibenzo-p-furan.  Non-detect...........         30   
2,3-Dichloro-1-propene.............  Non-detect...........         30   
2,3-Dichlorophenol.................  Non-detect...........        100   
2,4-D..............................  Non-detect...........          6.0 
2,5-Dichlorophenol.................  Non-detect...........        100   
2-Fluoroacetamide..................  Non-detect...........        100   
2-Methylnaphthalene................  3400.................  ............
2-Nitropropane.....................  Non-detect...........         30   
3,3'-Dimethoxybenzidine............  Non-detect...........        100   
3,4-Dichlorophenol.................  Non-detect...........        100   
3,5-Dichlorophenol.................  Non-detect...........        100   
3-/4-Chlorophenol..................  Non-detect...........        100   
3-Nitroaniline.....................  Non-detect...........       1200   
4,4'-methylene-bis(2-chloroaniline)  Non-detect...........        100   
4-Aminopyrridine...................  Non-detect...........        100   
4-Chlorophenyl phenyl ether........  Non-detect...........       1200   
6-Propyl-2-thiouracil..............  Non-detect...........        100   
Acenaphthene.......................  Non-detect...........       1200   
Acetone cyanohydrin................  Non-detect...........        100   
Allyl alcohol......................  Non-detect...........         30   
Ammonium vanadate..................  Non-detect...........         28   
Anthracene.........................  Non-detect...........       1200   
Arochlor-1016......................  Non-detect...........          1.2 
Arochlor-1221......................  Non-detect...........          1.2 
Arochlor-1232......................  Non-detect...........          1.2 
Arochlor-1242......................  Non-detect...........          1.2 
Arochlor-1248......................  Non-detect...........          1.2 
Arochlor-1254......................  Non-detect...........          1.2 
Arochlor-1260......................  Non-detect...........          1.2 
Arsenic acid.......................  Non-detect...........          0.23
Arsenic pentoxide..................  Non-detect...........          0.18
Arsenic trioxide...................  Non-detect...........          0.16
Barium Cyanide.....................  Non-detect...........          3.7 
Benzal chloride....................  Non-detect...........        100   
Benzenethiol.......................  Non-detect...........         30   
Benzyl chloride....................  Non-detect...........        100   
Bis(2-chloroethoxy)methane.........  Non-detect...........       1200   
Bis(2-chloroethyl)ether............  Non-detect...........       1200   
Bis(2-ethylhexyl)phthalate.........  Non-detect...........       1200   
Bromide............................  Non-detect...........          5.0 
Bromodichloromethane...............  Non-detect...........         34   
Calcium Cyanide....................  Non-detect...........          1.8 
Calcium chromate...................  Non-detect...........          3.6 
Chlordane..........................  Non-detect...........         12   

[[Page 43506]]

                                                                        
Chloride...........................  Non-detect...........          5.0 
Chloroethane.......................  Non-detect...........         34   
Copper Cyanide.....................  Non-detect...........          1.7 
Cyanide............................  Non-detect...........          1.0 
Cyanogen Bromide...................  Non-detect...........          6.6 
Cyanogen Chloride..................  Non-detect...........          8.6 
Di-selenium-tetra-sulfide..........  Non-detect...........        370   
Dibenzofuran.......................  Non-detect...........       1200   
Dibromochloromethane...............  Non-detect...........         34   
Endosulfan I.......................  Non-detect...........          1.2 
Endosulfan II......................  Non-detect...........          1.2 
Endothal...........................  Non-detect...........        100   
Endrin.............................  Non-detect...........          1.2 
Endrin aldehyde....................  Non-detect...........          1.2 
Endrin ketone......................  Non-detect...........          1.2 
Epichlorohydrin....................  Non-detect...........         30   
Ethyl carbamate....................  Non-detect...........        100   
Ethylene glycol monoethyl ether....  Non-detect...........        100   
Ethylenethiourea (2-                 Non-detect...........         12   
 Imidazolidinethione).                                                  
Fluoride...........................  Non-detect...........          3.0 
Heptachlor.........................  Non-detect...........          1.2 
Heptachlor epoxide.................  Non-detect...........          2.4 
Lead acetate.......................  Non-detect...........         22   
Lead phosphate.....................  Non-detect...........         15   
MNNG (N-Metyl-N-nitroso-N'-          Non-detect...........         12   
 nitroguanidine).                                                       
Methomyl...........................  Non-detect...........          6.0 
N-Nitrosodiphenylamine.............  Non-detect...........       1200   
Nickel Cyanide.....................  Non-detect...........          3.5 
Nickel carbonyl....................  Non-detect...........          7.0 
Nicotine...........................  Non-detect...........        100   
Octachlorodibenzodioxin............  Non-detect...........        150   
Octachlorodibenzofuran.............  Non-detect...........        150   
Osmium tetraoxide..................  Non-detect...........         40   
Phenanthrene.......................  860..................  ............
Phenylthiourea.....................  Non-detect...........          6.0 
Potassium Cyanide..................  Non-detect...........          2.5 
Potassium Silver Cyanide...........  Non-detect...........          2.9 
Propargyl alcohol..................  Non-detect...........         30   
Pyrene.............................  Non-detect...........       1200   
Selenium dioxide...................  Non-detect...........          0.21
Selenium sulfide...................  Non-detect...........          0.34
Silver Cyanide.....................  Non-detect...........          2.6 
Silvex.............................  Non-detect...........          6.0 
Strychnine.........................  Non-detect...........        100   
Tetra-selenium-tetra-sulfide.......  Non-detect...........        710   
Tetraethyl lead....................  Non-detect...........         18   
Thallium acetate...................  Non-detect...........         15   
Thallium carbonate.................  Non-detect...........         14   
Thallium chloride..................  Non-detect...........         14   
Thallium nitrate...................  Non-detect...........         16   
Thallium oxide.....................  Non-detect...........         12   
Thallium sulfate...................  Non-detect...........         15   
Thioacetamide......................  Non-detect...........          6.0 
Thiofanox..........................  Non-detect...........        100   
Thiourea...........................  Non-detect...........          6.0 
Toluene-2,4-diamine................  Non-detect...........          6.0 
Toluene-2,6-diamine................  Non-detect...........          6.0 
Vanadium pentoxide.................  Non-detect...........         18   
Zinc Cyanide.......................  Non-detect...........          2.3 
Zinc phosphide.....................  Non-detect...........          0.32
alpha-BHC..........................  Non-detect...........          1.2 
beta-BHC...........................  Non-detect...........          1.2 
delta-BHC..........................  Non-detect...........          1.2 
gamma-BHC (Lindane)................  Non-detect...........          1.2 
m-Dinitrobenzene...................  Non-detect...........       1200   
p-Toluidine........................  Non-detect...........        100   
trans-1,3-Dichloropropene..........  Non-detect...........         34   
------------------------------------------------------------------------



[[Page 43507]]



  Table 3.--Detection and Detection Limit Values for a Possile Number 4 
                         Fuel Oil Specification                         
------------------------------------------------------------------------
                                                               Maximum  
                                      Concentration limit     detection 
           Chemical name             (mg/kg at 10,000 Btu/   limit (mg/ 
                                              lb)                kg)    
------------------------------------------------------------------------
1,1,1-Trichloroethane..............  Non-detect...........         17   
1,1,2-Trichloro-1,2,2-               Non-detect...........         29   
 trifluoroethane.                                                       
1,1-Dichloro-1-propene.............  Non-detect...........         29   
1,1-Dichloroethane.................  Non-detect...........         17   
1,2,3,4,6,7,8-Heptachlorodibenzo-p-  Non-detect...........         72   
 dioxin.                                                                
1,2,3,4,6,7,8-Heptachlorodibenzo-p-  Non-detect...........         72   
 furan.                                                                 
1,2,3,4-Tetrachlorobenzene.........  Non-detect...........        100   
1,2,3,5-Tetrachlorobenzene.........  Non-detect...........        100   
1,2,3,6,7,8-Hexachlorodibenzo-p-     Non-detect...........         72   
 dioxin.                                                                
1,2,3,6,7,8-Hexachlorodibenzo-p-     Non-detect...........         72   
 furan.                                                                 
1,2,3,7,8-Pentachlorodibenzo-p-      Non-detect...........         72   
 dioxin.                                                                
1,2,3,7,8-Pentachlorodibenzo-p-      Non-detect...........         72   
 furan.                                                                 
1,2,3-Trichlorobenzene.............  Non-detect...........        100   
1,2-Dichloroethane.................  Non-detect...........         17   
1,2-Dichloropropane................  Non-detect...........         17   
1,3-Dichloro-2-propanol............  Non-detect...........         29   
1,3-Dichloropropane................  Non-detect...........         29   
1,3-Propane sultone................  Non-detect...........        100   
1-Chloronaphthalene................  Non-detect...........        100   
2,2-Dichloropropane................  Non-detect...........         29   
2,3,4,5-Tetrachlorophenol..........  Non-detect...........        100   
2,3,4-Trichlorophenol..............  Non-detect...........        100   
2,3,5-Trichlorophenol..............  Non-detect...........        100   
2,3,6-Trichlorophenol..............  Non-detect...........        100   
2,3,7,8-Tetrachlorodibenzo-p-dioxin  Non-detect...........         29   
2,3,7,8-Tetrachlorodibenzo-p-furan.  Non-detect...........         29   
2,3-Dichloro-1-propene.............  Non-detect...........         29   
2,3-Dichlorophenol.................  Non-detect...........        100   
2,4-D..............................  Non-detect...........          5.7 
2,5-Dichlorophenol.................  Non-detect...........        100   
2-Fluoroacetamide..................  Non-detect...........        100   
2-Methylnaphthalene................  1000.................          -   
2-Nitropropane.....................  Non-detect...........         29   
3,3'-Dimethoxybenzidine............  Non-detect...........        100   
3,4-Dichlorophenol.................  Non-detect...........        100   
3,5-Dichlorophenol.................  Non-detect...........        100   
3-/4-Chlorophenol..................  Non-detect...........        100   
3-Nitroaniline.....................  Non-detect...........        200   
4,4'-methylene-bis(2-chloroaniline)  Non-detect...........        100   
4-Aminopyrridine...................  Non-detect...........        100   
4-Chlorophenyl phenyl ether........  Non-detect...........        200   
6-Propyl-2-thiouracil..............  Non-detect...........        100   
Acenaphthene.......................  Non-detect...........        200   
Acetone cyanohydrin................  Non-detect...........        100   
Allyl alcohol......................  Non-detect...........         29   
Ammonium vanadate..................  Non-detect...........         68   
Anthracene.........................  Non-detect...........        200   
Arochlor-1016......................  Non-detect...........          1.1 
Arochlor-1221......................  Non-detect...........          1.1 
Arochlor-1232......................  Non-detect...........          1.1 
Arochlor-1242......................  Non-detect...........          1.1 
Arochlor-1248......................  Non-detect...........          1.1 
Arochlor-1254......................  Non-detect...........          1.1 
Arochlor-1260......................  Non-detect...........          1.1 
Arsenic acid.......................  Non-detect...........          0.43
Arsenic pentoxide..................  Non-detect...........          0.35
Arsenic trioxide...................  Non-detect...........          0.30
Barium Cyanide.....................  Non-detect...........          3.7 
Benzal chloride....................  Non-detect...........        100   
Benzenethiol.......................  Non-detect...........         29   
Benzyl chloride....................  Non-detect...........        100   
Bis(2-chloroethoxy)methane.........  Non-detect...........        200   
Bis(2-chloroethyl)ether............  Non-detect...........        200   
Bis(2-ethylhexyl)phthalate.........  Non-detect...........        200   
Bromide............................  Non-detect...........          5.0 
Bromodichloromethane...............  Non-detect...........         17   
Calcium Cyanide....................  Non-detect...........          1.8 
Calcium chromate...................  Non-detect...........          6.9 
Chlordane..........................  Non-detect...........         11   

[[Page 43508]]

                                                                        
Chloride...........................  Non-detect...........          5.0 
Chloroethane.......................  Non-detect...........         17   
Copper Cyanide.....................  Non-detect...........          1.7 
Cyanide............................  Non-detect...........          1.0 
Cyanogen Bromide...................  Non-detect...........          6.6 
Cyanogen Chloride..................  Non-detect...........          8.6 
Di-selenium-tetra-sulfide..........  Non-detect...........       1300   
Dibenzofuran.......................  Non-detect...........        200   
Dibromochloromethane...............  Non-detect...........         17   
Endosulfan I.......................  Non-detect...........          1.1 
Endosulfan II......................  Non-detect...........          1.1 
Endothal...........................  Non-detect...........        100   
Endrin.............................  Non-detect...........          1.1 
Endrin aldehyde....................  Non-detect...........          1.1 
Endrin ketone......................  Non-detect...........          1.1 
Epichlorohydrin....................  Non-detect...........         29   
Ethyl carbamate....................  Non-detect...........        100   
Ethylene glycol monoethyl ether....  Non-detect...........        100   
Ethylenethiourea (2-                 Non-detect...........        110   
 Imidazolidinethione).                                                  
Fluoride...........................  Non-detect...........          3.0 
Heptachlor.........................  Non-detect...........          1.1 
Heptachlor epoxide.................  Non-detect...........          2.3 
Lead acetate.......................  Non-detect...........         34   
Lead phosphate.....................  Non-detect...........         24   
MNNG (N-Metyl-N-nitroso-N'-          Non-detect...........        110   
 nitroguanidine).                                                       
Methomyl...........................  Non-detect...........         57   
N-Nitrosodiphenylamine.............  Non-detect...........        200   
Nickel Cyanide.....................  Non-detect...........          3.5 
Nickel carbonyl....................  Non-detect...........         13   
Nicotine...........................  Non-detect...........        100   
Octachlorodibenzodioxin............  Non-detect...........        140   
Octachlorodibenzofuran.............  Non-detect...........        140   
Osmium tetraoxide..................  Non-detect...........         40   
Phenanthrene.......................  250..................          -   
Phenylthiourea.....................  Non-detect...........         57   
Potassium Cyanide..................  Non-detect...........          2.5 
Potassium Silver Cyanide...........  Non-detect...........          2.9 
Propargyl alcohol..................  Non-detect...........         29   
Pyrene.............................  Non-detect...........        200   
Selenium dioxide...................  Non-detect...........          0.35
Selenium sulfide...................  Non-detect...........          0.56
Silver Cyanide.....................  Non-detect...........          2.6 
Silvex.............................  Non-detect...........          5.7 
Strychnine.........................  Non-detect...........        100   
Tetra-selenium-tetra-sulfide.......  Non-detect...........       2400   
Tetraethyl lead....................  Non-detect...........         29   
Thallium acetate...................  Non-detect...........         30   
Thallium carbonate.................  Non-detect...........         26   
Thallium chloride..................  Non-detect...........         27   
Thallium nitrate...................  Non-detect...........         30   
Thallium oxide.....................  Non-detect...........         24   
Thallium sulfate...................  Non-detect...........         28   
Thioacetamide......................  Non-detect...........         57   
Thiofanox..........................  Non-detect...........        100   
Thiourea...........................  Non-detect...........         57   
Toluene-2,4-diamine................  Non-detect...........         57   
Toluene-2,6-diamine................  Non-detect...........         57   
Vanadium pentoxide.................  Non-detect...........         18   
Zinc Cyanide.......................  Non-detect...........          2.3 
Zinc phosphide.....................  Non-detect...........          0.75
alpha-BHC..........................  Non-detect...........          1.1 
beta-BHC...........................  Non-detect...........          1.1 
delta-BHC..........................  Non-detect...........          1.1 
gamma-BHC (Lindane)................  Non-detect...........          1.1 
m-Dinitrobenzene...................  Non-detect...........        200   
p-Toluidine........................  Non-detect...........        100   
trans-1,3-Dichloropropene..........  Non-detect...........         17   
------------------------------------------------------------------------



[[Page 43509]]



 Table 4.--Detection and Detection Limit Values for a Possible Number 6 
                         Fuel Oil Specification                         
------------------------------------------------------------------------
                                                               Maximum  
                                      Concentration limit     detection 
           Chemical name             (mg/kg at 10,000 Btu/   limit (mg/ 
                                              lb)                kg)    
------------------------------------------------------------------------
1,1,1-Trichloroethane..............  Non-detect...........         21   
1,1,2-Trichloro-1,2,2-               Non-detect...........         26   
 trifluoroethane.                                                       
1,1-Dichloro-1-propene.............  Non-detect...........         26   
1,1-Dichloroethane.................  Non-detect...........         21   
1,2,3,4,6,7,8-Heptachlorodibenzo-p-  Non-detect...........         64   
 dioxin.                                                                
1,2,3,4,6,7,8-Heptachlorodibenzo-p-  Non-detect...........         64   
 furan.                                                                 
1,2,3,4-Tetrachlorobenzene.........  Non-detect...........        100   
1,2,3,5-Tetrachlorobenzene.........  Non-detect...........        100   
1,2,3,6,7,8-Hexachlorodibenzo-p-     Non-detect...........         64   
 dioxin.                                                                
1,2,3,6,7,8-Hexachlorodibenzo-p-     Non-detect...........         64   
 furan.                                                                 
1,2,3,7,8-Pentachlorodibenzo-p-      Non-detect...........         64   
 dioxin.                                                                
1,2,3,7,8-Pentachlorodibenzo-p-      Non-detect...........         64   
 furan.                                                                 
1,2,3-Trichlorobenzene.............  Non-detect...........        100   
1,2-Dichloroethane.................  Non-detect...........         21   
1,2-Dichloropropane................  Non-detect...........         21   
1,3-Dichloro-2-propanol............  Non-detect...........         26   
1,3-Dichloropropane................  Non-detect...........         26   
1,3-Propane sultone................  Non-detect...........        100   
1-Chloronaphthalene................  Non-detect...........        100   
2,2-Dichloropropane................  Non-detect...........         26   
2,3,4,5-Tetrachlorophenol..........  Non-detect...........        100   
2,3,4-Trichlorophenol..............  Non-detect...........        100   
2,3,5-Trichlorophenol..............  Non-detect...........        100   
2,3,6-Trichlorophenol..............  Non-detect...........        100   
2,3,7,8-Tetrachlorodibenzo-p-dioxin  Non-detect...........         26   
2,3,7,8-Tetrachlorodibenzo-p-furan.  Non-detect...........         26   
2,3-Dichloro-1-propene.............  Non-detect...........         26   
2,3-Dichlorophenol.................  Non-detect...........        100   
2,4-D..............................  Non-detect...........          5.1 
2,5-Dichlorophenol.................  Non-detect...........        100   
2-Fluoroacetamide..................  Non-detect...........        100   
2-Methylnaphthalene................  4200.................  ............
2-Nitropropane.....................  Non-detect...........         26   
3,3'-Dimethoxybenzidine............  Non-detect...........        100   
3,4-Dichlorophenol.................  Non-detect...........        100   
3,5-Dichlorophenol.................  Non-detect...........        100   
3-/4-Chlorophenol..................  Non-detect...........        100   
3-Nitroaniline.....................  Non-detect...........        980   
4,4'-methylene-bis(2-chloroaniline)  Non-detect...........        100   
4-Aminopyrridine...................  Non-detect...........        100   
4-Chlorophenyl phenyl ether........  Non-detect...........        980   
6-Propyl-2-thiouracil..............  Non-detect...........        100   
Acenaphthene.......................  Non-detect...........        980   
Acetone cyanohydrin................  Non-detect...........        100   
Allyl alcohol......................  Non-detect...........         26   
Ammonium vanadate..................  Non-detect...........        590   
Anthracene.........................  Non-detect...........        980   
Arochlor-1016......................  Non-detect...........          1.0 
Arochlor-1221......................  Non-detect...........          1.0 
Arochlor-1232......................  Non-detect...........          1.0 
Arochlor-1242......................  Non-detect...........          1.0 
Arochlor-1248......................  Non-detect...........          1.0 
Arochlor-1254......................  Non-detect...........          1.0 
Arochlor-1260......................  Non-detect...........          1.0 
Arsenic acid.......................  Non-detect...........          0.39
Arsenic pentoxide..................  Non-detect...........          0.31
Arsenic trioxide...................  Non-detect...........          0.27
Barium Cyanide.....................  Non-detect...........          3.7 
Benzal chloride....................  Non-detect...........        100   
Benzenethiol.......................  Non-detect...........         26   
Benzyl chloride....................  Non-detect...........        100   
Bis(2-chloroethoxy)methane.........  Non-detect...........        980   
Bis(2-chloroethyl)ether............  Non-detect...........        980   
Bis(2-ethylhexyl)phthalate.........  Non-detect...........        980   
Bromide............................  Non-detect...........          5.0 
Bromodichloromethane...............  Non-detect...........         21   
Calcium Cyanide....................  Non-detect...........          1.8 
Calcium chromate...................  Non-detect...........          6.1 
Chlordane..........................  Non-detect...........         10   

[[Page 43510]]

                                                                        
Chloride...........................  Non-detect...........          5.0 
Chloroethane.......................  Non-detect...........         21   
Copper Cyanide.....................  Non-detect...........          1.7 
Cyanide............................  Non-detect...........          1.0 
Cyanogen Bromide...................  Non-detect...........          6.6 
Cyanogen Chloride..................  Non-detect...........          8.6 
Di-selenium-tetra-sulfide..........  Non-detect...........       1400   
Dibenzofuran.......................  Non-detect...........        980   
Dibromochloromethane...............  Non-detect...........         21   
Endosulfan I.......................  Non-detect...........          1.0 
Endosulfan II......................  Non-detect...........          1.0 
Endothal...........................  Non-detect...........        100   
Endrin.............................  Non-detect...........          1.0 
Endrin aldehyde....................  Non-detect...........          1.0 
Endrin ketone......................  Non-detect...........          1.0 
Epichlorohydrin....................  Non-detect...........         26   
Ethyl carbamate....................  Non-detect...........        100   
Ethylene glycol monoethyl ether....  Non-detect...........        100   
Ethylenethiourea (2-                 Non-detect...........        100   
 Imidazolidinethione).                                                  
Fluoride...........................  Non-detect...........          3.0 
Heptachlor.........................  Non-detect...........          1.0 
Heptachlor epoxide.................  Non-detect...........          2.0 
Lead acetate.......................  Non-detect...........        110   
Lead phosphate.....................  Non-detect...........         79   
MNNG (N-Metyl-N-nitroso-N'-          Non-detect...........        100   
 nitroguanidine).                                                       
Methomyl...........................  Non-detect...........         50   
N-Nitrosodiphenylamine.............  Non-detect...........        980   
Nickel Cyanide.....................  Non-detect...........          3.5 
Nickel carbonyl....................  Non-detect...........        330   
Nicotine...........................  Non-detect...........        100   
Octachlorodibenzodioxin............  Non-detect...........        130   
Octachlorodibenzofuran.............  Non-detect...........        130   
Osmium tetraoxide..................  Non-detect...........         40   
Phenanthrene.......................  860..................  ............
Phenylthiourea.....................  Non-detect...........         50   
Potassium Cyanide..................  Non-detect...........          2.5 
Potassium Silver Cyanide...........  Non-detect...........          2.9 
Propargyl alcohol..................  Non-detect...........         26   
Pyrene.............................  610..................  ............
Selenium dioxide...................  Non-detect...........          0.40
Selenium sulfide...................  Non-detect...........          0.63
Silver Cyanide.....................  Non-detect...........          2.6 
Silvex.............................  Non-detect...........          5.1 
Strychnine.........................  Non-detect...........        100   
Tetra-selenium-tetra-sulfide.......  Non-detect...........       2600   
Tetraethyl lead....................  Non-detect...........         94   
Thallium acetate...................  Non-detect...........         26   
Thallium carbonate.................  Non-detect...........         23   
Thallium chloride..................  Non-detect...........         24   
Thallium nitrate...................  Non-detect...........         27   
Thallium oxide.....................  Non-detect...........         21   
Thallium sulfate...................  Non-detect...........         25   
Thioacetamide......................  Non-detect...........         50   
Thiofanox..........................  Non-detect...........        100   
Thiourea...........................  Non-detect...........         50   
Toluene-2,4-diamine................  Non-detect...........         50   
Toluene-2,6-diamine................  Non-detect...........         50   
Vanadium pentoxide.................  Non-detect...........         18   
Zinc Cyanide.......................  Non-detect...........          2.3 
Zinc phosphide.....................  Non-detect...........         11   
alpha-BHC..........................  Non-detect...........          5.0 
beta-BHC...........................  Non-detect...........          5.0 
delta-BHC..........................  Non-detect...........          1.0 
gamma-BHC (Lindane)................  Non-detect...........          1.0 
m-Dinitrobenzene...................  Non-detect...........        980   
p-Toluidine........................  Non-detect...........        100   
trans-1,3-Dichloropropene..........  Non-detect...........         21   
------------------------------------------------------------------------



[[Page 43511]]



 Table 5.--Detection and Detection Limit Values for a Possible Composite
              Fuel Specification--50th Percentile Analysis              
------------------------------------------------------------------------
                                                               Maximum  
                                      Concentration limit     detection 
           Chemical name             (mg/kg at 10,000 Btu/   limit (mg/ 
                                              lb)                kg)    
------------------------------------------------------------------------
1,1,1-Trichloroethane..............  Non-detect...........         17   
1,1,2-Trichloro-1,2,2-               Non-detect...........         29   
 trifluoroethane.                                                       
1,1-Dichloro-1-propene.............  Non-detect...........         29   
1,1-Dichloroethane.................  Non-detect...........         17   
1,2,3,4,6,7,8-Heptachlorodibenzo-p-  Non-detect...........         64   
 dioxin.                                                                
1,2,3,4,6,7,8-Heptachlorodibenzo-p-  Non-detect...........         64   
 furan.                                                                 
1,2,3,4-Tetrachlorobenzene.........  Non-detect...........        100   
1,2,3,5-Tetrachlorobenzene.........  Non-detect...........        100   
1,2,3,6,7,8-Hexachlorodibenzo-p-     Non-detect...........         64   
 dioxin.                                                                
1,2,3,6,7,8-Hexachlorodibenzo-p-     Non-detect...........         64   
 furan.                                                                 
1,2,3,7,8-Pentachlorodibenzo-p-      Non-detect...........         64   
 dioxin.                                                                
1,2,3,7,8-Pentachlorodibenzo-p-      Non-detect...........         64   
 furan.                                                                 
1,2,3-Trichlorobenzene.............  Non-detect...........        100   
1,2-Dichloroethane.................  Non-detect...........         17   
1,2-Dichloropropane................  Non-detect...........         17   
1,3-Dichloro-2-propanol............  Non-detect...........         29   
1,3-Dichloropropane................  Non-detect...........         29   
1,3-Propane sultone................  Non-detect...........        100   
1-Chloronaphthalene................  Non-detect...........        100   
2,2-Dichloropropane................  Non-detect...........         29   
2,3,4,5-Tetrachlorophenol..........  Non-detect...........        100   
2,3,4-Trichlorophenol..............  Non-detect...........        100   
2,3,5-Trichlorophenol..............  Non-detect...........        100   
2,3,6-Trichlorophenol..............  Non-detect...........        100   
2,3,7,8-Tetrachlorodibenzo-p-dioxin  Non-detect...........         26   
2,3,7,8-Tetrachlorodibenzo-p-furan.  Non-detect...........         26   
2,3-Dichloro-1-propene.............  Non-detect...........         29   
2,3-Dichlorophenol.................  Non-detect...........        100   
2,4-D..............................  Non-detect...........          5.7 
2,5-Dichlorophenol.................  Non-detect...........        100   
2-Fluoroacetamide..................  Non-detect...........        100   
2-Methylnaphthalene................  1000.................  ............
2-Nitropropane.....................  Non-detect...........         29   
3,3'-Dimethoxybenzidine............  Non-detect...........        100   
3,4-Dichlorophenol.................  Non-detect...........        100   
3,5-Dichlorophenol.................  Non-detect...........        100   
3-/4-Chlorophenol..................  Non-detect...........        100   
3-Nitroaniline.....................  Non-detect...........        220   
4,4'-methylene-bis(2-chloroaniline)  Non-detect...........        100   
4-Aminopyrridine...................  Non-detect...........        100   
4-Chlorophenyl phenyl ether........  Non-detect...........        220   
6-Propyl-2-thiouracil..............  Non-detect...........        100   
Acenaphthene.......................  Non-detect...........        220   
Acetone cyanohydrin................  Non-detect...........        100   
Allyl alcohol......................  Non-detect...........         29   
Ammonium vanadate..................  Non-detect...........         31   
Anthracene.........................  Non-detect...........        220   
Arochlor-1016......................  Non-detect...........          1.1 
Arochlor-1221......................  Non-detect...........          1.1 
Arochlor-1232......................  Non-detect...........          1.1 
Arochlor-1242......................  Non-detect...........          1.1 
Arochlor-1248......................  Non-detect...........          1.1 
Arochlor-1254......................  Non-detect...........          1.1 
Arochlor-1260......................  Non-detect...........          1.1 
Arsenic acid.......................  Non-detect...........          0.27
Arsenic pentoxide..................  Non-detect...........          0.22
Arsenic trioxide...................  Non-detect...........          0.19
Barium Cyanide.....................  Non-detect...........          3.7 
Benzal chloride....................  Non-detect...........        100   
Benzenethiol.......................  Non-detect...........         29   
Benzyl chloride....................  Non-detect...........        100   
Bis(2-chloroethoxy)methane.........  Non-detect...........        220   
Bis(2-chloroethyl)ether............  Non-detect...........        220   
Bis(2-ethylhexyl)phthalate.........  Non-detect...........        220   
Bromide............................  Non-detect...........          5.0 
Bromodichloromethane...............  Non-detect...........         17   
Calcium Cyanide....................  Non-detect...........          1.8 
Calcium chromate...................  Non-detect...........          4.2 

[[Page 43512]]

                                                                        
Chlordane..........................  Non-detect...........         11   
Chloride...........................  2.6..................  ............
Chloroethane.......................  Non-detect...........         17   
Copper Cyanide.....................  Non-detect...........          1.7 
Cyanide............................  Non-detect...........          1.0 
Cyanogen Bromide...................  Non-detect...........          6.6 
Cyanogen Chloride..................  Non-detect...........          8.6 
Di-selenium-tetra-sulfide..........  Non-detect...........        420   
Dibenzofuran.......................  Non-detect...........        220   
Dibromochloromethane...............  Non-detect...........         17   
Endosulfan I.......................  Non-detect...........          1.1 
Endosulfan II......................  Non-detect...........          1.1 
Endothal...........................  Non-detect...........        100   
Endrin.............................  Non-detect...........          1.1 
Endrin aldehyde....................  Non-detect...........          1.1 
Endrin ketone......................  Non-detect...........          1.1 
Epichlorohydrin....................  Non-detect...........         29   
Ethyl carbamate....................  Non-detect...........        100   
Ethylene glycol monoethyl ether....  Non-detect...........        100   
Ethylenethiourea (2-                 Non-detect...........         14   
 Imidazolidinethione).                                                  
Fluoride...........................  Non-detect...........          3.0 
Heptachlor.........................  Non-detect...........          1.1 
Heptachlor epoxide.................  Non-detect...........          2.3 
Lead acetate.......................  Non-detect...........         26   
Lead phosphate.....................  Non-detect...........         18   
MNNG (N-Metyl-N-nitroso-N'-          Non-detect...........         14   
 nitroguanidine).                                                       
Methomyl...........................  Non-detect...........          7.0 
N-Nitrosodiphenylamine.............  Non-detect...........        220   
Nickel Cyanide.....................  Non-detect...........          3.5 
Nickel carbonyl....................  Non-detect...........          8.2 
Nicotine...........................  Non-detect...........        100   
Octachlorodibenzodioxin............  Non-detect...........        130   
Octachlorodibenzofuran.............  Non-detect...........        130   
Osmium tetraoxide..................  Non-detect...........         40   
Phenanthrene.......................  250..................  ............
Phenylthiourea.....................  Non-detect...........          7.0 
Potassium Cyanide..................  Non-detect...........          2.5 
Potassium Silver Cyanide...........  Non-detect...........          2.9 
Propargyl alcohol..................  Non-detect...........         29   
Pyrene.............................  140..................  ............
Selenium dioxide...................  Non-detect...........          0.26
Selenium sulfide...................  Non-detect...........          0.41
Silver Cyanide.....................  Non-detect...........          2.6 
Silvex.............................  Non-detect...........          5.7 
Strychnine.........................  Non-detect...........        100   
Tetra-selenium-tetra-sulfide.......  Non-detect...........        810   
Tetraethyl lead....................  Non-detect...........         22   
Thallium acetate...................  Non-detect...........         18   
Thallium carbonate.................  Non-detect...........         16   
Thallium chloride..................  Non-detect...........         17   
Thallium nitrate...................  Non-detect...........         18   
Thallium oxide.....................  Non-detect...........         15   
Thallium sulfate...................  Non-detect...........         17   
Thioacetamide......................  Non-detect...........          7.0 
Thiofanox..........................  Non-detect...........        100   
Thiourea...........................  Non-detect...........          7.0 
Toluene-2,4-diamine................  Non-detect...........          7.0 
Toluene-2,6-diamine................  Non-detect...........          7.0 
Vanadium pentoxide.................  Non-detect...........         18   
Zinc Cyanide.......................  Non-detect...........          2.3 
Zinc phosphide.....................  Non-detect...........          0.37
alpha-BHC..........................  Non-detect...........          1.2 
beta-BHC...........................  Non-detect...........          1.2 
delta-BHC..........................  Non-detect...........          1.1 
gamma-BHC (Lindane)................  Non-detect...........          1.1 
m-Dinitrobenzene...................  Non-detect...........        220   
p-Toluidine........................  Non-detect...........        100   

[[Page 43513]]

                                                                        
trans-1,3-Dichloropropene..........  Non-detect...........         17   
------------------------------------------------------------------------



   Table 6.--Detection and Detection Limit Values for a Possible Composite Fuel Specification--90th Percentile  
                                                    Analysis                                                    
----------------------------------------------------------------------------------------------------------------
                                                                                                      Maximum   
                      Chemical name                         Concentration limit (mg/kg at 10,000     detection  
                                                                          Btu/lb)                  limit (mg/kg)
----------------------------------------------------------------------------------------------------------------
1,1,1-Trichloroethane....................................  Non-detect...........................          34    
1,1,2-Trichloro-1,2,2-trifluoroethane....................  Non-detect...........................          30    
1,1-Dichloro-1-propene...................................  Non-detect...........................          30    
1,1-Dichloroethane.......................................  Non-detect...........................          34    
1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin................  Non-detect...........................          74    
1,2,3,4,6,7,8-Heptachlorodibenzo-p-furan.................  Non-detect...........................          74    
1,2,3,4-Tetrachlorobenzene...............................  Non-detect...........................         100    
1,2,3,5-Tetrachlorobenzene...............................  Non-detect...........................         100    
1,2,3,6,7,8-Hexachlorodibenzo-p-dioxin...................  Non-detect...........................          74    
1,2,3,6,7,8-Hexachlorodibenzo-p-furan....................  Non-detect...........................          74    
1,2,3,7,8-Pentachlorodibenzo-p-dioxin....................  Non-detect...........................          74    
1,2,3,7,8-Pentachlorodibenzo-p-furan.....................  Non-detect...........................          74    
1,2,3-Trichlorobenzene...................................  Non-detect...........................         100    
1,2-Dichloroethane.......................................  Non-detect...........................          34    
1,2-Dichloropropane......................................  Non-detect...........................          34    
1,3-Dichloro-2-propanol..................................  Non-detect...........................          30    
1,3-Dichloropropane......................................  Non-detect...........................          30    
1,3-Propane sultone......................................  Non-detect...........................         100    
1-Chloronaphthalene......................................  Non-detect...........................         100    
2,2-Dichloropropane......................................  Non-detect...........................          30    
2,3,4,5-Tetrachlorophenol................................  Non-detect...........................         100    
2,3,4-Trichlorophenol....................................  Non-detect...........................         100    
2,3,5-Trichlorophenol....................................  Non-detect...........................         100    
2,3,6-Trichlorophenol....................................  Non-detect...........................         100    
2,3,7,8-Tetrachlorodibenzo-p-dioxin......................  Non-detect...........................          30    
2,3,7,8-Tetrachlorodibenzo-p-furan.......................  Non-detect...........................          30    
2,3-Dichloro-1-propene...................................  Non-detect...........................          30    
2,3-Dichlorophenol.......................................  Non-detect...........................         100    
2,4-D....................................................  Non-detect...........................           6.7  
2,5-Dichlorophenol.......................................  Non-detect...........................         100    
2-Fluoroacetamide........................................  Non-detect...........................         100    
2-Methylnaphthalene......................................  2500.................................           -    
2-Nitropropane...........................................  Non-detect...........................          30    
3,3'-Dimethoxybenzidine..................................  Non-detect...........................         100    
3,4-Dichlorophenol.......................................  Non-detect...........................         100    
3,5-Dichlorophenol.......................................  Non-detect...........................         100    
3-/4-Chlorophenol........................................  Non-detect...........................         100    
3-Nitroaniline...........................................  Non-detect...........................         700    
4,4'-methylene-bis(2-chloroaniline)......................  Non-detect...........................         100    
4-Aminopyrridine.........................................  Non-detect...........................         100    
4-Chlorophenyl phenyl ether..............................  Non-detect...........................         700    
6-Propyl-2-thiouracil....................................  Non-detect...........................         100    
Acenaphthene.............................................  Non-detect...........................         700    
Acetone cyanohydrin......................................  Non-detect...........................         100    
Allyl alcohol............................................  Non-detect...........................          30    
Ammonium vanadate........................................  Non-detect...........................          86    
Anthracene...............................................  Non-detect...........................         700    
Arochlor-1016............................................  Non-detect...........................           1.3  
Arochlor-1221............................................  Non-detect...........................           1.3  
Arochlor-1232............................................  Non-detect...........................           1.3  
Arochlor-1242............................................  Non-detect...........................           1.3  
Arochlor-1248............................................  Non-detect...........................           1.3  
Arochlor-1254............................................  Non-detect...........................           1.3  
Arochlor-1260............................................  Non-detect...........................           1.3  
Arsenic acid.............................................  Non-detect...........................           0.41 
Arsenic pentoxide........................................  Non-detect...........................           0.34 
Arsenic trioxide.........................................  Non-detect...........................           0.29 
Barium Cyanide...........................................  Non-detect...........................           3.7  

[[Page 43514]]

                                                                                                                
Benzal chloride..........................................  Non-detect...........................         100    
Benzenethiol.............................................  Non-detect...........................          30    
Benzyl chloride..........................................  Non-detect...........................         100    
Bis(2-chloroethoxy)methane...............................  Non-detect...........................         700    
Bis(2-chloroethyl)ether..................................  Non-detect...........................         700    
Bis(2-ethylhexyl)phthalate...............................  Non-detect...........................         700    
Bromide..................................................  Non-detect...........................           5.0  
Bromodichloromethane.....................................  Non-detect...........................          34    
Calcium Cyanide..........................................  Non-detect...........................           1.8  
Calcium chromate.........................................  Non-detect...........................           6.6  
Chlordane................................................  Non-detect...........................          13    
Chloride.................................................  2.7..................................           -    
Chloroethane.............................................  Non-detect...........................          34    
Copper Cyanide...........................................  Non-detect...........................           1.7  
Cyanide..................................................  Non-detect...........................           1.0  
Cyanogen Bromide.........................................  Non-detect...........................           6.6  
Cyanogen Chloride........................................  Non-detect...........................           8.6  
Di-selenium-tetra-sulfide................................  Non-detect...........................        1200    
Dibenzofuran.............................................  Non-detect...........................         700    
Dibromochloromethane.....................................  Non-detect...........................          34    
Endosulfan I.............................................  Non-detect...........................           1.3  
Endosulfan II............................................  Non-detect...........................           1.3  
Endothal.................................................  Non-detect...........................         100    
Endrin...................................................  Non-detect...........................           1.3  
Endrin aldehyde..........................................  Non-detect...........................           1.3  
Endrin ketone............................................  Non-detect...........................           1.3  
Epichlorohydrin..........................................  Non-detect...........................          30    
Ethyl carbamate..........................................  Non-detect...........................         100    
Ethylene glycol monoethyl ether..........................  Non-detect...........................         100    
Ethylenethiourea (2-Imidazolidinethione).................  Non-detect...........................         110    
Fluoride.................................................  Non-detect...........................           3.0  
Heptachlor...............................................  Non-detect...........................           1.3  
Heptachlor epoxide.......................................  Non-detect...........................           2.7  
Lead acetate.............................................  Non-detect...........................          74    
Lead phosphate...........................................  Non-detect...........................          53    
MNNG (N-Metyl-N-nitroso-N'-nitroguanidine)...............  Non-detect...........................         110    
Methomyl.................................................  Non-detect...........................          54    
N-Nitrosodiphenylamine...................................  Non-detect...........................         700    
Nickel Cyanide...........................................  Non-detect...........................           3.5  
Nickel carbonyl..........................................  Non-detect...........................          46    
Nicotine.................................................  Non-detect...........................         100    
Octachlorodibenzodioxin..................................  Non-detect...........................         150    
Octachlorodibenzofuran...................................  Non-detect...........................         150    
Osmium tetraoxide........................................  Non-detect...........................          40    
Phenanthrene.............................................  730..................................           -    
Phenylthiourea...........................................  Non-detect...........................          54    
Potassium Cyanide........................................  Non-detect...........................           2.5  
Potassium Silver Cyanide.................................  Non-detect...........................           2.9  
Propargyl alcohol........................................  Non-detect...........................          30    
Pyrene...................................................  600..................................           -    
Selenium dioxide.........................................  Non-detect...........................           0.34 
Selenium sulfide.........................................  Non-detect...........................           0.53 
Silver Cyanide...........................................  Non-detect...........................           2.6  
Silvex...................................................  Non-detect...........................           6.7  
Strychnine...............................................  Non-detect...........................         100    
Tetra-selenium-tetra-sulfide.............................  Non-detect...........................        2300    
Tetraethyl lead..........................................  Non-detect...........................          63    
Thallium acetate.........................................  Non-detect...........................          28    
Thallium carbonate.......................................  Non-detect...........................          25    
Thallium chloride........................................  Non-detect...........................          26    
Thallium nitrate.........................................  Non-detect...........................          29    
Thallium oxide...........................................  Non-detect...........................          23    
Thallium sulfate.........................................  Non-detect...........................          27    
Thioacetamide............................................  Non-detect...........................          54    
Thiofanox................................................  Non-detect...........................         100    
Thiourea.................................................  Non-detect...........................          54    
Toluene-2,4-diamine......................................  Non-detect...........................          54    
Toluene-2,6-diamine......................................  Non-detect...........................          54    
Vanadium pentoxide.......................................  Non-detect...........................          18    

[[Page 43515]]

                                                                                                                
Zinc Cyanide.............................................  Non-detect...........................           2.3  
Zinc phosphide...........................................  Non-detect...........................           1.7  
alpha-BHC................................................  Non-detect...........................           1.4  
beta-BHC.................................................  Non-detect...........................           1.4  
delta-BHC................................................  Non-detect...........................           1.3  
gamma-BHC (Lindane)......................................  Non-detect...........................           1.3  
m-Dinitrobenzene.........................................  Non-detect...........................         700    
p-Toluidine..............................................  Non-detect...........................         100    
trans-1,3-Dichloropropene................................  Non-detect...........................          34    
----------------------------------------------------------------------------------------------------------------


    Dated: August 15, 1996.
Elizabeth A. Cotsworth,
Acting Director, Office of Solid Waste.
[FR Doc. 96-21628 Filed 8-22-96; 8:45 am]
BILLING CODE 6560-50-P