[From the U.S. Government Printing Office, www.gpo.gov]



                               NOAA STATUS AND TRENDS
                                           Mussel Watch Project
                                                       Analytical Data
                                                               Year VIII


                                                        The Geochemical and
                                                         Environmental Research Group
                                                        Texas A&M Research Foundation






                                                                                                             Subttdffed to.

                                                                                                             artment of Commerce
                                                                                                      U.S. Dep
                                                                                                  National Oceanic & Atmospheric Adm.
                                                                                            A&         Ocean Assessment Division
                                                                                                     6001 Exec
                                                                                                              utive Blvd., Rm. 323
                                 g,                                                                    RockVdle, Maryland 20852







                          100*w                 95* W                 90, w                 85'W                   80o w
                                                                                                                    35' N









                                  Texas                            Miss! sippi     Alabama

                                                           Louisiana                               Florida              30* N
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             541.5
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             A-6 3
             year 8                                                                                                        241 N
             (1994)

                                                          Seotember 1994







                                                                                                      PXOPGZtY Of CSC Library
                                                             NOAA Status and Trends
                                                          Mussel Watch Project - Year 8
                                                                      Analytical Data

                                                                   Table of Contents
                                                                                                                                           Egge

                 MUSSEL WATCH PROJECT                            ..............................................................................................I


                           Field Station Data             ......................................................................................................2
                           Hydrocarbon Results            ................................................................................................7
                           Aromatic Data            .............................................................................................................8
                           Aromatic QC Data               ...................................................................................................  57
                           Pesticides and PCBs Data                   ....................................................................................  82
                           Pesticide QC Data              ................................................................................................. 131
                           Trace Metal           ............................................................................................................ 142
                           Trace Metal QC Data                 ........................................................................................... 147

                 ST. JOHN'S CORE DATA                       ............................................................................................... 152

                           Hydrocarbon Results            ........................................................................................... 153
                           Pesticide and PCB Results                    ................................................................................ 175


                 ANTARCTIC STUDIES                      ...........................................................I ....................................... 184

                           Limpet Aromatic Hydrocarbon Data                             ............................................................. 185
                           Limpet Pesticides and PCBs                       ............................................................................ 213
                           Urnpet Metal Data            ............................................................................................... 253

                           McMurdo Sediment Aromatic Hydrocarbon Data                                         ................................... 262
                           McMurdo Sediment Pesticides and PCB Data                                     .......................................... 271
                           McMurdo Sediment Metal Data                            ..................................................................... 284

                           Palmer Fish Aromatic Hydrocarbon Data                           ................................................... 288
                           Palmer Fish Pesticides and PCB Data                       .......................................................... 316
                           Palmer Fish Metal Data                  ...................................................................................... 353


                 ME"FHOD DE'1ECT[ON LITYUM                      .................................................................................. 358


                           Aromatic Method Detection Limits                            .............................................................. 359
                           Pesticides and PCBs Method Detection Limits                                    ........................................ 363
                           Trace Metals Method Detection Limits                               ...................................................... 369




                                                                                                      S    DEPARTMENT OF COMMERCE NCA
                                                                                                  COASTAL SERVICES CENTER
                                                                                                  ef,@4 SOUTH Holr@;Oi\, AVENUE




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                                                                                                              Mussel Watch Project Year 8 - Site Data



                                                                                Deg Min      Deg Min               M/D/Y Collection Bottom                                            (m)      *C      0/00 LocallIme LocalTime
               Site                           Name                              Latitude     Longitude    Type      Date        Method         Type Scientist         Species      Depth Temp, Salinity I-lighWater LawWater                   Reference    Horizonl
                                                                                                                                                                                                                                                               (m)
               LMSB SOUTH BAY LOWER LAGUNA MADRE                                26*02.42'    97110.49'      B      12/16/92         H          N      Roger Fay C. virginton          0.1      15        34         21:48          15:20       Galveston       0.25
                                                                                26*02.42*    97* 10.49'     B      12/16/92         H          N      Roger Fay    C. virginica       0.1      15        34         21:48          15:20       Galveston       0.25
                                                                                26002.42'    97110.49'      B      12/16/92         H          N      Roger Fay    C. virginica       0.1      15        34         21:48          15:20       Galveston       0.25
               CCNB NEUCES BAY CORPUS CHRISTI                                   27*51.24'    97*21.47-      B      12/15/92         H          SM       Wilson     C. virginica    0-0.5       11        28         21:21          14:14       Galveston       0.31
                                                                                27*51.24'    97*21.47-      B      12/15/92         H          SM       Wilson     C. virginica    0-0.5       11        25         21:21          14:14       Galveston       0.31
                                                                                27*51.24'    97021.47'      B      12/15/92         H          SM       Wilson     C. virginica    0-0.5       11        30         21:21          14:14       Galveston       0.31
               ABLR. LONG REEF ARANSAS BAY                                      28PO3.96'    96057.79'      B      12/16/92         H          MNSG     Wilson     C. uftptnica    0-0.5       15        20         21:48          15:20       Galveston       0.25
                                                                                28003.96'    96057.79'      B      12/16/92         H          MNSG     Wilson     C. virginim     0-0.5       15        20         21:48          15:20       Galveston       0.25
                                                                                28003.96'    96057.79'      B      12/16/92         H          MNSG     Wilson     C. virginica    0-0.5       15        20         21:48          15:20       Galveston       0.25
               MBAR AYRES REEF MESQUITE BAY                                     28009.82'    96049.96'      B      12/16/92         H                   Wilson     C. virginica    0-0.3       15        20         21:48          15:20       Galveston       0.25
                                                                                28009.82'    96*49.96'      B      12/16/92         H                   Wilson     C. virginfoa    0-0.3       15        20         21:48          15:20       Galveston       0.25
                                                                                28009.82'    96049.96'      B      12/16/92         H                   Wilson     C. virginica    0-0.3       15        20         21:48          15:20       Galveston       0.25
               SAPP PANTHER PT. REEF SAN ANTONIO BAY                            28113.87'    96*42.41'      B      12/16/92         D          S      Wilkinson C. vtrginica       1.0-2.0     14        20         21:48          15:20       Galveston       0.25
                                                                                28'13.87'    96'42.41'      B      12/16/92         D          S      Wilkinson    C. virginioa    1.0-2.0     14        20         21:48          15:20       Galveston       0.25
                                                                                28* 13.87'   96*42.41-      B      12/16/92         D          S      Wilkinson    C. v&ginfoa     1.0-2.0     14        20         21:48          15:20       Galveston       0.25
               ESBD BILL DAYS REEF ESPIRITU SANTO                               28025.02'    96*25.86-      B      12/17/92         H          SNA      Wilson     C. virginica    0-0.4       16        30         22:10          04:45       Galveston       0.27
                                                                                28025.02'    96125.86'      B      12/17/92         H          SNA      Wilson     C. virginloa    0-0.4       16        30         22:10          04:45       Galveston       0.27
                                                                                28025.02'    96*25.86-      B      12/17/92         H          SNA      Wilson     C. v&g1nfoa     0-0.4       16        30         22:10          04:45       Galveston       0.27
               MBGP GALLINIPPER PT.. MATAGORDA BAY                              28'35.13'    96034.25'      B      12/17/92         H          SR     Wilkinson C. virginfou          1.5      13        20         22:10          04:45       Galveston       0.27
                                                                                28*35. 1 T   96'34.22'      B      12/17/92         D          S      Wilkinson    C. virginim        2.0      13        20         22:10          04:45       Galveston       0.27
                                                                                28*35.29'    96*34.17-      B      12/17/92         D          SR     Wilkinson    C. virginfoa       2.0      13        20         22:10          04:45       Galveston       0.27
               MBLR LAVACA RIVER MOUTH MATAGORDA BAY                            28*39.63'    96135.04'      B      12/16/92         H          S      Wilkinson C. virginica          0.1      16        15         15:20          21:48       Galveston       0.25
                                                                                28*39,76'    96034.91'      B      12/16/92         H          SHM    Wilkinson    C. virginfou       0.1      16        15         15:20          21:48       Galveston       0.25
                                                                                28139.76'    96*34.9 1 -    B      12/16/92         H          SHM    Wilkinson    C. virginfoa       0.1      16        15         15:20          21:48       Galveston       0.25
               MBCB MATAGORDA BAY CARANCAHUA BAY                                walk up site                B      12/17/92         H          SR     Wilkinson C. virginica          0.1      16        20         22:10          04:45       Galveston       0.27
                                                                                walk up site                B      12/17/92         H          SR     Wilkinson    C. virginfoa       0.1      16        20         22:10          04:45       Galveston       0.27
                                                                                walk up site                B      12/17/92         H          SR     Wilkinson    C. v0pinica        0.1      16        20         22:10          04:45       Galveston       0.27
               MBTP TRES PALACIOS BAY MATAGORDA BAY                             28*39.72'    96013.17'      B      12/15/92         H          SMN    Wilkinson C. virginica          0.2      14        23         21:21          14:14       Galveston       0.31
                                                                                29'39.55'    96013.41'      B      12/15/92         H          MN     Wilkinson    C. v&ginim         0.2      15        23         21:21          14:14       Galveston       0.31
                                                                                28'39.29'    96* 13.66'     B      12/15/92         H          SMN    Wilkinson    C. virginfoa       0.2      15        20         21:21          14:14       Galveston       0.31
               MBEM EAST MATAGORDA MATAGORDA BAY                                28*42.77'    95*33.07'      B      12/15/92         H          R      Wilkinson C. vftykica           0.2      13        22         21:21          14:14       Galveston       0.31
                                                                                28*42.68'    95*53.07'      B      12/15/92         H          R      Wilkinson    C. virginica       0.2      13        22         21:21          14:14       Galveston       0.31
                                                                                28*42.80'    95*53.35'      B      12/15/92         H          R      Wilkinson    C. v&giniba        0.2      12        24         21:21          14:14       Galveston       0.31
               BRCL BRAZOS RIVER CEDAR LAKE                                     28151.46'    95*27.91'      B      12/8/92          H          R      Wilkinson C. virginim           0.1      13        24         16:54          08:39       Galveston       0.58
                                                                                28*51.00'    95*27.00'      B      12/8/92          H          R      Wilkinson    C. virginica       0.1      13        24         16:54          08:39       Galveston       0.58
                                                                                28*51.58'    95*27.70'      B      12/8/92          H          C      Wilkinson    C. Wginica         0.1      13        24         16:54          08:39       Galveston       0.58
               BRFS FREEPORT SURFSIDE BRAZOS RIVER                              28155.25'    95*20.35'      B      12/8/92          H          BC     Wilkinson C. v&yiniba           0.2      13        24         16:54          08:39       Galveston       0.58
                                                                                28*55.25'    95'20.35'      B      12/8/92          H          BC     Wilkinson    C. virginica       0.2      14        24         16:54          08:39       Galveston       0.58
                                                                                28055.25'    95020.35'      B      12/8/92          H          BC     Wilkinson    C. virginica       0.2      13        24         16:54          08:39       Galveston       0.58
               GBCR CONFEDERATE REEF GALVESTON BAY                              29015.80'    94054.85'      B      12/9/92          H          SR     Wilkinson C. virginica          0.1      13        20         17:40          09:22       Galveston       0.61
                                                                                29'15.80'    94*54.85-      B      12/9/92          H          SR     Wilkinson C. virginica          0.1      13        25         17:40          09:22       Galveston       0.61
                                                                                29'15.89     94154.85'      B      12/9/92          H          SR     Wilkinson    C. virginim        0.1      13        26         17:40          09:22       Galveston       0.61
               GBOB OFFATS BAYOU GALVESTON BAY                                  27'17.10'    94*50.16-      B      12/9/92          H          B      Wilkinson C. virginica          0.2      15        25         17:40          09:22       Galveston       0.61
                                                                                27'l 7. 10'  94050.16'      B      12/9/92          H          B      Wilkinson    C. virginica       0.2      14        25         17:40          09:22       Galveston       0.61
                                                                                27017.10'    94050.16'      B      12/9/92          H          B      Wilkinson    C. virginica       0.2      16        25         17:40          09:22       Galveston       0.61
               GBTD TODD'S DUMP GALVESTON BAY                                   29130.13'    94'53.71-      B      12/10/92         D          SM     Wilkinson C. virginica          1.5      14        18         18:30          10:05       Galveston       0.64
                                                                                29030.27'    94053.45@      B      12/10/92         D          SM     Wilkinson    C. 09irdoa         3.0      13        18         18:30          10:05       Galveston       0.64
                                                                                29030.03'    94053.18'      B      12/10/92         D          SM     Wilkinson    C. virginfou       3.0      13        18         18:30          10:05       Galveston       0.64
               GRYC YACHT CLUB GALVESTON BAY                                    29*37.36'    94059.73'      B      12/9/92          D          S      Wilkinson    C. vtTintca        3.0      13        16         17:40          09:22       Galveston       0.61
                                                                                29*37.36'    94059.73'      B      12/9/92          D          S      Wilkinson    C. virgirtica      3.0      13        16         17:40          09:22       Galveston       0.61
                                                                                29*37.36'    94*59.73-      B      12/9/92          D          S      Wilkinson    C. v&gtnica        3.0      13        20         17:40          09:22       Galveston       0.61
               GBSC SHIP CHANNEL GALVESTON BAY                                  29042.42'    94059.60'      B      12/9/92          T          SM       Wilson     C. virginica       1.0      14        15         17:40          09:22       Galveston       0.61
                                                                                29041.39'    94059.23'      B      12/9/92          T          SM       Wilson     C. virginica       1.0      14        15         17:40          09:22       Galveston       0.61
                                                                                29041.39'    94059.23'      B      12/9/92          T          SM       Wilson     C. virginica       1.0      14        15         17:40          09:22       Galveston       0.61



                               BOTrOM: S-SHELL,M-MUD.F-CONCIMM.N-SAND,G.GRASS.H-HASH.C-CLAY,[email protected] COUECTION MMOD: H-HAND.T-TONGS.D-DREDGE.R-RAKE SAMPIETYPE: B-BTVALVE.S-SEDIMEr-rr






                                                                                                               Mussel Watch Project Year 8 - Site Data



                                                                                 Deg Min      Deg Min                  M/D/Y     Collection Bottom                                      (m)       1C     061-00    Localmme Localmme                TkIal         Tt
                Site                            Name                             Latitude     Longitude    Type        Date       Method          Type Scientist        Species       Depth Temp salinity          High Water Low Water          Reference     H rizon
                                                                                                                                                                                                                                                                  (m)
                GBHR HANNA REEF GALVESTON BAY                                    29128.73'    94*43.57'       B    12/10/92           D           SMR   Wilkinson C. virginica          2.0       13        18        18:30           10:05      Galveston        0.64
                                                                                 29028.73'    94o43.57-       B    12/10/92           D           SMR   Wilkinson    C. virginim        2.0       13        is        18:30           10-05      Galveston        0.64
                                                                                 29*28.73'    94*43.57-       B    12/10/92           D           SMR   Wilkinson    C. virginica       2.0       13        18        18:30           10:05      Galveston        0.64
                SLBB BLUE BUCK POINT SABINE LAKE                                 29*47.09'    93054.36'       B    12/10/92           T           SM      Wilson     C. virginica       2.2       12        16        18:30           10:05      Galveston        0.64
                                                                                 29047.09'    93o54.36'       B    12/10/92           T           SM      Wilson     C. voyinica        2.2       12        16        18:30           10:05      Galveston        0.64
                                                                                 29*47.09'    93'54.36-       B    12/10/92           T           SM      Wilson     C. virgwoa         2.2       12        16        18:30           10:05      Galveston        0.64
                CLSJ ST. JOHNS ISLAND CALCASIEU LAKE                             29149.65'    93*23.04-       B    12/11/92         H/T           S       Wilson     C. virg&tka      0-2.5       17        17        19:12           10:49      Galveston        0.61
                                                                                 29049.65'    93023.0,C       B    12/11/92         H/T           S       Wilson     C. virginica     0-2.5       17        17        19:12           10:49      Galveston        0.61
                                                                                 29*49.65'    93*23.04-       B    12/11/92         H)r           S       Wilson     C. v&ginica      0-2.5       17        17        19:12           10:49      Galveston        0.61
                CLLC LAKE CHARLES CALCASIEU LAKE                                 30'03.5 F    93*18.43-       B    12/10/92           H           SM      Wilson     C. virginim      0-0.3       13        15        18:30           10:05      Galveston        0.64
                                                                                 30oO3.5 I'   93o 18.43'      B    12/10/92           H           SM      Wilson     C. virginica     0-0.3       13        14        18:30           10:05      Galveston        0.64
                                                                                 30oO3.5 1'   93'18.43'       8    12/10/92           H           SM      Wilson     C. 0ginica       0-0.3       13        13        18:30           10:05      Galveston        0.64
                JHJH JOSEPH HARBOR BAYOU J. HARBOR BAY01 29'37.96'                            92'45.78-       B    12/11/92           H           R       Wilson     C. viryinica                 13        10        19:12           10:49      Galveston        0.61
                VBSP SOU17HWEST PASS VERMILLION BAY                              29*34.45'    92'09.91'       B        1/5/93         D           SMH   Wilkinson C. virgirtim          2.0       18        5         16:07           07:37      Galveston        0.55
                                                                                 29*34.45'    92109.91'       B        1/5/93         D           SMH   Wilkinson    C. virgfttioa      2.0       18        5         16:07           07:37      Galveston        0.55
                                                                                 29'34.45'    92*09.9 1'      B        1/5/93         D           SMH   Wilkinson    C. virgintoa       2.0       18        5         16:07           07:37      Galveston        0.55
                ABOB OYSTER BAYOU ATCHAFALAYA BAY                                29o 14.5 1'  91008.13'       B        1/6/93         D           SM    Wilkinson C. virgWm             1.5       17        5         16:45           08:22      Galveston        0.61
                                                                                 29* 14.5 1'  9loO8.13'       B        1/6/93         H           SM    Wilkinson    C. virginim                            5         16:45           08:22      Galveston        0.61
                                                                                 29* 14.5 1'  91*08.13'       B        1/6/93         H           SM    Wilkinson    C. virghiica       0.2       17        5         16:45           08:22      Galveston        0.61
                CLCL CAILLOU LAKE CAILLOU LAKE                                   29'15.30'    90*56.02'       B        1/6/93         D           SM    Wilkinson    C. utirgUtica      2.0       18        8         16:45           08:22      Galveston        0.61
                                                                                 29'15.30'    90*56.02'       B        1/6/93         D           SM    Wilkinson    C. virg&tim        2.0       18        8         16:45           08:22      Galveston        0.61
                                                                                 29*15.30'    90056.02'       B        1/6/93         D           SM    Wilkinson    C. virginica       2.0       18        8         16:45           08:22      Galveston        0.61
                TBLB LAKE BARRE TERREBONNE BAY                                   29015.60'    90o35.76'       B        1/6/93         H           SM      Wilson     C. virginica     0-0.4       18        10        16:45           08:22      Galveston        0.61
                                                                                 29'15.60'    90*35.76'       B        1/6/93         H           SM      Wilson     C. virgMica      0-0.4       18        10        16:45           08:22      Galveston        0.61
                                                                                 29115.60'    90135.76'       B        1/6/93         H           SM      Wilson     C. virgUdba      0-0.4       18        10        16:45           08:22      Galveston        0.61
                TBLF LAKE FELicrTy TERREBONNE BAY                                29ol5.84'    90*23.88'       B        1/6/93         H           SM      Wilson     C. vtrg&doa      0-0.4       16        20        16:45           08:22      Galveston        0.61
                                                                                 29015.84'    90023.88'       B        1/6/93         H           M       Wilson     C. virginfoa     0-0.4       16        20        16:45           08:22      Galveston        0.61
                                                                                 29015.84'    90'23.88'       B        1/6/93         H           MG      Wilson     C. viryinica     0-0.4       16        20        16:45           08:22      Galveston        0.61
                BBSD BAYOU ST. DENIS BARATARIA BAY                               29124.05'    89*59.82'       B        1/5/93         T           M       Wilson     C. virgUdca        2.0       19        10        16:07           07:37      Galveston        0.55
                                                                                 29*24.05'    89'59.82'       B        1/5/93         T           M       Wilson     C. virginka        2.0       19        10        16:07           07:37      Galveston        0.55
                                                                                 29*24.05'    89o59.82'       B        1/5/93         T           M       Wilson     C. vtrginica       2.0       19        10        16:07           07:37      Galveston        0.55
                8BMB MIDDLE BANK BARATARIA BAY                                   29'16.55'    89o56.49'       B        1/5/93         H           MG      Wilson     C. virgWm        0-0.3       19        20        16:07           07:37      Galveston        0.55
                                                                                 29ol6.55'    89o56.49'       B        1/5/93         H           MG      Wilson     C. vtrgin(ca     0-0.3       19        20        16:07           07:37      Galveston        0.55
                                                                                 29ol6.55'    89*56.49'       B        1/5/93         H           MG      Wilson     C. virginica     0-0.3       19        20        16:07           07:37      Galveston        0.55
                MRTP TIGER PASS MISSISSIPPI RIVER                                29*08.64@    89*25.66'       B        1/7/93         H           G     Wilkinson    C. virgirtica      0.0       13        2         22:59           09:57         Mobile        0.76
                                                                                 29*08.64'    89*25.66'       B        1/7/93         H           G     Wilkinson    C. virginica       0.0       13        2         22:59           09:57         Mobile        0.76
                                                                                 29'08.64'    89'25.66'       B        1/7/93         H           G     Wilkinson    C. vtrgb-dca       0.0       13        2         22:59           09:57         Mobile        0.76
                MRPL PASS A LOUTRE MISSISSIPPI RIVER, LA                         29*04.90'    89*05.48'       B        1/7/93         D           MS    Wilkinson    C. vUyinica        2.0       13        5         22:59           09:57         Mobile        0.76
                                                                                 29'04.90'    89'05.49        B        1/7/93         D           MS    Wilkinson    C. virgirtica      2.0       13        5         22:59           09:57         Mobile        0.76
                                                                                 29*04.90'    89oO5.48'       B        1/7/93         D           MS    Wilkinson    C. vUgb-dm         2.0       13        5         22:59           09:57         Mobile        0.76
                BSSI SABLE ISLAND BRETON SOUND                                   29024.12'    89o29.21'       B        1/8/93         D           MS    Wilkinson    C. virglhfoa       1.0       10        2         23:48           10:33         Mobile        0.73
                                                                                 29*24.12'    89*29.2 1'      B        1/8/93         D           MS    Wilkinson    C. virginioa       1.0       10        2         23:48           10:33         Mobile        0.73
                                                                                 29*24.12'    89o29.2 I'      B        1/8/93         D           MS    Wilkinson    C. v&ghVca         1.0       10        2         23:48           10:33         Mobile        0.73
                BSBG BAY GARDERNE BRETON SOUND                                   29135.90'    89'37.27'       B        1/7/93         H           SM      Wilson     C. virginka      0-0.4       16        10        22:59           09:57         Mobile        0.76
                                                                                 29035.99     89'37.27'       B        1/7/93         H           SM      Wilson     C. virgihLca     0-0.4       16        10        22:59           09:57         Mobile        0.76
                                                                                 29*35.90'    89*37.27'       B        1/7/93         H           SM      Wilson     C. virg(Mm       0-0.4       16        10        22:59           09:57         Mobile        0.76
                LBMP MALHEUREUX POINT LAKE BORGNE                                29'51.99'    89*40.7 F       B        1/7/93         H           SM      Wilson     C. virgUifm      0-0.4       16        8         22:59           09:57         Mobile        0.76
                                                                                 29151.99'    89140.71'       B        1/7/93         H           SM      Wilson     C. virginim      0-0.4       16        8         22:59           09:57         Mobile        0.76
                                                                                 29051.99'    89040.7 F       B        1/7/93         H           Sm      Wilson     C. virg&tica     0-0.4       16        8         22:59           09:57         Mobile        0.76
                MSPC MISSISSIPPI SOUND PASS CHRISTIAN                            30'18.13'    89*19.70'       B        1/8/93         D           NSH   Wilkinson    C. virginica       2.5       15        10        23:48           10:33         Mobile        0.73
                                                                                 30* 18.13'   89o 19.70'      B        1/8/93         D           NSH   Wilkinson    C. virginica       2.5       15        10        23:48           10:33         Mobile        0.73
                                                                                 30'19.13'    89- 0.70'       B        1.'18,93                   NSH   Willrinqnn   r- ifirnink'a      2.5       15        10        23:48           10:33         Mobile        0.73
                MSBB MISSISSIPPI SOUND BILOXI BAY                                30123.55'    88'51.46'       B        1/8@93         H                   Wilson     C. virginica     0-0.3       16        10        23:48           10:33         Mobile        U. 7 3
                                                                                 30o23.55'    88o5l.46'       B        1/8/93         H                   Wilson     C. virgirtica    0-0.3       16        10        23:48           10:33         Mobile        0.73


                                 BOTMM: S-SHELLM-MUD.F-CONCRME,N-SAND,G-GRASS.H-HASH.C-CLAY.R-REEF.11-RUBBLE.K-KELPA-ALGAET-ROOTS.P.PFAT COUZCTION Mn'Huu:                                                                      9-R!VktVRS-qFr)1MEW






                                                                                                                     Mussel Watch Project Year 8 - Site Data



                                                                                     Deg Min       Deg Min                 M/D/Y        Collection Bottom                                         (m)        *C      0/00 UwalTlme IzWMme                         Tidal          Mdal
                Site                              Name                               Latitude      Longitude     Type        Date        Method           Type Scientist         Species         Depth Temp Salinity HighWater WwWater Reference Ho
                                                                                                                                                                                                                                                                                 (m)
                                                                                     30023.55'     88051.46'        B      1/8/93            H                     Wilson      C. 0yinica        0-0.3       16         10         23:48           10:33          Mobile         0.73
                MSPB PASCAGOULA BAY MISSISSIPPI SOUND                                30020.44!     88*35.55-        B      1/9/93            D            SR    Wilkinson C. v&ginica             1.0        12         6          24:00           11:05          Mobile         0.70
                                                                                     30020.44'     88035.55'        B      1/9/93            D            MS    Wilkinson      C. v&ginim         1.0        13         6          24:00           11:05          Mobile         0.70
                                                                                     30*20.44'     88'35.55'        B      1/9/93            D            SR    Wilkinson      C. vkginfca        2.0        15         6          24:00           11:05          Mobile         0.70
                MBCP CEDAR POINT REEF MOBILE BAY                                     30118.64'     88*08.15'        B      1/9/93            H            NS       Wilson      C. viTinica       00.5        14         7          24:00           11:05          Mobile         0.70
                                                                                     30'18.64'     88*08.15'        B      1/9/93            H            NS       Wilson      C. virgirtica     00.5        14         7          24:00           11:05          Mobile         0.70
                                                                                     30118.64'     88108.15'        B      1/9/93            H            NS       Wilson      C. virg&dca       00.5        14         7          24:00           11:05          Mobile         0.70
                MBHI HOUINGERS ISLE CHA MOBILE BAY                                   30*33.93'     88*04.59'        B      1/9/93            T            MSN      Wilson      C. vityinica       2.0        14         5          24:00           11:05          Mobile         0.70
                                                                                     30*33.93'     88*04.59'        B      1/9/93            T            MSN      Wilson      C. virginica       2.0        14         5          24:00           11:05          Mobile         0.70
                                                                                     30'33.93'     88004.59'        B      1/9/93            T            MSN      Wilson      C. virginica       2.0        14         5          24:00           11:05          Mobile         0.70
                PBPH PUBLIC HARBOR PENSACOLA BAY                                     30*24.62'     87* 11.43'       B      1/11/93           R            N        Wilson      C. voyinica        5.0        16         18         00:18           10:30       Pensacola         0.36
                                                                                     30*24.62'     87* 11.43'       B      1/11/93           R            N        Wilson      C. virginim        5.0        16         18         00:18           10:30       Pensacola         0.36
                                                                                     30024.62'     87011.43'        B      1/11/93           R            N        Wilson      C. virginfea       5.0        16         18         00:18           10:30       Pensacola         0.36
                PBIB INDIAN BAYOU, PENSAC01A BAY, FLORIDA                            30*31.02'     87-06.66-        B      1/11/93           D            SM    Wilkinson      C. virgirtica      2.0        15         20         00:18           10:30       Pensacola         0.36
                                                                                     30*31.02'     87*06.66-        B      1/11/93           D            SM    Wilkinson C. virgirtica           2.0        15         20         00:18           10:30       Pensacola         0.36
                                                                                     30*31.02'     87*06.66'        B      1/11/93           D            SM    Wilkinson      C. virginica       2.0        15         20         00:18           10:30       Pensacola         0.36
                PBSP PENSACOLA BAY SABINE POINT                                      30*20.67'     87009.03'        B      1/11/93           H            E     Wilkinson      C. virgMica        0.5        15         25         00:18           10:30       Pensacola         0.36
                                                                                     30*20.60'     87*09.08'        B      1/11/93           H            E     Wilkinson      C. vtrg&dca        0.5        16         25         00:18           10:30       Pensacola         0.36
                                                                                     30020.80'     87009.17'        B      1/11/93           H            PIER  Wilkinson      C. vlThiica        0.5        16         25         00:18           10:30       Pensacola         0.36
                CBJB CHOCTAWATCHEE BAY JOES BAYOU                                    30*24.63'     86*29.46-        B      1/12/93           H       SBRMN Wilson              C. virginioa    0.1-0.5       17         12         00:53           10:12       Pensacola         0.21
                                                                                     30024.63'     86029.46'        B      1/12/93           H       SBRMN Wilson              C. virginica    0.1-0.5       17         12         00:53           10:12       Pensacola         0.21
                                                                                     30*24.63'     86*29.46-        B      1/12/93           H       SBRMN Wilson              C. virybitca    0.1-0.5       17         12         00:53           10:12       Pensacola         0.21
                CBSR OFF SANTA ROSA CHOCTAWHATCHEE 13AY                              30024.73'     86ol2.38-        B      1/11/93           D            SM    Wilkinson C. virginica            3.0        16         10         00:18           10:30       Pensacola         0.36
                                                                                     30*24.70'     86ol2.26-        B      1/11/93           D            SM    Wilkinson      C. virginica       3.0        17         10         00:18           10:30       Pensacola         0.36
                                                                                     30*24.73'     86* 12.19'       B      1/11/93           D            SMR   Wilkinson      C. 0pinica         3.0        17         10         00:18           10:30       Pensacola         0.36
                CBPP SHIRK POINT CHOICTAWHATCHEE BAY                                 30128.74'     8628.75'         B      1/11/93           H            B        Wilson      C. virginica      0-0.3       17         10         00:18           10:30       Pensacola         0.36
                                                                                     30'28.74'     86*28.75'        B      1/11/93           H            B        Wilson      C. virginica      0-0.3       17         10         00:18           10:30       Pensacola         O@3
                                                                                     30028.74'     86028.75'        B      1/11/93           H            B        Wilson      C. virginka       0-0.3       17         10         00:18           10:30       Pensacola         0 3:
                PCLO PANAMA CrIY L=E OYSMR                                           30o 15.65'    85o4l.17'        B      1/12/93           H            PIER  Wilkinson      C. virginica       0.2        19         18         00:53           10:12       Pensacola         0.21
                                                                                     30* 15.06'    85*40.87-        B      1/12/93           HR           PIER  Wilkinson      C. virgiritca      0.3        19         20         00:53           10:12       Pensacola         0.21
                                                                                     30'15.2 V     85*40.93'        B      1/12/93           H            PIER  Wilkinson      C. vtTinica                              20         00:53           10:12       Pensacola         0.21
                PCMP PANAMA CITY MUNICIPAL PIER                                      30109.02'     85*39.85'        B      1/12/93           HR           E     Wilkinson      C. virginfoa       0.2        18         20         00:53           10:12       Pensacola         0.21
                                                                                     30009.05'     85o39.80-        B      1/12/93           HR           E     Wilkinson      C. virginim        0.2        20         20         00:53           10:12       Pensacola         0.21
                                                                                     30*09.03'     85039.79'        B      1/12/93           HR           E     Wilkinson      C. vLrgirilca      0.2        20         20         00:53           10:12       Pensacola         0.21
                SAWB WATSON BAYOU ST. ANDREW BAY                                     30'08.53'     85137.90'        B      1/12/93           If           NB    Wilkinson      C. virgbilca       0.2        18         20         00:53           10:12       Pensacola         0.21
                                                                                     30'08.53'     85137.90'        B      1/12/93           H            NB    Wilkinson      C. virgirifoa      0.2        18         20         00:53           10:12       Pensacola         0.21
                                                                                     30108.53'     85*37.90'        B      1/12/93           H            N13   Wilkinson      C. virginica       0.2        18         20         00:53           10:12       Pensacola         0.21
                APDB DRY BAR APALACHICOLA BAY                                        29140.44'     85*04.5 F        B      1/13/93           H            SNK      Wilson      C. virgirtica   0.1-0.5       20         5          16:51           08:53       Pensacola         0.12
                                                                                     29140.44*     85*04.51'        B      1/13/93           H            SNK      Wilson      C. vtTinica     0.1-0.5       20         5          16:51           08:53       Pensacola         0.12
                                                                                     29140.44'     85004.5 1'       B      1/13/93           H            SNK      Wilson      C. virghifea    0.1-0.5       20         5          16:51           08:53       Pensacola         0.12
                APCP CAT PT. BAR APALACHICOLA BAY                                    29'43.46'     84*53.22'        B      1/13/93           H            SNK      Wilson      C. virginioa    0.1-0.4       19         20         16:51           08:53       Pensacola         0.12
                                                                                     29143.46'     84153.22'        B      1/13/93           H            SNK      Wilson      C. virginica    0.1-0.4       19         20         16:51           08:53       Pensacola         0.12
                                                                                     29*43.46'     84*53.22'        B      1/13/93           H            SNK      Wilson      C. virgiriica   0.1-0.4       19         20         16:51           08:53       Pensacola         0.12
                AESP APPAIACHEE BAY SPRING CREEK                                     30*03.93'     84* 19.28'       B      1/13/93           H            SR    Wilkinson      C. utrg&dca        0.2        20         5          16:51           08:53       Pensacola         0.12
                                                                                     30103.89'     84* 19.28'       B      1/13/93           H            SR    Wilkinson      C. virgirtica      0.2        20         5          16:51           08:53       Pensacola         0.12
                                                                                     30'03.84'     84119.27'        B      1/13/93           H            SR    Wilkinson      C. v&pinica        0.2        20         5          16:51           08:53       Pensacola         0.12
                CKBP BLACK POINT CEDAR KEY                                           29o 12.42'    83oO4.14'        B      1/13/93           H            MSR   Wilkinson      C. v&g(nica        0.2        22         27         16:51           08:53       Pensacola         0.12
                                                                                     29012.42'     83004.14'        B      1/13/93           H            MSR   Wilkinson      C. uirgirtica      0.2        22         27         16:51           08:53       Pensacola         0.12
                                                                                     29o 12.42'    83oO4.14'        B      1/13/93           H            MSR   Wilkinson      C. virgoitca       0.2        22         27         16:51           08:53       Pensacola         0.12
                TBNP TAMPA BAY NAVAREZ PARK                                          27*47.28      82'45.28         B      1/14/93           H            B     Wilkinson      C. virginica       0.2        22         34         18:41           00:47       St. Petrsbg       0.49
                                                                                     27o47.28      82045.28         B      1/14/93           H            B     Wilkinson      C. vUginfba        0.2        22         34         18:41           00:47       St. Petrsbg       0.49
                                                                                     27*47.28      82*45.28         B      1/14/93           H            B     Wilkinson      C. v&ptnim         0.2        22         34         18:41           00:47       St. Petrsbg       0.49
                TBMK MULLET KEY BAYOU TAMPA BAY                                      27'37.25'     82*43.65-        B      1/14/93           If           S        Wilson      C. vir-giriica     0.5        22         33         18:41           00:47       St. Petrsbg       0.49
                                                                                     27'37.25'     82'43.65'        B      1/14/93           H            S        Wilson      C. virginica       0.5        22         33         18:41           00:47       St. Petrsbg       0.49



                                  HOTPOM: S-SHELL.M-MUD.E-CONCREM.N-SAND,G.GRASS.H-HASH.C-CLAYR-RFEF,B-RUBBLE.K-KELPA-ALGAE.T-ROarS,NPEAT COLLECnON M&MOD: H-HAND.T-T0NGS.D-DRED0E,PRAKF SAMPtZTYPP: B-BIVALVE.S-SEDIMEW







                                                                                                                   Mussel Watch Project Year 8 - Site Data


                                                                                   Deg Min       Deg Min                M/D/Y        Collection Bottom                                         (m)       *C      0/00      Local Time Imal Time               Tidal      -fiawl
             [-site                             Name                               Latitude      Longitude     Type       Date        Mediod          Type Scientist          Species        Depth Temp Salinity           High Water Low Water Reference                Horizonj
                                                                                                                                                                                                                                                                            (m)
                                                                                   27*37.25'     82*43.65-       B      1/14/93           H           S        Wilson      C. virghii6a        0.5       22        33          18:41          00:47        St. Petrsbg      0.49
              TBPB PAPYS BAYOU TAMPA BAY                                           27*50.46'     82*36.74'       B      1/15/93           H           SR     Wdldnson      C. viryintba        0.2       21        15          19:24          02:13        St. Petrsbg      0.61
                                                                                   27*50.46'     82*36.74-       B      1/15/93           H           SR     Wilkinson     C. wginfea          0.2       21        15          19:24          02:13        St. Petrsbg      0.61
                                                                                   27*50.46'     82o36.74-       B      1/15/93           H           SR     Wilkinson     C. virginica        0.2       21        15          19:24          02:13        St. Petrsbg      0.61
              TBOT TAMPA BAY OLD TAMPA BAY                                         28*01.48'     82'37.95-       B      1/14/93           H           NSR    Wilkinson     C. virginica        0.2       22        14          18:41          00:47        St. Petrsbg      0.49
                                                                                   28*01.48'     82137.95'       B      1/14/93           H           SR     Wilkinson     C. virgihiba        0.2       22        15          18:41          00:47        St Petrsbg       0.49
                                                                                   28101.48'     82037.95'       B      1/14/93           H           SR     Wilkinson     C. virginfou        0.2       22        15          18:41          00:47        St. Petrsbg      0.49
              T'BKA TAMPA BAY PETER 0. KNIGHT AIRPORT'                             27054.52'     82027.27'       B      1/14/93           H           NBH      Wilson      C. virginiou      0-0.4       22        27          18:41          00:47        St. Petrsbg      0.49
                                                                                   27154.52'     82*27.27'       B      1/14/93           H           NBH      Wilson      C. viryinica      0-0.4       22        27          18:41          00:47        St. Petrsbg      0.49
                                                                                   27*54.52'     82*27.27'       B      1/14/93           H           NBH      Wilson      C. virginica      0-0.4       22        27          18:41          00:47        St. Petrsbg      0.49
              TBHB TAMPA BAY HILLSBOROUGH                                          27051.31'     82023.70'       B      1/15/93           H                    Wilson      C. viryinim       0-0.3       20        15          19:24          02:13        St Petrsbg       0.61
                                                                                   27*51.31'     82023.70'       B      1/15/93           H                    Wilson      C. utTinica       0-0.3       20        15          19:24          02:13        St. Petirsbg     0.61
                                                                                   27*51.31*     82'23.70'       B      1/15/93           H                    Wilson      C. v(T&dm         0-0.3       20        is          19:24          02:13        St. Petrsbg      0.61
              TBCB COCKROACH BAY TAMPA BAY                                         27040.52'     82130.62'       B      1/15/93           H           SN       Wilson      C. virginim       0-0.4       22        14          19:24          02:13        St. Petrsbg      0.61
                                                                                   27'40.52'     82'30.62'       B      1/15/93           H           SN       Wilson      C. viryinica      0-0.4       22        14          19:24          02:13        St. Petrsbg      0.61
                                                                                   27140.52'     82'30.62'       B      1/15/93           H           SN       Wilson      C. v&gfn(ba       0-0.4       22        14          19:24          02:13        St. Petrsbg      0.61
              CBBI     BIRD ISLAND CHARLOTTE HARBOR                                26030.74'     82102.19'       B      1/18/93           H           SR     Wilkinson     C. virginica        0.2       20        24          22:13          05:57        St. Petrsbg      0.79
                                                                                   26*30.74'     82*02.19'       B      1/18/93           H           SR     Wilkinson     C. utrginfea        0.2      20.5       24          22:13          05:57        St. Petrsbg      0.79
                                                                                   26030.74'     82*02.19'       B      1/18/93           H           SR     Wilkinson     C. uirginim         0.2      20.5       24          22:13          05:57        St. Petrsbg      0.79
              CBF?A    FORT MEYERS CHARLOTTE HARBOR                                26133.19'     81155.75'       B      1/18/93           H           BN     Wilkinson     C. uIrginim         0.1       20        14          22:13          05:57        St. Petrsbg      0.79
                                                                                   26*33.19'     81*55.75-       B      1/18/93           H           B      Wilkinson     C. virginica        0.2       20        14          22:13          05:57        St. Petrsbg      0.79
                                                                                   26133.19'     81*55.75'       B      1/18/93           H           B      Wilkinson     C. virginica        0.2       20        14          22:13          05:57        St. Petrsbg      0.79
              NBNB;    NAPLES BAY NAPLES BAY                                       26006.73'     81047.13'       B      1/18/93           H           CHMK     Wilson      C. virginim       0-0.4       23        30          22:13          05:57        St. Petrsbg      0.79
                                                                                   26*06.73'     81*47.13-       B      1/18/93           H           SRNM     Wilson      C. viTirdm        0-0.4       23        30          22:13          05:57        St. Petrsbg      0.79
                                                                                   26006.73:     81-47.13-       B      1/18/93           H           SRNM     Wilson      C virginica       0-0.4       23        30          22:13          05:57        St. Petrsbg      0.79
              RBHC     HENDERSON CREEK ROOKERY BAY                                 26001.53      81*44.23-       B      1/18/93           H           SN       Wilson      C. virginica      0-0.4       21        35          22:13          05:57        St. Petrsbg      0.79
                                                                                   26*01.53'     8 1 *44.23'     B      1/18/93           H           SN       Wilson      C. virginica      0-0.4       21        35          22:13          05:57        St. Petrsbg      0.79
                                                                                   26*01.53'     8 1 *44.23'     B      1/18/93           H           SN       Wilson      C. virginica      0-0.4       21        35          22:13          05:57        St. Petrsbg      0.79
              EVFU     FAKA UNION BAY EVERGLADES                                   25*54.12'     81'30.87'       B      1/18/93           H           S        Wilson      C. virginica      0-0.3       22        13          22:13          05:57        St. Petrsbg      0.79
                                                                                   25*54.12'     81'30.87'       B      1/18/93           H           S        Wilson      C. virgftica      0-0.3       22        13          22:13          05:57        St. Petrsbg      0.79
                                                                                   25*54.12'     81030.87'       B      1/18/93           H           S        Wilson      C. virgirtica     0-0.3       22        13          22:13          05:57        St. Petrsbg      0.79
              PRBB     BAHIA DE BOQUERON PUERTO RICO                               18000.44'     67010.72'       B      2/19/93           H           M        Wilson      C. virginica      0-0.3       29        36          08:18          01:14        San Juan         0.49
                                                                                   18*00.44'     67'10.72'       B      2/19/93           H           M        Wilson      C. virgUtica      0-0.3       28        36          08:18          01:14        San Juan         0.49
                                                                                   18*00.44'     67*10.72'       B      2/19/93           H           M        Wilson      C. virginim       0-0.3       29        36          08:18          01:14        San Juan         0.49
              PRBM     BAHIA MONTALVA PUERTO RICO                                  17058.23'     66059.43'       B      2/20/93           H           T13      Wilson      C. virgiritca,    0-0.3       28        37          08:51          01:59        San Juan         0.43
                                                                                   17*58.23'     66159.43'       B      2/20/93           H           TB       Wilson      C. virginica      0-0.3       28        37          08:51          01:59        San Juan         0.43
                                                                                   l7o58.23:     66-59.43-       B      2/20/93           H           TB       Wilson      C. virginica      0-0.3       28        37          08:51          01:59        San Juan         0.43
              PRBJ     BAHIA DE JOBOS PUERTO RICO                                  17*56.33      66*10.95-       B      2/22/93           H           TN       Wilson      C. virginica      0-0.3       27        38          09:49          03:19        San Juan         0.37
                                                                                   17*56.33'     66*10.95-       B      2/22/93           H           TN       Wilson      C. virginica      0-0.3       26        38          09:49          03:19        San Juan         0.37
                                                                                   17*56.33'     66*10.95-       B      2/22/93           H           TN       Wilson      C. virgirtica     0-0.3       27        38          09:49          03:19        San Juan         0.37
















                                BOTrOM: S-SHELL,M-MUD.F-CONCRLIM.N-SAND.0-GRASS,H-HASH.C-CLAY,R-REEr.E@-RUBBIZ,K-KELPA-ALGAE.T-RO07B.NPEAT C011ZCM0N MMOD; H-HANDX-TONGS.D-DREDGEA-RAKE SAMPLEWPE: B-MALVE.8-SEDIMENr



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   M M M M M M M M M M M M                                                                                      M M M M M M @

                                                           Mussel Watch Project Year 8 - Aromatics Data

               INVEST#:                LMSB                        CCNB                     ABLR                      MBAR                       SAPP
                  ID:           L. lAiguna Madre             Corpus Christi            Aransas Bay              Mesquite Bay              San Antonio Bay
                 SITE                  South Bay             Ingleside Cove                 Long Reef                 Ayres Reef           Mosquito Point
               L4,BSAMNO:              X7030                       K7024                    K7034                     K7032                      K7042
               SAMPLE TYPE:            SAMP                        SAMP                     SAMP                      SAMP                       SAMP
                UNIT:                  ng/g                        ng/g                     ng/g                      ng/g                       ng/g
               Analyte (Cont)          Cone       DB QUAL          Cone      DB QUAL        Cone     D13 QUAL         Cone     DB QUAL           Cone       DB QUALI

               RECEIPT DATE:           12/18/96                    12/17/96                 12/18/96                  12/18/96                   12/18/96
               QCBATCH:                M1232                       M1232                    M1233                     M1232                      M1233
         EXTRACTION DATE:              9/15/97                     9/15/97                  11/12/97                  9/15/97                    9/15/97
               METHOD:                 GCMS                        GCMS                     GCMS                      GCMS                       GCMS
               ANALYSIS DATE:          10/21/97                    10/21/97                 12/24/97                  10/21/97                   10/25/97
               METHOD:                 GCECD                       GCECD                    GCECD                     GCECD                      GCECD
               ANALYSIS DATE:          7/31/98                     7/31/98                  8/24/98                   7/31/98                    8/24/98
               MATRIX                  TISSUE                      TISSUE                   TISSUE                    TISSUE                     TISSUE
               SUBMAT-
               WE'M:                   15.48                       15                       15.17                     15.51                      4.65
               DRYWT:                  2                           2.66                     2.52                      3.31                       0.96
               Vi'rUNTrS:              GRAMS         DRY           GRAMS       DRY          GRAMS       DRY           GRAMS       DRY            GRAMS         DRY
               PCTSOLIDS:              12.900/6                    17.800,6                 16.600A                   21.4006                    20.70%
               Upid Weight:
               TOTAL LIPID:            3.04                        7.56                     9.26                      9.52                       12.66
               LIPID UNITS:            % DRY                       % DRY                    % DRY                     % DRY                      % DRY
                VOL.
               VOLUNITS:               LITERS                      LITERS                   LITERS                    LITERS                     LITERS
         Surrogate Recoveries
                PAH's:
               NAPHD8:                 64.6                        68.6                     59.2                      61.7                       66.3
               ACENDIO:                67.1                        73.4                     59.5                      64.4                       74.3
               PHENDIO:                66.6                        81.2                     67.9                      72.6                       64.4
               CHRYD12:                69.1                        72.8                     71.6                      66.6                       55
               PERYD12-                65.5                        68.1                     52.7                      70                         50.2


               NAPHTHALENE             5.7                         4.5                      11.2                      4.6                        19.5
         CI-NAPHTHALENES               7              J            6.1                      8.7                       6.5                        16.9           J
         C2-NAPHTHALENES                             ND            9.4                      5.1                       6.4                                        ND
         C3-NAPHTHALENES                             ND            19.3                     17.9                                  ND                            ND
         C4-NAPHTHALENES                             ND            16.6                     14.5                                  ND                            ND
               BIPHENYL 0              1.9            J            2.8                      6.4                       2.6          J             7.8            J
         ACENAPHTHYLENE                0.5            J            1.3          J           0.3          J            0.8          J             4.1            J
         ACENAPHTHENE*                 2.9            J            3.2          J           1.4          J            0.2          J             2.7
               FLUORENE0               2.6            J            5.8                      4.1          J            1.8          J             3.9
               CI-FLUORENES                          ND            5.9          J           8.4          J                        ND                            ND






                                                             Mussel Watch Project Year 8 - Aromatics Data

                INVEST#:                  LMSB                       CCNB                      ABLR                     MBAR                        SAPP
                   ID:            L, Laguna Madre              Corpus Christi             Aransas Bay              Mesquite Bay              San Antonio Bay
                   SITE              South Bay                 Ingleside Cove              Long Reef                Ayres Reef                Mosquito Point
               LABSAMNO:                  K7030                      K7024                     K7034                    K7032                       K7042
               SAMPLE TYPE:               SAMP                       SAMP                      SAMP                     SAMP                        SAMP
                  UNIT.-                  ng/g                       nglg                      ng1g                     ng/g                        ng/g
               Analyte (Cont)             Conc      DB QUAL          Conc      DB QUAL         Conc    DB QUAL          Conc     DB QUAL            Conc       DB QUAL

               C2-F1,UORENES                           ND            28.5                      34.4                                  ND                           ND
               C3-FLUORENES                            ND            80.6                      56.1                                  ND                           ND
               PHENANTHRENE*              7.3                        30.4                      13.5                     3.8                         15.1
               ANTHRACENEO                1.1           J            7.3                       2.7          J           1.9           J             2.1            J
               CI-PHE?@_ANTHR             12                         27                        18.2                                  ND                           ND
               C2-PHEN-ANTHR              16.3                       35.4                      24.7                                  ND                           ND
               C3-PHEN-ANTHR                           ND                         ND                       ND                        ND                           ND
               C4-PHEN- ANTHR                          ND                         ND                       ND                        DID                          ND
               DIBENZOTHIO                1.2           J            2.4                       1.2          J           0.5           J             1.4            J
                CI-DIBEN                  2.8           J             4                        3.9                                   ND                           ND
                C2-DIBEN                  5.6                        9.1                       9.9                                   ND                           ND
                C3-DIBEN                  6.7                         7                        7.2                                   ND                           ND
               FLUORANTHENE               16                         42.5                      3.4                      0.7           J             2              J
        I-J     PYRENE*                   7.9                        26.3                      2.3                      0.6           J             1.5            J
        0 CI-FLUORAN-PYR                  8.3                        27.1                      10.2                                  ND                           ND
           BENaANTHRACENE                 1.1           J            11.4                      0.8          J           0.2           J             1.1            J
               CHRYSENE 0                 4                          18.7                      1.6          J           1.3           J             1.8            J
               Cl-CHRYSENES                            ND             5            J           9.9                                   ND                           ND
               C2-CHRYSENES                            ND            11.6                      3.4          J                        ND                           DID
               C3-CHRYSENES                            ND                         ND                       ND                        ND                           DID
               C4-CHRYSENES                            ND                         ND                       ND                        ND                           ND
               BENbFLUORAN                0.7           J            4.2                       0.3          J           0.4           J              I             J
               BENkFLUORAN                I             J            5.4                       0.3          J           0.5           J              I             J
               BENePYRENE 0               0.8           J            3.9                       0.6          J           0.9                         1.3            J
               BENaPYRENE *               0.7           J             2            J           0.6          J           0.8           J             0.6            J
               PERYLENE *                 1.2           J             2            J           2.1          J           1.7           J             4.8            J
               1123cdPYRENE               0.3           J            1.5                       0.5          J           0.3           J             0.4            J
               DBahANTHRA *               0.8           J            0.5           J           1.1          J           0.2           J             0.2            J
               BghtPERYLENE               o.5           J            1.6                       0.6          J           0.4                         0.4

               TOTAL PAH's                115.7                      468.3                     285.3                    35.3                        84.6
               (w/o PERYLENE)
               S&T Total PAHs             66.3                       184.8                     71                       31.4                        96.2






                                                           Mussel Watch Project Year 8 - Aromatics Data

                INVEST*:              LMSB                        CCNB                     ABLR                     MBAR                        SAPP
                  ID:           L Laguna Madre               Corpus Christi            Aransas Bay              Mesquite Bay              San Antonio Bay
                 SITE              South Bay                 Ingleside Cove              Long Reef               Ayres Reef                Mosquito Point
             LABSAMNO:                K7030                       K7024                    K7034                    K7032                       K7042
            SAMPLE TYPE:              SAMP                        SAMP                     SAMP                     SAMP                        SAMP
                UNIT:                 ng/g                        ng/g                     ng/g                     ng/g                        ng/g
            Analyte (Cont)            Cone        1313 QUAL       Cone      DB QUAL        Cone      DB QUAL        Cone       DB QUAL          Cone        DB QUAL


          2-MET1-IYLNAPH *              4             J           3.6            J          5.1                      3.5                         9.8            J
          I -METHYLSAPH 0               3.1           J           2.5           J           3.7                       3                          7.1

         2.6-DIMETI-INAPH               1.4           J           3.3                       3.7                      2.4           J             6.8

        2.3.5-TRIMETHNAPH               1.9           J           4.5                       3.2          J           0.8           J             6.3            J

          I -METHYLPHEN 0               2             J           9.6                       3.6                      0.5           J             2.1            J


         Surrogate Recoveries
               NAPI-1138:             64.6                        68.6                     59.2                     61.7                        66.3
               ACEND10:               67.1                        73.4                     59.5                     64.4                        74.3
               PHENDIO:               66.6                        81.2                     67.9                     72.6                        64.4
               CHRYD12,               69.1                        72.8                     71.6                     66.6                         55
               PERYD12:               65.5                        68.1                     52.7                      70                         50.2







                                                                    Mussel Watch Pro ect Year 8 - Aromatics Data
                                                                                             I

                           INVEST#:                   ESBD                             MBGP                              MBLR,                                    B
                               ID:              Espiritu Santo                 Matagorda Bay                      Matagorda Bay                     Matagorda Bay
                              SITE              Bill Day's Reef               Gallinipper Point                Lavaca River Mouth                  Carancahua Bay
                          LABSAMNO:                   K7044                            K7036                             K7038                             K7040
                        SAMPLE TYPE:                  SAMP                             SAMP                              SAMP                              SAMP
                              UNIT:                   ng/g                             ng/g                              ng/g                              ng/g
                         Analyte (Cont)               Conc       DB QUAL               Conc        DB QUAL               Conc          DB QUAL             Conc        DB QUALI

                        RECEIPT DATE:                 12/19/96                         12/19/96                          12/18/96                          12/19/96
                          QCBATCH:                    M1233                            M1233                             M1233                             M1233
                      F-X-f'RACMON DATE:              9/15/97                          9/15/97                           9/15/97                           9/15/97
                           METI-IOD:                  GCMS                             GCMS                              GCMS                              GCMS
                       ANALYSIS DATE:                 10/25/97                         10/25/97                          10/25/97                          10/25/97
                           METHOD:                    GCECD                            GCECD                             GCECD                             GCECD
                       ANALYSIS DATE:                 8/24/98                          8/24/98                           8/24/98                           8/24/98
                            MATRIX:                   TISSUE                           TISSUE                            TISSUE                            TISSUE
                           SUBMAT:
                            WETWT:                    15.14                            15.28                             15.3                              15.06
                            DRYWT:                    2.07                             2.2                               2.26                              2.19
                           ViTUNITS:                  GRAMS         DRY                GRAMS          DRY                GRAMS            DRY              GRAMS          DRY
                          PCTSOLIDS:                  13.600/6                         14.400/6                          14.800/6                          14.500,6
                         Lipid Weight:
        to               TOTAL LIPID:                 4.99                             5.53                              5.02                              9.78
                         LIPID UNITS:                 % DRY                            % DRY                             % DRY                             % DRY
                              VOL:
                          VOLUNITS:                   LITERS                           LITERS                            LITERS                            LITERS
                      Surrogate Recoveries
                              PAH's:
                            NAPHD8:                   64.6                             81.1                              66.5                              60r.8
                           ACENDIO:                   65.4                             77.1                              72                                70.3
                           PHENDIO:                   57.3                             67                                56.1                              57.8
                           CHRYD12:                   52                               53                                52.2                              48
                           PERYD12:                   47.1                             52.8                              45.3                              52.4


                       NA17ITITIALENE 0               10.8                             5.2                               4.5                               5.6
                      CI-NAPHTHALENES                 7.5                              6                                 8.1                               10.1
                      C2-NAPHTHALENES                                ND                                ND                                 ND               15.6
                      C3-NAPHTHALENES                                ND                18.9                                               ND               59.8
                      C4-NAPHTHALENES,                               ND                18                                                 ND               78.6
                          BIPHENYL *                  3.4                              2.8                               3.4                               2.4
                      ACENAPHTHYLENE                  2.3                              2.3                               1.1                               0.9
                      ACENAPHTHENE*                   4.6                              1.4                               2.5                               2.8
                          FLUORENE*                     2                              2.8             1                 2.4                               4.5
                        ,'I WT T If-%t1E- TZ-0
                                                                     Fv"                                                                  ND               9.9



                                                             m m m m m mm m m m m m @

                                                                Mussel Watch Project Year 8 - Aromatics Data

                         INVEST#:                  ESBD                           MBGP                            MBLR                              MBCB
                             ID-            Espiritu Santo                 Matagorda Bay                    Matagorda Bay                    Matagorda Bay
                            SITE             Bill Day's Reef              Gallinipper Point              Lavaca River Mouth                 Carancahua. Bay
                       LABSAMNO:                   K7044                          K7036                           K7038                             K7040
                       SAMPLE TYPE:                SAMP                           SAMP                            SAMP                              SAMP
                           UNIT-.                  ng/g                           ng/g                            ng/g                              ng/g
                       Analyte (Cont)              Conc      DB QUAL              Conc        DB QUAL             Conc          DB QUAL             Conc       DB QUAL


                       C2-FLUORENES,                             ND                              ND                                 ND              48.6
                       C3-FLUORENES                              ND                              ND                                 ND              92.5
                       PHENANTHRENE*               8.5                            10.3                            11.4                              18.6
                       ANTHRACENE*                 1.2            J               3.3             J               3.8                               3.5
                       Cl-PHEN-ANTHR               19                             28.9                            17.7                              27.8
                       C2-PHEN-ANTHR               23.4                           40.1                            24.4                              40.3
                       C3-PHEN-ANTHR                             ND                              ND                                 ND                             ND
                       C4-PHEN._ANTHR                            ND                              ND                                 ND                             ND
                       DIBENZOTHIO                 1.7            J               1.2             J                 I                J              1.7
                         Cl-DIBEN                  4.4                            4.6                             4.5                               5.8
                         C2-DIBEN                  10.9                           13                              9.2                               16.4
                         C3-DIBEN                  5.5                            12.9                            3.9                               9.6
                       FLUORANTHENE                8.4                            16.5                            23.5                              29.5
                         PYRENE*                   5.3                            12.6                            16.7                              19.7
                       CI-FLUORAN-PYR                            ND               20.9                            16.9                              17.1
                    BENaANTHRACENE                 1.4            J               4.7                             8.6                               5.6
                       CHRYSENE*                   2.6            J               9                               11.4                              11
                       CI-CHRYSENES                              ND                              ND                                 ND                             ND
                       C2-CHRYSENES                              ND                              ND                                 ND                             ND
                       C3-CHRYSENES                              ND                              ND                                 ND                             ND
                       C4-CHRYSENES                              ND                              ND                                 ND                             ND
                       BENbFLUORAN                  I             J               5.4                             7.5                               3
                       BENkFLUORAN                 0.9            J               5.1                              7                                2.8
                       BENePYRENE, 0               1.1            J               5.8                             7.7                               4.6
                       BENaPYRENE *                0.4            J               1.7                             3.3                               1.2
                       PERYLENE 0                  2.2            J               24.4                            3.8                               3.1
                       1123cdPYRENE                0.4            J               1.9                             3.1                               0.7
                       DBahANTHRA*                 0.3            J               0.7                             0.8                J              0.3             J
                       BghiPERYLENE                0.7            J               1.9                             3.2                               1.1             J

                       TOTAL PAH's                 127.5                          257.8                           207.3                             551.4
                       (w/o PERYLENE)
                       S&T Total PAHs (*)          68.7                           117                             118                               142.5






                                                             Mussel Watch Project Year 8 - Aromatics Data

                        INVEST#:                ESBD                         MBGP                           MBLR.                           MBCB
                            ID:           Espiritu Santo               Matagorda Bay                  Matagorda Bay                  Matagorda Bay
                           SITE            Bill Day's Reef            Gallinipper Point             Lavaca River Mouth              Carancahua Bay
                       LABSAMNO:                K7044                        K7036                          K7038                           K7040
                     SAMPLE TYPE:               SAMP                         SAMP                           SAMP                            SAMP
                          UNIT:                 ng/g                         ng/g                           ng/g                            ng/g
                      Analyte (Cont)            Conc       DB QUAL           Conc        DB QUAL            Conc         DB QUAL            Conc       DB QUAL


                    2-METHYLNAPH *              4.4            J             4.1             J               4.5             J              6.1
                    I-METHYLNAPH *              3.1            J             1.9             J               3.6                            4

                   2,6-DIME`f14NAPH             3.1            J             4.1                             2.3             J              5.8

                  2.3.5-TRIMETHNAPH             3.3            J             2.5             J               2               J              8.4

                    I -MBITMPHEN                2.7            J             3.3             J               1.9             J              5.9


                   Surrogate Recoveries
                        NAPHD8:                 64.6                         81.1                           66.5                            60.8
                        ACENDIO:                65.4                         77.1                            72                             70.3
                        PHENDIO:                57.3                         67                             56.1                            57.8
                        CHRYD12:                52                           53                             52.2                            48
                        PERYD12:                47.1                         52.8                           45.3                            52.4






                                                             Mussel Watch Project Year 8 - Aromatics Data

                            INVEST#:                 MBT?                          MBEM                       BRCL                        BRFS
                              ID:              Matagorda Bay                Matagorda Bay                Brazos River                Brazos River
                             SITE            Tres Palaclos Bay              East Matagorda               Cedar Lakes              Freeport SurfMde
                            LABSAMNO:                K7026                         K7028                      K7002                       K7000
                            SAMPLE TYPE:             SAMP                          SAMP                       SAMP                        SAMP
                             UNIT:                   ng/g                          ng/g                       ng/g                        ng/g
                            Analyte (Cont)           Cone        D13 QUAL          Cone      DB QUAL          Cone     DB QUAL,           Cone        D13 QUAL

                            RECEIPT DATE:            12/17/96                      12/17/96                   12/10196                    12/10/96
                            QCBATCH:                 M1232                         M1232                      M1232                       M1232
                      EXTRACMON DATE:                9/15/97                       9/15/97                    9/15/97                     9/15/97
                            METHOD:                  GCMS                          GCMS                       GCMS                        GCMS,
                            ANALYSIS DATE:           10/21/97                      10/21/97                   10/20/97                    10/20/97
                            METHOD:                  GCECD                         GCECD                      GCECD                       GCECD
                            ANALYSIS DATE:           7/31/98                       7/31/98                    7/30/98                     7/30/98
                            MATRIX                   TISSUE                        TISSUE                     TISSUE                      TISSUE
                            SUBMAT-
                            WETWT.                   15.36                         15.24                      15.13                       15.28
                            DRYW`r.-                 2.57                          2.73                       1.79                        2.69
                            W`rUNITS:                GRAMS          DRY            GRAMS        DRY           GRAMS       DRY             GRAMS         DRY
                            PCTSOLIDS:               16.70036                      17.900A                    11.800A                     17.60%
                            Upid Weight:
       V-4                  TOTAL LIPID:             8.2                           7.34                       3.85                        6.69
       Ul                   LIPID UNITS:             % DRY                         % DRY                      % DRY                       % DRY
                             VOL.
                            VOLUNITS:                IXIERS                        LITERS                     LITERS                      LITERS
                      Surrogate Recoveries
                             PAH's:
                            NAPHD8-                  68.9                          58.9                       53.7                        56.9
                            ACENDIO:                 73.4                          67.3                       62.8                        62.7
                            PHENDIO:                 72.7                          69.5                       68.8                        68
                            CHRYD12:                 75.1                          62.2                       66.8                        70.2
                            PERYD12:                 60.6                          62.4                       58.4                        56.8


                            NAPHTIMENE               4.6                           7.7                        7.4                         6.5
                      CI-NAPHTHALENES,               4.5             1             7.9                        10.6                        8.6
                      C2-NAPHTHALENES                                ND            8.6                        20.3                        24.9
                      C3-NAPHTHALENES                                ND            34.7                       63.4                        57.3
                      C4-NAPHTHALENES                                ND            67.8                       83.2                        71.7
                            BIPHENYL *               2.6             1             2.9            1           4.5          1              3.7
                      ACENAPHTHYLENE                 0.6             1             0.7            1           10.8                        26.1
                      ACENAPHTHENE0                  0.9             1              2             1           2.6          1              10
                            FLUORENE*                1.5             1             2.8            1            4           1              12.1
                            CI-FLUORENES                             ND            9.9                        15.9                        20






                                                             Mussel Watch Project Year 8 - Aromatics Data

                           INVEST#:                  MBTP                         MBEM                       BRCL                         BRFS
                              ID:             Matagorda Bay                 Matagorda Bay               Brazos River                 Brazos River
                             SITE            Tres Palaclos Bay              East Matagorda              Cedar Lakes               Freeport Surfslde
                         LABSAMNO:                   K7026                        K7028                      K7002                        K7000
                         SAMPLE TYPE:                SAMP                         SAMP                       SAMP                         SAMP
                             UNIT:                   ng/g                         ng/g                       ng/g                         ng/g
                         Analyte (Cont)              Cone        DB QUAL          Cone       DB QUAL         Cone      DB QUAL            Cone       DB QUAL

                         C2-FLUORENES                               ND            72.9                       54.2                         85.3
                         C3-FLUORENES                               ND            172.9                      126                          158.6
                         PHENANTHRENE*               6.7                          8.3                        22.7                         49
                         ANTHRACENE0                 4.2                          4.2                        7.2                          23
                         Cl-PHEN-ANTHR               20.6                         46.2                       62.4                         74.2
                         C2-PHEN-ANTHR               27.7                         124.7                      137.3                        123.9
                         C3-PHEN-ANTHR                              ND            126.7                      146.8                        171.6
                         C4-PHEN-ANTHR                              ND            42.2                       63.9                         127.4
                         DIBENZOTHIO                 0.8             J            1.4                        2.7                          4.4
                           CI-DIBEN                  2.9                          20.3                       11.6                         16.5
                           C2-DIBEN                  9.5                          108.7                      48.6                         50.7
                           C3-DIBEN                   9                           100.2                      47.1                         50.4
                         FLUORANTHENE*               4.2                          45.8                       36.9                         189.6
                           PYRENE*                   3.5                          34.2                       38.6                         141.7
                         CI-FLUORAN   PYR.                          ND            21.3                       36.3                         104.1
       0)            BENaANTHRACENE                  0.9             J             5                          9                           49.4
                         CHRYSENEO                    3                           7.4                        20.6                         75.6
                         CI-CHRYSENES                               ND            4.1            J           12.1                         16.6
                         C2-CHRYSENES                               ND            12.5                       10.9                         8.9
                         C3-CHRYSENES                               ND                          ND                        ND                             ND
                         C4-CHRYSENES                               ND                          ND                        ND                             ND
                         BENbFLUORAN                 0.7             J            1.4            J           4.2                          14.2
                         BENkFLUORAN                  1              J            1.8            J           5.5                          18.5
                         BENePYRENE 0                1.4                          1.8                        4.9                          15.1
                         BENaPYRENE*                  I              J            1.2            J           1.5           J              2.9
                         PERYLEENE0                  4.1                          2.6                        4.9
                         1123cdPYRENE                0.3             J            0.2            J           0.9           J              1.6
                         DBahANTHRA *                0.4             J            0.1            J           0.4           J              1.1            J
                         B&PERYLENE                  0.5             J            0.9            J           1.7                          2.5

                         TOTAL PAH's                 112.9                        1111.3                     1136.6                       1817.2
                         (w/o PERYLENE)
                         S&T Total PAHs N            51.2                         150.2                      204.4                        627.7






                                                           Mussel Watch Project Year 8 - Aromatics Data

                          INVEST#:                 MBTP                        MBEM                     BRCL                       BRFS
                             ID:             Matagorda Bay               Matagorda Bay              Brazos River              Brazos River
                            SITE            Tres Palaclos Bay            East Matagorda             Cedar Lakes             Freeport Surfstde
                         LABSAMNO:                 K7026                       K7028                    K7002                     K7000
                       SAMPLE'rYPE:                SAMP                        SAMP                     SAMP                       SAMP
                            UNIT:                  ng/g                        ng/g                     ng/g                       ng/g
                        Analyte (Cont)             Conc       DB QUAL          Conc      DB QUAL        Conc     DB QUAL           Conc       DB gUALI


                      2-METHYLNAPH *               2.5            J             5                       5.7          J              4
                      1-METHYLNAPH 0                2             J             3                       4.9                        4.6


                     2.6-DIML-MNAPH                2.3            J            2.8           J          4.7          J             7.3


                    2,3.5-TRIMETHNAPH               1             J            4.3                      10.7                        11.5


                      I-METHYLPHEN *               4.5                         9.3                      13.2                        14.3



                     Surrogate Recoveries
                          NAPHD8-                  68.9                        58.9                     53.7                       56.9
                          ACENDIO:                 73.4                        67.3                     62.8                        62.7
                          PHENDIO:                 72.7                        69.5                     68.8                       68
       -4                 CHRYD12:                 75.1                        62.2                     66.8                        70.2
                          PERYD12:                 60.6                        62.4                     58.4                        56.8






                                                                    Mussel Watch Project Year 8 - Aromatics Data

                   INVEST#:                   GBCR                          GBOB                          GBTD                         GBYC                          GBSC
                      ID:              Galveston Bay                  Galveston Bay                Galveston Bay                Galveston Bay                 Galveston Bay
                     SITE             Confederate Reef                  Offats Bayo                 Todd's Dump                   Yacht Club                  Ship Channel
                 LABSAMNO:                    K7006                         K7010                         K7012                        K7004                         K7008
               SAMPLE TYPE:                   SAMP                          SAMP                          SAMP                         SAMP                          SAMP
                     UNIT:                    ng/g                          ng/g                          ng/g                         ng/g                          ng/g
               Analyte (Cont)                 Conc        D13 QUAL          Conc       DB QUAL            Conc      DB QUAL            Conc       DI3 QUAL           Conc      D13 QUALI

              RECEIPT DATE:                   12/11/96                      12/11/96                      12/12/96                     12/11/96                      12/11/96
                  QCBATCH:                    M1232                         M1232                         M1232                        M1232                         M1232
            EXTRACTION DATE:                  9/15/97                       9/15/97                       9/15/97                      9/15/97                       9/15/97
                   MErHOD:                    GCMS                          GCMS                          GCMS                         GCMS                          GCMS
              ANALYSIS DATE:                  10/20/97                      10/20/97                      10/21/97                     10/20/97                      10/20/97
                   METHOD:                    GCECD                         GCECD                         GCECD                        GCECD                         GCECD
              ANALYSIS DATE:                  7/30/98                       7/31/98                       7/31/98                      7/30/98                       7/31/98
                    MATRIX:                   TISSUE                        TISSUE                        TISSUE                       TISSUE                        TISSUE
                   SUBMAT:
                    WETW17:                   15.02                         15.1                          15.46                        15.69                         15
                    DRYWT`-.                  1.97                          2.77                          2.59                         2.85                          3.13
                   WTUNITS:                   GRAMS          DRY            GRAMS         DRY             GRAMS        DRY             GRAMS         DRY             GRAMS        DRY
                  PCTSOLIDS:                  13.100/6                      18.400/6                      16.70%                       18.100/6                      20.800/6
                I.Apid Weight:
                TOTAL LIPID:                  5.39                          8.38                          8.82                         8.38                          11.56
         00     LIPID UNITS:                  % DRY                         % DRY                         % DRY                        % DRY                         % DRY
                     VOL:
                  VOLUNITS:                   LITERS                        LITERS                        LITERS                       LITERS                        LITERS
            Surrogate Recoveries
                     PAH's:
                   NAPHD8:                    57.5                          57.1                          54.6                         52.6                          51.7
                   ACENDIO:                   62.4                          65.4                          69.9                         58.2                          41.1
                   PHENDIO:                   68.5                          70.8                          70.6                         69.6                          49.7
                   CHRYD12:                   68.3                          73.3                          65.1                         70.3                          51.2
                   PERYD12:                   49                            62.5                          59.1                         54.9                          49.3


               NAPIrriMENE                    4.4                            6.2                          8.6                          6.4                           7.8
             CI-NAPHTHALENES                   6               J             9.2                          17.4                         6.6                           11.3
             C2-NAPHTHALENES                  11.1                           9.4                          51                           11.8                          32.4
             C3-NAPHTHALENES                  31.7                          24.1                          143.8                        47.5                          150.1
             C4-NAPHTHALENES                  35.6                          29.7                          153.3                        94.8                          337.6
                 BTPT4F,?V", 0                .1. 1            J              .14           J             q: R             T           R. I            J             q. 7
              ACENAPHTHYLENE                  6.3                            3.4            J             3.7             J            3.7                           7.6
              ACENAPHTHENE*                   10.8                           7.8                          3.1             J            2.8             J             5.7
                 FLUORENE *                   5.6              J             7.3                          6.2                          3.7             J             8.9
               C 1 -FLUORENES                 i 1.7            J             8.5                          22.1                         25                            102.2






                                                                Mussel Watch Project Year 8 - Aromatics Data

                 INVEST#:                  GBCR                          GBOB                        GBTD                         GBYC                        GBSC
                    ID:              Galveston Bay                 Galveston Bay              Galveston Bay                Galveston Bay               Galveston Bay
                   SITE            Confederate Reef                 Offats Bayo                Todd's Dump                  Yacht Club                  Ship Channel
               1ABSAMNO:                   K7006                         K7010                       K7012                        K7004                       K7008
               S"PLE TYPE:                 SAMP                          SAMP                        SAMP                         SAMP                        SAMP
                  UNrr-                    ng/g                          ng/g                        ng/g                         ng/g                        ng/g
                 alyte (Cont)              Cone        DB; QUAL          Conc      DB QUAL           Conc      DB, QUAL           Conc      1313 QUAL         Conc      DB QUAL

               C2-FLUORENES                47.4                          68.1                        104.3                        101.5                       344.9
               C3-FLUORENES                103.4                         132.7                       159.8                        202.3                       644.9
               PHENANTIMENE0               22.7                          37.4                        22.6                         12                          35.7
               ANrHRACENE*                 15.6                          15                          9.6                          10.6                        23.3
               CI-PHEN-ANTHR               38.7                          43.6                        94.6                         42.7                        156.8
               C2-PHEN-ANTHR               78.9                          86.1                        156.2                        127.3                       487.8
               C3-PHEN-ANTHR               114.7                         162.2                       139.9                        224                         1000.3
               C4-PHEN-ANTHR               42.6                          142                         86.5                         173                         1063.7
               DIBENZOTI-110               2.5                           2.9                         3.4                          2.5                         9.4
                 CI-DIBEN                   8                            8.3                         19.6                         12.6                        56.3
                 C2-DIBEN                  30.5                          38.1                        56.7                         46.1                        176.4
                 C3-DIBEN                  24.8                          59.3                        47.3                         60.8                        366.2
               FLUORANTHENEO               244.2                         164.8                       29.6                         43.7                        186.1
                 PYRENE*                   123                           105.8                       25.3                         61.3                        448.8
               CI-FLUORAN  -PYR            67.6                          84.4                        25.6                         62.4                        931
       (0 BENaANTHRACENE                   24.4                          37.6                        4.8                          13.3                        54.3
               CHRYSENE 0                  37.8                          81.4                        10.9                         31.2                        238.5
               CI-CHRYSENES                10.9                          32.2                        6.6                          24.8                        437.6
               C2-CHRYSENES                10.9                          23                          10.4                         29.8                        477.7
               C3-CHRYSENES                               ND             3.3            J                         ND                           ND             87.7
               C4-CHRYSENES                               ND             4.5            J                          ND                          ND             13.2
               BENbFLUORAN                 7.1                           26.4                        3                            5                           54.7
               BENkFLUORAN                 9.3                           34.5                        3.8                          6.5                         71.5
               BENePYRENE                  7.3                           30.2                        4.1                          10.8                        138.4
               BENaPYRENE                  2.4             J             7.4                          1            J              1.6           J             26.3
               PERYLENE*                   2.9                           3.7                         2.3                          2.8                         47
               1123cdPYRENE                1.6                           7.2                         0.6           J              0.9                         7.3
               DBahANTHRA 0                0.5             J             2.2                         0.6           J              0.9           J             9.4
               BghiPERYLENE                2.9                           9.6                         1.6                          2.1                         20.4

               TOTAL PAH's                 1205.8                        1558.6                      1441.2                       1514.8                      8235.9
               (w/o PERYLENE)
               S&T Total PAHs (0)          528.6                         534.4                       214                          234.5                       1344.3






                                                               Mussel Watch Project Year 8 - Aromatics Data

                 INVEST#:                 GBCR                         GBOB                       GBTD                        GBYC                       GBSC
                    ID:             Galveston Bay                Galveston Bay              Galveston Bay               Galveston Bay              Galveston Bay
                   S]TE            Confederate Reef                Offats Bayo               Todd's Dump                 Yacht Club                 Ship Channel
               LABSANINO:                 K7006                        K7010                      K7012                       K7004                      K7008
             SAMPLE TYPE:                 SAMP                         SAMP                       SAMP                        SAMP                       SAMP
                  UNIT:                   ng/g                         ng/g                       ng/g                        ng/g                       ng/g
              Analyte (Cont)              Conc        DB QUAL          Conc      DB QUAL          Conc      DB QUAL           Conc      DB QUAL          Conc       DB QUAL


            2-MEITIYLNAPH *               3.2             J            5.4                        11.1                        3.7                        7.3
            1 -METHYLNAPH *               2.8             J            3.8                        6.3                         2.9                         4


           2.6-DIMETHNAPH                 3.2             J            4.8                        22.5                        4.7                        16.4


          2,3.5-TRIMETHNAPH               5.5                          3.4           J            26.2                        10.1                       47.2


            I -METHYLPHEN                 9.3                          7.4                        15.6                        9.2                        35.5



           Surrogate Recoveries
                 NAPHD8:                  57.5                         57.1                       54.6                        52.6                       51.7
        N        ACENDIO:                 62.4                         65.4                       69.9                        58.2                       41.1
        0        PHENDIO:                 68.5                         70.8                       70.6                        69.6                       49.7
                 CHRYD12:                 68.3                         73.3                       65.1                        70.3                       51.2
                 PERYD12:                 49                           62.5                       59.1                        54.9                       49.3






                                                             Mussel Watch "ect Year 8 - Aromatics Data
                             INVEST#:               GBHR                       SLBB                         CLSJ                       ZUC
                               ID*            Galveston Bay                Sabine Lake               Calcasieu Lake              Calcasieu Lake
                              SITE             Hanna Reef                Blue Buck Point             St. Johns Island             Lake Charles
                             LABSAMNO:              K7014                      K7016                        K7020                      K7018
                             SAMPLE TYPE:           SAMP                       SAMP                         SAMP                       SAMP
                              UNIT.                 ng/g                       ng/g                         ng/9                       ng/g
                             Analyte (Cont)         Cone      DB QUAL          Cone       DB QUAL           Cone      DB QUAL          Cone       DB QUAL

                             RECEIPT DATE:          12/12/96                   12/12/96                     12/13/96                   12/12/96
                             QCBATCH:               M1232                      M1232                        M1232                      M1232
                       EXTRACTION DATE:             9/15/97                    9/15/97                      9/15/97                    9/15/97
                             METHOD:                GCMS                       GCMS                         GCMS                       GCMS
                             ANALYSIS DATE:         10/21/97                   10/21/97                     10/21/97                   10/21/97
                             METHOD:                GCECD                      GCECD                        GCECD                      GCECD
                             ANALYSIS DA7E:         7/31/98                    7/31/98                      7/31/98                    7/31/98
                             MATRIX:                TISSUE                     TISSUE                       TISSUE                     TISSUE
                             SUBMAT-
                             WE,1wr:                15.39                      15.27                        15.06                      15.09
                             DRYWT:                 2.4                        2.68                         1.93                       3.07
                             WTUNITS:               GRAMS        DRY           GRAMS        DRY             GRAMS        DRY           GRAMS        DRY
                             PCTSOLIDS:             15.60%                     17.600A                      12.80%                     20.40%
                             lApid Weight:
                             TOTAL LIPID-           6.64                       8.03                         5.65                       10-56
                             LIPID UNITS:           % DRY                      % DRY                        % DRY                      % DRY
                              VOL:
                             VOLUNITS:              LITERS                     LnERS                        LrMRS                      LTMRS
                       Surrogate Recoveries
                              PAH's:
                             NAPHD8:                54.9                       52.8                         58.9                       37.9
                             ACENDIO:               63. 1                      60.6                         65.1                       41.8
                             PHEND10:               70.1                       64.4                         69.2                       44.3
                             CHRYD12:               65.2                       65.5                         70                         49.9
                             PERYD12:               63.1                       62.1                         54.5                       41.8


                             NAPf f IIMENE          8.6                        8.3                          9.2                        8.7
                       Cl-NAPHTHALENES              7.5                        10.4                         9.2                        27.6
                       C2-NAPHTHALENES              11.7                       21.8                         17.9                       105
                       C3-NAPHTHALENES              40.9                       82.4                         45.5                       314.9
                       C4-NAPHTHALENES              53.2                       98.5                         47.5                       398.7
                             BtPHENYL 0             2.6           J            3.4            j             3.7                        19.2
                       ACENAPHTHYLENE               1.7           J            6.4                          0.7                        8.9
                       ACENAPHTHENE*                3-1           J            2.1            J             1.9           J            15.4
                             FLUORENE 0             4.4           J            5.4                          3.6           J            27.7
                             CI-FLUORENES           12.6                       15.6                         8.7           1            73.9






                                                              Mussel Watch Project Year 8 - Aromatics Data

                            INVEST#:                 GBHR                        SLBB                         CLSJ                         CLLC
                                ID:            Galveston Bay                Sabine Lake                Calcasieu Lake               Calcasieu Lake
                               SITE             Hanna Reef                Blue Buck Point              St. Johns Island              Lake Charles
                           LABSAMNO:                 K7014                       K7016                        K7020                        K7018
                           SAMPLE TYPE:              SAMP                        SAMP                         SAMP                         SAMP
                              UNIT:                  ng/g                        ng/g                         ng/g                         ng/g
                           Analyte (Cont)            Conc      DB QUAL           Conc      DB QUAL            Conc       DB QUAL           Conc      DB QUAL

                           C2-FIAJORENES             51.3                        96.4                         39.6                         318.3
                           C3-FLUORENES              116.8                       174.3                        100.6                        554.1
                           PHENANTHRENE*             14.6                        18.8                         19.3                         121.6
                           ANTHRACENE *              7.2                         10.2                         1.2            J             36.7
                           CI-PHEN-ANTHR             38.6                        74.1                         34.2                         294.5
                           C2-PHEN-ANTHR             61.9                        132.9                        52.3                         550.8
                           C3-PHEN-ANTHR             93.7                        206.2                                      ND             674.8
                           C4-PHEN-ANTHR             37.1                        173                                        ND             507.9
                           DIBENZOTH10               1.7                         3.3                          1.4            J             11.8
                            CI-DIBEN                 8.2                         16.7                         7.1                          65
                            C2-DIBEN                 25.8                        55.9                         20.1                         214.4
                            C3-DIBEN                 19.4                        52.7                         18.1                         262
                           F'LUORANrHENE*            65.5                        31.2                         13.1                         297
                            PYRENE*                  46.1                        38.6                         10.6                         362.5
        t1a                Cl-FLUORAN-PYR            28                          47.8                         16                           305.5
                       BENaANTHRACENE                10.8                        8.9                          165.6                        48.4
                           CHRYSENEO                 9.4                         15.4                         423.9                        103.1
                           CI-CHRYSENES              5.7           J             17.5                         342                          85.6
                           C2-CHRYSENES              13.4                        20.6                         463.1                        64.1
                           C3-CHRYSENES                           ND                           ND                           ND             12.6
                           C4-CHRYSENES                           ND                           ND                           ND              5            J
                           BENbFLUORAN               2.3           J             3.2                          113.7                        13.3
                           BENkFLUORAN                 3                         4.2                          148.4                        17.4
                           BENePYRENE *              2.9                          7                           155.8                        28.1
                           BENaPYRENE 0              0.7           J             1.1            J             166.7                        6.2
                                                                                                                                           in In
                           PERYLENE                  3.1                         6.7                          2.5            J             JLU.U
                           I123cdPYRENE                1                         0.8                          31.1                         1.8
                           DBahANTHRA *              0.6           J             0.6            J             30.3                         1.8
                           BghIPERYLENE              0.8           J             1.5                          54.6                         3.6


                           TOTAL PAH's               812.9                       1466.7                       2576.7                       5967.5
                           (w/o PERYLENE)
                           S&T Total PAHs            207.6                       205                          1038.3                       1370.1





                                                           Mussel Watch Project Year 8 - Aromatics Data

                                                  GBHR                        SLBB                        CLSJ                       CLLC
                              ID:            Galveston Bay               Sabine Lake                Calcasieu Lake              Calcasieu Lake
                             SI'm             Hanna Reef               Blue Buck Point             St. Johns Island              Lake Charles
                         LABSAMNO:                K7014                       K7016                       K7020                      K7018
                        SAMPLE TYPE:              SAMP                        SAMP                        SAMP                       SAMP
                             UNrr:                ng/g                        ng/g                        ng/g                       ng/g
                        Analyte (Cont)            Conc      DB QUAL           Conc      DB QUAL           Conc       DB QUAL         Conc       1313 QUALI


                      2-METHYLNAPH *               4.6                        6.1                         5.6                        16.5
                       1-METHYLNAPH *              2.9          J             4.3                         3.6            J           11.2


                      2.6-DIMEMNAPH                5.6                        8.6                         5.7                        44.8


                    2,3,5-IMMETHNAPH               7.8                        17.2                        9.3                        69.9


                       I-METHYLPHEN 0              7.2                        11.5                        6.8                        131.8



                     Surrogate Recoveries
                            NAPHD8:               54.9                        52.8                        58.9                       37.9           Q
                           ACENDIO:               63.1                        60.6                        65.1                       41.8
                           PHENDIO:               70.1                        64.4                        69.2                       44.3
                           CHRYD12:               65.2                        65.5                        70                         49.9
                           PERYD12:               63.1                        62.1                        54.5                       41.8






                                                                   Mussel Watch Project Year 8 - Aromatics Data

                             INVEST#:                      JHJH                              VBSP                           ABOB                          CLCL
                                ID:             Joseph Harbor Bayou                   Vennillion Bay                 Atchafalaya Bay                Cafflou Lake
                               SITE               Joseph Harbor Bay                   Southwest Pass                  Oyster Bayou                  Caillou Lake
                             LABSAMNO:                     K7022                             K7046                          K7056                         K7058
                             SAMPLE TYPE:                  &AIMP,                            SAMP                           SAMP                          SAMP
                               UNIT:                       ng/g                              ng/g                           ng/g                          ng/g
                             Analyte (Cont)                Cone           DB QUAL            Cone       DB QUAL             Cone        DB QUAL           Cone      DB QUALI

                             RECEIPT DATE:                 12/13/96                          1/7/97                         1/8/97                        1/8/97
                             QCBATCH:                      M1232                             M1233                          M1233                         M1233
                       EXTRACTION DATE:                    9/15/97                           11/12/97                       9/15/97                       9/15/97
                             METHOD:                       GCMS                              Gems                           GCMS                          GCMS,
                             ANALYSIS DATE:                10121/97                          12/24/97                       10/26/97                      10/26/97
                             METHOD:                       GCECD                             GCECD                          GCECD                         GCECD
                             ANALYSIS DATE:                7/31/98                           8/24/98                        8/25/98                       8/25/98
                             MATRIX:                       TISSUE                            TISSUE                         TISSUE                        TISSUE
                             SUBMAT-
                             WEIW17:                       15,02                             15.08                          15.04                         15.24
                             DRYW17:                       2.01                              1.78                           2.3                           2.46
                             Vn'UNITS:                     GRAMS             DRY             GRAMS         DRY              GRAMS           DRY           GRAMS         DRY
                             PCTSOLIDS:                    13.409/6                          11.800/0                       15.300/6                      16.200/6
                             lAptd Weight:
         t..)                TOTAL IAPID:                  7.58                              11.01                          12.22                         10.66
                             LIPID, UNITS:                 % DRY                             % DRY                          % DRY                         % DRY
                               VOL:
                             VOLUNITS:                     LITERS                            LITERS                         LITERS                        LITERS
                       Surrogate Recoveries
                              PAH's:
                             NAPHD8:                       55.7                              58.4                           62.4                          67.8
                             ACENDIO:                      62.3                              57                             69.4                          82.5
                             PHENDIO:                      62.2                              70.7                           60.7                          72
                             CHRYD12:                      60.5                              69.1                           51.9                          59
                             PERYD12:                      46.7                              60.6                           45.9                          103.8

                             NAPHTHALENE                   10.4                              15.6                           10.5                          11
                       CI-NAPHTHALENES                     11.3                              17.2                           8.4                           7.9
                       C2-NAPHTHALENES                     16                                20                                             ND                          ND
                       C3-NAPHTHALENES,                    39.1                              23,3                                           ND                          ND
                       C4-NAPHTHALENES                     33.4                              37.3                                           ND                          ND
                             B)PHENYL                      3.7                J              fi..13                                                       7.9.
                       ACENAPHTHYLENE                      3.1                J               2              J              1.2              J            4.7
                       ACENAPHTHENE*                       3.5                J               3              J              2.1              J            31.9
                             FLUORENEO                     7,4                               7.2                            3.5              J            9.8
                             C1-F1:U0RENES                 9,1                i              13.9                                           ND                          ND

                             M M M M                             = = =                         M         M = M @                                                      MUMMM






                                                              Mussel Watch Project Year 8 - Aromatics Data

                          INVEST#:                    JHJH                            VBSP                         ABOB                        CLCL
                             ID:.           Joseph Harbor Bayou                Verndllion Bay               Atchafalaya Bay               Cafflou Lake
                             ITE             Joseph Harbor Bay                 Southwest Pass                Oyster Bayou                 Calllou. Lake
                        LABSAMNO:                     K7022                           K7046                        K7056                       K7058
                        SAMPLE TYPE:                  SAMP                            SAMP                         SAMP                        SAMP
                            LTW.                      ng/g                            ng/g                         ng/g                        ng/g
                        Analyte (Cont)                Conc          DB QUAL           Conc      DB QUAL            Conc       DB QUAL          Conc      DB QUALI

                        C2-FLUORENES                  34.6                            56.4                                        ND                        ND
                        C3-FLUORENES                  83.8                            67                                          ND                        ND
                        PHENANTURENE                  25                              19.8                         8.3                         4.8
                        ANTHRACENE*                   5.5                               3            J             3.2             J           5.3
                        CI-PHEN@ANTHR                 24.5                            21.3                         26.2                        19.9
                        C2-PHEN-ANTHR                 32                              44                           44.7                        46
                        C3-PHEN-ANTHR                                  ND             82.6                                        ND                        ND
                        C4-PHEN@ANTHR                                  ND             71                                          ND                        ND
                        DIBENZOTHIO                   1.3               J             1.5            J             0.8             J           0.2           J
                          Cl.-DIBEN                   3.8                             6.4                          4.7                                      ND
                          C2-DIBEN                    11.1                            13.9                         13.6                        10.2
                          C3-DIBEN                    8.2                             14.5                         13.5                        9.4
                        FUJORANTHENE                  23.8                            15.5                         9.8                         0.5           J
                          PYRENE*                     18                              20.8                         8.4                         0.8           J
                        CI-FLUORAN PYR                15.6                            22.9                         16.1                                     ND
                    BENaANTHRACENE                    2.3                             1.8                          2.6                         1.5
                        CHRYSENE*                     3.2               J             8.1                          4.2                         2.4           J
                        Cl-CHRYSENES                                   ND             4.7            J                            ND                        ND
                        C2-CHRYSENES                                   ND             9.1                                         ND                        ND
                        C3-CHRYSENES                                   ND                           ND                            ND                        ND
                        C4-CHRYSENES                                   ND                           ND                            ND                        ND
                        BENbF'LUORAN                  0.7               J             1.1            J             1.2             J            I            J
                        BENkFLUORAN                   0.9               J             1.1            J             1.1             J           0.9           J
                        BENePYRENE *                  1.2               J             2.3                          1.7                         1.4
                        BENaPYRENE*                   0.6               J             1.2            J             0.8             J           0.4
                        PERYLENE *                    5.5                             6.4                          10.6                        3.8
                        1123cdPYRENE                  0.4               J             0.7            J             0.8             J           0.4           J
                        DBahANTFIRA 0                 0.2               J             2.1            J             0.4             J           0.1           J
                        BghIPERYLENE                  0.4               J             1.1            J             0.7             J           0.7           J


                        TOTAL PAH's                   433.9                           639.6                        191.1                       178.3
                        (w/o PERYLENE)
                        S&T Total PAHs (*)            140                             146.2                        88.6                        107.9






                                                            Mussel Watch Project Year 8 - Aromatics Data

                          INVEST#:                  JHJH                           VBSP                       ABOB                       CLCL
                             ID:           Joseph Harbor Bayou               Vennfillon Bay             Atchafalaya Bay             CallIou Lake
                            SITE            Joseph Harbor Bay               Southwest Pass               Oyster Bayou               Caillou Lake
                        LABSAMNO:                   K7022                          K7046                      K7056                      K7058'
                       SAMPLE TYPE:                 SAMP                           SAMP                       SAMP                       SAMP
                           UNIT:                    ng/g                           ng/g                       ng/g                       ng/g
                       Analyte (Cont)               Conc          DB QUAL          Conc      DB QUAL          Conc       DB QUAL         Conc     D13 QUALI


                     2-MEITrILNAPH *                 7                             8.9                        4.8                        4.5
                     I-METHYLNAPH *                 4.3                            8.3                        3.7                        3.5


                    2,6-DIMETHNAPH                  6.4                            6.4                         4                         5.5


                   2.3.5-TRIMETHNAPH                8.3                            4.2           J            2.3            J           11.8


                     I-ME11ffLPHEN *                3.8               J            5.3                        5.1                        1.7          J



                    Surrogate Recoveries
                          NAPHD8:                   55.7                           58.4                       62.4                       67.8
                          ACENDIO:                  62.3                           57                         69.4                       82.5
        W                 PHENDIO:                  62.2                           70.7                       60.7                       72
        0)                CHRYD12:                  60.5                           69.1                       51.9                       59
                          PERYD12:                  46.7                           60.6                       45.9                       103.8






                                                                 Mussel Watch Project Year 8 - Aromatics Data

                             INVEST#:                  TBLB                           TBLF                            BBSD                           BBMB
                                ID:             Terrebonne Bay                Terrebonne Bay                   Barataria Bay                  Barataria Bay
                               SITE                Lake Barre                   Lake Felicity                Bayou Saint Denis                 Middle Bank
                             LABSAMNO:                 K7052                          K7054                           K7048                          K7050
                             SAMPLETYPE:               SAMP                           SAMP                            SAMP                           SAMP
                               UNIT:                   ng/g                           ng/g                            ng/g                           ng/g
                             Analyte (Cont)            Conc        DB QUAL,           Conc       DB QUAL              Conc        DB QUAL            Conc      DB QUAL

                             RECEIPT DATE:             1/8/97                         1/8/97                          1/7/97                         1/7/97
                             QCBATCH:                  M1233                          M1233                           M1233                          M1233
                       EXTRACTION DATE:                9/15/97                        9/15/97                         9/15/97                        9/15/97
                             METHOD:                   GCMS                           GCMS                            GCMS                           GCMS
                             ANALYSIS DATE:            10/25/97                       10/26/97                        10/25/97                       10/25/97
                             METHOD:                   GCECD                          GCECD                           GCECD                          GCECD
                             ANALYSIS DATE:            8/25/98                        8/25/98                         8/25/98                        8/25/98
                             MATRIX:                   TISSUE                         TISSUE                          TISSUE                         TISSUE
                             SUBMAT:
                             WETWr:                    15.1                           15.09                           15.2                           15.47
                             DRYWT-                    2.2                            3.16                            2.66                           2.71
                             WTUNITS:                  GRAMS          DRY             GRAMS         DRY               GRAMS          DRY             GRAMS        DRY
                             PCTSOLIDS-                14. FOA                        20.90%                          17.500/6                       17.50%
                             Lipid Weight:
                             TOTAL LIPID:              8.14                           8.8                             11.77                          8.65
                             LIPID, UNITS:             % DRY                          % DRY                           % DRY                          % DRY
                               VOL:
                             VOLUNrIS:                 LITERS                         LITERS                          LITERS                         LITERS
                       Surrogate Recoveries
                               PAH's:
                             NAPHD8:                   69.7                           59.7                            64.6                           66.6
                             ACENDIO:                  77.2                           74.7                            59.8                           73.6
                             PHENDIO:                  64.9                           61.1                            59.8                           60.9
                             CHRYD12:                  58.3                           60.2                            52.6                           59.6
                             PERYD12:                  46.7                           48.8                            43.5                           41.9


                             NAPHTHALENE               11.2                           13.9                            6.1                            12.1
                       CI-NAPHTHALENES                 9.3                             17                             5.2              J             32.4
                       C2-NAPHTHALENES                                ND              23.8                                            ND             23.6
                       C3-NAPHTHALENES                                ND              38.4                            17.9                           38.9
                       C4-NAPHTHALENES                                ND              27.1                            16.9                           45.6
                             BIPHENYL 0                2.5             J                6                             3.4              J             0.9            J
                       ACENAPHTHYLENE                  1.6             J              3.2                             0.6              J             0.7
                       ACENAPHTHENE*                   0.6             J              34.9                            1.8              J             40.3
                             FLUORENE *                1.7             J              37.6                            2.6              J              I
                             CI-FLUORENES                             ND               19                             9.9                            25.7






                                                               Mussel Watch Project Year 8 - Aromatics Data

                           INVEST#:                   TBLB                        TBLF                          BBSD                          BBMB
                               ID:            Terrebonne Bay               Terrebonne Bay                 Barataria Bay                 Barataria Bay
                              SITE              Lake Barre                   Lake Felicity              Bayou Saint Denis                Middle Bank
                          1ABSAMNO:                   K7052                       K7054                         K7048                         K7050
                          SAMPLE TYPE:                SAMP                        SAMP                          SAMP                          SAMP
                             UNIT.                    ng/g                        ng/g                          ng/g                          ng/g
                          Analyte (Cont)              Cone      DB QUAL           Cone       DB QUAL            Cone         DB QUAL          Cone      DB QUAL

                          C2-FLUORENES,                            ND             37.5                                          ND            53.1
                          C3-FLUORENES                             ND             64.5                                          ND            83.5
                          PHENANrHRENE*               5                           208.6                         5.3                           157.7
                          ANTHRACENE*                 2.5           J             61.5                          2.2              J            68
                          CI-PHEN-ANTHR               17                          84.9                          22.3                          78.6
                          C2-PHEN-ANTHR               22.7                        69.7                          25.1                          98.4
                          C3-PHEN-ANTHR                            ND                           ND                              ND            100.8
                          C4-PHEN-ANTHR                            ND                           ND                              ND            61.2
                          DIBENZOTHIO                 1             J             9.2                            1               J            9.2
                           CI-DIBEN                                ND             9.4                           3.8                           12.7
                           C2-DIBEN                   8.4                         13.9                           9                            40
                           C3-DIBEN                   9.6                         8.6                                           ND            40.6
                          FLUORANTHENEO               5                           294.5                         2.7                           285
                           PYRENE 0                   4.5                         170.7                         3.3                           150.5
        ba                CI-FLUORAN-PYR              10                          148.6                                         ND            165.9
        00            BENaANTHRACENE                  1.2           J             105.8                         0.9              J            78.3
                          CHRYSENE 0                  2.5           J             79.2                          1.7              J            91.7
                          CI-CHRYSENES,                            ND             25                                            ND            18.3
                          C2-CHRYSENES                             ND             11.3                                          ND            8.7
                          C3-CHRYSENES                             ND                           ND                              ND                          ND
                          C4-CHRYSENES                             ND                           ND                              ND                          ND
                          BENbFLUORAN                 0.8           J             22.1                          0.5              J            15.7
                          BENkFLUORAN                 0.8           J             22.6                          0.4              J            14.7
                          BENePYRENE 0                1.2                         15.7                           1                            16.7
                          BENaPYRENE 0                0.2           J             6.8                           0.1              J              3
                          PERYLENE 0                  8.9                         10.1                          2.1              J            3.4
                          1123cdFYRENE                0.5           J             1.4                           0.2              J            0.8
                          DBahANTHRA 0                0.1           J             0.5            J               0               J            0.4            J
                          Bgh1PERYLENE                0.6           J             1.6                           0.3              J            1.3

                          TOTAL PAH's                 120.3                       1694.3                        144.2                         1876
                          (w/o PERYLENE)
                          S&T Total PAHs              63.8                        1105.9                        46.2                          968.6






                                                            Mussel Watch Project Year 8 - Aromatics Data

                           INVEST#:               TBLB                         TBLF                        BBSD                        BBMI3
                              ID:            Ten-ebonne Bay             Terrebonne Bay                Barataria Bay               Barataria Bay
                              SITE             Lake Barre                 Lake Felicity            Bayou Saint Denis              Middle Bank
                          LABSAMNO:               K7052                        K7054                       K7048                       K7050
                        SAMPLE TYPE:              SAMP                         SAMP                        SAMP                        SAMP
                             UNTP.                ng/g                         ng/g                        ng/g                        ng/g
                    I    Analyte (Cont)           Conc        DB QUAL          Conc      DB QUAL           Conc        DB QUAL         Conc      DB; QUALI


                       2-METHYLNAPH *              5.1                         9.7                         2.5             J           21.7
                       1-METHYLNAPH *              4.3                         7.3                         2.7                         10.7


                      2,6-DIMETI-INAPH             3.4            J            8.4                         4.6                         2.5           J

                     2,3.5-TRIMETFiNAPH            1.1            J            5                           1.7             J           8.2

                       1 -METHYLPHEN *             3.1            J            29.9                        1.5             J           16.5



                      Surrogate Recoveries
                           NAPHD8:                69.7                         59.7                        64.6                        66.6
                           ACENDIO:               77.2                         74.7                        59.8                        73.6
                           PHENDIO:               64.9                         61.1                        59.8                        60.9
         (D                CHRYD12:               58.3                         60.2                        52.6                        59.6
                           PERYD12:               46.7                         48.8                        43.5                        41.9






                                                                  Mussel Watch Project Year 8 - Aromatics Data

                              INVEST#:                    MRIP                             MRPL                          BSSI                          BSBG
                                 ID:              Mississippi River                Mississippi River               Breton Sound                 Breton Sound
                                SITE                 Tiger Pass                      Pass a Loutre                  Sable island                Bay Garderne
                             LABSAMNO:                    K7062                            K7060                         K7072                         K7064
                          SAMPLE TYPE:                    SAMP                             SAMP                          SAMP                          SAMP
                                UNIT:                     ng/g                             ng/g                          ng/g                          ng/g
                           Analyte (Cont)                 Conc        DB QUAL              Conc        DB QUAL           Conc       DB QUAL            Conc      DB QUAL

                          RECEIPT DATE:                   1/9/97                           1/9/97                        1/10/97                       1/9/97
                              QCBATCH:                    M1233                            M1233                         M1234                         M1233
                       EXTRACTION DATE:                   9/15/97                          9/15/97                       9/17/97                       9/15/97
                              METHOD:                     GCMS                             GCMS                          GCMS                          GCMS
                         ANALYSIS DATE:                   10/26/97                         10/26/97                      10/29/97                      10/26/97
                              ME-17HOD:                   G-CECD                           GCECD                         GCECD                         GCECD
                         ANALYSIS DATE:                   8/25/98                          8/25/98                       8/23/98                       8/25/98
                               MATRIX*                    TISSUE                           TISSUE                        TISSUE                        TISSUE
                               SUBMAT.
                               WE7wr:                     15.32                            15.02                         15.01                         15.03
                               DRYWT:                     2.23                             1.69                          1.69                          2.48
                              vlr@k                       GRAMS          DRY               GRAMS          DRY            GRAMS         DRY             GRAMS        DRY
                             PCTSOLIDS:                   14.500k                          11.300/6                      11.300/6                      16.500/6
                            I.Apid Weight:
                           TOTAL LIPID:                   11.41                            7.01                          9.11                          8.69
                            LIPID UNITS:                  % DRY                            % DRY                         % DRY                         % DRY
                                VOU.
                              VOLUNITS:                   LITERS                           LITERS                        LITERS                        LITERS
                       Surrogate Recoveries
                                PAH's:
                               NAPHD8-                    60.4                             50.6                          50.9                          69.5
                              ACENDIO:                    73.2                             65.1                          66.3                          83.2
                              PHENDIO:                    86.2                             52.5                          67.2                          70
                              CHRYD12:                    53.4                             54.7                          66.5                          61.4
                              PERYD12:                    49.5                             49.3                          66.2                          47.6


                          NAPHTHALENE                     16.2                             10.4                          18.6                          10.6
                         CI-NAPHTHALENES                  31.2                             16.3                          45.9                          12.4
                         C2-NAPHTHALENES                  54.2                             34.6                          100.6                         30.4
                         C3-NAPHTHALENES                  126.3                            112.1                         251.1                         194.4
                         C4-NAPHTHALENES                  151.5                            143.3                         347.4                         390.3
                             BIPHENYL *                   4.7              J               3.5              J            10.9                          1.9            J
                         ACENAPHTHYLENE                   3.2              J               6.6                           3.9             J             2.1            J
                          ACENAPHTHENE0                    7                                1               J            4.1             J             2.3            J
                             FLUORENE*                    9.5                              5.8              J            17.4                          5.1
                                            "I
                              F L 1-7 10    E@            Ae).A                                                                                        38.3



                                                  mmm MM M M M

                                                              Mussel Watch "ect Year 8 - Aromatics Data

                            INVEST#:                    MRT`P                         MRPL                        BSSI                       BSBG
                                ID:            Mississippi River              Mississippi River             Breton Sound               Breton Sound
                               SITE               Tiger Pass                    Pass a Loutre                Sable Island               Bay Garderne
                           IABSAMNO:                    K7062                         X7060                       K7072                      K7064
                           SAMPLE TYPE:                 SAMP                          SAMP                        SAMP                       SAMP
                              UNIT:                     ng/g                          ng/g                        ng/g                       ng/g
                           Analyte (Cont)               Cone      DB QUAL             Cone       DB QUAL          Cone      DB QUAL          Cone      DB QUAL

                           C2-FLUORENES                 117.5                         78.2                        190.8                      189.5
                           C3-FLUORENES                 175.2                         190.3                       336.3                      358.7
                           PHENANTHRENE*                15.8                          20.5                        37.6                       26.1
                           ANTHRACENE*                  6.4                           8.2                         12.1                       13.2
                           CI-PHEN-ANTHR                71.7                          83.6                        176.3                      230.7
                           C2-PHEN-ANTHR                133.6                         236                         336.1                      599.9
                           C3-PHEN-ANTHR                197.5                         382.4                       538.4                      528.5
                           C4-PHEN_ANrHR                153.9                         373.4                       350.3                      279.5
                           DIBENZOTH10                  5.8                           3.6                          6                         5.3
                            CI-DIBEN                    17.5                          25.7                        41.3                       43.4
                            C2-DIBEN                    60.7                          109.5                       150.5                      189
                            C3-DIBEN                    70.8                          168.6                       170.3                      188.3
                           FLUORANTHENE                 16                            30.1                        39                         23.1
                            PYRENE *                    28.9                          59                          64.9                       27.6
                           CI-FLUORAN-PYR               37.3                          81.3                        90.6                       58.1
                      BENaANTHRACENE*                   11.5                          14.4                        13.9                        7
        w                  CHRYSENE *                   19.2                          30.1                        29.2                       15.8
                           Cl-CHRYSENES,                22                            37.3                        43.9                       12.9
                           C2-CHRYSENES                 23.5                          35                          35.9                       13.6
                           C3-CHRYSENES                               ND                             ND                         ND                         ND
                           C4-CHRYSENES                               ND                             ND                         ND                         ND
                           BENbFLUORAN                  6                             13.1                        7.2                        3.4
                           BENkFLUORAN                  5.6                           12.2                        7.7                        3.2
                           BENePYRENE *                 11.2                          21.4                        11.9                       4.4
                           BENaPYRENE 0                 1.4                           6.7                         2.8           j            1.1
                           PERYLENE 0                   30.7                          65.4                        26.5                       3.4
                           I123cdPYRENE                 1                              4                           2                         0.5
                           DBahANTHRA *                 0.4            1              1.6            1            0.8           1            0.3
                           BghIPERYLENE                 2                              6                           3                         0.9

                           TOTAL PAH's                  1658.4                        2384.7                      3556.4                     3511.8
                           (w/o PERYLENE)
                           S&T Total PAHs N             273.2                         339.8                       475.8                      260.2






                                                              Mussel Watch Project Year 8 - Aromatics Data

                            INVEST#:                  MRT?                            MRPL                        BSSJ                        BSBG
                                ID:            Mississippi River              Mississippi River             Breton Sound               Breton Sound
                               SITE               Tiger Pass                    Pass a Loutre                Sable Island               Bay Garderne  '
                           LABSAMNO:                  K7062                           K7060                       K7072                       K7064
                         SAMPLE TYPE:                 SAMP                            SAMP                        SAMP                        SAMP
                              UNIT:                   ng/g                            ng/g                        ng/g                        ng/g
                          Analyte (Cont)              Cone         DB QUAL            Cone       DB QUAL          Cone      DB QUAL           Cone     DB QUALI


                        2-METHYLNAPH *                19.2                            10                          27.8                        8.7
                        1-METHYLNAPH 0                11.9                            6.2                         18.1                        3.7


                       2,6-DIMETHNAPH                 22.7                            9.2                         42.8                        11.8


                     2,3.5-TRIMETHNAPH                26.6                            18.4                        49.9                        39.7


                        I-METHYLPHEN                  13.8                            17.8                        47.9                        54.4



                      Surrogate Recoveries
                            NAPHD8:                   60.4                            50.6                        50.9                        69.5
                            ACENDIO:                  73.2                            65.1                        66.3                        83.2
                            PHEND10:                  86.2                            52.5                        67.2                        70
        N)                  CHRYD12:                  53.4                            54.7                        66.5                        61.4
                            PERYD12:                  49.5                            49.3                        66.2                        47.6






                                                                  Mussel Watch Project Year 8 - Aromatics Data

                        INVEST#:                    LBMP                             MSPC                             MSBB                              MSPB
                           ID:                 Lake Borgne                   Mississippi Sound                Mississippi Sound                Mississippi Sound
                          SITE              Malheureux Point                   Pass Christian                         Biloid Bay                 Pascagoula Bay
                        LABSAMNO:                   K7066                            K7070                            K7068                             K7078
                        SAMPLETYPE:                 SAMP                             SAMP                             SAMP                              SAMP
                          UNrr                      ng/g                             ng/g                             ng/g                              ng/g
                        Analyte (Cont)              Conc         DB QUAL             Conc         DB QUAL             Conc         DB QUAL              Conc         DB QUAL

                        RECEIPT DATE:               1/9/97                           1/10/97                          1/10/97                           1/11/97
                        QCBATCH:                    M1233                            M1234                            M1234                             M1234
                   EXTRAC11ON DATE:                 9/15/97                          9/17/97                          9/17/97                           9/17/97
                        ME'n-IOD:                   GCMS                             GCMS                             GCMS                              GCMS
                        ANALYSIS DATE:              5/12/98                          10/29/97                         10/29/97                          10/29/97
                        METHOD:                     GCECD                            GCECD                            GCECD                             GCECD
                        ANALYSIS DATE:              8/25/98                          8/23/98                          8/23/98                           8/24/98
                        MATRIX                      TISSUE                           TISSUE                           TISSUE                            TISSUE
                        SUBMAT:
                        WE`1WT-                     15.17                            15.22                            15.32                             15.34
                        DRYWT:                      2.32                             2.94                             2.32                              1.93
                        WTUNITS:                    GRAMS           DRY              GRAMS           DRY              GRAMS           DRY               GRAMS           DRY
                        PCTSOLIDS:                  15.300/6                         19.30%                           15.20%                            12.60%
                        Lipid Weight:
        co              TOTAL LIPID:                9.48                             9.85                             13.16                             9.62
        W               LIPID UNITS:                % DRY                            % DRY                            % DRY                             % DRY'
                          VOL.
                        VOLUNITS:                   LITERS                           LITERS                           LITERS                            LITERS
                   Surrogate Recoveries
                         PAH's:
                        NAPHD8:                     71.6                             49.6                             50.1                              49
                        ACENDIO:                    74.1                             78.7                             67.6                              70.1
                        PHENDIO:                    58.8                             75.3                             66.3                              69.5
                        CHRYD12:                    73                               63.7                             60.4                              64
                        PERYD12:                    73.2                             65.2                             59.9                              66.1


                        NAPHTHALENE                 6.3                               12                              13.8                              13.9
                   Cl-NAPHTHALENES,                 5.5              J               13.1                             20.7                              15.7
                   C2-NAPHTHALENES                                  ND                               ND               109                               11
                   C3-NAPHTHALENES                                  ND                               ND               233                               23.3
                   C4-NAPHTHALENES                                  ND                               ND               236.2                             55.2
                        BIPHENYL *                  3.1              J               2.4              J               6.5                               4.7              J
                   ACENAPHTHYLENE                   1.3              J               2.8              J               4.6                               3.4
                   ACENAPHTHENE                     1.5              J               2.1              J               16.2                              5.7
                        FLUORENE 0                  2.5              J               7.6                              29.9                              10.5
                        CI-FLUORENES                                ND                               ND               64.1                              60.8






                                                                Mussel Watch Project Year 8 - Aromatics Data

                       INVE&R:                   LBMP                              MSPC                            MSBB                             MSPB
                          ID:                Lake Borgne                  Mississippi Sound               Mississippi Sound                Mississippi Sound
                         SITE             Malheureux Point                  Pass Christian                     Biloid Bay                   Pascagoula. Bay
                      LABSAMNO:                  K7066                             K7070                           K7068                            K7079
                    SAMPLE TYPE:                 SAMP                              SAMP                            SAMP                             SAMP
                         UNIT:                    ng/g                             ng/g                            ng/g                             ng/g
                    Analyte (Cont)                Conc        DB QUAL              Conc        DB QUAL             Conc        DB QUAL              Conc        DB QUAL

                    C2-FLUORENES                                  DID                             ND               194.5                            16.5
                    C3-FLUORENES                                  ND                              ND               325.6                            60.3
                    PHENANTHRENEO                  7                               11.1                            79.8                             25.5
                    ANMRACENE *                    3.5             J               15.5                            20.7                             12
                    CI-PHEN-ANTHR                                 ND                              ND               182.3                            128.8
                    C2-PHEN@ANTHR                                 ND                              ND               285.6                            53.5
                    C3-PHEN-ANTHR                                 ND                              ND               348.4                            78.4
                    C4-PHEN-ANTHR                                 ND                              ND               199.9                                           ND
                    DIBENZOTHIO                    1.8                             1.2             J               14.3                             2.8
                       CI-DIBEN                                   ND                              ND               84.2                             0              ND
                       C2-DIBEN                                   ND                              ND               264.5                            20.2
                       C3-131BEN                                  ND                              ND               225.6                            60.4
                    FLUORANTHENE                   10.9                            17.9                            116.4                            92.1
                       PYRENEO                     6.6                             10.9                            114.6                            55.9
                    CI-FLUORAN-PYR                                ND                              ND               100.4                            65.4
                 BENaANTHRACENE*                   1.4                             5.9                             26.8                             19.4
                      CHRYSENE *                   3.5                             8.1                             50.3                             21
                    CI-CHRYSENES                                  ND                              ND               27.3                             62.7
                    C2-CHRYSENES                                  ND                              ND               22.2                             17.2
                    C3-CHRYSENES                                  ND                              ND                               ND               10.2
                    C4-CHRYSENES                                  ND                              ND                               ND                               ND
                    BENbFLUORAN                    1.2             J               2.4                             13.3                             6.7
                    BENkF'LUORAN                   1.2             J               2.5                             14.2                             7.1
                    BENePYRENE *                   1.3                             2.8                             16.1                             6.6
                    BENaPYRENE *                   0.9             J               0.6             J               3.5                              2                J
                      PERYLENEO                    2.9                             1.4             J               4.8                              11.8
                    1123cdPYRENE                   0.7             J               0.6                             2.5                              1.3
                    DBahANTHRA *                   0.5             J               0.4             J               1.3              J               0.7              J
                    BghiPERYLENE                   0.9             J               0.5             J               3.9                              1.6

                      TUTAL PAH's                  61.5                            120.2                           3472.1                           1032.2
                      (w!o PERYLENE.)
                    S&T Total PAHs                 63.9                            122.1                           664.4                            327






                                                               Mussel Watch Project Year 8 - Aromatics Data

                         INVEST#:                LBMP                           MSPC                             MSBB                          MSPB
                           ID:               Lake Borgne                  Mississippi Sound              Mississippi Sound              Missimippi Sound
                          SITE            Malheureux Point                 Pass Christian                    Btlo)d Bay                   Pascagoula Bay
                      1ABSAMNO:                  K7066                          K7070                            K7068                        K7078
                     SAMPLE TYPE:                SAMP                           SAMP                             SAMP                          SAMP
                          UNIT:                  ng/g                           ng/g                             ng/g                          ng/g
                     Analyte (Cont)              Conc         DB QUAL           Conc         DB QUAL             Conc        DB QUAL           Conc          1313 QUAL


                   2-METHYLNAPH *                 2.9             J              6.2                             13.1                           9.4
                    I-METHYLNAPH 4                2.6             J               7                              7.6                            6.3

                  2,6-DIMETHNAPH                  2.4             J              3.7                             39.1                            9

                 2.3.5-TRIMETHNAPH                2.3             J              4.2                             51.9                           9.4

                   1-METHYLPHEN 0                 1.8             J              2.7                             52                             11.2



                  Surrogate Recoveries
                        NAPHI38:                 71.6                           49.6                             50.1                           49
                        ACEND10:                 74.1                           78.7                             67.6                          70.1
         to             PHEND10:                 58.8                           75.3                             66.3                          69.5
         U1             CHRYD12:                  73                            63.7                             60.4                           64
                        PERYD12:                 73.2                           65.2                             59.9                          66.1







                                                                     Mussel Watch Pro ect Year 8 - Aromatics Data

                INVEST'#:                    MBCP                             MBHI                            PBPH                           PBIB                          PBSP
                   ID:              Mobile Bay Cedar                  Mobile Bay Cedar                  Pensacola Bay                 Pensacola Bay                  Pensacola Bay
                  SITE              Cedar Point Reef                  Hollingers Island                 Public Harbor                 Indian Bayou                    Sabine Point
                LABSAMNO:                    K7076                            K7074                           K7088                          K7086                         K7090
                SAMPLE TYPE:                 SAMP                             SAMP                            SAMP                           SAMP                          SAMP
                  UNIT:                      ng/g                             ng/g                            ng/g                           ng/g                          ng/g
                Analyte (Cont)               Cone        DB QUAL              Cone         DB QUAL            Cone       DB QUAL             Cone       DB QUAL            Cone       DB QUALI

                RECEIP17 DATE:               1/11/97                          1/11/97                         1/13/97                        1/13/97                       1/13/97
                QCBATCH:                     M1234                            M1234                           M1234                          M1234                         M1234
                EXTRACTION DATE:             9/17/97                          9/17/97                         9/17/97                        9/17/97                       9/17/97
                METHOD:                      Gems                             GCMs                            GCMs                           GCMS                          GCMs
                ANALYSIS DATE:               10/29/97                         10/29/97                        10/29/97                       10/29/97                      10/29/97
                METHOD:                      GCECD                            GCECD                           GCECD                          GCECD                         GCECD
                ANALYSIS DATE:               8/24/98                          8/24/98                         8/24/98                        8/25/98                       8/24/98
                MATRIX:                      TISSUE                           77SSUE                          TISSUE                         TISSUE                        TISSUE
                SUBMAT,
                WETWI`:                      15.17                            15.22                           15.16                          15.37                         15.4
                DRYWT.                       2.39                             2.37                            2.52                           1.72                          2.43
                WT`UNITS:                    GRAMS           DRY              GRAMS           DRY             GRAMS          DRY             GRAMS         DRY             GRAMS          DRY
                PCT'SOLIDS:                  15.70%                           15.60%                          16.60%                         11.20%                        15.800,6
         CO     Llptd Weight:
                TOTAL LIPID:                 9.93                             9.72                            10.44                          7.12                          9.24
                LIPID UNITS:                 % DRY                            % DRY                           % DRY                          % DRY                         % DRY
                  VOL:
                VOLUNITS:                    LITERS                           LITERS                          LITERS                         LITERS                        LITERS
                Surrogate Recoveries
                 PAH's:
                NAPHDS:                      55.9                             663.9                           57.8                           58.4                          56.9
                ACEND10:                     88.3                             75.2                            77.1                           66.2                          77.2
                PHENDIO:                     72.9                             69.5                            70.7                           63.5                          75.8
                CHRYD12:                     68.9                             67.3                            61.4                           65                            64.9
                PERYD12:                     70.4                             62.4                            66.9                           53.1                          66.2


                NAPHTHALENE$                 8.4                              8.4                              8                             10.7                          9.9
                CI-NAPHTHALENES               9                               11.5                            10.1                           11.2                          8.9
                C2-NAPHTHALENES              18.4                             11.8                            16.1                                          ND             15.8
                C3-NAPHTHALENES              31.7                             23.5                            32.4                                          ND             24.7
                C4-NAPHTHALENES              26.1                             37.6                            36.8                                          ND             17.2
                BIPHENYL *                    4                               2.9               1              4              .1             4.4              j            3. 1
                ACENAPHTHYLENE               2.6              1               3.8               1             3.9             1              2.7              1            2.3
                ACENAPHTHENE*                0.8              1               3.3               1             5.6                            4.8              1            2.9
                FLUORENE*                    5.7                              3.1               1             8.5                            3.6              T            5.2
                Cl-FUUORENES                 8. i              i              iLi                             10.7                                          ND             9.9






                                                              Mussel Watch Project Year 8 - Aromatics Data

              INVEST#-                  MBCP                          MBHI                          PBPH                       PBIB                       PBSP
                 ID:            Mobile Bay Cedar              Mobile Bay Cedar               Pensacola Bay              Pensacola Bay               Pensacola Bay
                SITE            Cedar Point Reef               Hollingers Island             Public Harbor               Indian Bayou                Sabine Point
            LABSAMNO:                   K7076                         K7074                         K7088                      K7086                      K7090
            SAMPLE TYPE:                SAMP                          SAMP                          SAMP                       SAMP                       SAMP
                UNIT:                   ng/g                          ng/g                          ng/g                       ng/g                       ng/g
            Analyte (Cont)              Cone       DB QUAL            Conc        DB QUAL           Conc     1313 QUAL         Conc     DB QUAL           Conc      DB QUALI

            C2-FLUORENES                33.8                          57.7                          40.4                                    ND            36.5
            C3-FLUORENES                78.3                          153.2                         77.5                                    ND                         ND
            PHENANTHRENE*               12.9                          13.2                          26.4                       7.8                        17.8
            ANTHRACENE*                 7.8                           10.8                          13.9                       7.5                        6.7
            CI-PHEN_ANTHR               24.5                          42.1                          45.3                       11.1                       22
            C2-PHEN_ANTHR               34.9                          69.8                          69.1                       16.7                       25
            C3-PHEN_ANTHR                              ND                            ND                         ND                          ND                         ND
            C4-PHEkANTHR                               ND                            ND                         ND                          ND                         ND
            DIBENZOTHIO                 1.5             J             1.6                           2                          1.1                        1.1           J
              CI-DIBEN                  6.6                           12.2                          10.7                       4.7                        5.2
              C2-DIBEN                  23                            43.5                          37.6                       7.1                        16.4
              C3-DIBEN                  20.8                          45.4                          36.4                       5.6                        11.9
            FLUORANTHENE                20.4                          42                            90                         14.5                       32.2
              PYRENE*                   33.8                          65.9                          60.7                       11.2                       17.1
       UCI-FLUORAN       PYR            23.2                          49.7                          60.7                       14.4                       20.4
        I*NaANTHRACENE                  8.3                           12.8                          38.5                       5                          8.3
            CHRYSENE *                  9.6                           20.7                          60.7                       7.8                        14.5
            CI-CHRYSENES                8.3                           13.9                          23.3                       12                          7
            C2-CHRYSENES                6.3             J             9.8                           12.5                       6.5           J            6.3           J
            C3-CHRYSENES                               ND                            ND                         ND                          ND                         ND
            C4-CHRYSENES                               ND                            ND                         ND                          ND                         ND
            BENbFLUORAN                 2.8             J             4.6                           16.8                       6.3                        4.2
            BENkFLUORAN                 3                             4.8                           17.9                       6.7                        4.5
            BENePYRENE*                 4.4                           8.3                           17.1                       5.4                        5.2
            BENaPYRENE                  0.7             J             1.2             J             2.7                        2.7           J            1.8           J
            PERYLENE*                   5.4                           8.2                           5.2                        5.5                        1.9           J
            I 123cdPYRENE               0.2             J             1.1                           1.5                        1.8                        1.1
            DBahANTHRA*                 0.4             J             0.2             J             0.6          J             0.5           J            0.5           J
            BghtPERYLENE                0.8             J              2                            2.6                        3.4                         1            J

            TOTAL PAH's                 481                           803.5                         900.9                      196.9                      366.4
            (w/o PERYLENE)
            S&T Total PAHs (*)          144.2                         232                           375.9                      114.2                      148.6






                                                            Mussel Watch Project Year 8 - Aromatics Data

             INVEST#:                 MBCP                          MBH1                        PBPH                       PBIB                       PBSP
                ID:           Mobile Bay Cedar               Mobile Bay Cedar             Pensacola Bay              Pensacola Bay              Pensacola Bay
               SITE            Cedar Point Reef              Hollingers Island            Public Harbor              Indian Bayou                Sabine Point
           LABSAMNO:                  K7076                         K7074                       K7088                     K7086                       K7090
          SAMPLE TYPE:                SAMP                          SAMP                        SAMP                      SAMP                        SAMP
               UNIT-.                 ng/g                          ng/g                        ng/g                       ng/g                       ng/g
          Analyte (Cont)              Conc       DB QUAL            Conc       DB QUAL          Conc      DB QUAL          Conc      DB QUAL          Conc     DB QUAL


         2-METHYLNAPH *               5.1                           4.7                         5.6                         5.6          J            5.7
         i-METHYLNAPH *                4                            6.9                         4.5                         5.6                       3.2


        2,6-DIMETHNAPH                3.7                           1.7            J            5.3                         6.4                       4.3


       2,3,5-TRIML'rHNAPH             3.2                           6.4                         6.1                         3            J            3.3           J


         I -METHYLPHEN                5.7                           11.3                        12.5                        2.3          J            5.3



        Surrogate Recoveries
             NAPHD8:                  55.9                          63.9                        57.8                       58.4                       56.9
        CO   ACEND10:                 88.3                          75.2                        77.1                       66.2                       77.2
        00   PHENDIO:                 72.9                          69.5                        70.7                       63.5                       75.8
             CHRYD12:                 68.9                          67.3                        61.4                        65                        64.9
             PERYD12:                 70.4                          62.4                        66.9                       53.1                       66.2






                                                                  Mussel Watch Project Year 8 - Aromatics Data

                             INVEST#:                  CBJB                            CBSR                           CBPP                           PCLO
                                ID:             Choctawhatchee                 Choctawhatchee                 Choctawhatchee                    Panama City
                               SITE               Joe's Bayou                   Off Santa Rosa                   Postil Point                Little Oyster Bar
                             LABSAMNO:                 K7082                           K7084                          K7080                          K7092
                             SAMPLE TYPE:              SAMP                            SAMP                           SAMP                           SAMP
                               UNIT.-                  ng/g                            ng/g                           ng/g                           ng/g
                             Analyte (Cont)            Conc        DB QUAL             Conc       DB QUAL             Conc        DB QUAL            Conc        DB QUALI

                             RECEIPT DATE:             1/14/97                         1/13/97                        1/13/97                        1/14/97
                             QCBATCH:                  M1234                           M1234                          M1234                          M1234
                       EXTRACTION DATE:                9/17/97                         9/17/97                        9/17/97                        9/17/97
                             METHOD:                   GCMS,                           GCMS                           GCMS                           GCMS
                             ANALYSIS DATE:            10/29/97                        10/29/97                       10/29/97                       10/29/97
                             METHOD:                   GCECD                           GCECD                          GCECD                          GCECD
                             ANALYSIS DATE:            8/24/98                         8/24/98                        8/24/98                        8/24/98
                             MATRIX.                   TISSUE                          TISSUE                         TISSUE                         TISSUE
                             SUBMAT:
                             WETWT.                    15-16                           15.09                          15.17                          15.31
                             DRYVvT-                   2.73                            1.89                           2.16                           2.83
                             WTUNITS:                  GRAMS          DRY              GRAMS         DRY              GRAMS          DRY             GRAMS          DRY
                             PCTSOLIDS-.               18.00%                          12.5M                          14.20%                         18.500/0
                             Lipid Weight:
         co                  TOTAL LIPID:              10.56                           7.66                           10.5                           9.09
         (D                  LIPID UNITS:              % DRY                           % DRY                          % DRY                          % DRY
                               VOL:
                             VOLUNITS:                 LITERS                          LITERS                         LITERS                         LITERS
                       Surrogate Recoveries
                              PAH's:
                             NAPHD8:                   57.3                            67                             58.5                           54
                             ACENDIO:                  103.1                           73.1                           77                             67.4
                             PHENDIO:                  89.9                            73.8                           72.7                           68.2
                             CHRYD12:                  73.7                            68.8                           67                             57.4
                             PERYD12:                  73.7                            62.7                           59.1                           61.9


                             NAPHTHALENE*              14.8                            9.2                            10                             7.8
                       Cl-NAPHTHALENES                 55.1                            6.6             J              14.8                           12.2
                       C2-NAPHTHALENES                 150.7                           17.3                           20.6                           14.5
                       C3-NAPHTHALENES                 315.2                           27.1                           39.2                           27.1
                       C4-NAPHTHALENES                 393.2                           29                             35.5                           22.3
                             BIPHENYL *                5.8                             3               J              4.8             J              2.7             J
                       ACENAPHTHYLENE                  33.8                            1.3             J              2.8             J              1.5             J
                       ACENAPHTHENE*                   60.7                            2.4             J              4.5                            2.3             J
                             FLUORENE 0                77.2                            3.4             J              8.8                            4.7
                             Cl-FLUORENES              63.3                            11.5            J              15.8                           8.7






                                                               Mussel Watch Project Year 8 - Aromatics Data

                          INVFSr#:                  CBJB                           CBSR                          CBPP                           PCLO
                              ID:            Choctawhatchee                Choctawhatchee                Choctawhatchee                   Panam City
                             SITE              Joe's Bayou                  Off Santa Rosa                  Postil Point                Little Oyster Bar
                         LABSAMNO:                  K7082                          K7084                         K7080                          K7092
                         SAMPLE TYPE:               SAMP                           SAMP                          SAMP                           SAMP
                            UNIT:                   ng/g                           ng/g                          ng/g                           ng/g
                         Analyte (Cont)             Cone        DB QUAL            Cone       DB QUAL            Cone       DB QUAL             Cone      -DB QUALI

                         C2-FLUORENES,              241.8                          40.6                          58.8                           33.3
                         C3-FLUORENES               527.2                          73                            97.8                           50.6
                         PHENANTHRENE*              387.4                          6.1                           23.9                           16.9
                         ANTHRACENEO                154.2                          4              J              11.2                           5.1
                         CI-PHEN-ANTHR              518.8                          16.8                          81.9                           20.1
                         C2-PHEN-ANTHR              1016.9                         33.1                          127.8                          34.2
                         C3-PHEN-ANTHR              1177.5                                        ND                            M                             ND
                         C4-PHEN-ANTHR              628.8                                         ND                            M                             ND
                         DIBENZOTHIO,               19.5                           1.3            J              2.8                            1.4
                          CI-DIBEN                  95.4                           4.8                           15.4                           3.3
                          C2-DIBEN                  448.7                          16.3                          53.8                           16
                          C3-DIBEN                  568.7                          19.1                          52.7                           12.2
                         FLUORANTHENE               1486.5                         14.1                          79                             32.9
                          PYRENE*                   1132.9                         8.4                           80.4                           19.1
                         CI-FLUORAN-PYR             908.9                          14.3                          105.2                          16.4
                     BENaANTHRACENE                 919.7                          2.5                           53.5                           5.3
                         CHRYSENE *                 858.8                          4.5                           94.7                           10.3
                         CI-CHRYSENES               525.3                                         ND             145.9                          6.1
                         C2-CHRYSENES,              117.3                                         ND             104.5                          6.4
                         C3-CHRYSENES               10.7                                          ND             27.6                                         ND
                         C4-CHRYSENES               17.3                                          ND             13.7                                         ND
                         BENbFLUORAN                513.9                          2.1            J              27.4                           1.9            J
                         BENkFLUORAN                545.6                          2.2            J              29.1                           2              J
                         BENePMNE *                 476.5                          2.5                           54.3                           3.2
                         BENaPYRENE 0               127.4                          0.9            J              29.5                           1              J
                         PERYLENE *                 77.5                           5.1                           12.6                           2.2
                         1123cdPYRENE               35.7                           1.1                           14.4                           0.4            J
                         DBahANTHRA *               15.7                           0.2            J              4.6                            0.1            J
                         BghIPERYLENE               69.8                           0.6            J              25.5                           0.5            J


                         TOTAL PAH's                14716.4                        379.1                         1572.3                         402.3
                         (w/o PERYLENE)
                         S&T Total PAHs             6041.3                         83.9                          519.8                          141.1






                                                             Mussel Watch Project Year 8 - Aromatics Data

                           INVEST#:                CBJB                        CBSR                        CBPP                        PCLIO
                              ID:            Choctawhatchee              Choctawhatchee              Choctawhatchee                Panania City
                             SUE               Joe's Bayou                Off Santa Rosa                Postil Point             I.Attle Oyster Bar
                          LABSAMNO:                K7082                       K7084                       K7080                       K7092
                        SAMPLE TYPE:               SAMP                        SAMP                        SAMP                        SAMP
                             UNIT-                 ng/g                        ng/g                         ng/g                       ng/g
                         Analyte (Cont)            Conc       DB QUAL          Conc       DB QUAL           Conc       DB QUAL         Conc        DB QUALI


                       2-METHYLNAPH *              35.5                         4.2           J              8.8                        7.4
                       1 -METHYLNAPH *             19.7                         2.5           J              6.1                        4.8


                      2.6-DIMETHNAPH               40.4                         5.8                          6.7                        5.3

                    2.3.5-TRIMETHNAPH              43.1                         1.8           J             9                           5. 1


                       I -METHYLPHEN *             107.7                        3.5           J             17.4                        5.1



                     Surrogate Recoveries
                       -   NAPHDS:                 57.3                         67                          58.5                        54
                           ACENDIO:                103.1                       73.1                          77                        67.4
                           PHENDIO:                89.9                        73.8                         72.7                       68.2
                           CHRYD12:                73.7                        68.8                          67                        57.4
                           PERYD12:                73.7                        62.7                         59.1                       61.9






                                                            Mussel Watch Project Year 8 - Aromatics Data

                           INVEST#:                PCMP                       SAWB                       APDB                           APCP
                             ID:             Panama City                 St. And                 Apalachicola Bay              Apalachicola Bay
                             SITE           Municipal Pier             Watson Bayou                      Dry Bar                 Cat Point Bar
                         LABSAMNO:                 K7096                      K7094                      K7098                          K7104
                       SAMPLE TYPE:                SAMP                       SAMP                       SAMP                           SAMP
                             UNIT:                 ng/g                       ng/g                       ng/g                           ng/g
                       Analyte (Cont)              Conc     DB QUAL           Conc    DB QUAL            Conc       DB QUAL             Conc       DB QUALI

                       RECEIPT DATE:               1/14/97                    1/14/97                    1/15/97                        1/15/97
                          gCBATCH:                 M1234                      M1234                      M1234                          M1235
                    EXTRACTION DATE:               9/17/97                    9/17/97                    9/17/97                        9/18/97
                           METHOD:                 GCMS                       GCMS,                      GCMS                           GCMS
                      ANALYSIS DATE:               10/30/97                   10/30/97                   10/30/97                       10/31/97
                           METHOD:                 GCECD                      GCECD                      GCECD                          GCECD
                      ANALYSIS DATE:               8/24/98                    8/24/98                    8/24/98                        8/23/98
                            MATRIX:                TISSUE                     TISSUE                     TISSUE                         TISSUE
                           SUBMAT:
                            WETWT:                 15.13                      15.04                      15.09                          15.22
                            DRYWT:                 2.37                       2.43                       1.49                           2.55
                           WTUNITS:                GRAMS       DRY            GRAMS      DRY             GRAMS          DRY             GRAMS        DRY
                          PCTSOLIDS:               15.700A                    16.20%                     9.90016                        16.80%
                        Lipid Weight:
                        TOTAL LIPID:               8.53                       7.16                       6.1                            7.16
       ba               LIPID UNITS:               % DRY'                     % DRY                      % DRY                          % DRY
                             VOL:
                          VOLUNITS:                LITERS                     LITERS                     LITERS                         LITERS
                     Surrogate Recoveries
                             PAH's:
                           NAPHD8:                 55.7                       57.2                       56.8                           58.3
                           ACENDIO:                67.9                       61.1                       70.8                           65.6
                           PHENDIO:                78                         69.7                       70.3                           74.1
                           CHRYD12:                75.3                       59.7                       65.6                           69.7
                           PERYD12:                62                         66.4                       66.4                           67.6


                       NAPHTHALENE                 15.9                       7.9                        10.9                           9.6
                      CI-NAPHTHALENES              55.3                       8.7                        16.4                           23.1
                      C2-NAPHTHALENES              194                        47.2                                      ND              51.5
                      C3-NAPHTHALENES              364.8                      169.9                                     ND              145.3
                      C4-NAPHTRALENES              388.3                      278.5                                     ND              171.5
                         BIPHENYL *                10.3                       6            J               4             J              3.6
                      ACENAPHTHYLENE               6.9                        6.5                        1.2             J              2.9            J
                       ACENAPHTHENE*               13.5                       9.6                        1.4             J              3.6
                          FLUORENE*                27.2                       13                         3.5             J              5. 1
                                                                                                                                        A
                                                                              59.9                                      ND
                          .-FT I TrNEM-M 0






                                                          Mussel Watch Project Year 8 - Aromatics Data
                                                 PCMP                ---    SAWB                      APDB  -                         vrp
                           ID.,            Panama City                 St. Andrew               Apalachicola Bay              Apalactdcola, Day
                          SrM             Municipal Pier             Watson Bayou                   Dry Bar                     Cat Point Bar
                       LAELSAMNO:                K7096                      K7094                     K7098                           K7104
                       SAMPLE IYPE:              SAMP                       SAMP                      SAMP                            SAMP
                          UNrP,                  ng/9                       ng/g                       ng/g                           ng/g
                       Analyte (Cont)            Cone     DB QUAL           Conc     DB gUAL           Conc        DB QUAL            Conc       DB g
                       C2-FWORENF,S              231.9                      231                                           ND          134.3
                       C3-FLUORENES              419.4                      417.2                                         ND          218.4
                       PHENANTffRENE*            104.2                      50.4                        4.2                           35.9
                       ANTHRACENE*               49.6                       3615                        2.1               J           22.9
                       Cl-PHEN-ANTHR             349.4                      247.9                       19.7                          141.3
                       C2-PHEN_AN-THR            683.9                      518.2                       20.4                          239.4
                       C3-PHEN_ANTHR             727.3                      495.5                                         ND          293.6
                       C4-PHEN_ANTHR             415.4                      225.6                                         ND          168.7
                       DIBENZOTHIO               13                         6.1                          1.2              J           5.8
                        Cl-DI13EN                81.4                       66.1                                          ND          42.5
                        C2-DIBEN                 339.2                      240.2                                         ND          1215
                        C3-DIBEN                 478                        211.9                                         ND          140.6
                       FLUORANTHENE              274.2                      289.4                       7.6                           63.8
                        PYRENE*                  211.3                      227.8                       6.6                           72.3
                       Cl-FLUORAN_M              265.6                      157.9                                         ND          74.1
                   BENaANTHRACENE                91.1                       58,6                         1A               J           14.1
                       CHRYSSNE 0                168.8                      122.1                         4               J           20.8
                       CI-CHRYSENES              101.4                      46.4                                          ND                         ND
                       C2-CHRYSENES              43                         24.7                                          ND                         ND
                       C3-CHRYSENES              4.2           J              7                                           ND                         ND
                       C4-CHRYSENES              5.8           J            6.1          J                                ND                         ND
                       BENbFIXORAN               53.2                       30.9                         1.5              J           5.5
                       BENkFWORAN                56.4                       32.8                         1.6              J           5.8
                       SENePMENE:                52.2                       36.9                         L7                           6.8
                       BENaPYFEM                 9.8                        8.1                          0.3              J           1.2             J
                       PERYLENE *                8.2                        6.6                           5                           5.2
                       1123edPYRENE              5.1                        5.3                          0.6              J           0.6
                       DBahANTHRA *              1.3            J             2                          0.3              J           0.4             J
                       BghlPEMENE                11.7                       8.5                          1.2              J           2.1
                       TMAL PAH's.               6400.2                     4418.3                      111.6                         2289.3
                       (w/o PERYLENE)
                       S&T Total PAHs (0)        1325.7                     1002                         76.3                         371.8






                                                             Mussel Watch Project Year 8 - Aromatics Data

                           INVEST#:               PCMP                       SAWB                        APDB                          APCP
                              ID:             Panama City                St. Andrew               Apalachicola Bay              ApalacMeola Bay
                             STM             Municipal Pier             Watson Bayou                   Dry Bar                    Cat Point Bar
                         LABSAMNO:                K7096                      K7094                       K7098                         K7104
                        SAMPLE TYPE:              SAMP                       SAMP                        SAMP                          SAMP
                             UNIT:                ng/g                       ng/g                        ng/g                          ng/g
                        Analyte (Cont)            Cone       DB QUAL         Cone      DB QUAL           Cone        DB QUAL           Cone        DB QUAL



                      2-METHYl,NAPH *             31.9                       5.2                         8.5                           15.7
                       1 -MLrHYLNAPH 0            23.4                       3.5                         7.9                           7.4


                      2,6-DIMETHNAPH               74                        18.5                        5.4             J             20.4


                    2.3.5-IMME114NAPH             81.9                       41.9                        1.2             J             31.5


                       I-METHYLPHEN *              77                        57.9                        0.5             J             31.6



                     Surrogate Recoveries
                           NAPHD8:                55.7                       57.2                        56.8                          58.3
                           ACENDIO:               67.9                       61.1                        70.8                          65.6
                           PHENDIO:                78                        69.7                        70.3                          74.1
                           CHRYD12:               75.3                       59.7                        65.6                          69.7
                           PERYD12:                62                        66.4                        66.4                          67.6






                                                                    Mussel Watch Project Year 8 - Aromatics Data

                     INVEST#:                  AESP                        CKBP                       TBNP                          TBMK                          TBPB
                        ID:             Apalachee Bay                      Cedar Kay             Tampa Bay                     Tampa Bay                     Tampa Bay
                       SITE              Spring Creek                      Black Point          Navarez Park                Mullet Key Bayou                Papys Bayou
                     LABSAMNO:                 K7102                       K7100                      K71 10                        K7106                         K7118
                 SAMPLE TYPE:                  SAMP                        SAMP                       SAMP                          SAMP                          SAMP
                      UNIT:                    ng/g                        ng/g                       ng/g                          ng/g                          ng/g
            L Analyte (Cont)                   Conc       DB QUAL          Conc     DB QUAL           Conc      DB QUAL             Conc         DB QUAL          Conc      D13 QUAL

                 RECEIPT DATE:                 1/15/97                     1/15/97                    1/16/97                       1/16/97                       1/17/97
                     QCBATCH:                  M1235                       M1234                      M1235                         M1235                         M1235
               EXTRACTION DATE:                9/18/97                     9/17/97                    9/18/97                       9/18/97                       9/18/97
                     ME17HOD:                  GCMS                        GCMS                       GCMS                          GCMS                          GCMS
                ANALYSIS DATE:                 10/31/97                    10/30/97                   10/31/97                      10/31/97                      11/1/97
                     MErHOD:                   GCECD                       GCECD                      GCECD                         GCECD                         GCECD
                ANALYSIS DATE:                 8/23/98                     8/25/98                    8/24/98                       8/23/98                       8/24/98
                     MATRIX:                   TISSUE                      TISSUE                     TISSUE                        TISSUE                        TISSUE
                     SUBMAT:
                     WETwr:                    15                          15.16                      15.07                         15.13                         15.35
                     DRYWr:                    1.49                        2.67                       2.67                          3.7                           2.67
                     WrUNITS:                  GRAMS         DRY           GRAMS       DRY            GRAMS        DRY              GRAMS          DRY            GRAMS        DRY
                     PCTSOLIDS:                9.900/6                     17.600A                    17.700A                       24.500/6                      17.400,6
                     I.Apid Weight:
                     TOTAL LIPID:              4.83                        7.8                        6.96                          7.45                          7.62
                     LIPID UNITS:              % DRY                       % DRY                      % DRY                         % DRY                         % DRY
                       VOL:
                     VOLUNITS:                 LITERS                      LITERS                     LITERS                        LITERS                        LITERS
               Surrogate Recoveries
                      PAH's:
                     NAPHD8:                   66.5                        51.6                       48.9                          59.9                          59.7
                     ACENDIO:                  70.7                        65.9                       57.7                          84.1                          81.9
                     PHENDIO:                  70.1                        70                         70.3                          75.4                          78
                     CHRYD12:                  68.9                        57.1                       65.6                          64.4                          71.3
                     PERYD12:                  63.1                        59.4                       57.1                          65.1                          62.7


                NAPI-1714ALENE 0               10.9                        8.1                        19.5                          5.3                           11.3
               Cl.-NAPHTHALENES                13.8                        11.4                       51                            7.6                           11
               C2-NAPHTHALENES                               ND            16.2                       57.5                          11.9                          15.7
               C3-NAPHTHALENES,                              ND                        ND             76.9                          17.3                          26.9
               C4-NAPHTHALENES                               ND                        ND             85.2                          22.5                          28.8
                     BIPHENYL 0                5.5            J            2.1          J             3.7            J              1.9              J            1.9           J
               ACENAPHTHYLENE                  1.3            J            0.5          J             2.5            J              0.8              J            1.9           J
               ACENAPHTHENE*                   2.9            J            0.8          J             6.5                           9.1                           6.9
                     FLUORENEO                 2.3            J            2.8          J             7.3                           6.9                           8.1
                  Cl-FLUORENES,                              ND                        ND             27                            5.1              J            4.7           J






                                                              Mussel Watch "ect Year 8 - Aromatics Data

                  INVEST#:                AESP                       CKBP                     TBNP                        TBMK                        T13PB
                     ID:            Apalachee Bay                Cedar Kay               Tampa Bay                    Tampa Bay                   Tampa Bay
                    sITE             Spring Creek               Black Point             Navarez Park               Mullet Key Bayou              Papys Bayou
                LABSAMNO:                 K7102                      K7100                    K71 10                      K7106                       K7118
                SAMPLE TYPE:              SAMP                       SAMP                     SAMP                        SAMP                        SAMP
                    UNIT:                 ng/g                       ng/g                     ng/g                        ng/g                        ng/g
                Analyte (Cont)            Cone       DB QUAL         Cone    DB QUAL          Cone     DB QUAL            Cone        DB QUAL         Cone     DB QUALI

                C2-FLUORENES,                           ND                       ND           56.8                                       ND                        ND
                C3-FLUORENES,                           ND                       ND           83.9                                       ND                        ND
                PHENANTHRENE*              4                         4.2                      20.7                        26.7                        30.9
                ANTHRACENE*               2.3            1           0.9         1            11.2                        7.4                         10.9
                CI-PHEN-ANTHR                           ND           11                       40.7                        39.5                        29
                C2-PHEN-ANrHR                           ND           9.7                      62.9                        22.7                        20.6
                C3-PHEN ANTHR                           ND                       ND           70.9                                       ND                        ND
                C4-PHEN  ANTHR                          ND                       ND           37.9                                       ND                        ND
                DIBENZOTHIO               0.5            1           0.5         1            2.2                         1.8                         2.2
                  CI-DIBEN                              ND                       ND           6.4                         3.5                         4.2
                  C2-DIBEN                              ND                       ND           15.8                        5.8                         6.9
                  C3-13IBEN                             ND                       ND           15.5                                       ND                        ND
                FLUORANTHENE              3.5            1           4.6                      128                         56.4                        81.5
                  PYRENEO                 2.7                        3                        74.4                        30.7                        49.9
       0) CI-FLUORAN-PYR                                ND           9                        45.5                        22.2                        29.2
            BENaANTFIRACENE               2.1                        0.9         j            12.4                         9                          10.9
                CHRYSENE*                  2             1           1.3         1            42.3                        10.8                        32.7
                CI-CHRYSENES                            ND                       ND           14.2                                       ND           6.7
                C2-CHRYSENES                            ND                       ND           10.6                                       ND           4.4           j
                C3-CHRYSENES                            ND                       ND                        ND                            ND                        ND
                C4-CHRYSENES,                           ND                       ND                        ND                            ND                        ND
                BENbFLUORAN               1.2            j           0.4         1            13.2                        2.9                         8.7
                BENkFLUORAN               1.2            j           0.4         1            14.1                         3                          9.3
                BENePYRENE *              1.2            1           1                        16.4                        3.3                         10.1
                BENaPYRENE*               0.9            j           0.4         1            2.4                         0.6             j           1.1
                PERYLENE                  3.4            1           1.4         j            1.9           1                                         1.6           i
                1123cdPYRENE                I            j           0.5         1            2.7                         0.7                         1.8
                DBahANTHRA 0              0.9            j           0.1         j            0.8           j             0.3             1           1.4           j
                BghiPERYLENE              0.7            j           0.8         1            5.4                         0.9                         3.2

                TOTAL PAH's               60.7                       90.5                     1144.5                      336.3                       472.7
                (w/o PERYLENE)
                S&T Total PAHs            66.9                       53.2                     444.4                       187.2                       280.6





                                                            Mussel Watch Project Year 8 - Aromatics Data

                  INVEST#:               AESP                     CKBP                     TBNP                       TBMK                        TBPB
                     ID:           Apalachee Bay               Cedar Kay               Tampa Bay                  Tampa Bay                  Twnpa Bay
                    SITE            Spring Creek              Black Point             Navarez Park             Mullet Key Bayou             Papys Bayou
                LABSAMNO:                K7102                    K7100                    K71 10                     K7106                       K7118
               SAMPLE TYPE:              SAMP                     SAMP                     SAMP                       SAMP                        SAMP
                    UNIT-                ng/g                      ng/g                    ng/g                       ng/g                        ng/9
                Analyte (Cont)           Conc      DB QUAL         Conc    DB QUAL         Conc     DB QUAL           Conc        DB QUAL         Conc    DB QUAL


              2-METHYLNAPH 0              5.7          J            7.2                    32.6                       4.4                         5.4
              1-METHYLNAPH *              8.1                       4.3                    18.5                       3.3                         5.6

             2.6-DIMETHNAPH               5.5          J            5.7                    20.9                       4.5                         4.1

           2,3,5-TRIMETHNAPH              1.8          J           3           J           17.8                       3.2                         2.4         J

              I -METFIYLPHEN 0            1.4          J            1.5        J           7.2                        3.2                         3.9


            Surrogate Recoveries
                  NAPH138:               66.5                      51.6                    48.9                       59.9                        59.7
                  ACENDIO:               70.7                      65.9                    57.7                       84.1                        81.9
                  PHENDIG-               70.1                       70                     70.3                       75.4                        78
                  CHRYD12:               68.9                      57.1                    65.6                       64.4                        71.3
                  PERYD12:               63.1                      59.4                    57.1                       65.1                        62.7






                                                                   Mussel Watch Project Year 8 - Aromatics Data

                 INVEST#:                  TBOT                            TBKA                         TBHB                          TBCB                           CBBI
                   ID:               Tampa Bay                       Tampa Bay                    Tampa Bay                     Tampa Bay                    Charlotte Harbor
                  SITE             Old Tampa Bay                   Knights Airport                Hfflsborough                Cockroach Bay                     Bird Island
                 LABSAMNO:                 K7112                           K7108                        K7116                         K7114                          K7128
             SAMPLE TYPE:                  SAMP                            SAMP                         SAMP                          SAMP                           SAMP
                  UNIT:                    ng/g                            ng/g                         ng/g                          ng/g                           ng/g
             Analyte (Cont)                Conc       DB QUAL              Conc       DB QUAL           Conc      DB QUAL             Conc      DB QUAL              Conc         DB QUALI

            RECEIPT DATE:                  1/16/97                         1/16/97                      1/17/97                       1/17/97                        1/20/97
                 QCBATCH:                  M1235                           M1235                        M1235                         M1235                          M1235
          EXTRACTION DATE:                 9/18/97                         9/18/97                      9/18/97                       9/18/97                        9/18/97
                 METHOD;                   GCMS                            GCMS                         GCMS                          GCMS                           GCMS
            ANALYSIS DATE:                 10/31/97                        10/31/97                     II/l/97                       II/l/97                        II/l/97
                 METHOD:                   GCECD                           GCECD                        GCECD                         GCECD                          GCECD
            ANALYSIS DATE:                 8/24/98                         8/24/98                      8/24/98                       8/24/98                        8/24/98
                 MATRIX:                   TISSUE                          TISSUE                       TISSUE                        TISSUE                         TISSUE
                 SUBMAT:
                 WETWT-.                   15.07                           15.28                        14.75                         15.07                          8.11
                 DRYWT:                    1.98                            2.91                         2.78                          2.85                           1.11
                 WrUNITS:                  GRAMS          DRY              GRAMS         DRY            GRAMS        DRY              GRAMS         DRY              GRAMS            DRY
                 PCTSOLIDS:                13.10%                          19.00016                     18.900/6                      18.900/0                       13.700,6
                 Lipid. Weight:
        00       TOTAL LIPID:              5.49                            5.62                         6.97                          8.39                           4.23
                 LIPID UNITS:              % DRY                           % DRY                        % DRY                         % DRY                          % DRY
                   VOL:
                 VOLUNITS:                 LITERS                          LITERS                       LITERS                        LITERS                         LITERS
          Surrogate Recoveries
                  PAH's:
                 NAPHD8:                   45.1                            51.9                         52.4                          62.3                           57.3
                 ACENDIO:                  69.3                            64.5                         72                            78.2                           76.2
                 PHEND10:                  66.1                            75                           67.4                          81.4                           72.1
                 CHRYD12:                  67                              68.6                         62.8                          76                             72.7
                 PERYD12:                  49.7                            67.6                         58.2                          67                             57.2

            NAPHTHALENE 0                  12.4                            7.1                          10.7                          9.5                              15
           CI-NAPHTHALENES                 9.4                             8.8                          14.6                          19.3                           22.3
           C2-NAPHTHALENES                                 ND              20.1                         27.4                          28.1                                             ND
            C3-NAPHTHALENES                                ND              56.2                         49.4                          26.6                                             ND
            C4-NAPHTHALENES                                ND              65.3                         57.2                          24.2                                             ND
                 BIPHENYL *                1.6              1              3.3             1            3.6            1              2.4             1               3.4
            ACENAPHTHYLENE                 1.6              j              9.1                          6.5                           1.9             1               2.5
            ACENAPHTHENE*                  3.2                             4.7                          4.8                           1.3                             3.2
                 FLUORENE*                 3.3                             10                           9,8                            4                              7
             C 1 - F Ut i 0 R E 'NE-Sa                     IND             zz                           20.8                                         IND






                                                                Mussel Watch Project Year 8 - Aromatics Data

                INVEST#:                 TBOT                         TBKA                        TBHB                        TBCB                        CBBI
                    ID:              Tampa Bay                    Tampa Bay                  Tampa Bay                   Tampa Bay                  Charlotte Harbor
                   SITE            Old Tampa Bay                Knights Airport              Hillsborough              Cockroach Bay                   Bird Island
               LABSAMNO:                 K7112                        K7108                       K7116                       K7114                       K7128
               SAMPLE TYPE:              SAMP                         SAMP                        SAMP                        SAMP                        SAMP
                  UNIT-                  ng/g                         ng/g                        ng/g                        ng/g                        ng/g
               Analyte (Cont)            Conc       DB gUAL           Conc       DB gUAL          Conc      DB QUAL           Conc      DB gUAL           Co c         DB gUAL

               C2-FLUORENES,                           ND             63.1                        48.6                                      ND                            ND
               C3-FLUORENES                            ND             99.6                        147.6                                     ND                            ND
               PHENANTHRENE0             13.3                         21.5                        29.6                        8.5                          6.3
               ANTHRACENE4               6.2                          21.5                        29.8                        2              J             2.7             J
               CI-PHEN-ANT1-1R           17.6                         66.3                        103.4                       17.4                                        ND
               C2-PHEN-ANTfiR            20.5                         71.8                        94.5                        16.7                                        ND
               C3-PHEN-ANTHR                           ND             110.8                       216.9                                     ND                            ND
               C4-PHEN-ANTHR                           ND             61.4                        130.8                                     ND                            ND
               DIBENZOTHIO               1.5            J              2                          2.2                         1.1            J             2.4             J
                CI-DIBEN                               ND             12.8                        11.7                                      ND                            ND
                C2-DIBEN                               ND             31.3                        36.9                                      ND                            ND
                C3-DIBEN                               ND             31.8                        48.2                                      ND                            ND
               FLUORANTHENE              44.5                         114.6                       143.9                       10.7                         9.6
                PYRENEO                  32.4                         117.6                       117.3                       6.7                          7.3
          ,;"CI-FLUORAN    -PYR          24.1                         88.1                        113.8                       10                                          ND
          'gENaANTHRACENE                7.2                          19.1                        42.6                        1.1                          1.4             J
               CHRYSENE *                13.6                         50.7                        52.7                        4.3                          3.7             J
               CI-CHRYSENES              10.6                         30.9                        76.8                                      ND                            ND
               C2-CHRYSENES              6.1            J             19.6                        56.2                                      ND                            ND
               C3-CHRYSENES                            ND                            ND           11.5                                      ND                            ND
               C4-CHRYSENES                            ND                            ND           6.3                                       ND                            ND
               BENbFLUORAN               7.6                          19.5                        22.4                        0.8            J             1.5             J
               BENkFLUORAN                8                           20.7                        23.8                        0.9            J             1.6             J
               BENePYRENE *              7.6                          28.5                        28.5                        1.8                           2              J
               BENaPYRF,NE *             1.5            J             7.1                         3.5                         0.5            J             1.2             J
               PERYLENE, 0               2.6            J             2.7                         5.4                         0.7            J             0.8             J
               1123cdPYRENE              1.9                          4.5                         2.7                         0.4            J              I              J
               DBahANTHRA *              0.7            J             1.8                         1.8                         0.5            J             0.8             J
               BghiPERYLENE              2.7                          8.4                         20.4                        0.8            J             1.1             J

               TOTAL PAH's               258.9                        1331.3                      1828.8                      201.3                       95.8
               (w/o PERYLENE)
               S&T Total PAHs (*)        167                          445.3                       528.4                       88.4                        99.2






                                                            Mussel Watch Project Year 8 - Aromatics Data

              INVEST#:                TBOT                       TBKA                       TBHB                       TBCB                        CBBI
                 ID:             Tampa Bay                   Tampa Bay                  Tampa Bay                 Tampa Bay                 Charlotte Harbor
                SITE           Old Tampa Bay                Knights Airport            Hillsborough             Cockroach Bay                  Bird Island
            LABSAMNO:                 K7112                      K7108                      K7116                      K7114                       K7128
           SAMPLE TYPE:               SAMP                       SAMP                       SAMP                       SAMP                        SAMP
                UNIT:                 ng/g                        ng/g                      ng/g                       ng/g                        ng/g
            Analyte (Cont)            Conc      DB QUAL           Conc      DB QUAL         Conc     DB QUAL           Conc      DB QUAL           Conc       DB QUALI


          2-METHYLNAPH *              5.3                          3.4          J           9.2                        13.4                        15.2
          I-METHYLNAPH *              4.1                          5.4                      5.4                        5.9                         7.1

         2,6-DIMETHNAPH                2            J              5.8                      9.8                        9.6                         3.2            J

        2,3.5-TRIMETHNAPH             1.9           J             9                         9.8                        2.7                         7.5            J

          1-METHYLPHEN 4              3.6           J             11.5                      10.5                       2.7                         1.9            J



         Surrogate Recoveries
              NAPHD8:                 45.1                        51.9                      52.4                       62.3                        57.3
        01    ACENDIO:                69.3                        64.5                      72                         78.2                        76.2
        0     PHENDIO:                66.1                         75                       67.4                       81.4                        72.1
              CHRYD12:                67                          68.6                      62.8                       76                          72.7
              PERYD12:                49.7                        67.6                      58.2                       67                          57.2






                                                                     Mussel Watch Project Year 8 - Aromatics Data

                                  INVEST#:                    CBFM                         NBNB                         RBHC                            EVFU
                                     ID:             Charlotte Harbor                 Naples Bay                  Rookery Bay                      Everglades
                                    SITE                Fort Meyers                   Naples Bay               Henderson Creek                  Faka Union Bay
                                  LABSAMNO:                   K7126                        K7120                        K7122                           K7124
                                  SAMPLE TYPE:                SAMP                         SAMP                         SAMP                            SAMP
                                   UNIT:                      ng/g                         ng/g                         ng/g                            ng/g
                                  Analyte (Cont)              Cone        DB QUAL          Cone    DB QUAL              Cone        DB QUAL             Cone        1313 QUAL

                                  RECEIPT DATE:               1/20/97                      1/20/97                      1/20/97                         1/20/97
                                  QCBATCH:                    M1235                        M1235                        M1235                           M1235
                            EXTRACTION DATE:                  9/18/97                      9/18/97                      9/18/97                         9/18/97
                                  METHOD:                     GCMS                         GCMS                         GCMS                            GCMS
                             ANALYSIS DATE:                   11/1/97                      11/1/97                      11/1/97                         11/1/97
                                  METHOD:                     GCECD                        GCECD                        GCECD                           GCECD
                             ANALYSIS DATE*                   8/24/98                      8/24/98                      8/24/98                         8/24/98
                                  MATRIX:                     TISSUE                       TISSUE                       TISSUE                          TISSUE
                                  SUBMAT.-
                                  WETWT:                      15.11                        14.97                        14.92                           15.16
                                  DRYWT:                      2.45                         2.65                         2.68                            1.78
                                  WTUNITS:                    GRAMS          DRY           GRAMS      DRY               GRAMS          DRY              GRAMS          DRY
                                  PCTSOLIDS:                  16.200A                      17.700A                      17.900/6                        11.80%
                                  I.Apid Weight:
                                  TOTAL LIPID:                6.95                         6.33                         6.4                             6.02
                                  LIPID UNITS:                % DRY                        % DRY                        % DRY                           % DRY
                                    VOL.-
                                  VOLUNITS:                   LITERS                       LITERS                       LITERS                          LITERS
                            Surrogate Recoveries
                                   PAH's:
                                  NAPHD8:                     71.3                         55.4                         69.2                            43.7
                                  ACENDIO:                    79.7                         80                           75                              79.4
                                  PHENDIO:                    79.7                         70.8                         74.3                            72.6
                                  CHRYD12:                    73.3                         69.5                         74.9                            75.8
                                  PERYD12:                    64.6                         55.5                         66.5                            61.5


                             NAPH' TIIALENE                   8.9                          18.6                         10.5                            16.2
                            CI-NAPHTHALENES                   13.3                         44.5                         21.5                            41.4
                            C2-NAPHTHALENES                   18                           49.8                         23.1                            45.3
                            C3-NAPHTHALENES,                  21.6                         72.9                         22.2                            68.3
                            C4-NAPHITIALENES                  19.1                         90.8                         22.9                            62.3
                                  BIPHENYL 0                  3.8             J            3.2          J               3.5              J              4.5              J
                            ACENAPHTHYLENE                    2.1             J            2.3          J               0.9              J              2.2              J
                            ACENAPHTHENE*                     2.7             J            1.1          J                I               J              4.1              J
                                  FLUORENE*                   3.7             J            8.6                          2.4              J              5.3              J
                                  Cl-FLUORENES                9.6             J            20.6                         12.1                            14.7






                                                              Mussel Watch Project Year 8 - Aromatics Data

                            INVEST#:                  CBFM                       NBNB,                      RBHC                          EVFU
                                 ID:           Charlotte Harbor              Naples Bay                Rookery Bay                    Everglades
                               SITE               Fort Meyers                Naples Bay              Henderson Creek               Faka Union Bay
                           LABSAMNO:                  K7126                      K7120                      K7122                         K7124
                           SAMPLE TYPE:               SAMP                       SAMP                       SAMP                          SAMP
                              UNrr*                   ng/g                       ng/g                       ng/g                          ng/g
                           Analyte (Cont)             Cone        DB QUAL        Cone     DB QUAL           Cone       DB QUAL            Cone       DB QUALI

                           C2-FLUORENES                              ND          66.5                                      ND                            ND
                           C3-FLUORENES                              ND          106                                       ND                            ND
                        PHENANTHRENE*                 8.3                        13.2                       3.9                           3.7
                           ANTHRACENE0                5.2                        17.1                        4                            2.3            J
                        Cl-PHEN    ANTHR              32.1                       68.1                       26.4                          23.7
                        C2-PHEN    -ANTHR.            32.2                       103.3                      26.1                          35.3
                        C3-PHEN_ANTHR                                ND          141.1                                     ND                            ND
                        C4-PHEN-ANTHR                                ND          48.8                                      ND                            ND
                           DIBENZOTHIO                0.9             J          1.8                        0.3             J             1.6            J
                            Cl-DIBEN                   4                         6.6                                       ND                            ND
                            C2-DIBEN                  10.4                       20.2                                      ND                            ND
                            C3-DIBEN                  8.7                        29.5                                      ND                            ND
                        FLUORANTHENE                  40.9                       92.3                       15.7                          11.5
                            PYRENE0                   33.2                       106.1                      13.4                          13.1
                        Cl-FLUORAN     PYR.           24.9                       83.7                       17.8                          26.5
                       BENaANTHRACENE                 7.4                        15.9                       3.6                           1.9
                           CHRYSENEO                  22.8                       41.8                        4                            4.3            J
                           CI-CHRYSENES                9                         17.5                                      ND                            ND
                           C2-CHRYSENES               9.8                        7.9                                       ND                            ND
                           C3-CHRYSENES                              ND                      ND                            ND                            ND
                           C4-CHRYSENES                              ND                      ND                            ND                            ND
                           BENbFLUORAN                8.9                        10.9                       1.4             J              I             J
                           BENkFLUORAN                9.5                        11.6                       1.5             J             1.1            J
                           BENePYRENE 0               11.4                       16.9                       2.4                           2.1
                           BENaPYRENE 0               1.6             J          1.6          J             0.8             J             0.6            J
                           PERYLENE0                  1.6             J          1.5          J             0.8             J             0.6            J
                           1123cdPYRENE               1.7                        1.4                        0.7             J              1             J
                           DBahANTHRA*                0.5             J          0.8          J             0.5             J             0.5            J
                           BghtPERYLENE               3.3                        6.7                        1.3                           1.9

                           TOTAL PAH's                389.1                      1349.7                     243.7                         396.4
                           (w/o PERYLENE)
                        S&T Total PAHs N              178.6                      425                        104.4                         132.2






                                                                  Mussel Watch Project Year 8 - Aromatics Data

                                INVEST#:                  CBFM                        NBNB                        RBHC                          EVFU
                                   ID:             Charlotte Harbor               Naples Bay                Rookery Bay                     Everglades
                                  Srm                Fort Meyers                  Naples Bay              Henderson Creek                Faka. Union Bay
                              LABSAMNO:                   K7126                       K7120                       K7122                         K7124
                             SAMPLE TYPE:                 SAMP                        SAMP                        SAMP                          SAMP
                                  UNn%                    ng/g                        ng/g                        ng/g                          ng/g
                             Analyte (Cont)               Conc        DB QUAL         Conc     DB QUAL            Conc       DB QUAL            Conc        DB QUALI


                           2-MEI1rfLNAPH                   8                          27.4                        14.2                          26.7
                           I-METHYLNAPH*                  5.3                         17.1                        7.3                           14.7


                          2,6-DIMETHNAPH                  6.2                         14.5                        8.3                           10.6

                         2,3.5-TRIMETHNAPH d'             3.2              J          13.6                        4.8                           5.3             J


                           I -MLFHYLPHEN 0                4.1                         13.9                        3.3                           4.1             J



                          Surrogate Recoveries
                                NAPHD8:                   71.3                        55.4                        69.2                          43.7
                                ACENDIO:                  79.7                        80                          75                            79.4
          01                    PHENDIO:                  79.7                        70.8                        74.3                          72.6
          CO                    CHRYD12:                  73.3                        69.5                        74.9                          75.8
                                PERYD12:                  64.6                        55.5                        66.5                          61.5






                                                                   Mussel Watch Project Year 8 - Aromatics Data

                                             INVEST#:                   PFBB                                PR13M                         PRBJ
                                               ID:                  Puerto Rico                      Puerto Rico                    Puerto Rico
                                              SITE              Bahia de Boquieron                 Bahia Montalva                 Bahia de Jobos
                                             IABSAMNO:                  R7130                               K7132                         K7134
                                        SAMPLE TYPE:                    SAMP                                SAMP                          SAMP
                                              UNIT-                     ng/g                                ng/g                          ng/g
                                         Analyte (Cont)                 Conc           DB QUAL              Conc      DB QUAL,            Conc       DB QUALI

                                        RECEIPT DATE:                   1/21/97                             1/22/97                       1/23/97
                                             QCBATCH:                   M1235                               M1235                         M1235
                                      EXTRACTION DATE:                  9/18/97                             9/18/97                       9/18/97
                                             METHOD:                    GCMS                                GCMS                          GCMS
                                       ANALYSIS DATE:                   11/1/97                             11/1/97                       11/1/97
                                             METHOD:                    GCECD                               GCECD                         GCECD
                                       ANALYSIS DATE:                   8/24/98                             8/24/98                       8/25/98
                                             MATRIX:                    TISSUE                              TISSUE                        TISSUE
                                             SUBMAT:
                                             WETWT:                       9.4                               6.64                          8.22
                                             DRYWT-                       1.89                              1.03                          1.39
                                             WTUNITS:                   GRAMS             DRY               GRAMS         DRY             GRAMS          DRY
                                             PCTSOLIDS:                 20. 1 OOA                           15.500/6                      16.900/6
                                             Lipid Weight:
                                             TOTAL LIPID:                 6.2                               2.3                           3.77
                                             LIPID UNITS:               % DRY                               % DRY                         % DRY
                                              VOL.-
                                             VOLUNTrS:                  LITERS                              LITERS                        LITERS
                                      Surrogate Recoveries
                                              PAH's:
                                             NAPHD8-.                     65.9                              65.3                          59
                                             ACENDIO:                     72.8                              73.9                          70.6
                                             PHENDIO:                     82.3                              79.2                          77.3
                                             CHRYD12:                     74.1                              72                            68.2
                                             PERYD12:                     62                                59.2                          54.6


                                         NAPFITHALENE                     10.7                              21.5                          15.7
                                      CI-NAPHTHALENES                     8.3               J               16              J             11.1            J
                                      C2-NAPHTHALENES                     13.5                                              ND                           ND
                                      C3-NAPHTHALENES                     34.6                                              ND                           ND
                                      C4-NAPHTTIALENES                                     ND                               ND                           ND
                                             BIPHENYL *                   2.5               J               6               J             4.7             J
                                      ACENAPHTHYLENE                      0.9               J               1.6             J             1.5             J
                                        ACENAPHTHENE*                     1.2               J               2.7             J             1.8             J
                                             FLUORENE                     3.3               J               2.7             J             4.9             J
                                         Cl-FLUOREENESS                                                                                                  114 LJ






                                                             Mussel Watch Project Year 8 - Aromatics Data

                                        INVESr#:                  PRBB                        PRBM                          PRBJ
                                           ID:                Puerto Rico                  Puerto Meo                 Puerto Rico
                                          SITE           Bahia de Boquieron              Bahia Montalva              Bahia de Jobos
                                      LABSAMNO:                   K7130                       K7132                         K7134
                                      SAMPLE TYPE:                SAMP                        SAMP                          SAMP
                                          UNIT.                   ng/g                        ng/g                          ng/g
                                      Analyte (Cont)              Conc        DB QUAL         Conc        DB QUAL           Conc     DB QUALI

                                      C2-FLUORENES                               ND                          ND                         ND
                                      C3-FLUORENES                               ND                          ND                         ND
                                      PHENANMRENEO                2.6                           5                           6
                                      ANTHRACENE*                 0.9             J            2.9            J             2.4          J
                                      CI-PHEN@_ANMR               22.7                                       ND             9.7          J
                                      C2-PHEN-ANTHR               16.2                                       ND             11           J
                                      C3-PHEN-ANTHR                              ND                          ND                         ND
                                      C4-PliEN_ANMR                              ND                          ND                         ND
                                      DIBENZOTH10                 0.6             J            1.3            J             0.7          J
                                        Cl-DIBEN                                 ND                          ND                         ND
                                        C2-DIBEN                                 ND                          ND                         ND
                                        C3-131BEN                                ND                          ND                         ND
                                      FLUORANTHENE*               6.5                          6.9                          19.4
                                        PYRENE 0                  6.7                           5                           8.5
                                      Cl.-FLUORAf@_PYR            11.4                                       ND                         ND
                                 BENaANTHRACENE*                  1.2             J            1.8            J             4.6
                                      CHRYSENE *                  2.6             J            4.8            J             6.7
                                      CI-CHRYSENES                               ND                          ND                         ND
                                      C2-CHRYSENES                               ND                          ND                         ND
                                      C3-CHRYSENES                               ND                          ND                         ND
                                      C4-CHRYSENES                               ND                          ND                         ND
                                      BENbFLU0RAN                 0.8             J             2             J             2.6          J
                                      BENkFLUORAN                 0.8             J            2.2            J             2.8          J
                                      BENePYRENE 0                1.2             J            2.4                          2.6
                                      BENaPYRENE *                0.3             J            1.5            J             1.2          J
                                      PERYLENEO                    1              J            0.5            J             0.7          J
                                      I123cdPYRENE                0.3             J            1.5            J             I            J
                                      DBahANTHRA *                0.6             J            0.8            J             0.7          J
                                      BghIPERYLENE                0.6             J            1.8            J             2.3

                                      TOTAL PAH's                 150.9                       90.2                          121.7
                                      (w/o PERYLENE)
                                      S&T Total PAHs (0)          57.3                        88.6                          100.8







                                                          Mussel Watch Project Year 8 - Aromatics Data

                                      INVEST#:                 PRBB                          PRBM                       PRBtJ
                                         ID:               Puerto Rico                  Puerto Rico                Puerto Rico
                                        Srm            Bahia de Boquieron             Bahia Montalva              Bahia de Jobos
                                    LABSAMNO:                  K7130                         K7132                      K7134
                                   SAMPLE TYPE:                SAMP                          SAMP                       SAMP
                                       UNrr..                  ng/g                          ng/g                       ng/g
                                   Analyte (Cont)              Cone        DB QUAL           Conc      DB QUAL          Cone      DB QUAL



                                 2-MElTrILNAPH *               4.6             J             9.7           J            6.6           J
                                 I -METHYLNAPH *               3,7             J             6.3           J            4.6           J


                                2,6-DIMETHNAPH                 4.2             J             3.4           J             5            J


                               2.3,5-TRIMETHNAPH               1.5             J             2.3           J            1.1           J


                                 I -MErHYLPHEN *                2              J             2.7           J            3.9           J



                                Surrogate Recoverles
                                      NAPHD8:                  65.9                          65.3                       59
                                      ACENDIO:                 72.8                          73.9                       70.6
                                      PHENDIO-                 82.3                          79.2                       77.3
                                      CHRYD12:                 74.1                          72                         68.2
                                      PERYD12:                 62                            59.2                       54.6




















                                           - -Mumma wo M M M @ M M M M M @ M =



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                                                           Mussel Watch Project Year 8 - Aromatic QC Data


                          INVEST#:          LAB QA SAMPLE                 LAB QA SAMPLE                     GBYC                 LAB QA SAMPLE
                             ID:              PROC BLANK                   SPIKE BLANK                 Galveston Bay                    GBYC ,
                            SITE:                                                                       Yacht Club                 Galveston Bay
                          IABSAMNO:                Q6336                        Q6337                       K7004                       Q6338
                          SAMPLE TYPE:             BLANK                        LBS                         SAMP                    DUPLICATE


                          RECEIP`r DATE:                                                                    12/10/92                    12/10/92
                          QCBATCH-                 M1232                        M1232                       M1232                       M1232
                    EXTRACTION DATE:               9/14/93                      9/14/93                     9/14/93                     9/14/93
                          METHOD:                  GCMS                         GCMS                        GCMS                        GCMS
                      ANALYSIS DATE.               10/19/93                     10/19/93                    10/19/93                    10/19/93
                          MEI'HOD:                 GCECD                        GCECD                       GCECD                       GCECD
                      ANALYSIS DATE:               7/31/94                      7/31/94                     7/29/94                     7/31/94
                          MATRIX:                  TISSUE                       TISSUE                      TISSUE                      TISSUE
                          SUBMAT:
                          WETWT:                                                                            15.69                       15.07
                          DRYW71%                  10                            10                         2.85                        2.68
                          WMNITS:                  GRAMS         DRY            GRAMS         DRY           GRAMS        DRY            GRAMS         DRY
                          PCTSOLJDS:                                                                        18.10%                      17.80%
                          Lipid Weight-
      CA                  TOTAL LIPID:                           NA                            NA           8.38                        8.17
      00                  LIPID UNITS:             % DRY                        % DRY                       % DRY                       % DRY
                            VOL:
                          VOLUNrrS:                LITERS                       LITERS                      LITERS                      LITERS
                    Surrogate Recoveries
                           PAH's:
                          NAPHD8:                  64.2                         70.2                        52.6                        54.7
                          ACEND10.                 68.9                         67.5                        58.2                        70.1
                          PHENDIO:                 62.5                         82.3                        69.6                        68.3
                          CHRYD12:                 59.9                         65.4                        70.3                        65.8
                          PERYD12:                 45.7                         43.7                        54.9                        60.6
                   PESTICIDES & PCB's:
                          DBOFB:                   75.5                         76.5                        71.8                        70.1
                          PCB# 103:                83                           84.6                        59.5                        68.1
                          PCB# 198:                79.7                         76.6                        68.8                        72.6

                           UNIT:                   ng/g                          %                          ng/g                        ng/g
                          PNA Analyte              Conc       DB QUAL       % RECOV        DB QUAL          Conc      DB QUAL           Conc       DB QUAL

                       NAPHTHALENE                 0.5            J             80.6                        6.4                         6.4






                                                             Mussel Watch "ect Year 8 - Aromatic QC Data


                            INVESr#:          LAB QA SAMPLE                 LAB QA SAMPLE                       GBYC                 IAB9A9WRR
                               ID:              PROC BLANK                    SPIKE BLANK                 Galveston Bay                     GBYC
                              Srm:                                                                         Yacht Club                 Galveston Ba@
                           LABSAMNO:               Q6336                         Q6337                          X7004                       Q6338
                         SAMPLE TYPE,              BLANK                           LBS                          SAMP                    DUPLICATE

                         Cl-NAPHTHALENES             0.9             j                            NA            6.6                         5.4             j
                         C2-NAPHTHALENES                             ND                           NA            11.8                        12.6
                         C3-NAPHTHALENES                             ND                           NA            47.5                        51.2
                         C4-NAPHTHALENES                             ND                           NA            94.8                        83
                          BIPHENYL *                 0.5             j             84.3                         3.1           j             3.4             j
                         ACENAPHTHYLENE               0              1             81.6                         3.7                         3.5             j
                         ACENAPHTHENE*               0.3             j              80                          2.8           j               2
                          FLUORENE*                  0.3             1             87.4                         3.7           1             4.4
                         CI-FLUORENES                                ND                           NA            25                          24.6
                         C2-FLUORENES                                ND                           NA            101.5                       97
                         C3-FLUORENES                                ND                           NA            202.3                       209.2
                         PHENANTHRENEO               0.3             j             68.3                         12                          14.1
                         ANTHRACENE*                 0.2             1             55.1                         10.6                        10.3
                         Cl-PHEN_ANTHR                               ND                           NA            42.7                        50.1
         U1              C2-PliEN_ANTfiR                             ND                           NA            127.3                       146.1
         to              C3-PHEN ANTHR                               ND                           NA            224                         266.6
                         C4-PHEN_AN-THR                              ND                           NA            173                         231.7
                         DIBENZOTHIO                 0.1             1             63.6                         2.5                         2.7
                            Cl-DIBEN                                 ND                           NA            12.6                        15.7
                            C2-DIBEN                                 ND                           NA            46.1                        54
                            C3-DIBEN                                 ND                           NA            60.8                        69.1
                         FLUORANTHENE*               0.1             1             75.2                         43.7                        46.2
                            PYRENEO                  0.2             1             71.9                         61.3                        71.2
                         Cl-FLUORAN_PYR                              ND                           NA            62.4                        96.3
                      BENaANTHRACENE                 0.1             1             90.5                         13.3                        9.7
                         CHRYSENE *                  0.1             j             74.2                         31.2                        42.1
                         Cl-CHRYSENES                                ND                           NA            24.8                        25.4
                         C2-CHRYSENES,                               ND                           NA            29.8                        31.4
                         C3-CHRYSENES                                ND                           NA                         ND                            ND
                         C4-CHRYSENES                                ND                           NA                         ND                            ND
                         BENbFLUORAN                  0              1             63.6                         5                           5.4
                         BENkFLUORAN                  0              1             83.4                         6.5                         7.1
                         BENePMENE *                  n              .1            71 @9                        10.A                        12A
                         BENaPYRENE *                 0              1             55.3                         1.6           j             2.2




                         = = M M M M M M M = Ows -






                                                             Mussel Watch Project Year 8 - Aromatic QC Data


                           INVESr#:          LAB QA SAMPLE                 LAB QA SAMPLE                       GBYC                  LAB QA SAMPLE
                              ID:              PROC BLANK                    SPIKE BLANK                 Galveston Bay                    GBYC ;
                             SITE:                                                                         Yacht Club                 Galveston Bay
                         LABSAMNO:                Q6336                           Q6337                        K7004                      g6338
                        SAMPLE TYPE:              BLANK                           LBS,                         SAMP                    DUPLICATE


                         PERYLENE*                  0.1             J             114.5                        2.8                          3.7
                         1123cdPYRENF,              0.1             J             65.2                         0.9                           1
                       DBahANTHRA *                 0.1             J             79.2                         0.9           J              1.6
                        BghIPERVLENE                 0              J             63.7                         2.1                          2.4

                         TOTAL PAH's                3.7                     AVG % RECOV                        1514.8                     1717.9
                        (w/o PERYLENE)                                             79
                       S&T Total PAHs (*)           4.2                                                        234.5                      258.6


                       2-METHYLNAPH 0               0.4             J             124.9                        3.7                          2.8             J
                       I -MEMiYLNAPH *              0.5             J             88.3                         2.9                          2.6


                      2.6-DIMETHNAPH                0.3             J             80.1                         4.7                          4.4


                    2,3,5-77UMETHNAPH               0.3             J             106.6                        10.1                         8.9

        0
                       1 -METHYLPHEN                0.1             J             67.5                         9.2                          9.7


                     Surrogate Recoveries
                           NAPHD8:                  64.2                          70.2                         52.6                         54.7
                           ACEND10:                 68.9                          67.5                         58.2                         70.1
                           PHENDIO:                 62.5                          82.3                         69.6                         68.3
                           CHRYD12:                 59.9                          65.4                         70.3                         65.8
                           PERYD12:                 45.7                          43.7                         54.9                         60.6






                                                              Mussel Watch "ect Year 8 - Aromatic QC Data


                           INVEST#:          LAB QA SAMPLE                   LAB QA SAMPLE                  LAB QA SAMPLE                        VBSP
                              ID:                    GBYC                     PROC BLANK                     SPIKE BLANK                   Verrnillion 134y
                             SITE:             Galveston Bay                                                                               Southwest Pass
                           LABSAMNO:                 Q6339                        Q6340                          Q6341                           K7046
                       SAMPLE TYPE:                  MS                           BLANK                            LBS                           SAMP

                      RECEIPT DATE:                  12/10/92                                                                                    1/6/93
                           QCBATCH:                  M 1232                       M1233                          M1233                           M1233
                    EXTRACTION DATE:                 9/14/93                      9/14/93                        9/14/93                         ll/II/93
                           METMOD:                   GCMS                         GCMS                           GCMS,                           GCMS,
                      ANALYSIS DATE-                 10/19/93                     7/14/94                        10124/93                        12/23/93
                           METHOD:                   GCECD                        GCECD                          GCECD                           GCECD,
                      ANALYSIS DATE:                 7/31/94                      8/24/94                        8/24/94                         8/23/94
                           MATRDC-                   TISSUE                       TISSUE                         TISSUE                          TISSUE
                           SUBMAT:
                           WETWT-                    15.13                                                                                       15.08
                           DRYWT-                    2.75                             10                            10                           1.78
                           WTUNITS:                  GRAMS          DRY           GRAMS            DRY           GRAMS            DRY            GRAMS          DRY
                           PCTSOLIDS:                18.20%                                                                                      11.800/6
                           Lipid Weight:
                           TOTAL LIPID:              8.38                                           NA                             NA            9.78
                           LIPID UNITS:              % DRY                        % DRY                          % DRY                           % DRY
                             VOL:
                           VOLUNITS:                 LITERS                       LITERS                         LITERS                          LITERS
                    Surrogate Recoveries
                             PAH's:
                           NAPHD8:                   48.6                           75.3                           61.5                          58.4
                           ACENDIO:                  58.4                           66.7                           64.4                           57
                           PHENDIO:                   69                            62.4                            67                           70.7
                           CHRYD12:                   63                            65.1                           56.4                          69.1
                           PERYD12:                  55.8                           41.4                           33.1                          60.6
                    PESTICIDES & PCB'9:
                           DBOFB:                    73.2                           80.3                           73.6                          70.3
                           PCB# 103:                 72.2                           90.5                           85.2                          53.2
                           PCB#198:                  71.8                           79.4                           75.1                          50.6

                             UNIT-.                    %                            ng/g                            %                            ng/g
                           PNA Analyte               % RECOV     DB QUAL            Conc        DB QUAL          % RECOV        DB QUAL          Conc        DB QUAL

                      NAPHTHALENE                    87.3                            0.5             1              95                           15.6






                                                          Mussel Watch Project Year 8 - Aromatic QC Data


                         INVEST#:          LAB QA SAMPLE               LAB QA SAMPLE                LAB 9A SAMPLE                     VBSP
                            ID:                   GBYC                   PROC BLANK                   SPIKE BLANK                Vermillion Bay
                           SfTE:            Galveston Bay                                                                        Southwest Pass
                        LABSAMNO:                 Q6339                     Q6340                        Q6341                       K7046
                      SAMPLE TYPE:                MS                        BLANK                         LBS                         SAMP


                    Cl-NAPIrMAIENES                             NA            0.7            1                            NA            17.2
                    C2-NAPHTHALENES                             NA                           ND                           NA            20
                    C3-NAPh`THALENES                            NA                           ND                           NA            23.3
                    C4-NAPHTfIALENES                            NA                           ND                           NA            37.3
                       BIPHENYL 0                 80.9                        0.4            1            88.7                          ra. 3         J
                    ACENAPHTHYLENE                83                          0.1            1            90.8                          2             1
                    ACENAPHTHENEO                 71.4                        0.2            1            88.6                          3             J
                        FLUORENE*                 85.1                        0.2            J            93.6                          7.2
                      CI-FLUORENES                              NA                           ND                           NA            13.9
                      C2-FLUORENES                              NA                           ND                           NA            56.4
                      C3-FLUORENES                              NA                           ND                           NA            67
                    PHENANTHRENEO                 61.9                        0.6                         71.1                          19.8
                      ANTHRACENEO                 47.8                        0.1            1            71.8                          3             1
                      CI-PHEN,ANTHR                             NA                           ND                           NA            21.3
                      C2-PHEN_ANTHR                             NA                           ND                           NA            44
                      C3-PHEN_ANTIiR                            NA                           ND                           NA            82.6
                      C4-PHEN_ANTHR                             NA                           ND                           NA            71
                      DIBENZOTHIO                 64.6                        0.5                         71.1                          1.5           1
                         CI-DIBEN                               NA                           ND                           NA            6.4
                         C2-DIBEN                               NA                           ND                           NA            13.9
                         C3-DIBEN                               NA                           ND                           NA            14.5
                    FLUORANTHENEO                 66.3                        0.2            J            88.4                          15.5
                         PYRENE*                  78.7                        0.4                         85.2                          20.8
                    Cl-FLUORAN-PYR                              NA                           ND                           NA            22.9
                    BENaANTHRACENF,               105.9                       0.1            J            102.9                         1.8
                       CHRYSENE *                 76.7                         0             1            87.1                          8.1
                      CI-CHRYSENES                              NA                           ND                           NA            4.7
                      C2-CHRYSENES                              NA                           ND                           NA            9.1
                      C3-CHRYSENES                              NA                           ND                           NA                         NI)
                      C4-CHRYSENES                              NA                           ND                           NA                         ND
                      BENbFLUORAN                 69                           0             1             89                           1.1
                      BENkFLUORAN                 90.5                         0             1            83.5                          1.1
                      BENePYRENE 0                78                           0             1            99.9                          2.3
                      BENaPYRENE*                 73.6                         0             J            93.6                          1.2           J






                                                         Mussel Watch Project Year 8 - Aromatic QC Data


                         INVEST#:         LAB QA SAMPLE                LAB QA SAMPLE                LAB QA SAMPLE                      VBSP
                           ID:                    GBYC                  PROC BLANK                   SPIKE BLANK                 Vernifflon. Eky
                          SITE:            Galveston Bay                                                                        Southwest Pass
                       LABSAMNO:                  Q6339                     Q6340                         Q6341                        K7046
                     SAMPLE TYPE:                 MS                        BLANK                         LBS                          SAMP


                       PERYLENE 0                 103.5                       0.2            J            74.1                         6.4
                      1123cdPYRENE                90.1                        0              J            81.8                         0.7
                     DBahANTHRA 0                 111.8                       0              J            100.6                        2.1           J
                      BghiPERYLENE                87.1                        0.1            J            84.2                         1.1           J

                      TOTAL PAH's          AVG % RECOV                        3.9                    AVG % RECOV                       639.6
                      (w/o PERYLENE)              84.2                                                    90.9
                    S&T Total PAHs (*)                                        4.1                                                      146.2


                    2-METHYLNAPH *                144.6                       0.4            J            149.4                        8.9
                    I-METHYLNAPH *                92                          0.3            J            106.2                        8.3


                   2,6-DIMETUNAPH                 75.1                        0.2            J            84.6                         6.4


                  2.3,5-TRIMETHNAPH               105                         0.1            J            116.6                        4.2           J


                     I -METHYLPHEN                74.9                        0.4            J            75.6                         5.3


                   Surrogate Recoveries
                         NAPHD8:                  48.6                        75.3                        61.5                         58.4
                         ACENDIO:                 58.4                        66.7                        64.4                         57
                         PHENDIO:                 69                          62.4                          67                         70.7
                         CHRYD12:                 63                          65.1                        56.4                         69.1
                         PERYD12:                 55.8                        41.4                        33.1                         60.6






                                                            Mussel Watch Project Year 8 - Aromatic QC Data


                          INVEST#:         LAB QA SAMPLE                 LAB 9A SAMPLE                IAB QA SAMPLE                 LAB GA SAMPIZ
                            ID:                   VBSP                          VBSP                    PROC BLANK                   SPIKE BLANK
                           SITE1.           Vermillion Bay                Vermillion Bay
                          LABSAMNO:               P6342                         Q6343                       Qw"                           Q6345
                      SAMPLE 7YPE:            LUPLICATE                         MS                          BLANK                          LBS

                      RECEIP`r DATE:              1/6/93                        1/6/93
                          QCBATCH:                M1233                         M1233                       M1234                         M1234
                   EXTRACTION DATE:               9/14/93                       9/14/93                     9/16/93                       9/16/93
                          ML-17HOD,               GCmS                          Gems                        GCMS                          GCMS
                     ANALYSIS DATE:               10/24/93                      10/24/93                    10/28/93                      10/28/93
                          METHOD:                 GCECD                         GCECD                       GCECD                         GCECD
                     ANALYSIS DATE:               8/24/94                       8/25/94                     8/24/94                       8/24/94
                          MATRDL-                 TISSUE                        TISSUE                      TISSUE                        TISSUE
                          SUBMAT.
                          WETwr-                  15.1                          15.2
                          DRYWT.                  2.2                           2.37                          10                            10
                          WTUNITS:                GRAMS         DRY             GRAMS         DRY           GRAMS          DRY            GRAMS          DRY
                          PCTSOLIDS:              14.60%                        15-60%
                          I.Apid Weight:
       0)                 TOTAL LIPID:            13.2                          12.59                                       NA                            NA
       &-                 LIPID UNTM:             % DRY                         % DRY                       % DRY                         % DRY
                           VOL,
                          VOLUNIT"S:              LITERS                        LTTERS                      LTMRS                         LITERS
                   Surrogate Recoveries
                          PAH's:
                          NAPHD8:                 63.8                          48.3                          58.5                         65.4
                          ACENDIO:                62.2                          65.4                          66.7                         67.9
                          PHENDIO:                59.8                          64.1                          69                           81.2
                          CHRYD12,                54.5                          51.1                          67.8                         68.8
                          PERYD12:                46                            41.3                          2.5            Q             57.8
                   PESTICIDES & PCB's:
                          DBOFB:                  75.5                          71.7                          77.4                         73.3
                          PCB# 103:               86.5                          87.5                          87.2                         77.6
                          PCB#198:                75.6                          75.5                          83.4                         71.8

                           UNn-                   ng/g                          %                             ng/g                          %
                          PNA Analyte             Conc        DB QUAL           % RECOV    DI3 gUAL           Conc       DB QUAL          %RECOV       DB QUAL

                     NAPHTHALENE                  6,7                           92.8                          0.8            J             87







                                                        Mussel Watch Project Year 8 - Aromatic QC Data


                      iNVEST#:         LAB 9A SAMPLE                 LAB QA SAMPLE               LAB QA SAMPLE                LAB QA KUM
                         ID,                  VBSP                         VBSP                    PROC BLANK                   SPOE BLANK
                        Srm:             Vern-dIllan Say              Vermillion Bay
                     LABSAMNO:                96342                        Q6343                      Q6344                        Q6345
                   SAMPLE IYPE:           DUPLICATE                         MS                        BLANK                          LBS


                   Cl-NAPHTHALENES              11.2                                      NA            0.8            J                            NA
                   C2-NAPHTHALENES              11.6                                      NA                           ND                           NA
                   C3-NAPHTHALENES              38                                        NA                           ND                           NA
                   C4-NAPHTHALENES              33.8                                      NA                           ND                           NA
                     BIPHENYL 0                 3.8           J             75.4                        0.5            J             93.4
                   ACENAPHTHYLENE               1.7           J             86.7                        0.1            J             93.8
                   ACENAPHTHENEO                1.2           J             77.6                        0.3            J             89.6
                     FLUORENE*                  4             J             81.5                        0.2            J             97.9
                   CI-FLUORENES                               ND                          NA                           ND                           NA
                   C2-FLUORENES                               ND                          NA                           ND                           NA
                   C3-FLUORENES                               ND                          NA                           ND                           NA
                   PHENANTHRENE*                14.2                        57.9                        0.2            J             78.1
                   ANTHRACENEO                  3             J             59.6                        0.2            J             75.5
                   CI-PREN-ANTHR                              ND                          NA                           ND                           NA
                   C2-PHEN-AM-HR                48.4                                      NA                           ND                           NA
                   C3-PHEN@ANTHR                              ND                          NA                           ND                           NA
                   C4-PHEN-ANTHR                              ND                          NA                           ND                           NA
                   DIBENZOTHIO                  1.4           J             72.4                        0.1            J             71.5
                      CI-DIBEN                  6.1                                       NA                           ND                           NA
                      C2-DIBEN                  19,3                                      NA                           ND                           NA
                      C3-DIBEN                  18.7                                      NA                           ND                           NA
                   FUJORANTHENE                 15,3                        77                          0.2            J             89.3
                      PYRENE#                   20.1                        75                          0.2            J             86.1
                   CI-FLUORAN_M                 23.7                                      NA                           ND                           NA
                   BENaANTHRACENE               0.7           J             101                          0             J              97
                     CHRYSENE *                 6.8                         80.6                        0.1            J             96.1
                   CI-CHRYSENES                               ND                          NA                           ND                           NA
                   C2-CHRYSENES                               ND                          NA                           ND                           NA
                   C3-CHRYSENES                               ND                          NA                           ND                           MA
                   C4-CHRYSENES                               ND                          NA                           ND                           NA
                   BENbFLUORAN                  1.4           J             90.1                        0.1            J             90.3
                   BENkFLUORAN                  1.3           J             84.4                        0.1            J             96.2
                   BENePYRENE 0                 2.3                         451@2                        0             i             nr.0
                   BENaPYRENE *                 0.3           J             85.4                        0.1            J             86.4






                                                          Mussel Watch Project Year 8 - Aromatic QC Data


                         INVEST#:         LAB QA SAMPLE                LAB QA SAMPLE               LAB QA SAMPLE                LAB QA SAMPLE
                           ID:                  VBSP                         VBSP                    PROC BLANK                   SPIKE BIANK
                          SITE:           Vennfillon Bay                Vernifflon Bay
                      1ABSAMNO:                 Q6342                        Q6343                      Q6344                         Q6U5
                     SAMPLE TYPE:           DUPLICATE                         MS                        BLANK                          LBS


                      PERYLENE 0                6.9                          111.3                        0.2            J             119.9
                      1123cdPYRENE              0.4             J            86.2                         0.1            J             96.7
                     DBahANTHRA *               0.2             J             107                           0            J             114.5
                      BghIPERYLENE              0.7             J            87.8                         0.1            J             93.4

                      TOTAL PAH's               296.2                  AVG % RECOV                        4.2                    AVG % RECOV
                     (w/o PERYLENE)                                          88.4                                                      95.1
                    S&T Total PAHs (0)          109                                                         5


                    2-METHYLNAPH 0              6.9                          165.7                        0.5            J             138.2
                    1-MEIMYLNAPH 0              4.3                          107.1                        0.4            J             102.4


                    2,6-DIMETHNAPH              5.7                          74.3                         0.7            J             93.2

                  2.3.5-TRIML-MNAPH               4             J            105.6                        0.4            J             120.9          Q

                    I -METHYLPHEN 0             2.8             J            72.7                         0.1            J             74


                  Surrogate Recoveries
                         NAPHD8:                63.8                         48.3                         58.5                         65.4
                        ACENDIO:                62.2                         65.4                         66.7                         67.9
                        PHEND10:                59.8                         64.1                         69                           81.2
                        CHRYD12:                54.5                         51.1                         67.8                         68.8
                        PERYD12:                46                           41.3                         2.5            Q             57.8






                                                          Mussel Watch Project Year 8 - Aromatic QC Data


                       INVEST#:                MSPB                    LAB QA SAMPLE                 LAB QA SAMPLE                  LAB QA SAMPLE
                         ID:            Mississippi Sound                     MSPI3                          MSPB                    PROC BLANK
                        SITE:            Pascagoula Bay                Mississippi Sound             Mississippi Sound
                       LABSAMNO:               K7078                          Q6346                          Q6347                       Q6348
                   SAMPLE ITPE:                SAMP                       DUPLICATE                          MS,                         BLANK


                  RECEIP`r DATE:               1/10/93                        1/10/93                        1/10/93
                       QCBATCH:                M1234                          M1234                          M1234                       M1235
                EXTPAC11ON DATE:               9/16/93                        9/16/93                        9/16/93                     9/17/93
                       METHOD:                 GCMS,                          GCMS                           GCMS                        GCMS
                  ANALYSIS DATE:               10/28/93                       10/28/93                       10/28/93                    10/30/93
                       METHOD:                 GCECD                          GCECD                          GCECD                       GCECD
                  ANALYSIS DATE:               8/23/94                        8/24/94                        8/24/94                     8/24/94
                       MATRIX:                 TISSUE                         TISSUE                         TISSUE                      TISSUE
                       SUBMAT-
                       WETWT.                  15.34                          15.35                          15.15
                       DRYWT.                  1.93                           1.94                           1.92                           10
                       W'I'UNITS:              GRAMS          DRY             GRAMS          DRY             GRAMS         DRY           GRAMS           DRY
                       PCTSOIIDS:              12.60%                         12.700/6                       12.700/6
                       Lipid Weight:
                       TOTAL LIPID:            9.62                           10.37                          9.26                                        NA
                       LIPID UNM:              % DRY                          % DRY                          % DRY                       % DRY
                        VOL:
                       VOLUNI'M                LITERS                         L1TERS,                        LITERS                      LITERS
                Surrogate Recoveries
                        PAH's:
                       NAPHD8:                  49                            53.4                           54.6                         64.6
                       ACENDIO:                70.1                           67.8                           72.7                         84.1
                       PHEND10:                69.5                           70.9                           80.4                         69.9
                       CHRYD12:                 64                            67.9                           62.5                         73.5
                       PERYD12:                66.1                           64.9                           70.9                         49.1
                PESTICIDES & PCB's:
                       DBOF'B:                 74.4                           75                             75.1                           67
                       PCB#103:                82.4                           77.8                           76.1                         63.3
                       PCB# 198:               77.6                           83.7                           84.5                         70.6


                        UNIT-                  ng/g                           ng/g                           %                            ng/g
                       PNA Analyte             Cone         DB QUAL           Cone        DB QUAL            % RECOV     DB QUAL          Cone        DB QUAL

                  NAPHTHALENE*                 13.9                           13.5                           76                             1.2






                                                          Mussel Watch Project Year 8 - Aromatic QC Data


                      INVFSr#-.                 MSPB                  LAB QA SAMPLE                  LAB QA SAMPLE                LAB - gA
                         ID:            MississIppi Sound                     MSPB;                        MSPB                     PROC BLANK
                        srm.             Pascagoula Bay               Misstssippi Sound             Mississtppt Sound
                    LABSAMNO:                   R7078                         Q6346                        Q6347                       Q6348
                   SAMPLE 7WE:                  SAMP                     DUPLICATE                         ms                          BLANK

                   CI-NAPHTHALENES              15.7                          14.8                                         NA             1.8
                   C2-NAPHINALENES              11                            25                                           NA                            ND
                   C3-NAPHTHALENES              23.3                          50.4                                         NA                            ND
                   C4-NAPHTHALENES              55.2                          41.1                                         NA                            ND
                    BIPHENYL *                  4.7                           5.1            J             78.7                           0.2
                   ACENAPHTHYLENE               3.4                           3.4                          87.2                           0.1
                   ACENAPHTHENE*                5.7                           6.6                          82.8                           0.3            J
                    FLUORENE *                  10.5                          8.9                          85.9                           0.2            J
                   CI-FLUORENES,                60.8                          16.4                                         NA                            ND
                   C2-FLUORENES                 16.5                          52.3                                         NA                            ND
                   C3-FLUORENES                 60.3                          118.6                                        NA                            ND
                   PRENAWHRENE*                 25.5                          24.5                         63.6                           0.2
                   AN'niRACENE *                12                            13.6                         64.1                           0.3
                   Cl-PHEN_ANTHR                128.8                         43.7                                         NA                            ND
                   C2-PHEN-ANTHR                53.5                          78.6
                                                                                                                           NA                            ND
                   C3-PHEN_ANTHR                78.4                          143.8                                        NA                            ND
                   C4-PHEN-ANITIR                             ND              137.4                                        NA                            ND
                   DIBENZOTHIO                  2.8                           3.4                          70.3                           0.1            1
                      CI-DIBEN                  0             ND              22.5                                         NA                            ND
                      C2-DIBEN                  20.2                          69.8                                         NA                            ND
                      C3-DIBEN                  60.4                          69.6                                         NA                            ND
                   FLUORANTHENE                 92.1                          99.1                         60.4                           0.1
                      PYRENE*                   55.9                          60.2                         68.7                           0.1
                   Cl-FLUORAN_PYR               65.4                          64.3                                         NA                            ND
                   BENaANMRACENE                19.4                          16.8                         102.4                          0.2            J
                    CHRYSENE 0                  21                            25.2                         8511                           0.4            1
                   CI-CHRYSENES,                662,7                         19.8                                         NA                            ND
                   C2-CHRYSENES,                17.2                          11.5                                         NA                            ND
                   C3-CHRYSENES                 10,2                                         ND                            NA                            ND
                   C4-CHRYSENES                                ND                            ND                            NA                            ND
                   BENbFLUORAN                  6.7                           6.8                          91.3                           0              J
                   BENkFLUORAN                  7.1                           7.2                          97.4                           0              J
                   BENePYRENE 0                 6.6                             8                          94.5                           0.1            J
                   BENaPYRENE 0                 2                             1.5            J             87.6                           0.1






                                                         Mussel Watch Project Year 8 - Aromatic QC Data


                     INVESTC                 MSPB                    LAB QA SAMPLE                 LAB QA SAMPLE                LAB QA SAMPLE
                        ID:            Mississippi Sound                   MSPB                           MSPB                    PROC BLANK
                       SITE.,           Pascagoula Bay               Mississippi Sound            Mississippi Sound
                    LABSAMNO:                K7078                        Q6346                           Q6347                      Q6348
                  SAMPLE TYPE:               SAMP                       DUPLICATE                         Ms                         BLANK


                    PERYLENEO                  11.8                          14.6                         102.6                        0.2            J
                   1123cdPYRENE                1.3                           0.9            J             93.8                         0.2
                  DBahANTHRA *                 0.7            J              0.5            J             117                          0.1            J
                   BghlPERYLENE                1.6                           1.5                          98.2                         0.1            J

                   TOTAL PAH's               1032.2                       1286.1                    AVG % RECOV                        5.7
                   (w/o PERYLENE)                                                                         89.6
                 S&T Total PAHs (0)            327                           342                                                       6.7


                 2-MEIIfYLNAPH *               9.4                           8.7                          153.1                        0.9            J
                 1-METHYLNAPH 0                6.3                           6                            107                          0.8


                 2,6-DIMETHNAPH                9                             7                            79.5                         0.3            J

      0)       2,3,5-TRIMETHNAPH               9.4                           11.2                         103.6                        0.6            J


                 I -METHYLPHEN                 11.2                          11                           88.2                         0.4            J


                Surrogate Recoveries
                     NAPH138:                  49                            53.4                         54.6                         64.6
                     ACENDIO:                  70.1                          67.8                         72.7                         84.1
                     PHENDIO:                  69.5                          70.9                         80.4                         69.9
                     CHRYD12:                  64                            67.9                         62.5                         73.5
                     PERYD12:                  66.1                          64.9                         70.9                         49.1






                                                                 Mussel Watch Project Year 8 - Aromatic QC Data


                             INVEST#:           LAB QA SAMPLE                         TBMK                    LAB 9A SAMPLE                   LAB 9A SAMPLE
                                ID:              SPIKE BLANK                      Tampa Bay                           713MK                     SPIKE K7106
                               SITE:                                           Mullet Key Bayou                  Tampa Bay                       Tampa Bak
                             LABSAMNO:               Q6349                            K7106                           Q6350                          Q6351
                             SAMPLE TYPE:             LBS                             SAMP                       DUPLICATE                            MS

                             RECEIPT DATE:                                            1/15/93                         1/15/93                        1/15/93
                             QCBATCH:                M1235                            M1235                           M1235                          M1235
                      EXTRACTION DATE:               9/17/93                          9/17/93                         9/17/93                        9/17/93
                             METHOD:                 GCMS                             GCMS                            GCMS                           GCMS
                        ANALYSIS DATE:               10/30/93                         10/30/93                        10/30/93                       10/30/93
                             METHOD:                 GCECD                            GCECD                           GCECD                          GCECD
                        ANALYSIS DATE:               8/24/94                          8/22/94                         8/24/94                        8/24/94
                             MATRIX,                 TISSUE                           TISSUE                          TISSUE                         TISSUE
                             SUBMAT:                                                                                                                 15.12
                             WETWT:                                                   15.13                           15.13
                             DRYWT:                     10                            3.7                             3.81                           3.71
                             WTUNITS:                GRAMS            DRY             GRAMS          DRY              GRAMS          DRY             GRAMS          DRY
                             PCTSOLIDS:                                               24.50036                        25.200/6                       24.500/6
                             Lipid Weight:
                             TOTAL LIPID:                              NA             7.45                            6.75                           7.09
         0                   LIPID UNITS:            % DRY                            % DRY                           % DRY                          % DRY
                              VOL:
                             VOLUNITS:               LITERS                           LITERS                          LITERS                         LITERS
                      Surrogate Recoveries
                              PAH's:
                             NAPHD8:                  67.7                            59.9                            61.8                           53.8
                             ACENDID.,                77.8                            84.1                            81.2                           66.8
                             PHENDIO:                 88.1                            75.4                            79.9                           87.3
                             CHRYD12:                 87.6                            64.4                            77                             73.8
                             PERYD12:                 63.2                            65.1                            66.1                           65.1
                     PESMCIDES & PCB's:
                             DBOF'B:                  65.9                            80.7                            75.9                           79.2
                             PCB# 103:                69.4                            60.9                            68.6                           96.6
                             PCB# 198:                69.5                            61.2                            81.5                           98.3

                              UNIT:                     %                             ng/g                            ng/g                            %
                             PNA Analyte           % RECOV         DS QUAL            Conc        DB QUAL             Conc       DB QUAL         % RECOV         DB QUAL

                        NAPHTHALENE*                  84.6                            5.3                             5.6                            80







                                                          Mussel Watch "ect Year 8 - Aromatic QC Data


                        INVEST#:         LAB QA SAMPLE                      TBMK.                  LAB QA SAMPLE               LAM QA MUM
                           ID:             SPIKE BLANK                   Tampa Bay                      TBMK.                    SPIKE K7106
                          SITE:                                       Mullet Key Bayou               Tampa Bay                    Tampa Bay
                       LABSAMNO:              Q6349                         K7106                      Q6350                        Q6351
                      SAMPLE TYPE:              LBS                          SAMP                    DUPLICATE                        MS

                      Cl-NAPHTHALENES                          NA            7.6                          7.7                                       NA
                      C2-NAPHTHALENES                          NA            11.9                         14.4                                      NA
                      C3-NAPHTRALENES                          NA            17.3                         19.9                                      NA
                      C4-NAP)TrHALENES                         NA            22.5                         21.2                                      NA
                       BIPHENYL 0               79.4                         1.9            j             2.1           1             80
                      ACENAPHTHYLENE            73.9                         0.8            1             0.8           j             87.4
                      ACENAPHTHENEO             76.4                         9.1                          9                           81
                       FLUORENEO                 86                          6.9                          7.3                         90.7
                      CI-FLUORENES                             NA            5.1            j             9                                         NA
                      C2-FLUORENES                             NA                          ND                           ND                          NA
                      C3-FLUORENES                             NA                          ND                           ND                          NA
                      PHENANTHRENE              69.5                         26.7                         26,6                        47.5
                      ANTHRACENEO               93.4                         7.4                          6.6                         66.5
                      CI-PHEN-ANTHR                            NA            39.5                                       ND                          NA
                      C2-PHEN-ANTHR                            NA            22.7                                       ND                          NA
                      C3-PHEN-ANTHR                            NA                          ND                           ND                          NA
                      C4-PHEN-ANTHR                            NA                          ND                           ND                          NA
                      DIBENZOTHIO               49.9                         1.8                          1.4                         57.6
                        CI-DIBEN                               NA            3.5                          3.5                                       NA
                        C2-DIBEN                               NA            5.8                          7.1                                       NA
                        C3-DIBEN                               NA                          ND             5.5                                       NA
                      FLUORANTHENE              72.8                         56.4                         53.9                        43.8
                        PYMNE *                 71.5                         30.7                         28.4                        50
                      Cl-FLUORAN_PYR                           NA            22.2                         19.2                                      NA
                      BENaANTHRACENE*           71.5                          9                           9.1                         76.9
                       CHRYSENE 0               71.5                         10.8                         7.5                         61.9
                      CI-CHRYSENES                             NA                          ND                           ND                          NA
                      C2-CHRYSENES                             NA                          ND                           ND                          NA
                      C3-CHRYSENES                             NA                          ND                           ND                          I,',A
                      C4-CHRYSENES                             NA                          ND                           ND                          NA
                      BENbFLUORAN               70.4                         2.9                          2.6                         69.8
                      BENkFLUORAN               71.1                          3                           2.5                         74.4
                      BENePYRENE                71.2                         3-11                         0. ev                       70.6
                      BENaPYRENE*               62.5                         0.6            1             0.8           d             66.9





                                                                                                                moo






                                                          Mussel Watch Project Year 8 - Aromatic QC Data


                         INVEST#:         LAB QA SAMPLE                      TBMK                  LAB QA SAMPLE               LAB QA SAMPLE
                            ID:            SPIKE BLANK                   Tampa Bay                       TBMK.                   SPIKE K7106
                          SITE:                                       Mullet Key Bayou               Tampa Bay                    Tampa Bay
                       LABSAMNO:               g6349                         K7106                       Q6350                       96351
                      SAMPLE TYPE:              LBS                          SAMP                    DUPLICATE                        MS

                       PERYLENE 0               87.7                         0.5            J             0.6           J             88.9
                      1123cdPYRENE              60.8                         0.7                          0.5                         72
                     DBahANTHRA 0               71.4                         0.3            J             0.4                         90.1
                     B&PERYLENE                 62.2                         0.9                          0.9                         69.5

                       TOTAL PAH's         AVG % RECOV                       336.3                       276.1                  AVG % RECOV
                      (w/o PERYLENE)            77.4                                                                                  77.1
                     S&T Total PAHs (*)                                      187.2                        179

                     2-METHYLNAPH *             132.1                        4.4                          4.1                         142.4
                     I-ME11-IYLNAPH *           92.1                         3.3                          3.6                         102.4

                    2.6-DIMETHNAPH              85.3                         4.5                          4.3                         83.3

                   2,3,5-TPJMETHNAPH            99.9                         3.2                          2.6           J             105.9
        bz           I -MErHYLPHEN 4            68.2                         3.2                          3.6                         67.3
                   Surrogate Recoveries                                                                   61.8                        53.8
                         NAPHI)8:               67.7                         59.9
                         ACENDIO:               77.8                         84.1                         81.2                        66.8
                         PHEND10:               88.1                         75.4                         79.9                        87.3
                         CHRYD12:               87.6                         64.4                         77                          73.8
                         PERYD12:               63.2                         65.1                         66.1                        65.1






                                                               Mussel Watch "ect Year 8 - Aromatic QC Data


                            INVEST#:          I.AB QA SAMPLE                 LAB QA SAMPLE                         VBSP                   LAB QA SAMPLE
                              ID:               PROC BLANK                     SPIKE BLANK                   Vernifilion Bay                     VBSP ,
                             SITE:                                                                          Southwest Pass                 Vernifflion Biy
                            LABSAMNO:               Q6439                          Q6440                           K7046                         Q6441
                        SAMPLE TYPE:                BLANK                           LBS                            SAMP                      DUPLICATE


                       RECEIPT DATE:                                                                               1/6/93                        1/6/93
                            QCBATCH:                M1243                          M1243                           M1233                         M1243
                     EXTRACTION DATE:             11/11/93                       11/11/93                       11/11/93                      11/11/93
                            METHOD:                 GCMS                           GCMS                            GCMS                          GCMS
                      ANALYSIS DATE:              12/22/93                       12/22/93                       12/23/93                      12/22/93
                            METHOD:                 GCECD                          GCECD                           GCECD                         GCECD
                       ANALYSIS DATE:
                            MATRIX:                 TISSUE                         TISSUE                          TISSUE                        TISSUE
                            SUBMAT-
                            WETWT:                                                                                 15.08                         15.13
                            DRYWT:                     10                             10                           1.78                          1.72
                            WTUNITS:                GRAMS            DRY           GRAMS            DRY            GRAMS         DRY             GRAMS           DRY
                            PCTSOLIDS:                                                                             11.80016                      11.30%
                            I.Apid Weight:
       *4                   TOTAL LIPID:                              NA                             NA            11.01                         11.58
       to                   LIPID UNITS:            % DRY                          % DRY                           % DRY                         % DRY
                             VOL:
                            VOLUNITS:               LITERS                         LITERS                          LITERS                        LITERS
                     Surrogate Recoveries
                             PAH's:
                            NAPHD8:                  71.2                             62                           58.4                          71.2
                            ACENDIO:                 52.9                             64                            57                           65.8
                            PHENDIO:                 66.9                           67.9                           70.7                          72.7
                            CHRYD12:                 55.3                           56.1                           69.1                          73.9
                            PERYD12:                 23.2                           36.2                           60.6                          60.8
                    PESMCIDES & PCB's:
                            DBOF13:                                   NA                             NA                           NA                              NA
                            PCB# 103:                                 NA                             NA                           NA                              NA
                            PCB#198:                                  NA                             NA                           NA                              NA

                             UNIT:                   ng/g                             %                            ng/g                          ng/g
                            PNA Analyte              Conc         D13 QUAL       % RECOV         DB QUAL           Conc        DB QUAL           Conc         DB QUAL

                       NAPHTHALENE*                    1.2                          73.1                           15.6                          14.6






                                                          Mussel Watch Project Year 8 - Aromatic QC Data


                         INVEST*:          LAB QA SAMPLE               LAB QA SAMPLE                     VBSP                  LAB QA SAMPLE
                             ID:            PROC BLANK                   SPIKE BLANK                Vennfillon Bay                    VBSP .
                           SITE:                                                                    Southwest Pass              Vennffilon Bay
                        LABSAMNO:               Q6439                       Q6440                        K7046                        Q6441
                       SAMPLE TYPE:             BLANK                         LBS                        SAMP                    DUPLICATE


                       CI-NAPHTHALENES            1.4            J                          NA             17.2                       14.7
                       C2-NAPHTHALENES                          ND                          NA             20                         20.8
                       C3-NAPHTHALENES                          ND                          NA             23.3                       28.5
                       C4-NAPFrrHALENES                         ND                          NA             37.3                       25.7
                        BIPHENYL 0                0.9            J            72.7                         6.3          J             6.9            J
                       ACENAPHTHYLENE             0.1            J            69.8                         2            J             2              J
                       ACENAPHTHENE*              0.2            J            66.5                         3            J             3.8            J
                        FLUORENE*                 0.6            J            73.8                         7.2                        6.3            J
                       CI-FLUORENES                             ND                          NA             13.9                       14.4
                       C2-FLUORENES                             ND                          NA             56.4                       44.5
                       C3-FLUORENES                             ND                          NA             67                         111.8
                       PHENANTHRENEO              0.5                         77.8                         19.8                       19
                       ANTHRACENEO                0.3            J            88.2                         3            J             3              J
                       C1-PHEN_ANTHR                            ND                          NA             21.3                       24.2
                       C2-PHEN-AN'THR                           ND                          NA             44                         33.1
                       C3-PHEN ANMR                             ND                          NA             82.6                       84.8
                       C4-PHEN-ANTHR                            ND                          NA             71                         78.7
                       DIBENZOTHIO                0.2            J            65.4                         1.5          J             2.4
                         CI-DIBEN                               ND                          NA             6.4                        5.4
                         C2-DIBEN                               ND                          NA             13.9                       17.6
                         C3-DIBEN                               ND                          NA             14.5                       15.4
                       FLUORANTHENE               0.1            J            75.6                         15.5                       17.4
                         PYRENE 0                 0.1            J            74.4                         20.8                       23.5
                       CI-FLUORAN-PYR                           ND                          NA             22.9                       21.5
                       BENaANTHRACENE             0.2            J            73.1                         1.8                        1.6            J
                        CHRYSENEO                 0.2            J            79.8                         8.1                        7.6
                       Cl-CHRYSENES                             ND                          NA             4.7          J             4.4            J
                       C2-CHRYSENES                             ND                          NA             9.1                        9.3
                       C3-CHRYSENES                             ND                          NA                         ND                           ND
                       C4-CHRYSENES                             ND                          NA                         ND                           ND
                       BENbFLUORAN                0.1            J            58                           1.1          J             1.1            J
                       BENkFLUORAN                0.1            J            58.2                         1.1          J             1.1
                       BENePYRENE *               0.1            J            60.1                         2.3                        1.9
                       BENaPYRENE*                0.1            J            58                           1.2          J             1.4            J






                                                        Mussel Watch Prqject Year 8 - Aromatic QC Data


                        INVEST#:         LAB 9A SAMPLE                LAB 9A SAMPLE                     VBSP                 LAB QA Wn
                           ID:             PROC BLANK                  SPIKE BLANK                Vermillion Bay                   V13SP :
                          SM                                                                      Southwest Pass              Vemill1lon Bay
                      LABSAMNO:               Q6439                         Q6440                       K7046                      Q6441
                     SAMPLE TYPE:             BLANK                         LBS,                        SAMP                   DUPLICATE

                      PERYLENE*                 0.7                         113.7                       6.4                         6.7
                      1123cdPYRENE              0.4                         56.7                        0.7                         0.6
                      DBahANTHRA*               0.4            j            81.6                        2.1                         1.4
                      BghIPERYLENE              0.1            1            68.9                        1.1           j             0.4

                      TOTAL PAH's               7.4                   AVG % RECOV                       639.6                      670.1
                     (w/o PERYLENE)                                         74.1
                    S&r Total PAHs (*)          8.5                                                     146.2                      146.9


                    2-METHYLNAPH *              0.8            1            111.8                       8.9                         7.2
                    I-METHYLNAPH 0              0.6            j            79.3                        8.3                         7.5


                   2.6-DIMETHNAPH               0.5            j            73.8                        6.4                         8.1


                 2.3,5-IMMETHNAPH               0.6            j            75.6                        4.2           j             4.7

      U1
                    I -MLTHYLPHEN               0.3            j            66.2                        5.3                         4.6


                  Surrogate Recoveries
                        NAPHD8-.                71.2                         62                         58.4                       71.2
                        ACENDIO:                52.9                         64                         57                         65.8
                        PHENDIO:                66.9                        67.9                        70.7                       72.7
                        CHRYD12:                55.3                        56.1                        69.1                       73.9
                        PERYD12:                23.2                        36.2                        60.6                       60.8






                                                          Mussel Watch Project Year 8 - Aromatic QC Data


                     INVEST#:         LAB QA SAMPLE                               G.E.R.G.             LAB QA SAMPLE               LAB QA SAMPLE
                       ID:                   VBSP                                    STD               GERG STD CHK                 GERGSIVCHK
                      SITE:            Vermillion Bay                                CHK
                     LABSAMNO:               Q6442                               RUNNING                    W9670                        W9685
                     SAMPLE IWE:             MS                                  AVERAGE                      REF                         REF


                     RECEIPT DATE:           1/6/93
                     QCBATCH:                M1243                                                          M1232                        M1233
               EXTRACT[ON DATE:          11/11/93
                     METHOD:                 GCMS                                                            GCMS                        GCMS
                ANALYSIS DATE:           12/23/93                                                         10/19/93                     10/23/93
                     METHOD:                 GCECD                                                          GCECD                        GCECD
                ANALYSIS DATE:
                     MATRIX                  TISSUE                                  REF                    TISSUE                       TISSUE
                     SUBMAT-
                     WETWT.,                 15.06
                     DRYWT:                  1.72
                     WTUNITS:                GRAMS        DRY
                     PCTSOLIDS:              11.40%
                     I.Apid Weight:
                     TOTAL LIPID:            12.62                                                                          NA                          NA
        C)           IIPID UNITS:            % DRY                                                         % DRY                         % DRY
                      VOL:                                                                                    I                            I
                     VOLUNITS:               LITERS                                                      AMPOULES                     AMPOULES
               Surrogate Recoveries
                      PAH's:
                     NAPHD8:                 69.8                                              NA                           NA                          NA
                     ACENDIO:                66.6                                              NA                           NA                          NA
                     PHENDIO:                88.7                                              NA                           NA                          NA
                     CHRYD12:                78.6                                              NA                           NA                          NA
                     PERYD12:                56                                                NA                           NA                          NA
              PESTICIDES & PCB's:
                     DBOFB:                                NA                                  NA                           NA                          NA
                     PCB#103:                              NA                                  NA                           NA                          NA
                     PCB#198:                              NA                                  NA                           NA                          NA


                      Uw.                    %                                   AVERAGE                    ng/amp                       ng/amp
                     PNA Analyte         % RECOV       DB QUAL                              DB QUAL          Conc       DB QUAL          Conc        DB QUAL

                NAPHTHALENE                  58.4                                   541.5                    582.4                       588.4






                                                              Mussel Watch Project Year 8 - Aromatic QC Data


                      INVEST#:          LAB QA SAMPLE                                   G.E.R.G.              LAB QA SAMPLE                  LAB QA SAMPLE
                          ID:                  VBSP                                        STD                GERG STD CHK                   GERG SM CHK
                        SITE.             Vermillion Bay                                   CHK
                     LA13SAMNO:                Q6442                                   RUNNING                         W9670                      W9685
                   SAMPLE TYPE:                 MS                                     AVERAGE                         REF                           REF


                   CI-NAPHTHALENES                              NA                         2332.5                      2443.6                     2378.7
                   C2-NAPHTHALENES                              NA                         2398.5                      2373.3                     2204.6
                   C3-NAPHTHALENES                              NA                         2066.2                      2252.3                     2229.3
                   C4-NAPHTHALENES                              NA                         1121.4                      1239.8                        1207
                     BIPHENYL 0                 72                                         184.7                       190.6                         212.7
                   ACENAPHTHYLENE               83.6                                       1.1         J               0.2                           1.6            J
                   ACENAPHTHENE*                76.5                                       18.1        J               18.7           J              19.7           J
                     FLUORENE*                  84.7                                       97.1                        101.5                         88.6
                   CI-FLUORENES                                 NA                         257.5                       253.8                         352.8
                   C2-FLUORENES                                 NA                         373.9                       384.5                         500.9
                   C3-FLUORENES                                 NA                         369.4                       425.6                         457.1
                   PHENANTHRENEO                66.4                                       256.4                       243                           239.3
                   ANTHRACENEO                  79.7                                       4.7         J               9.5            J              6.1            J
                   CI-PHEN   ANTHR                              NA                         589.2                       653.7                         590.7
                   C2-PHEN   ANTHR                              NA                         669.6                       793                           769.2
                   C3-PHEN   ANTHR                              NA                         554.3                       613.2                         589.1
                   C4-PHEN_ANTHR                                NA                         301                         340.2                         420.4
                   DIBENZOTHIO                  63.9                                       150.4                       151.9                         123.9
                      CI-DIBEN                                  NA                         439.3                       306.4                         920.5
                      C2-DIBEN                                  NA                         452.6                       490.8                         484.6
                      C3-DIBEN                                  NA                         378.3                       424.6                         412.7
                   FLUORANTHENE                 75.6                                       8.8         J               4.6            J              17             J
                      PYRENE*                   71.4                                       19.7        J               16.4           J              27.3
                   CI-FLUORAN-PYR                               NA                         87.8                        77.9                          99.6
                   BENaANTHRACENE               81.5                                       10.9        J               9.8            J              31.6
                     CHRYSENE, 0                76.6                                       53                          46                            60.9
                   CI-CHRYSENES                                 NA                         136.5                       94                            315.3
                   C2-CHRYSENES,                                NA                         185.9                       137.7                         432.9
                   C3-CHRYSENES                                 NA                         39.1                        32.2                          100.2
                   C4-CHRYSENES                                 NA                         48.4                        13             J              62.8
                   BENbFLUORAN                  59.4                                       6.2         J               3.2            J              16.9           J
                   BENkFLUORAN                  59.6                                       6.2         J               4              J              15.8           J
                   BENePYRENE *                 61.9                                       13.2        J               13             .7             21.3
                   BENaPMENE *                  70.9                                       4.3         J               2.3            J              11.3           J






                                                            Mussel Watch Project Year 8 - Aromatic QC Data


                       INVEST#:         LAB QA SAMPLE                               G.E.R.G.             LAB QA SAMPLE                LAB QA SAMPLE
                          ID:                  VBSP                                   STI)                GERG SID CHK                GERG SM CHK
                         SITE:           Vermillion Bay                               CHIC
                     LABSAMNO:                 Q6442                                RUNNING                    W9670                       W9685
                    SAMPLE TYPE:                MS                                 AVERAGE                      REF                          REF


                     PERYLENEO                 105.1                                   3.5         J            4.3                           6.8           J
                     1123cdPYRENE              80.1                                    2.3         J            1.4            J              5.3           J
                    DBahANTI-IRA 0             122.8          Q                         2          J            1.4            J              2.4           J
                     BghiPERYLENE              87.6                                    4.5         J            4.6            J              5.5           J

                     TOTAL PAH's         AVG % RECOV                                 14186.3                  14753.6                     16023.6
                    (w/o PERYLENE)              78
                   S&T Total PAHs (*)                                                4894.9                    5084.7                      5149.2

                   2-METHYLNAPH 0              105.1                                 1281.7                    1345.9                        1307
                   1 -METHYLNAPH *             72.4                                  1050.8                    1097.7                      1071.7


                   2.6-DIMETHNAPH              80.9                                   753.7                    767.5                        807.3

         -4      2,3,5-TRIMETHNAPli            90.7                                  430.1                     451.3                        501.1
         00
                   I -METHYLPHEN               62.4                                   160.7                     179                         128.7


                 Surrogate Recoveries
                       NAPHD8:                 69.8                                               NA                          NA                           NA
                       ACENDIO:                66.6                                               NA                          NA                           NA
                       PHENDIO:                88.7                                               NA                          NA                           NA
                       CHRYD12:                78.6                                               NA                          NA                           NA
                       PERYD12:                 56                                                NA                          NA                           NA






                                                            Mussel Watch Project Year 8 - Aromatic QC Data


                                         INVEST#:         LAB QA SAMPLE                LAB QA SAMPLE                LAB QA SAMPLE
                                           ID:            GERG STD CHK                 GERG STI) CHK                GERG STD CHK
                                          SITE:
                                         LABSAMNO:             W9728                         W9750                       W0061
                                     SAMPLE TYPE:               REF                          REF                          REF


                                     RECEIPT DATE:
                                         QCBATCH:              M1234                         M1235                       M1243
                                  EXTRACTION DATE:                                          9/17/93
                                         METHOD:               GCMS                          GCMS                        GCMS
                                    ANALYSIS DATE:            10/28/93                     10/30/93                    12/22/93
                                         METHOD:               GCECD                        GCECD                        GCECD
                                    ANALYSIS DATE:
                                         MATRIX                TISSUE                       TISSUE                       TISSUE
                                         SUBMAT:
                                         WETWT:
                                         DRYWr
                                         VVFTUNITS:
                                         PCTSOLIDS:
                                         Lipid Weight:
                                         TOTAL LIPID:                           NA                           NA                           NA
        CD                               LIPID UNITS:          % DRY                        % DRY                        % DRY
                                          VOL:                    1                            1                            1
                                         VOLUNITS:           AMPOULES                    AMPOULES                     AMPOULES
                                   Surrogate Recoveries
                                          PAH's:
                                         NAPHD8:                                NA                           NA                           NA
                                         ACEND10:                               NA                           NA                           NA
                                         PHENDIO:                               NA                           NA                           NA
                                         CHRYD12:                               NA                           NA                           NA
                                         PERYD12:                               NA                           NA                           NA
                                  PESTICIDES & PCB's:
                                         DBOFB:                                 NA                           NA                           NA
                                         PCB# 103:                              NA                           NA                           NA
                                         PCB# 198:                              NA                           NA                           NA


                                          UNIT:                ng/amp                        ng/amp                      ng/amp
                                         PNA Analyte            Conc        DB QUAL           Conc       DB QUAL          Conc        DB QUAL

                                     NAPHTHALENE*               530.9                         549.5                       456.1



  mmmmlm@@Mmm mmmm@ @. -

                                                                Mussel Watch ProJect Yew 8 - Aromatic QC Data


                                           BwFsr#:            LAB GA SAMPLE                 LAB 9A SAMPLE                 LAB @Tk SAMPLE
                                               ID:            GERG STD CHK                  GERGMCHK                      GERG M CHK
                                              Srm:
                                           LABSAMNO:                 W9728                          W9750                        WWI
                                         SAMPLE ITPE:                REP                            REF                          RFF


                                      Cl-NAPHTHALENM                 2492                           2580.1                       1768.1
                                      C2-NAPHTHALENF,S               2799.2                         2839.7                       1775.6
                                      C3-NAPH7HALENES                2250.3                         2254.7                       1344.4
                                      C4-NAPHTHALENES                1173.1                         1235.4                       751.7
                                          BIPHENYL 0                 174.7                          179.3                        166.1
                                      ACENAPInTrYIEW                  I              j              1.1                          1.6
                                      ACENAPHTHENE*                  18.1                           17.6                         16.5            j
                                         FLUORENE 0                  100.6                          93.1                         101.8
                                         CI-FLUORENES                218.3                          228.5                        234
                                         C2-FLUORENES                310.4                          350.5                        323
                                         C3-FwORF,Nm                 306                            322.2                        336.4
                                      PHENANTHRENE*                  269                            263.9                        266.9
                                         ANMRACENE *                  0                             3.5                          4.3
                                         CI-PHEN-ANTHR               565                            W.4                          568.1
         OD                              C2-PHEN-ANTHR               577.6                          585.5                        622.6
                                         C3-PHEN-ANMR                534.3                          544.7                        490.5
                                         C4-PHF,N-ANMR               233.8                          264.7                        245.9
                                         DIBENZOTHIO                 164                            158.5                        153.6
                                           CI-DIBEN                  339.4                          323.3                        306.8
                                           C2-DIBEN                  440                            447.3                        400.1
                                           C3-DIBEN                  351.1                          378.9                        324.5
                                      FLUORAMMENE                    6.7                            9.2                          6.2
                                           PYRENEO                   22.5                           19.7                         12.8
                                      CI-FLUORAN-PYR                 91.6                           83                           86.8
                                      BENaMMRACENE                   3.6                            3.9            j             5.7
                                         CHRYSENF, *                 45.4                           53.1                         59.9
                                         CI-CHRYSENES                101.6                          96.9                         74.5
                                         C2-CHRYSENES                145.7                          120.7                        92.4
                                         C3-CHRysENEs                29.7                           22                           11.6
                                         C4-CHRYSENES                70.3                           82.2                         13.8
                                         BENbFLUORAN                  4                             4                            2.8
                                         BENkFLUORAN                 4.3                            4.2                          2.8
                                         BENePYRENF-                 10.9                           10.8                         10.1
                                         BENaPYRF-NE                 3.3                            2.1                          2.6






                                                            Mussel Watch Project Year 8 - Aromatic QC Data


                                         uqvFsr#:          LAB QA SAMPLE                LAB QA SAMPLE                 LAB QA SAMPLE
                                            ID:            GERG SM CHK                   GERG M CHK                   GERG SM CHK
                                          srm:
                                       LABSAMNO:                 W9728                       W9750                          W0061
                                     SAMPLE IYPE:                REF                            REF                          REF


                                       PERYLENE 0                 2.1             J             1.9            J              2.5            J
                                      I123cdPYRENE                2.1             J             0.4            J              2.4            J
                                     DBahANTHRA 0                  2              J             2.6            J               1.6           J
                                      BghtPERYLENE                4.1             J             3.3            J              5.1            J

                                      T(YrAL PAH's               14396.5                     14708.3                       11049.4
                                      (w/o PERYLENE)
                                    S&r Total PAlis (0)          4977.9                       5158.5                        4104.2


                                    2-METHYLNAPH *               1367.5                       1425.1                         962.8
                                    I-METHYLNAPH *               1124.5                       1155.1                         805.3


                                   2.6-DIMETHNAPH                 712.6                       745.1                          735.8

        OD                        2.3.5-11UNILrHNAPH              426.7                       429.2                          342.1


                                    I -METHYLPHEN                 156.8                         194                          145.2


                                   Surrogate Recoveries
                                         NAPHD8:                                  NA                           NA                            NA
                                         ACENDIO:                                 NA                           NA                            NA
                                         PHENDIO:                                 NA                           NA                            NA
                                         CHRYD12:                                 NA                           NA                            NA
                                         PERYD12:                                 NA                           NA                            NA




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                                                         m m m m m mm m m m m M m

                                                      Mussel Watch Project Year 8 - Pesticides and PCBs Data


                 INVEST#:                LMSB                        CCNB                     ABLR                    MBAR                       SAPP
                   ID,            1. Laguna Madre              Corpus Christi           Aransas Bay              Mesquite Bay             San Antonio Bay
                  SME:                   South Bay             Ingleside Cove                 Long Reef               Ayres Reef           Mosquito Point
                LABSAMNO:                K7030                       K7024                    K7034                   K7032                      K7042
             SMPLE TYPE:                 SAMP                        SAMP                     SAMP                    SAMP                       SAMP
                  UNrr.-                 ng1g                        ng1g                     ng/g                    11919                      nglg
                  Analyte                Conc       1313 QUAL        Conc     DB QUAL         Conc    DB QUAL         Conc     DS QUAL           Conc       1313 QUAL



             RECEIPT DATE:               12/17/92                    12/16/92                 12/17/92                12/17/92                   12/17/92
                QCBATCH:                 M1232                       M1232                    M1233                   M1232                      M1233
           EXTRAC71ON DATE:              9/14/93                     9/14/93                  11/11/93                9/14/93                    9/14/93
                 METHOD:                 Gems                        Gems                     GCMS                    Gems                       GCMS
            ANALYSIS DATE:               10/20/93                    10/20/93                 12/M/93                 10/20/93                   10124/93
                 METHOD:                 GCECD                       GCECD                    GCECD                   GCECD                      GCECD
            ANALYSIS DATE:               7/30/94                     7/30/94                  8/23/94                 7/30/94                    8/23/94
                 MAIRIX                  InSSUE                      77SSUE                   TISSUE                  IISSUE                     77SSUE
                 SUBMAT:
                 WETWT.-                 15.48                       15                       15.17                   15.51                      4.65
                 DRYWr-                    2                         2.66                     2.52                    3.31                       0.96
       00       WTUNITS:                 GRAMS        DRY            GRAMS       DRY          GRAMS      DRY          GRAMS       DRY            GRAMS         DRY
       co      PCTSOLIDS:                12.90%                      17.80%                   16.60%                  21.40%                     20.70%
              Lipid Weight:
              TOTAL UPID:                3.04                        7.56                     9.26                    9.52                       12.66
              UPID UNITS:                % DRY                       % DRY                    % DRY                   % DRY                      % DRY
                  VOL.
                VOLUNITS-                LITERS                      LITERS                   =RS                     LITERS                     I.XrERS


                 DBOFB:                  73.8                        78                       75                      74.3                       68.3
                 PCB*103:                76.9                        79.3                     82.9                    76.3                       69.4
                 PCB#198:                70.1                        77.7                     83.7                    75.8                       67.6
              TOTAL BHCs                 0.3            J            1.2          J           1.2         J           1.5                         4             J
        TOT CHLORDANES, (ALU             0.3                         3.8                      2.9                     1.1                        3.8
        TOT CHLORDANES JS&'T)            0.1            J            1.6                      1.7                     0.4          J             2.1            J
              TOTAL DDT9                 2.7            J            11.7                     17                      3.8                        5.1            J
           TOTAL PCBs (S&II              12.9           .1           31                       23.7        J           17.5         J             21.9           J


               ALPHA-BHC                 0.2            J            0.7                      1.2                     0.9                         2
                  HCB                      0            J            0            J           0.1                     0            J             0.2
                BETA-BHC                 0.1            J            0.5                      0          ND           0.1          J              0            ND
               GAMMA-BHC                 0.1            J            0           ND           0          ND           0.5                         2
               DELTA-BHC                 0.1            J            0           ND           0          ND           0           ND              0            ND
              HEPTACHLOR                  0            ND            0           ND           0.1         J           0           ND              0            ND






                                                      Mussel Watch Project Year 8 - Pesticides and PCBs Data


                INVEST#:               LMSB                         CCNB                      ABLR                    MBAR                       SAPP
                  ID:            L 1,aguna Madre              Corpus Christi             Aransas Bay             Mesquite Bay              San Antonio Bay
                 SITE:               South Bay                 Ingleside Cove             Long Reef                Ayres Reef               Mosquito Point
             LhBSAMNO:                 K7030                       K7024                      K7034                   K7032                      K7042
            SAMPLE TYPE:               SAMP                         SAMP                      SAMP                    SAMP                       SAMP
                 UNIT.                 ng/g                         ng/g                      ng/g                     ng/g                      ng/g
                Analyte                Cone        1313 QUAL        Cone      DB QUAL         Cone     DB QUAL         Cone     DB QUAL          Cone         DB QUAL


           HEPTA-EPO)aDE                 0             ND            0.2          J           0.4                      0.2          J              0.7            J
           OXYCHLORDANE                  0              J            0.1          J           0.2          J           0.1          J              0.1            J
        GAMMA-CH1A)RDANE                 0.1            J            1.1                      0.5                      0.4                         0.8            J
        ALPHA-CHLORDANE 0                0.1            J            0.7                      0.5                       0           ND             0.9            J
        TRANS-NONACHILOR 0               0              J            0.6                      0.7                      0.2          J              0.6            J
           CIS-NONACHLOR                 0.1            J            1                        0.4                      0.3          J              0.7            J
                ALDRIN                   0             ND            0           ND            0          ND            0           ND             0             ND
                DIELDRIN                 0.1            J            0.3          J           1.3                      0.4                         1.5
                ENDRIN                   0             ND            0           ND           0.2          J            0           ND             0             ND
                MIREX                    0             ND            0            J            0          ND            0           J              0             ND
           2.4'DDE (O,PDDE)              0              J            0            J            0          ND           0.2          J              0             ND
     00    4,4'DDE (P.P'DDE)             2.4                         10                       14.9                      3                          4.2
           2.4'DDD (O.P'DDD)             0              J            0.1          J            0           J            0           J              0             ND
           4.4'DDD (P.VDDD)              0.1            J            1.1                      0.8                      0.4                         0             ND
           2.4'DDT (0,P'DErn             0.1            J            0.3          J           0.1          J           0.1          J              0             ND
           4.4'DDT (P.PIDM               0.1            J            0.1          J            1                       0.1          J              0.9            J

        PCB # (CLORINATION)
           NOAA S&-T PCBs
                8 (CL2)                  0             ND            0.2          J            0          ND            0           ND             0             ND
                18 (CL3)                 0              J            0.2          J            0          ND           0.2          J              0             ND
                28 (CL3)                 1.1                         0           ND           0.1          J           0.6          J              0.4            J
                44 (CIA)                 0             ND            0            J           0.6          J           0.7                         0             ND
                52 (CL4)                 0.7            J            1                        0.3          J           0.7                         0             ND
                66 (CIA)                 0.6            J            0.3          J           0.8                      1.2                         0             ND
                101 (CL5)                0.1            J            0.8                      0.3          J            0           ND             0             ND
                105 (CL5)                0              J            0.1          J           0.3          J            0           ND             03             i
            1101/77 (CL5/4)              0              J            0.5          J            0          ND           0.2          J              0             ND





     = m = m m m m                                                    m        = m m M M M M M M m M



   m m m m m m m m m m m m m m                                                                                                   m m m m @

                                                      Mussel Watch Project Year 8 - Pesticides and PCBs Data


                 INVEST#:                LMSB                        CCNB                      ABLR                   MBAR                       SAPP
                    ID:            L. Laguna Madre             Corpus Christi            Aransas Bay             Mesquite Bay             San Antonio Bay
                   SITE:              South Bay                Ingleside Cove             Long Reef               Ayres Reef               Mosquito Point
                 LABSAMNO:               K7030                       K7024                     K7034                  K7032                      K7042
              SAMPLE TYPE:               SAMP                        SAMP                      SAMP                   SAMP                       SAMP
                  UNrI%                  ng/g                        ng/g                      ng/g                   ng/g                       ng/g
                 Analyte                 Conc       DB QUAL          Conc     DB QUAL          Conc   DB QUAL         Conc     DB QUAL           Conc       DB QUAL


          118/108/149(CL5/5/6)           0.1            J            0.9                       1.4                    0.1          J             0.5            J
                 128 (CL6)                0             J            0.3          J            0          ND          0.1          J             0.5            J
                 138 (CL6)               0.7            J            2.6                       3.1                    1.3                        2.7
                 126 (CL5)                0            ND            0            ND           0          ND            0          ND             0            ND
                 153 (CLAS)              0.6            J            3.8                       3.4                    0.6          J             3.5
                 170 (CL7)               0.7            J            0.5          J            0          ND          0.3          J             0.9            J
                 180 (CL7)               0.1            J            1.2                       0          ND          0.1          J              0            ND
          18711821159(CL7/7/6)           0.1            J            1.3                       0.9                    0.3          J             0.8            J
                 195 (CL8)               0.2            J            0.3          J            0          ND          0.8                         0            ND
                 206 (CL9)                0            ND            0            ND           0          ND            0          ND             0            ND
                 209 (CLIO)               0            ND            0            ND           0          ND            0          ND             0            ND

       00 Surrogate Recoveries
       al        DBOFB%:                 73.8                        78                        75                     74.3                       68.3
                 PCB#103%:               76.9                        79.3                      82.9                   76.3                       69.4
                 PCB#198%:               70.1                        77.7                      83.7                   75.8                       67.6






                                                               Mussel Watch PrQject Year 8 - Pesticides and PCBs Data


                             INVEST#:                   ESBD                            MBGP                              MBLR                               MI3CB
                                ID:              Espiritu Santo                  Matagorda Bay                     Matagorda Bay                     Matagorda B4y
                               Syr&              Bill Days Reef                 Gaffilnipper Point               Lavaca River Mouth                  Carancahua Bay
                             LABSAMNO:                  K7044                           K7036                             K7038                              K7040
                         SAMPLE TYPE:                   SAMP                            SAMP                              SAMP                               SAMP
                               UNIT-                    ng/g                            ng/g                              ng/g                               ng/g
                             Analyte                    Cone       DB QUAL              Cone        D13 QUAL              Cone          D13 QUAL             Cone        DB QUAL



                        RECEIPT DATE:                   12/18/92                        12/18/92                          12/17/92                           12/18/92
                             QCBATCH:                   M1233                           M1233                             M1233                              M1233
                      EXTRACTION DATE:                  9/14/93                         9/14/93                           9/14/93                            9/14/93
                             METHOD:                    GCMS                            GCMS                              GCMS                               GCMS
                        ANALYSIS DATE:                  10/24/93                        10/24/93                          10/24/93                           10/24/93
                             METHOD:                    GCECD                           GCECD                             GCECD                              GCECD
                        ANALYSIS DATE:                  8/23/94                         8/23/94                           8/23/94                            8/23/94
                             MATRIX:                    TISSUE                          TISSUE                            TISSUE                             TISSUE
                             SUBMAT:
                             WE-Ewr..                   15.14                           15.29                             15.3                               15.06
                             DRYWT`:                    2.07                            2.2                               2.26                               2.19
        00                   WIUNITS:                   GRAMS          DRY              GRAMS            DRY              GRAMS             DRY              GRAMS          DRY
        C)                   PCTSOLIDS:                 13.600/6                        14.400/6                          14.800/6                           14.500/6
                             Lipid Weight:
                             TOTAL LIPID:               4.99                            5.53                              5.02                               9.78
                             LIPID UNITS:               % DRY                           % DRY                             % DRY                              % DRY
                                VOL:
                             VOLUNITS:                  LITERS                          LITERS                            LITERS                             LITERS


                             DBOFB:                     79.1                            80.2                              76.8                               72.2
                             PCB# 103:                  84.1                            85.3                              83.8                               73.7
                             PCB# 198:                  79.3                            85.7                              77.3                               82.4
                             TOTAL BHCs                 0.8             1               0.9              j                0.9                                1.3              1
                   TOT CHLORDANES, (ALL)                1.1                              5                                3.5                                6.9
                   TOT CHLORDANES (S&IJ                 0.7             j               2.6                                2                                 3.9
                             TOTAL DDT9                 9.5                             31.3                               9                                 25.6
                       TOTAL PCBs (S&T)                 10.3            1               35.6             j                45.6                               32.6             j


                             ALPHA-BHC                  0.8                             0.9                               0.9                                1.3
                                HC13                    0.1             1               0.1                               0-1                                ni
                             BETA-BHC                    0              ND               0               ND                0                ND                 0             ND
                             GAMMA-BHC                   0              ND               0               ND                0                ND                 0             ND
                             DELTA-BHC                   0              ND               0               ND                0                ND
                         HEPLACHI-OR 0
                                                                                         0               ND                0                ND               0. i






                                                       Mussel Watch Project Year 8 - Pesticides and PCBs Data


                           INVEST#:              ESBD                         MBGP                          MBLR                           MBCB
                             ID:            Espiritu Santo              Matagorda Bay                  Matagorda Bay                 Matagorda I@ay
                            SITE:           Bill Day's Reef            Gallinipper Point            lavaca River Mouth              Carancahua Bay
                        LABSAMNO:               K7044                         K7036                         K7038                          K7040
                       SAMPLE TYPE-              SAMP                         SAMP                          SAMP                           SAMP
                           UNIT-                 ng/g                         ng/g                           ng/g                          ng/g
                           Analyte               Conc       DB gUAL           Conc        DB QUAL            Conc        DB QUAL           Conc       DB gUAL



                      HEVrA-EPOXIDE                0           ND             0.4                            0.2                           0.7
                      OXYCHLORDANE,                0           ND             0.1                            0.1                           0.2
                   GAMMA-CHLORDANE,               0.3                          1                             0.7                           1.3
                   ALPHA-CHLORDANE *              0.4                         0.9                            0.9                           1.6
                   TRANS-NONACHLOR *              0.3                         1.3                            0.9                           1.6
                      CIS-NONACHLOR               0.2                         1.3                            0.7                           1.5
                           ALDRIN                  0           ND              0             ND              0               ND             0            ND
                           DIELDRIN               0.9                         1.3                            0.8                            2
                           ENDRIN                  0           ND              0             ND              0               ND             0            ND
                           MIREX                   0           ND             0.3                            0               ND            0.4
                      2,4'DDE (O.PIDDE)           0.1                         0.2                            0               ND            0.2
      00              4,4-DDE (P,P'DDE)           7.5                         26.2                           7                             19.2
                      2.4'DDD (O,P'DDD)            0           ND             0.6                            0.3                           0.3
                      4.4'DDD IP,P'DDD)           0.7                         2.4                            1.2                           3.9
                      2,4'DDT (O.P-DD-n           0.2                         0.3                            0               ND            0.6
                      4.4'DDT (P.PIDDII           1.1                         1.6                            0.5                           1.4


                   PCB # (CLORINATION)
                      NOAA S&T PCBs
                           8 (CL2)                 0           ND              0             ND              0               ND             0            ND
                           18 (CL3)                0           ND              0             ND              0.2                           0.2
                           28 (CL3)               0.2           j             0.5                            0.5                           0.4
                           44 (CIA)                0           ND             0.8                            1.1                            0            ND
                           52 (CIA)                0           ND             1.2                            2.4                           0.9            1
                           66 (CIA)                0           ND              0             ND              1.2                            0            ND
                           101 (CL5)              0.3                         1.7                            2.1                            1
                           105 (CL5)              0.1                         0.4                            0.9                           0.4
                      110/77 (CL5/4)               0           ND             0.2                            1.9                            0            ND






                                                     Mussel Watch Project Year 8 - Pestictdes and PCBs Data


                         INVEST#:               ESBD                        MBGP                          MBLR.                         MBCB
                           ID:            Espiritu Santo              Matagorda Bay                Matagorda Bay                 Matagorda Bgy
                          SITE:           Bill Day's Reef            Gallinipper Point           Lavaca River Mouth             Carancahma Bay
                       LABSAMNO:                K7044                       K7036                         K7038                         K7040
                     SAMPLE TYPE:               SAMP                        SAMP                          SAMP                          SAMP
                          UNIT.                 ng/g                        ng/g                          ng/g                          ng/g
                         Analyte                Conc      DB QUAL           Conc       DB QUAL            Conc        D13 QUAL          Conc      DB QUAL


                 118/108/149(CL5/5/6)           0.3           J             1.8                           2.1                           0.8           J
                         128 (CL6)               0           ND              0            ND              0              ND             2.3
                         138 (CLO               1.4                         4.5                           4.3                           5.6
                         126 (CL5)               0           ND              0            ND              0              ND             0            ND
                         153 (CL6)              1.1                         3.4                           3.6                           2.1
                         170 (CL7)              0.4           J              0            ND              0              ND             0            ND
                         180 (CL7)               0           ND             0.5            J              0              ND             0            ND
                 187/182/159(CL7/7/6)           0.3           J              2                            1.6                           1.1
                         195 (CL8)               0           ND              0            ND              0              ND             0            ND
                         206 (CL9)               0           ND              0            ND              0              ND             0            ND
                         209 (CLIO)              0           ND              0            ND              0              ND             0            ND
      OD           Surrogate Recoveries
      OD
                         DBOFB%:                79.1                        80.2                          76.8                          72.2
                         PCB#103%:              84.1                        85.3                          83.8                          73.7
                         PCB# 198%:             79.3                        85.7                          77.3                          82.4



   m m m m m m m m m m m m                                                                                          m m m m m m M

                                                        Mussel Watch Project Year 8 - Pesticides and PCB9 Data


                             INVEST#-                   MBT?                        MBEM                       BRCL                       BRFS
                               ID:               Matagorda Bay                Matagorda Bay              Brazos River                Brazos River
                              SITE:            Tres Palaclos Bay             East Matagorda              Cedar Lakes              Freeport Surfs1de
                             LABSAMNO:                  K7026                       K7028                      K7002                      K7000
                         SAMPLE TYPE:                   SAMP                        SAMP                       SAMP                       SAMP
                              UNIT:                     ng/g                        ng/g                       ngJg                       ng/g
                             Analyte                    Cone      DB QUAL           Conc      DI3 QUAL         Conc    DB QUAL,           Conc       DB QUAL




                         RECEIPT DATE:                  12/16/92                    12/16/92                   12/9/92                    12/9/92
                             QC13ATCH:                  M1232                       M1232                      M1232                      M1232
                      EXTRACTION DATE:                  9/14/93                     9/14/93                    9/14/93                    9/14/93
                             METHOD:                    GCMS                        GCMS                       GCMS                       GCMS
                        ANALYSIS DATE:                  10/20/93                    10/20/93                   10/19/93                   10/19/93
                             METHOD:                    GCECD                       GCECD                      GCECD                      GCECD
                        ANALYSIS DATE:                  7/30/94                     7/30/94                    7/29/94                    7/29/94
                             MATTUX:                    TISSUE                      TISSUE                     TISSUE                     TISSUE
                             SUBMAT.
                             WE-TWT`-                   15.36                       15.24                      15.13                      15.28
                             DRYWT:                     2.57                        2.73                       1.79                       2.69
       OD                    WTUNITS:                   GRAMS        DRY            GRAMS        DRY           GRAMS      DRY             GRAMS         DRY
       co                    PCTSOLIDS:                 16.70%                      17.900/6                   11.80%                     17.60%
                             Lipid Weight:
                             TOTAL LIPID:               8.2                         7.34                       3.85                       6.69
                             LIPID UNITS:               % DRY                       % DRY                      % DRY                      % DRY
                              VOL.
                             VOLUNITS:                  =RS                         LITERS                     LITERS                     LrMRS


                             DBOF13:                    73.9                        76.3                       75.5                       80.7
                             PCB#103:                   77.2                        79.8                       79.3                       79.1
                             PCB#198:                   75                          79.9                       78                         84.2
                             TOTAL BHCs                 1.6                         1.6                        1.2         J              2.1
                    70T CHLORDANES WJJ                  4                           2.4                        3.8                        11.6
                    TOT CHLORDANES (S&TJ                1.4                         1.2           J            1.7         J              4.8
                             TOTAL DDTs                 56.1                        7.2                        65.1                       292
                       TOTAL PCBs (S&1J                 35.3                        11.7          J            46.1                       189.9


                             ALPHA-BHC                  0.9                         0.8                        0.4         J              0.8
                              HCB                       0                           0             J            0.4         J              1.2
                             BETA-BHC                   0.5                         0.4                        0           ND             0.3
                             GAMMA-BHC                  0.2            J            0.3           J            0.7                        0.9
                             DELTA-BHC                  0.1            J            0             J            0           ND             0             ND
                          HEPTACHLOR                    0             J             0             J            0.1         J              0.3            J






                                                      Mussel Watch Project Year 8 - Pesticides and PCBs Data


                            INVEST#:                  MBTP                     MBEM                        BRCL                      BRFS
                              ID:              Matagorda Bay               Matagorda Bay               Brazos River               Brazos River
                             SITE:            Tres Palaclos Bay            East Matagorda              Cedar Lakes             Freeport Surfs1de
                         LABSAMNO:                    K7026                    K7028                       K7002                     K7000
                        SAMPLE TYPE:                  SAMP                      SAMP                       SAMP                      SAMP
                            UNIT:                     ng/g                      ng/g                       ng/g                      ng/g
                            Analyte                   Conc      DB QUAL         Conc        DB QUAL        Conc     DB QUAL          Conc         DB QUAL


                       HEPTA-EP03UDE                  0.1           J            0.1            J           0.1         J             0.5
                       OXYCHLORDANE                   0.1           J            0.1            J           0           J             0.3             J
                    GAMMA-CHLORDANE                   1.1                        0.7                        1.1                       3.5
                    ALPHA-CHLORDANE 0                 0.5                        0.7                        0.7                        2
                    TRANS-NONACHLOR 4                 0.7                        0.4                        0.8                        2
                       CIS-NONACHLOR                  1.4                        0.4                        1                         2.9
                            ALDRIN                    0            ND             0            ND           0          ND             0.5
                            DIELDRIN                  0            ND             0            ND           0.6                       3.5
                            ENDRIN                    0            ND            0.1            J           0          ND              0             ND
                            MIREX                     0.4           J             0             J           0.7                       5.4
                       2.4'DDE (O.P'DDEJ              0.4                        0.1            J           0.2         J             0.8
                       4.4'DDE (P.P'DDE)              48.6                        6                         60                       277.2
                       2,4'DDD (O.P'DDD)              0.5                         0             J           0.6         J             1.8
                       4,4*DDD (P.P'DDD)              4.7                        0.7                        2.7                       9.8
                       2.4'DDT (0,P'DDII              0.8                        0.2            J           0.8                       1.1
                       4,4'DDT (P.P'DDT]              1.1                        0.1            J           0.9                       1.3


                    PCB # (CLORINATION)
                       NOAA S&T PCBs
                            8 (CL2)                   0.1           J             0            ND           0.1         J             0.6             J
                            18 (CL3)                  0.1           J            0.2            J           0          ND              0             ND
                            28 (CL3)                  0            ND             0             J           0.1         J             0.2             J
                            44 (CIA)                  0            ND             0            ND           0.3         J             1.4
                            52 (CIA)                  0.6           J            0.3            J           2.1                      25.3
                            66 (CIA)                  0.1           i             0            ND           0.3         J             0.9
                            101 (CL5)                 0.4           J            0.3            J           1.5                       7.6
                            105 (CL5)                 0.1           J             0             J           0          ND             1.3
                        110/77(CL5/4)                 0.2           J            0.2            J           1.6                       7.8






                                                        Mussel Watch Project Year 8 - Pesticides and PC139 Data


                             INVEST#-                   MBTP                       MBEM                      BRCL                      BRFS
                                ID:              Matagorda Bay               Matagorda Bay              Brazos River               Brazos River
                               Sm              Tres Palaclos Bay             East Matagorda             Cedar Lakes             Freeport Surfaide
                             LABSAMNO:                  K7026                      K7028                     K7002                     K7000
                          SAMPLE IYPE:                  SAMP                       SAMP                      SAMP                      SAMP
                               UNrr:                    ng/g                       ng/g                      ng/g                      ng/g
                              Analyte                   Conc      DB QUAL          Conc      DB QUAL         Conc    DB QUAL           Conc       DB QUAL


                      118/108/149(CL5/5/6)              0.2           J            0.1           J           1.3                       9.9
                             128 (CL)6)                 3.1                        0.2           J           2.1                       5.3
                             138 (CL6)                  6.5                        1.3                       5.4                       15.4
                             126 (CL5)                  0            ND             0           ND           0           ND             5
                             153 (CL6)                  1.7                        0.8                       4.8                       13.2
                             170 (CL7)                  0.4           J            0.4           J           0           ND             0             ND
                             180 (CL7)                  0.2           J            0.3           J           0.8         J             3.7
                      187/182/159(CL7/7/6)              1.3                        0.2           J           0.9         J             2.8
                             195 (CL8)                  0.2           J            0.1           J           0           ND             0             ND
                             206 (CL9)                  0            ND             0           ND           0           ND             0             ND
                             209 (CLIO)                 0            ND             0           ND           0           ND            0.1             J

        CD             Surrogate Recoveries
                             DBOFB%:                    73.9                       76.3                      75.5                      80.7
                             PCB#103%:                  77.2                       79.8                      79.3                      79.1
                             PCB#198%:                  75                         79.9                      78                        84.2






                                                              Mussel Watch Project Year 8 - Pesticides and PCBs Data


                   INVEST#:                     GBCR                           GBOB                           GBT`D                       GBYC                           GBSC
                      ID:                Galveston Bay                  Galveston Bay                 Galveston Bay                 Galveston Bay                 Galveston Bay
                     SITE:             Confederate Reef                   Offats Bayo                 Todd's Dump                    Yacht Club                   Ship Channel
                   LABSAMNO:                    K7006                          K7010                          K7012                       K7004                          K7008
               SAMPLE TYPE:                     SAMP                           SAMP                           SAMP                        SAMP                           SAMP
                     UNIT.                      ng/g                           ng/g                           ng/g                        ng/g                           ng/g
                   Analyte                      Conc        DI3 QUAL           Conc       DB QUAL             Conc     DB QUAL            Conc       D13 QUAL            Conc       DB QUAL



              RECEIPT DATE:                     12/10/92                       12/10/92                       12/11/92                    12/10/92                       12/10/92
                   QCBATCH:                     M1232                          M1232                          M1232                       M1232                          M1232
            EXTRACTION DATE:                    9/14/93                        9/14/93                        9/14/93                     9/14/93                        9/14/93
                   METHOD:                      GCMS,                          GCMS                           GCMS                        GCMS                           GCMS
              ANALYSIS DATE:                    10/19/93                       10/19/93                       10/20/93                    10/19/93                       10/19/93
                   METHOD:                      GCECD                          GCECD                          GCECD                       GCECD                          GCECD
              ANALYSIS DATE:                    7/29/94                        7/30/94                        7/30/94                     7/29/94                        7/30/94
                   MATRIX                       TISSUE                         TISSUE                         TISSUE                      TISSUE                         TISSUE
                   SUBMAT:
                   WETwr:                       15.02                          15.1                           15.46                       15.69                          15
                   DRYWT-                       1.97                           2.77                           2.59                        2.85                           3.13
       CD          W7UNITS:                     GRAMS          DRY             GRAMS         DRY              GRAMS        DRY            GRAMS          DRY             GRAMS         DRY
                   PCTSOLIDS:                   13.100,6                       18.40%                         16.700/6                    18.100/6                       20.80%
                   Lipid Weight:
                   TOTAL LIPID:                 5.39                           8.38                           8.82                        8.38                           11.56
                   LIPID UNITS:                 % DRY                          % DRY                          % DRY                       % DRY                          % DRY
                      VOL:
                   VOLUNITS:                    LITERS                         LITERS                         LITERS                      LITERS                         LITERS


                   DBOFB:                       77.7                           78                             78.5                        73.4                           74.8
                   PCB#103:                     83.5                           79.5                           81.1                        75.4                           54.4
                   PCB# 198:                    79.4                           79.1                           82.6                        75.8                           75.1
                   TOTAL BHCs                   1.5              J             2.5                            6.6                         9.5                            18.4
          TOT CHLORDANES (ALIJ                  4.6                            207.6                          12.1                        36.5                           129.9
         TOT CHLORDANES, (S&11                  1.9              J             117.6                          6                           20.7                           74.9
                   TOTAL DDTs                   5.9                            49.8                           10                          26.2                           107.1
             TOTAL PCBs (S&11                   50.2                           195.9                          64.8                        162.7                          760.4

                   ALPHA-BHC                    0.6                            0.6                            1.8                         2.4                            4.7
                      HCB                        0               J               0            J               0                            0                             0             Nr)
                   BETA-BHC                     0.3              J             0.6                            1.8                         2.9                            6.3
                   GAMMA-BHC                    0.4              J             1.2                            2.3                         3.1                            5.8
                   DEI,TA-BHC                   0.2              J             0.1             J              0.7                         1.1
               TJTPT@A  I IT @"  0               -
               I I@r I    ILAJIN                 V                                                            V                           0.1






                                                         Mussel Watch Project Year 8 - Pesticides and PCBs Data


                   INVEST#:                GBCR                          GBOB                      GBM                          GBYC                       GEISC
                     ID:              Galveston Bay                Galveston Bay              Galveston Bay              Galveston Bay               Ga*eston Bay
                   SITE:             Confederate Reef               Offats, Bayo              Todd's Dump                  Yacht Club                Ship Channel
                LABSAMNO:                  K7006                         K7010                     K7012                        K7004                      K7008
              SAMPLE TYPE:                 SAMP,                         SAMP                      SAMP                         SAMP                       SAMP
                   UNIT.                    ng/g                         ng/g                       ng/g                        ng/g                       ng/g
                   Analyte                  Cone       DB QUAL           Cone      DB QUAL          Cone      DB QUAL           Cone     DB QUAL           Cone      DB Q


             HEPTA-EPO)aDE                   0.1            J            3.7                         2.4                        6.9                        20.8
             OXYCHLORDANE                    0.1            J            3.5                         0.4                        1                          2.7
           GAMMA-CHLORDANE                   1.4                         58.2                        3.2                        10                         35.5
           ALPHA-CHLORDANE 0                 1.1                         57.9                        1.8                        8                          30.5
           TRANS-NONACHLOR *                 0.7                         55                          1.7                        5.8                        22.8
             CIS-NONACHLA)R                  1.1                         28.2                        2.4                        4.8                        16.8
                   ALDRIN                    0             ND            0             J             0           ND             0            ND             0           ND
                   DIELDRIN                  0.5            J            9.7                         3.8                        9.3                        30.3
                   ENDRIN                    0             ND            0             J             0           ND             0            ND             0           ND
                   MIREX                     0             ND            0.2           J             0.1          J             0.4                        0.3
             2.4-13DE (0,P'DDE)              0.1            J            0.1           J             0.1                        0.3           J            1.1
             4,4'DDE (P,PDDE)                3.9                         32.5                        5.8                        13.8                       57.9
       (0    2.4'DDD (O.P'DDD)               0.1            J            0.8                         0.4                        1.2                        5.1
             4.4'DDD (P,PDDD)                1.4                         11.1                        3                          9.5                        37.5
             2.4'DDT (0,P'DDTI               0.3            J            1.1                         0.4          J             0.8                        2.9
             4.4'DDT (P,P'DD11               0.1            J            4.3                         0.3                        0.6                        2.7


           PCB; # (CLORINATION)
             NOAA S&T PCBs
                   8 (CL2)                   0.3            J            0.8                         0           ND             0            ND             0           ND
                   18 (Cw)                   0             ND            1.1                         0.2          J             1.2                        7.5
                   28 (CL3)                  0.1            J            1.9                         0.6          J             2.6                        12.7
                   44 (CIA)                  0.2            J            10.8                        2.2                        7.2                        26.8
                   52 (CIA)                  1.3                         10.1                        2.6                        10.4                       45.1
                   66 (CIA)                  0.2            J            2.4                         0.5          J             1.5                         8
                   101 (CL5)                 2.5                         11.8                        2.7                        9                          49.8
                   105 (CL5)                 0.4            J            2.1                         0.5          J             3.5                        18.1
              110/77 (CL5/4)                 1.6                         14.2                        2.5                        8                          63.8






                                                            Mussel Watch Project Year 8 - Pesticides and PCBs Data


                   INVEST#:                   GBCR                           GBOB                       GBM                          GBYC                         GBï¿½-C
                      ID:               Galveston Bay                 Galveston Bay               Galveston Bay               Galveston Bay                Galveston Bay
                    SITE:             Confederate Reef                  Offats Bayo                Todd's Dump                  Yacht Club                  Ship Channel
                   LA13SAMNO:                 K7006                          K7010                      X7012                        K7004                        K7008
               SAMPLE TYPE-                   SAMP                           SAMP                       SAMP                         SAMP                         SAMP
                    UNtr.                     ng/g                           ng/g                       ng/g                         ng/g                         ng/g
                   Analyte                    Cone        DB, QUAL           Conc     DB QUAL           Conc       DB QUAL           Conc      DB QUAL            Conc      DB,


           118/108/149(CL5/5/6)               1.9                            11.8                       2.4                          6.1                          37.8
                   128 (CL65)                 0.2              J             0.8                        0.3            J             0.7            J             3.1
                   138 (CL6)                  4.2                            9.3                        4.8                          8.7                          39
                   126 (CL5)                   0              ND             0            ND             0            ND              0            ND             0            ND
                   153 (CLAG)                 7.1                            12.9                       7.9                          14.2                         55.2
                   170 (CL71                  0.9              J             0.5           J            0.8            J             0.3            J             0            ND
                   180 (CL7)                  0.8              J             6.6                        0.6            J             2.6                          8.6
           187/182/159(CL7/7/6)                2                             2.3                        2.4                          3.4                          8
                   195 (CL8)                   0              ND             0.6           J             0            ND              0            ND             0             J
                   206 (CL9)                   0              ND             0.4           J             0            ND              0            ND             0.1           J
                   209 (CLIO)                 0.3              J             0             J             0            ND              0            ND             0.3           J

       CD
            Surrogate Recoveries
                   DBOF'B%:                   77.7                           78                         78.5                         73.4                         74.8
                   PCB#103%:                  83.5                           79.5                       81.1                         75.4                         68.3
                   PCB#198%:                  79.4                           79.1                       82.6                         75.8                         75.1






                                                             Mussel Watch Project Year 8 - Pesticides and PCBs Data


                                 INVEST#:                   GBHR                         SLBB                           CLSJ                           CLLC
                                    ID:              Galveston Bay                  Sabine Lake                  Calcasieu Lake                 Calcasieu Lake,,
                                  SITE:               Hanna Reef                  Blue Buck Point               St. Johns island                 Lake Charles
                                 LABSAMNO:                  K7014                        K7016                          K7020                          K7018
                                 SAMPLE TYPE:               SAMP                         SAMP                           SAMP                           SAMP
                                  UNIT:                     ng/g                         ng/g                           ng/g                           ng/g
                                 Analyte                    Cone      DB QUAL            Cone       DB QUAL             Cone        DB QUAL            Cone      DB QUAL



                                 RECEIPT DATE:              12/11/92                     12/11/92                       12/12/92                       12/11/92
                                 QCBATCH:                   M1232                        M1232                          M1232                          M1232
                          EXTRACTION DATE:                  9/14/93                      9/14/93                        9/14/93                        9/14/93
                                 METHOD:                    GCMS                         GCMS                           GCMS                           GCMS
                           ANALYSIS DATE:                   10/20/93                     10/20/93                       10/20/93                       10/20/93
                                 METHOD:                    GCECD                        GCECD                          GCECD                          GCECD
                           ANALYSIS DATE:                   7/30/94                      7/30/94                        7/30/94                        7/30/94
                                 MATRIX:                    TISSUE                       TISSUE                         TISSUE                         TISSUE
                                 SUBMA7%
                                 WETWT.-                    15.39                        15-27                          15.06                          15.09
                                 DRYW"r%                    2.4                          2.68                           1.93                           3.07
       CD                        W`IUNITS:                  GRAMS        DRY             GRAMS         DRY              GRAMS         DRY              GRAMS        DRY
                                 PCTSOLIDS:                 15.60%                       17.600/6                       12.800/6                       20.400/6
                                 lApid Weight:
                                 TOTAL UPID:                6.64                         8.03                           5.65                           10-56
                                 LIPID UNITS:               % DRY                        % DRY                          % DRY                          % DRY
                                  VOL:
                                 VOLUNITS:                  LITERS                       LITERS                         LITERS                         UIERS


                                 DBOF'B:                    78.8                         77.3                           79.8                           73.9
                                 PCB# 103:                  80.7                         79.4                           83.9                           79
                                 PCB#198:                   81.9                         82.4                           82.7                           83.6
                                 7WAL BHCs                  2.2                          1.4             J              0.4             J              0.2            J
                       TOT CHLORDANES (ALL)                 3.8                          6.9                            2.1                            21.9
                       TOT CHLORDANEs fs"                   1.6           J              2.9                            0.8             J              6.8
                                 TOTAL DDTs                 5.4                          7.8                            4                              61.4
                          TOTAL PCBs (S&TJ                  25.3          J              40.1                           35              J              350.6


                                 ALPHA-BHC                  0.9                          0.9                            0              ND              0             ND
                                  HC13                      0             J                0             J              0               J              1.4
                                 BETA-BHC                   0.6                            0            ND              0               J              0             ND
                                 GAMMA-BHC                  0.6                          0.4                            0.3             J              0.2            J
                                 DELTA-BHC                  0.1           J              0.1             J              0              ND              0             ND
                                 HEPTACHLOR.                0             J              0.1             J              0               J              0.4






                                                      Mussel Watch Project Year 8 - Pesticides and PCBs Data


                             INVESr#:             GBHR                        SLBB                        CLSJ                        ;C-Uc
                              ID:             Galveston Bay               Sabine Lake               Calcasieu Lake              Calcasieu Lake
                             Srm:              Hanna Reef               Blue Buck Point             St. Johns Island             Lake Charles
                          LABSAMNO:               K7014                       K7016                       K7020                       K7018
                        SWPLE 7YPE:               Smp                         SAMP                        SAMP                        SAMP
                             UNIT:                 ng/g                       ng/g                         ng/g                       ng/g
                             Analyte               Conc      DB gUAL          Conc       DB gUAL          Conc       DB QUAL          Conc      DB Q


                       HEPTA-EPO)aDE                  0.2         J            0.4           J             0.3           J             2
                       OXYCHLORDANE                   0.2         J            0.3           J             0.1           J            0.6
                     GAMMA-CHLORDANE                  0.9                      2                           0.8                        12.4
                     ALPHA-CHLORDANE *                0.7                      1.3                         0.3           J            2.4
                     TRANS-NONACHLOR *                0.7                      1.2                         0.3           J            2. 1
                       CIS-NONACHLOR                  1                        1.7                         0.4           J             2
                             ALDRIN                   0          ND            0            ND             0             ND            0            ND
                             DIELDRIN                 0.9                      0.9                         0.6                        6.5
                             ENDRIN                   0          ND            0.2           J             0             ND            0            ND
                             MIREX                    0.1         J            0.2           J             0             J            0.4
                       2.4'DDE (O.P'DDE)              0           J            0             J             0             ND           0.3           J
                       4,4'DDE (P,P'DDE)              4                        5.2                         3.1                        58.5
     (D                2.4'DDD (0,P'DDD)              0.1         J            0.1           J             0             J            0.7
     a)                4.4'DDD (P,IYDDD)              1                        1.8                         0.8                        1.9
                       2.4'DDT (0,P'DM                0.1         J            0.4                         0             J             0            ND
                       4.4'DDT (P,P'DDII              0.1         J            0.2           J             0             J             0            ND


                     PCB # (CLORINAMON)
                        NOAA S&T PCBs
                             8 (CL2)                  0          ND            0            ND             7.7                        85.6
                             18 (CL3)                 0.1         J            0.1           J             0.1           J            0.7
                             28(CL3)                  0.1         J            0.2           J             0.1           J            2.5
                             44 (CIA)                 0.2         J            0.5           J             0.1           J            2.4
                             52(CLA)                  0.7         J            1.5                         0.4           J             0            ND
                             66 (CIA)                 0.1         J            0.2           J             0.1           J            2.7
                             101 (CL5)                1.1                      1.4                         0.7           J            11.9
                             105 (CL5)                0.1         J            0.4           J             0.1           J            1.3
                        110/77 (CL5/4)                0.8         J            2.2                         0.4           J            13.4





                                                     Mussel Watch Project Year 8 - Pesticides and PCBs Data


                           INVEST#:                GBHR                      SLBB                        CLSJ                        CLLC
                              ID:            Galveston Bay               Sabine Lake               Calcasieu lake             Calcasieu Lake
                             SITE:            Hanna Reef               Blue Buck Point            St. Johns Island             Lake Charles
                           LABSAMNO:               K7014                     K7016                       K7020                       K7018
                        SAMPLE TYPE:               SAMP                      SAMP                        SAMP                        SAMP
                            UNIT:                  ng/g                      ng/g                        ng/g                        ng/g
                           Analyte                 Conc     DB QUAL          Conc       DB QUAL          Conc      DB QUAL           Conc     1313 QUAL


                    118/108/149(CL5/5/6)           0.7          J            1.1                         0.4            J            10.2
                           128 (CL6)               0.2          J            0.3            J            0.1            J            1.2
                           138 (CL6)               2.4                       3.5                         1.8                         12.9
                           126 (CL5)                 0          ND            0            ND             0            ND            0           ND
                           153 (CL6)               3.2                       4.4                          2                          17.2
                           170 (CL7)               0.4          J            0.7                         0.5            J            0.9
                           180 (CL7)               0.1          J            0.8                         0.1            J            2.9
                    187/182/159(CL7/7/6)             1                        1                          0.5            J            2.4
                           195 (CL8)                 0          ND            0            ND            0.2            J            1.1
                           206 (CL9)                 0          ND            0            ND             0            ND            0            J
                           209 (CLIO)                0          ND            0            ND             0            ND            0           ND

                     Surrogate Recoveries
                           DBOFB%:                 78.8                      77.3                        79.8                        73.9
                           PCB#103%:               80.7                      79.4                        83.9                        79
                           PCB#198%:               81.9                      82.4                        82.7                        83.6






                                                         Mussel Watch Prqject, Year 8 - Pesticides and PCBs Data


                             INVEST#:                   JHJH                            VBSP                       ABOB                        CLCL
                               ID:            Joseph Harbor Bayou               Vermillion Bay              Atchafalaya Bay              Calflou Lake
                               SITE.           Joseph Harbor Bay                Southwest Pass               Oyster Bayou                Caillou Lake
                             LABSAMNO:                  K7022                           K7046                      K7056                       K7058
                         SAMPLE TYPE:                   SAMP                            SAMP                       SAMP                        SAMP
                              UNIT:                     ng/g                            ng/g                       ng/g                        ng/g
                             Analyte                    Conc         DB QUAL            Conc     DB QUAL           Conc       DB QUAL          Conc    DB QUAL



                        RECEIPT DATE:                   12/12/92                        1/6/93                     1/7/93                      1/7/93
                             QCBATCH:                   M1232                           M1233                      M1233                       M1233
                      EXTRACTION DATE:                  9/14/93                         11/11/93                   9/14/93                     9/14/93
                             METHOD:                    GCMS                            GCMS                       GCMS                        GCMS
                        ANALYSIS DATE:                  10/20/93                        12/23/93                   10/25/93                    10/25/93
                             METHOD:                    GCECD                           GCECD                      GCECD                       GCECD
                        ANALYSIS DATE:                  7/30/94                         8/23/94                    8/24/94                     8/24/94
                             MATRIX:                    TISSUE                          TISSUE                     TISSUE                      TISSUE
                             SUBMAT,
                             VIETNW..                   15.02                           15.08                      15.04                       15.24
                             DRYWT-                     2.01                            1.78                       2.3                         2.46
                             WTUNITS:                   GRAMS           DRY             GRAMS        DRY           GRAMS         DRY           GRAMS      DRY
        OD                   PCTSOLIDS:                 13.40%                          11.800/0                   15.300/6                    16.200/6
                             Liptd Weight:
                             TOTAL LIPID:               7.58                            11.01                      12.22                       10.66
                             LIPID UNITS:               % DRY                           % DRY                      % DRY                       % DRY
                               VOL:
                             VOLUNITS:                  LITERS                          LITERS                     LITERS                      LITERS


                             DBOFB:                     77.2                            75.3                       75.1                        77.8
                             PCB#103:                   82.1                            81.6                       73.1                        76
                             PCB#198:                    78                             77                         83.3                        87.5
                             TOTAL BHCs                  1                1             2.2          1             1.3            1            1.4           1
                    TOT CHLORDANES (ALL)                 2.7                            17                         6.3                         5.4
                    TOT CHLORDANES (S&Tj                 1.1              1             9.9                        3.7                         3.1
                             TOTAL DDTs                 25.2                            52.7                       14.2                        6.8
                       TOTAL PCBs (S&T)                 32.6              1             87.2                       48.5                        32.2          1


                             ALPHA-BHC                   0.6                            1.4                        0.8                         1.1
                                HCB                      0                              0             ND           0.1             '1          0.1           1
                             BETA-BHC                    0                J             0             ND            0             ND           0           ND
                             GAMMA-BHC                   0.3              1             0.8                        0.5                         0.3           1
                             DELTA-BHC                   0               ND             0             ND            0             ND           0           ND
                         HE17AC' 1"111-100 R6                                                                                                                T
                                                                         N D            0.2           i            0. i






                                                         Mussel Watch Project Year 8 - Pesticides and PCEls Data


                             INVEST#:                    JHJH                          VBSP                       ABOB                       CLCL
                               ID-             Joseph Harbor Bayou               Vennillion Bay              Atchafalaya Bay              CallIou Lake
                              SITE:             Joseph Harbor Bay                Southwest Pass               Oyster Bayou                Calliou I.A6
                           LABSAMNO:                     K7022                         K7046                      K7056                      K7058
                         SAMPLE TYPE:                    SAMP                          SAMP                       SAMP                       SAMP
                              UNIT:                      ng/g                          ng/g                       ng/g                        ng/g
                             Analyte                     Conc         DB QUAL          Conc       DB QUAL         Conc         DB QUAL        Conc      DB QUAL


                        HEPTA-EPOXIDE                    0.3              J            2.7                           0.9                       0.6
                        OXYCHLORDANE                     0                J            0.5            J              0.2           J           0.2          J
                      GAMMA-CHLORDANE                    0.8                           3.7                           1.4                       1.3
                      ALPHA-CHLORDANE *                  0.5              J            3.6                           1.4                       1.3
                      TRANS-NONACHLOR *                  0.3              J            3.5                           1.3                       1.2
                        CIS-NONACHLOR                    0.8                           2.9                           0.9                       0.8
                             ALDRIN                      0               ND             0            ND              0            ND            0          ND
                             DIELDRIN                    1.5                           11.5                          3                         1.7
                             ENDRIN                      0.3              J            0.8                           1                         0.4          J
                             MIREX                       0.1              J            0.5            J              0            ND            0          ND
                        2.4'DDE (O.P'DDE)                0.1              J             0            ND              0.3           J            0           J
                        4ADDE (P,P'DDE)                  15.5                          30.1                          7.4                       3.2
                        2,4'DDD (O,P'DDD)                0.2              J            1.2                           0.3           J           0.1          J
        to              4.4'DDD (P.P'DDD)                9                             15.4                          4                         1.6
                        2.4'DDT (O,P'DDTI                0.2              J            1.7                           0.6                       0.4
                        4.4'DDT (P.P'D"                  0.1              J            4.3                           1.6                       1.5


                      PCB # (CLORINAMON)
                        NOAA S&T PCBs
                             8 (CL2)                     0               ND             0            ND              0            ND            0          ND
                             18 (CL3)                    0               ND             0            ND              0            ND           0.1          J
                             28 (CL3)                    0                J            0.3            J              0.4           J           0.4          J
                             44 (CIA)                    0.1              J            1.3                           0            ND            0          ND
                             52 (CIA)                    0.2              J            1.8                           1.3                       1.1
                             66 (CIA)                    0.4              J            0.6            J              0.7           J           0.4          J
                             101 (CL5)                   1.3                           4.2                           3                         2.1
                             105 (CL5)                   0.1              J            1.7                           0.7           J           0.5          J
                         110/77 (CL5/4)                  1.6                           4.4                           1.3                       0.6          J






                                                       Mussel Watch Project Year 8 - Pesticides and PCBs Data


                          INVEST#*                     JHJH                          VBSP                      ABOB                       Cl.CL
                             ID:            Joseph Harbor Bayou               Vermillion Bay             Atchafalaya Bay              Caillou Lake
                            SrM:              Joseph Harbor Bay               Southwest Pass               Oyster Bayou               Caillou Lake
                          LABSAMNO:                    K7022                         K7046                     K7056                      K7058
                       SAMPLE'TYPE:                    SAMP                          SAMP                      SAMP                       SAMP
                            UNM                        ng/g                          ng/g                      ng/g                       ng/g
                           Analyte                     Conc        DB QUAL           Conc     DB QUAL          Conc        DB QUAL        Conc      DB QUAL


                   118/108/149(CIZ/5/6)                0.7             J             2.3                        2.2                         1.6
                          128 (CL6)                    0.2             J             0            ND            0.9                         0.5         J
                          138 (CL6)                    3.1                           10.2                       4.8                         3.6
                          126 (CIZ)                    0               ND            0            ND             0             ND           0          ND
                          153 (CL6)                    4.6                           9.6                        5.7                         3.6
                          170 (CL7)                    0.5             J             0            ND            0.3            J            0          ND
                          180 (CL7)                    0.1             J             0            ND             0             ND           0          ND
                   187/182/159(CL7/7/6)                1.6                           4.6                        2.1                         1
                          195 (CL8)                    0.1             J             0            ND             0             ND           0          ND
                          206 (CL9)                    0               ND            0            ND             0             ND           0          ND
                          209 (CLIO)                   0               ND            0            ND             0             DID          0          ND

                    Surrogate Recoveries
      0
                          DBOFB%:                      77.2                          75.3                      75.1                       77.8
                          PCB#103%:                    82.1                          81.6                      73.1                         76
                          PCB#198%:                    78                            77                        83.3                       87.5






                                                            Mussel Watch Project Year 8 - Pesticides and PCBs Data


                             INVEST#:                  77BLB                       TBLF                         BBSD                          BBMB
                               ID:             Terrebonne Bay               Terrebonne Bay                Barataria Bay                 Barataria Bay,
                              SITE:               Lake Barre                  Lake Felicity             Bayou Saint Dents               Middle Bank
                             LABSAMNO:                 K7052                       K7054                        K7048                         K7050
                         SAMPLE IYPE:                  SAMP                        SAMP                         SAMP                          SAMP
                              UNIT:                    ng/g                        ng/g                         ng/g                          ng/g
                             Analyte                   Conc      DB QUAL           Conc      DB QUAL            Conc        DB QUAL           Conc     DB QUAL



                        RECEIPT DATE:                  1/7/93                      1/7/93                       1/6/93                        1/6/93
                             QCBA,TCH-                 M1233                       M1233                        M1233                         M1233
                      EXTRACTION DATE:                 9/14/93                     9/14/93                      9/14/93                       9/14/93
                             METF-IOD:                 GCMS                        GCMS                         GCMS                          GCMS
                        ANALYSIS DATE:                 10/24/93                    10/25/93                     10/24/93                      10/24/93
                             ME71-IOD:                 GCECD                       CCECD                        GCECD                         GCECD
                        ANALYSIS DATE:                 8/24/94                     8/24/94                      8/24/94                       8/24/94
                             MATRIX:                   TISSUE                      TISSUE                       TISSUE                        TISSUE
                             SUBMAT-
                             WE7w.                     15.1                        15.09                        15.2                          15-47
                             DRYW`r:                   2.2                         3.16                         2.66                          2.71
      0                      WIUNITS:                  GRAMS        DRY            GRAMS        DRY             GRAMS          DRY            GRAMS       DRY
                             PCTSOLIDS:                14.5M/6                     20.90%                       17-50%                        17.50%
                             Lipid Weight:
                             TOTAL LIPID:              8.14                        8.8                          11.77                         8.65
                             UPID UNITS:               % DRY                       % DRY                        % DRY                         % DRY
                              VOL.
                             VOLUNITS:                 LITERS                      LITERS                       LITERS                        LITERS


                             DBOFB:                    77.1                        69                           65.6                          75.3
                             PCB#103:                  86.4                        76.6                         79.5                          78.7
                             PCB#198:                  72.9                        75.1                         81.6                          77.9
                             TCTAL BHC9                1.1           J             1.2           J              1.43             J            1.3
                    TOT CHLORDANES WLL)                3.3                         3                            7.2                           6.4
                   TOT CHLORDANES (S"                  2                           1.5                          4.2                           3.8
                             TOTAL DDTs                2.3           J             3.3                          7.1                           5. 1
                       TOTAL PCB9 (S&11                16            J             18.3          J              21.1             J            26.3         J


                             ALPHA-BHC                 1.1                         0.9                          0.7                           0.9
                              HCB                      0.1           J             0.1           J              0.1              J            0           ND
                             BETA-BHC                  0            ND             0            ND              0.2              J            0           ND
                             GAMMA-BHC                 0            ND             0.3           J              0.5                           0.4
                             DELTA-BHC                 0            ND             0            ND              0.1              J            0           ND
                         HEPTACHLOR                    0            ND             0            ND               0              ND            0           ND






                                                        Mussel Watch Prqject Year 8 - Pesticides and PCBs Data


                             INVEST#:               TBLB                        713LF                       BBSD                        BBMB
                              ID:             Terrebonne Bay              Terrebonne Bay                Barataria Bay               Barataria Bay
                             SITE:              Lake Barre                 Lake Felicity             Bayou Saint Dents               Middle Bank
                          LABSAMNO:                 K7052                      K7054                       K7048                        K7050
                        SAMPLE TYPE:                SAMP                        SAMP                        SAMP                        SAMP
                             UNrr:                   ng/g                       ng/g                        ng/g                        ng/g
                             Analyte                Cone       DB QUAL          Cone       DB QUAL          Cone         DB QUAL        Cone       DB Q



                       HEPrA-EPOXIDE                 0.4           1            0.4                           1                           0.9
                       OXYCHLORDANE                  0.1           1            0.2            1             0.3             1            0.3          1
                     GAMMA-CHLA)RDANE                0.8                        0.9                          1.7                          1.4
                     ALPHA-CHLORDANE *               0.9                        0.3                          1.9                          1.5
                     TRANS-NONACHLOR *               0.7                        0.9                          1.3                          1.5
                       CIS-NONACHLOR                 0.4           1            0.5                           1                           0.9
                             ALDRIN                     0         ND             0            ND              0             ND            0           ND
                             DIELDRIN                   1                        1                           2.6                          3.1
                             ENDRIN                     0         ND             0            ND              0             ND            0           ND
                             MIREX                      0         ND             0            ND              0             ND            0           ND
                       2,4'DDE (0,PDDE)                 0         ND             0            ND              0             ND            0.2          1
                       -4.4'DDE (P.P'DDE)            1.6                        1.9                          3.9                          3
                       2,4'DDD (O.VDDD)                 0         ND             0            ND             0.3                          0           ND
                       4,4'DDD (P.P'DDD)             0.7                         1                           1.8                          1.7
       ba              2.4'DlYr (O.P'DIM                0         ND             0            ND             0.5                          0.2          j
                       4.4'DDT (P,P'DEM                 0         ND            0.3                          0.6                          0           ND


                     PCB # (CLORINATION)
                       NOAA S&T PCBs
                             8 (CL2)                    0         ND             0            ND              0             ND            0           ND
                             18 (CL3)                   0         ND             0            ND             0.4                          0.2          1
                             28 (CL3)                   0         ND             0            ND             0.1                          0.6          j
                             44 (CIA)                0.5           1            0.5            1             0.6                          0.9
                             52 (CIA)                0.6           1            0.6            j             0.7                          1.2
                             66 (CIA)                0.4           1             0            NO             0.3                          0.8
                             101 (CL5)                  1                       1.5                          1.4                          1.4
                             105 (CL51               0.2           1            0.3            1             0.3                          0.4          J
                        110/77 (CL5/4)                  0         ND             0            ND              0             ND            0           ND



 mmm mmmmm m@@mmm@ @ @ @
                                                       Mussel Watch Project Year 8 - Pesticides and PCBs Data


                          INVEST#:                TBLB                       TBLF                        BBSD                         BBMB
                             ID:            Terrebonne Bay             Terrcbonne Bay                Barataria Bay               Barataria Bar
                           SITE:              Lake Barre                 Lake Felicity             Bayou Saint Dents             Middle Bank
                          LABSAMNO:               K7052                      K7054                       K7048                        K7050
                       SAMPLE TYPE:               SAMP                       SAMP                        SAMP                         SAMP,
                           UNIT:                  ng/g                       ng/g                        ng/g                         ng/g
                          Analyte                 Cone       DB QUAL         Cone       DB QUAL          Cone         DB QUAL         Cone      DB QUAL



                   118/1081149(CL5/5/6)           0.8            J            1.2                         0.9                         1.3
                          128 (CL6)                0            ND            0            ND             0.2             J            0           ND
                          138 (CL6)               1.3                         1.8                         2.4                         1.8
                          126 (CL5)                0            ND            0            ND              0             ND            0           ND
                          153 (CL61               1.4                         1.8                         0.3             J            2
                          170 (CL7)               0.6            J            0.5           J             1.3                         0.6           J
                          180 (CL7)                0            ND            0            ND              0             ND           0.3           J
                  187/182/159(CL7/7/6)            0.3            J            0.4           J             0.7             J           0.6           J
                          195 (CLS)                0            ND            0            ND              0             ND            0           ND
                          206 (CL9)                0            ND            0            ND              0             ND            0           ND
                          209 (CLIO)               0            ND            0            ND              0             ND            0           ND

     0              Surrogate Recoveries
     CO                   DBOFB%:                 77.1                        69                         65.6                         75.3
                          PCB#103%:               86.4                       76.6                        79.5                         78.7
                          PCB#198%:               72.9                       75.1                        81.6                         77.9






                                                       Mussel Watch Prqject Year 8 - Pesticides and PCBs Data


                             INVEST#:                  MRTP                        MRPL                        BSSI                    BSBG
                               ID:             Mississippi River            Mississippi River           Breton Sound              Breton Sound.
                               SITE:              Tiger Pass                  Pass a Loutrc              Sable Island             Bay Garderne
                             1ABSAMNO:                 K7062                       K7060                       K7072                   K7064
                          SAMPLE TYPE:                 SAMP                        SAMP                        SAMP                    SAMP
                               UNIT:                   ng/g                        ng/g                        ng/g                    ng/g
                             Analyte                   Cone      DB QUAL           Cone       DB QUAL          Cone    DB QUAL         Cone      1313 QUAL



                         RECEIPT DATE:                 1/8/93                      1/8/93                      1/9/93                  1/8/93
                             QCBATCH:                  M1233                       M1233                       M1234                   M1233
                       EXTRACTION DATE:                9/14/93                     9/14/93                     9/16/93                 9/14/93
                             METHOD:                   GCMS                        GCMS                        GCMS                    GCMS
                        ANALYSIS DATE:                 10/25/93                    10/25/93                    10/28/93                10/25/93
                             METHOD:                   GCECD                       GCECD                       GCECD                   GCECD
                         ANALYSIS DATE:                8/24/94                     8/24/94                     8/22/94                 8/24/94
                             MATRIX:                   TISSUE                      TISSUE                      TISSUE                  TISSUE
                             SUBMAT-
                             V&-INVT-.                 15.32                       15.02                       15.01                   15.03
                             DRYW`17-                  2.23                        1.69                        1.69                    2.48
       0                     WTUNITS:                  GRAMS        DRY            GRAMS          DRY          GRAMS      DRY          GRAMS         DRY
                             PCTSOLIDS:                14.50%                      11.300A                     11.300/6                16.500/6
                             Lipid Weight:
                             TOTAL LIPID:              11.41                       7.01                        9.11                    8.69
                             LIPID UNITS:              % DRY                       % DRY                       % DRY                   % DRY
                                VOL.
                             VOLUNrrS:                 LITERS                      LITERS                      LITERS                  LITERS


                             DBOF13:                   77.3                        78.5                        58.4                    81.3
                             PCB#103:                  89.7                        81.6                        85.5                    86.5
                             PCB#198:                  82                          83.6                        74.3                    82.7
                             TOTAL BHCs                2.4                         0.5             1           2.3                       1.1
                     TOT CHLORDANES (ALL)              29.4                        38.4                        28.6                      4.9
                     TOT CHLORDANES, (S&1j             16.5                        20.9                        16.3                      2.7
                             TOTAL DDTs                55.8                        66.7                        45.4                      5.5
                        TOTAL PCBs (S&II               150.8                       259.3                       119.8                     11


                             ALPHA-BHC                 1.2                          0              ND          1.2                       1.1
                                HCB                     0            ND            0.2             1           0.1          .1           n           Nn
                             BETA-BHC                  0.3            1             0              ND          0           ND            0           ND
                             GAMMA-BHC                 0.9                         0.5             1           1.1                       0           ND
                             DELTA-BHC                  0            ND             0              ND          0           ND            0           ND
                          THEPTACHTL"ONIX 0            Cv. 2                       0.6             j           0.3          j            0           'ND



                                                              m m m m m mm m m m m m @

                                                          Mussel Watch Project Year 8 - Pesticides and PCBs Data


                               INVEST#:                   MR7P                            MRPL                        BSSI                       BSBG
                                 ID:              Mississippi River               Mississippi River             Breton Sound                Breton Sound
                                SITE:                 Tiger Pass                   Pass a Loutre                 Sable Island               Bay Gardeme
                            LABSAMNO:                     K7062                           K7060                       K7072                     K7064
                           SAMPLE TYPE:                   SAMP                            SAMP                        SAMP                       SAMP
                                UNIT-                     ng/g                            ng/g                        ng/g                       ng/g
                               Analyte                    Conc        1313 QUAL           Conc       DB QUAL          Conc      DB QUAL,         Conc      1313 QUAL


                          HEPTA-EPOXIDE                   3.7                             2.3                         2.6                         0.5
                          OXYCHLORDANE                    0.9                             1.1                         0.6                         0.3           J
                       GAMMA-CHLORDANE                    7.5                             11                          8.2                         1.2
                       ALPHA-CHLORDANE *                  6.7                             8.9                         6.8                         1.2
                       TRANS-NONACHLOR 0                  5.9                             9.2                         6.6                          1
                          CIS-NONACHLOR                   4.6                             5.4                         3.5                         0.7
                               ALDRIN                     0.4                             1.2                         0.8                          0           ND
                               DIELDRIN                   16.2                            11.4                        14.1                         0           ND
                               ENDRIN                     2.5                             1                           1.1                         0.1           J
                               MIREX                      0              ND               0.5            J             0            ND             0           ND
                          2,4'DDE (O,VDDE)                0.4             J               1                           0.4            J             0           ND
                          4,4'DDE (P.P'DDE)               27.8                            35.1                        23.7                        3.4
                          2,4'DDD (0,P'DDD)               2.4                             2.9                         1.7                         0.3           J
                          4.4-131313 (P,P'DDD)            21.7                            20                          14.2                        1.9
                          2.4'DDT (0,P'DDTI               2.1                             3.5                         1.3                          0           ND
                          4,4'DDT (P,P'DDII               1.5                             4.2                         4.1                          0           ND


                       PCB # (CLORINATION)
                          NOAA S&T PCB9
                               8 (CL2)                    0              ND               0             ND             0            ND             0           ND
                               18 (CL3)                   0              ND               0.4            J             0            ND             0           ND
                               28 (CL3)                   0.7             J               1.4                         0.6           J             0.1           J
                               44 (CIA)                   2.7                             3.7                         1.9                          0           ND
                               52 (CIA)                   4.6                             8.1                         6.6                          0           ND
                               66 (CIA)                   1.4                             3.5                         1.2            J             0           ND
                               101 (CL5)                  10.5                            17.6                        7.5                         0.8
                               105 (CL5)                  2.5                             4                           2.1                         0.3           J
                           110/77 (CL5/4)                 17.2                            23.3                         0            ND            0.8           J







                                                          Mussel Watch Project Year 8 - Pesticides and PCBs Data


                               INVEST#:                   MRTP                        MRPL                         BSSI                     OSr3G-
                                  ID:             Mississippi River             Mississippi River            Breton Sound              Breton Sound,
                                SITE:                71ger Pass                  Pass a Loutre                Sable Island             Bay Garderne
                               LABSAMNO:                  K7062                       K7060                        K7072                    K7064
                            SAMPLE TYPE:                  SAMP                        SAMP                         SAMP                     SAMP
                                UNIT:                     ng/g                        ng/g                         ng/g                     ng/g
                               Analyte                    Cone      DB gUAL           Cone        DB QUAL          Cone     1313 QUAL       Cone      DB gUAL


                       118/108/149(CIZ/5/6)               515                         8.5                          4.3                       0.8
                               128 (CL6)                  1.3                         0.9             J            1.9                       0           ND
                               138 (CL6)                  0             ND             0             ND            12.9                      0           ND
                               126 (CIZ)                  0             ND             0             ND            0           ND            0           ND
                               153 (CL6)                  19.1                        36.8                         12.8                      116
                               170 (CL7)                  1                            2                           0.9          J            0           ND
                               180 (CL7)                  0             ND             0             ND            0           ND            0           ND
                       187/182/159(CL7/716)               6.9                         15.6                         5.2                       0.4          J
                               195 (CL8)                  0             ND             0             ND            0           ND            0           ND
                               206 (CL9)                  0             ND             0             ND            0           ND            0           DID
                               209 (CLIO)                 0             ND             0             ND            0           ND            0           ND

                         Surrogate Recoveries
         0)                    DBOFB%:                    77.3                        78.5                         58.4                     81.3
                               PCB#103%:                  89.7                        81.6                         85.5                     86.5
                               PCB#1980/o:                82                          83.6                         74.3                     82.7




























                                                                                                                       mom






                                                            Mussel Watch Project Year 8 - Pesticides and PCBs Data


                           INVEM:                     LBMP                             MSPC                            MSBB                              MSPB
                             ID:                 Lake Borgne                  Mississippi Sound                Mississippi Sound               Mississippi S@mnd
                            SITE:             Malheureux Point                  Pass Christian                         B11o7d Bay                Pascagoula Bay
                           LABSAMNO:                  K7066                            K7070                           K7068                             K7078
                       SAMPLE TVPE:                   SAMP                             S"P                             SAMP                              SAMP
                            UNIT.*                    ng/g                             ng/g                            ng/g                              ng/g
                           Analyte                    Cone         DB QUAL             Cone        DB QUAL             Cone         DB QUAL              Cone        DB Q




                      RECEIPr DATE,                   1/6/93                           1/9/93                          1/9/93                            1/10/93
                           QCBATCH:                   M1233                            M1234                           M1234                             M1234
                    EXTRACTION DATE:                  9/14/93                          9/16/93                         9/16/93                           9/16/93
                           MET'HOD:                   GCMS                             GCMS                            GCMS                              GCMS
                      ANALYSIS DATE:                  5/11/94                          10/28/93                        10/28/93                          10/28/93
                           MEMOD-                     GCECD                            GCECD                           GCECD                             GCECD
                     ANALYSIS DATE:                   8/24/94                          8/22/94                         8/22/94                           8/23/94
                           MATRIX:                    TISSUE                           IISSUE                          TISSUE                            TISSUE
                           SUBMAT-
                           WE`r%VT.                   15.17                            15.22                           15.32                             15.34
                           DRYWT-.                    2.32                             2.94                            2.32                              1.93
                           WTUNITS:                   GRAMS           DRY              GRAMS          DRY              GRAMS           DRY               GRAMS          DRY
                           PCTSOLIDS:                 15.30%                           19.30%                          15.20%                            12.600/6
                           Upid Weight:
                           TOTAL UPID:                9.48                             9.85                            13.16                             9.62
                           LIPID UNITS:               % DRY                            % DRY                           % DRY                             % DRY
                            VOL.
                           VOLUNI'M:                  LITERS                           LITERS                          LITERS                            LITERS


                           DBOFB:                     78.9                             79.6                            79.1                              82.5
                           PCB#103:                   90.5                             86.2                            82.5                              88
                           PCB#198:                   78.7                             80.4                            82.5                              86.8
                           TOTAL BHCs                 1.4                              1.3             J               2.2                               1.6
                 TOT CHLORDANES (ALL)                 5.1                              12.7                            62.4                              9.1
                 TOT CHLORDANES (S&II                 2.7                              7.1                             35.5                              5.8
                           TOTAL DI)Ts                5.3                              7.7                             31.4                              23.2
                     TOTAL PCBs (S8M                  9.3              J               22.1            J               201.5                             153.6


                           ALPHA-BHC                   1                               0.7                             0.8                               1.1
                            HCB                        0              ND               0               J                0              ND                0              ND
                           BETA-BHC                    0              ND               0               ND               0              ND                0              ND
                           GAMMA-BHC                  0.4              J               0.6                             1.4                               0.5
                           DELTA-BHC,                  0              ND               0              ND                0              ND                0              ND
                       HEPTACHLOR                      0              ND               0.3             J               0.3              J                0.1             J






                                                        Mussel Watch "ect Year 8 - Pesticides and PCEls Data


                        INVEST#:                 LBMP                           MSPC                             MSBB                            MSPB
                          ID:                Lake Borgne                 Mississippi Sound              Mississippi Sound               Mississippi Spund
                         SITE:             Malbeureux Point                Pass Christian                    Biloid Bay                  Pascagoula Bay
                     LABSAMNO:                  K7066                          K7070                             K7068                           K7078
                    SAMPLE TYPE:                 SAMP                           SAMP                             SAMP                            SAMP
                         UNIT:                   ng/g                           ng/g                             ng/g                            ng/g
                        Analyte                  Conc         1313 QUAL         Conc         DB QUAL             Conc       DB QUAL              Conc       DB QUAL


                   HEPTA-EPO)aDE                   0.6                            0.9                            1.8                             0.7
                   OXYCHLORDANE                    0.3            1               0.5                            1.9                             0.4
                GAMMA-CHLORDANE                    1.1                            3.1                            18.3                            2.9
                ALPHA-CHLORDANE 0                  0.7                            2.5                            19.6                            2.6
                TRANS-NONACHLOR 0                  1.4                            3.4                            13.7                            2.4
                   CIS-NONACHLOR                   0.9                            2.1                            6.8                             0             ND
                        ALDRIN                     0              ND              0              ND              0.5                             0             ND
                        DIELDRIN                   1.9                            3.3                            7.9                             3
                        ENDRIN                     0              ND              0              ND              0              ND               0             ND
                        MIREX                      0              ND              1.1                            0.7                             0.7
                   2.4!DDE JOYIDDE)                0              ND              0              ND              0.5                             2.5
                   4,4'DDE (P,P'DDE)               3.4                            4.7                            14.7                            13.1
      0            2,4'DDD (O,P'DDD)               0              ND              0.1            1               2                               1.2
      OD           4.4'DDD (P,P'DDD)               1.3                            1.8                            11                              4.6
                   2.4'DDT (O.P'DDTI               0              ND              0.2            1               1.2                             0.8
                   4,4'DDT (P.P'DDII               0.6                            0.8                            2                               0.9


                PCB # (CLORINATION)
                   NOAA S&-T PC139
                        8 (CL2)                    0              ND              0              ND              1                               0             ND
                        18 (CL3)                   0              ND              0              DID             2.8                             0             ND
                        28 (CL3)                   0              ND              0.3            1               5.1                             0.5            1
                        44 (CIA)                   0              ND              0.4            1               5.3                             1.2
                        52 (CIA)                   0.6            1               1.2                            9.7                             2.3
                        66 (CIA)                   0.2            1               0.4            1               6.9                             0.9
                        101 (CL5)                  0.7            1               1                              12.3                            4.1
                        105 (CL5)                  0.3            1               0.4            1               3.6                             43.1
                    110/77(CL5/4)                  0              ND              0              ND              0              ND               0             ND






                                                       Mussel Watch Project Year 8 - Pesticides and PCBs Data


                        INVEST#:                 LBMP                         MSPC,                          MSBB                         MSPB,
                           ID:               Lake Borgne                Mississippi Sound             Mississippi Sound             Mississippi Sgund
                         SITE:            Malheureux Point                Pass Christian                  Biloxi Bay                 Pascagoula Bay
                        1ABSAMNO:                K7066                        K7070                          K7068                        K7078
                    SAMPLE TYPE:                 SAMP                         SAMP                           SAMP                         SAMP
                         UNIT:                   ng/g                         ng/g                           ng/g                         ng/g
                        Analyte                  Conc        DB QUAL          Conc         DB QUAL           Conc        DB QUAL          Conc         DB QUAL


                118/108/149(CL5/5/6)             0.8             J             1.3                           9.7                            4
                        128 (CL6)                 0             ND              0             ND             1.3                            0             ND
                        138 (CL6)                 0             ND             2.7                           14.4                          9.6
                        126 (CLS)                 0             ND              0             ND              0             ND              0             ND
                        153 (CL6)                 1                            1.1                           21.3                          6.7
                        170 (CL7)                 0             ND             0.3             J             0.6                           0.7
                        180 (CL7)                 0             ND              0             ND              0             ND              0             ND
                187/182/159(CL7/7/6)             0.5             J             1.2                           6.9                            0             ND
                        195 (CLS)                 0             ND              0             ND              0             ND              0             ND
                        206 (CL9)                 0             ND              0             ND              0             ND              0             ND
                        209 (CLIO)                0             ND              0             ND              0             ND              0             ND

                  Surrogate Recoveries
       (D               DBOF'B%:                 78.9                         79.6                           79.1                         82.5
                        PCB# 103%:               90.5                         86.2                           82.5                          88
                        PCB#198%:                78.7                         80.4                           82.5                         86.8






                                                       Mussel Watch Project Year 8 - Pesticides and PCBs Data


                         INVEST#:                  MBCP                            MBHI                            PBPH                      PBI8
                           ID:            Mobile Bay Cedar                  Mobile Bay Cedar                 Pensacola Bay             Pensacola Bay
                           SITE:           Cedar Point Reef             Hollingers Island Channel            Public Harbor              Indian Bayou
                         LABSAMNO:                 K7076                           K7074                           K7088                     K7086
                     SAMPLE TYPE:                  SAMP                            SAMP                            SAMP                      SAMP
                           LJNrP.                  ng/g                            ng/g                            ng/g                      ng/g
                         Analyte                   Conc      DB QUAL               Conc           D13 QUAL         Conc      DB QUAL         Conc      D13 QUAL



                     RECEIPT DATE:                 1/10/93                         1/10/93                         1/12/93                   1/12/93
                         QCBATCH:                  M 1234                          M1234                           M1234                     M1234
                  EXTRACTION DATE:                 9/16/93                         9/16/93                         9/16/93                   9/16/93
                         METHOD:                   GCMS                            GCMS                            GCMS                      GCMS
                    ANALYSIS DATE:                 10/28/93                        10/28/93                        10/28/93                  10/28/93
                         METHOD:                   GCECD                           GCECD                           GCECD                     GCECD
                    ANALYSIS DATE:                 8/23/94                         8/23/94                         8/23/94                   8/24/94
                         MATRIX:                   TISSUE                          TISSUE                          TISSUE                    TISSUE
                         SUBMAT*
                         WETW17:                   15.17                           15.22                           15.16                     15.37
                         DRYWT:                    2.39                            2.37                            2.52                      1.72
                         VVIUNITS:                 GRAMS        DRY                GRAMS             DRY           GRAMS       DRY           GRAMS       DRY
                         PCTSOLIDS:                15.70%                          15.600/6                        16.600/6                  11.20%
                         Upid Weight:
                         TOTAL LIPID:              9.93                            9.72                            10.44                     7.12
                         UPID UNITS:               % DRY                           % DRY                           % DRY                     % DRY
                           VOL:
                         VOLUNITS:                 LITERS                          LITERS                          LITERS                    LITERS


                         DBOFB:                    82.7                            81.5                            82.8                      78.1
                         PCB# 103:                 88                              85.4                            89.5                      90.8
                         PCB#198:                  83.3                            84.6                            85.7                      85.8
                         TOTAL BHCs                1.8                             1.9                             1.3           J           0.4           J
                TOT CHLORDANES (ALL)               13.9                            19.6                            31.6                      7.3
                TOT CHLORDANES, (S&TJ              9                               10.9                            18.5                      3.6
                         TOTAL DDTs                117.4                           127.3                           29.9                      20.2
                   TOTAL PCBs (S&II                114.8                           135.6                           240.7                     368.4

                         ALPHA-BHC                 0.8                             0.8                             0.5                       0.2           J
                            14CR                   0            ND                  0                 ND            0           ND            0            J
                         BETA-BHC                  0            ND                  0                 ND            0           ND            0           ND
                         GAMMA-BHC                 1.1                             1.1                             0.8                       0.2           J
                         DELTA-BHC                 0            ND                  0                 ND            0           ND            0           ND
                      HEPTIACHLOR                  0.2           i                 0.2                 i           1.1                        0           ND






                                                          Mussel Watch Project Year 8 - Pesticides and PCEls Data


                          INVEST#:                  MBCP                               MBHI                             PBPH                       PBIB
                            ID:             Mobile Bay Cedar                   Mobile Bay Cedar                   Pensacola Bay              PensacoI4 Bay
                           SITE:             Cedar Point Reef              Hollingers Island Channel              Public Harbor               Indian Bayou
                       LABSAMNO:                    K7076                              K7074                            K7088                      K7086
                      SAMPLE TYPE:                  SAMP                               SAMP                             SAMP                       SAMP
                           UNM.                     ng/g                               ng/g                             ng/g                       ng/g
                          Analyte                   Conc        DB QUAL                Conc            DB QUAL          Conc      1313 QUAL        Conc      DB QUAL



                     HEPTA-EPO)aDE                  1.7                                1.8                              3.4                        0.4            J
                     OXYCHLORDANE                   0.4             J                  0.5                              0.7                        0.4            J
                  GAMMA-CHLA)RDANE                  4.6                                5.6                              8.2                        1.4
                  ALPHA-CHLORDANE d'                3.7                                4.3                              7.1                        1.8
                  TRANS-NONACHLOR                   3.4                                4.6                               7                         1.5
                     CIS-NONACHLOR                   0             ND                  2.7                              4.1                        1.9
                          ALDRIN                     0             ND                   0                 ND            0.1           J             0            ND
                          DIELDRIN                  5.2                                5.9                              9.1                        2.3
                          ENDRIN                    0.5                                0.6                               1                          0            ND
                          MIREX                     0.2             J                  0.3                 J            0.2           J             0            ND
                     2.4'DDE (O.P'DDE)              36.7                               38.3                             0.4           J            0.2            J
                     4.4'DDE (P.P'DDE)              51.6                               56.8                             16.6                       14.1
                     2.4'DDD (O.P'DDD)               6                                 6.4                               1                          1
                     4,4'DDD (P.P'DDD)              17.7                               20.5                             4.9                         2
                     2.4'DDT (O.P'DDT3               4                                 3.6                              2.8                        2.3
                     4,4*DDT (P.P'DDTI              1.5                                1.8                              4.3                        0.6            J

                  PCB 0 (CLORINAMON)
                     NOAA S&T PCBs
                          8 (CL2)                    0             ND                   0                 ND             0           ND             0            ND
                          18 (CL3)                   0             ND                   0                 ND            1.5                        0.3            J
                          28 (CL3)                  0.3             J                  0.5                 J            2.1                        0.5            J
                          44 (CIA)                  0.9                                1.1                              2.4                        1.6
                          52 (CIA)                   3                                 3.9                              9.8                        6.7
                          66 (CIA)                  0.5             J                  0.7                 J            2.9                         0            ND
                          101 (CI.5)                 5                                 5.5                              22.5                       28.8
                          105 (CL5)                 18.6                               22.6                             2.6                        2.2
                      110/77 (CL5/4)                 0             ND                   0                 ND             0           ND            28.8






                                                      Mussel Watch Project Year 8 - Pesticides and PCBs Data


                       INVEST#:                  MBCp                             MBHI                           PBPH                       PBIB
                         ID:             Mobile Bay Cedar                 Mobile Bay Cedar                 Pensacola Bay             Pensacola,Bay
                        SITE:            Cedar Point Reef             Hollingers Island Channel            Public Harbor             Indian Bayou
                      LABSAMNO:                  K7076                            K7074                          K7088                      K7086
                    SAMPLE TYPE:                 SAMP                             SAMP                           SAMP                       SAMP
                        UNIT:                    ng/g                             ng/g                           ng/g                       ng/g
                       Analyte                   Conc      DB QUAL                Conc          1313 QUAL        Conc     DB QUAL           Conc    DB QUAL


                118/1081149(CL5/5/6)             0             ND                 4                              14.9                       18.5
                       128 (CL6)                 0             DID                0                 ND           3.5                        4
                       138 (CL6)                 9.2                              11                             23.7                       31.9
                       126 (CL5)                 0             ND                 0                 ND            0           ND            0           ND
                       153 (CL6)                 7.8                              8                              32.7                       53.9
                       170 (CL7)                 0.3           J                  0.3               J            0.6          J             1.8
                       180 (CL7)                 1.5                              2.3                             0           ND            0           ND
                187/182/159(CL7/7/6)             4.3                              5                              4.7                        6.2
                       195 (CL8)                 0             ND                 0                 ND            0           ND            0.4         J
                       206 (CL9)                 0             ND                 0                 ND            0           ND            0           ND
                       209 (CLIO)                0             ND                 0                 ND            0           ND            0           ND

                 Surrogate Recoveries
       t-0             DBOFB%:                   82.7                             81.5                           82.8                       78.1
                       PCB#103%:                 88                               85.4                           89.5                       90.8
                       PCB# 198%:                83.3                             84.6                           85.7                       85.8




                                                                 mm M = M = @

                                                             Mussel Watch Project Year 8 - Pesticides and PCBs Data


                                INVEST#:                   PBSP                         CBJB                           CBSR                            CBPp
                                   ID:              Pensacola Bay               Choctawhatchee                 Choctawhatchee                 Choctawhatchee,
                                  SITE:              Sabine Point                  Joe's Bayou                  Off Santa Rosa                   Postil Point
                                LABSAMNO:                  K7090                        K7082                          K7084                           K7080
                            SAMPLE TYPE*                   SAMP                         SAMP                           SAMP                            SAMP
                                  UNM.                     ng/g                         ng/g                           ng/g                            ng/g
                                Analyte                    Cone      DB QUAL            Cone       DB QUAL             Cone        DB QUAL             Cone       DB gUAL



                            RECEIPT DATE,                  1/12/93                      1/13/93                        1/12/93                         1/12/93
                                QCBATCH:                   M1234                        M1234                          M1234                           M1234
                         EXT'RACnON DATE:                  9/16/93                      9/16/93                        9/16/93                         9/16/93
                                METHOD:                    GCMS                         GCMS                           GCMS                            GCMS
                           ANALYSIS DATS:                  10/28/93                     10/28/93                       10/28/93                        10/28/93
                                ML-niOD:                   GCECD                        GCECD                          GCECD                           GCECD
                           ANALYSIS DATE:                  8/23/94                      8/23/94                        8/23/94                         8/23/94
                                MATRIX                     TISSUE                       TISSUE                         TISSUE                          TISSUE
                                SUBMAT:
                                WE-f VVT-                  15.4                         15.16                          15.09                           15.17
                                DRYWT:                     2.43                         2.73                           1.89                            2.16
                                WTUNITS:                   GRAMS        DRY             GRAMS          DRY             GRAMS         DRY               GRAMS         DRY
                                PCISOLIDS:                 15.8(rA                      18.OOOA                        12,50%                          14.200A
                                I.Apid Weight:
                                TOTAL LIPID:               9.24                         10.56                          7.66                            10.5
                                UPID UNITS:                % DRY                        % DRY                          % DRY                           % DRY
                                  VOL.
                                VOLUNrl7S:                 LITERS                       LrrERS                         1,177ERS                        LrMRS


                                DBOFB:                     80.8                         77.5                           77.4                            81.9
                                PCB#103:                   86.7                         77.9                           82.8                            91.5
                                PCB#198:                   82.5                         88.9                           82.6                            83
                                TOTAL BHC9                 1.1           J              0.9             J              0.5             J               0.6            J
                      TOT CHLORDANES, (ALL)                11                           31.3                           6.9                             52.3
                      TOT CHLORDANES (S"                   6.6                          18.3                           4.2                             30.8
                                TOTAL DDT9                 16.8                         71.5                           21.7                            670.3
                          TOTAL PCBs (S&II                 69.9                         87.8                           19.1            J               99.8

                                ALPHA-BHC                  0.5                          0.4                            0.3             J               0.3            J
                                  HCB                      0            ND               0             ND               0              J               0.1            J
                                BETA-BHC                   0            ND               0             ND               0             ND               0             ND
                                GAMMA-BHC                  0.6                          0.4                            0.2             J               0.3            J
                                DELTA-BHC                  0            ND               0             ND               0             ND               0             ND
                             HEPTACHLOR                    0.2           J              0.5                            0.1             J               0             ND






                                                           Mussel Watch Project Year 8 - Pesticides and PCBs Data


                                INVEST#:               PBSP                           CBJB                          CBSR                         CBPP
                                 ID:              Pensacola Bay               Choetawhatchee                Choctawhatchee                 Choctawhatche  'e
                                Srm:               Sabine Point                 Joe's Bayou                  Off Santa Rosa                 Postil Point
                            IABSAMNO:                 K7090                           K7082                         K7084                        K7080
                           SAMPLE TYPE:               SAMP                            SAMP                          SAMP                         SAMP
                                UNIT:                  ng/g                           ng/g                          ng/g                         ng/g
                                Analyte                Conc       DB QUAL             Cone      DB QUAL             Conc      DB QUAL            Cone       DB QUAL


                          HEPTA-EPOXIDE                  1                            6.2                           0.3            J             1.4
                          OXYCHLORDANE                  0.3            J              0.8                           0.2            J             1.1
                       GAMMA-CHLORDANE                  2.8                           10.1                          1.5                          16.8
                       ALPHA-CHLORDANE *                2.7                           5.4                           1.9                          15.2
                       TRANS-NONACHLOR *                2.6                           6.1                           1.9                          14.3
                          CIS-NONACHLOR                 1.2                           2.2                           0.9                          3.5
                                ALDRIN                   0            ND              0.4                           0             ND             0.1             J
                                DIELDRIN                3.2                           6.3                           1.4                           6
                                ENDRIN                  0.2            J              0             ND              0             ND              0             ND
                                MIREX                    0            ND              1.6                           0.3            J             0.6
                          2.4'DDE (0,713DE)              0            ND              0.3           J               0             ND             4.2
                          4.4-13DE (P.P'DDE)            9.1                           22.1                          17.7                         293.9
                          2.4'DDD (O,P'DDD)             0.6                           7.2                           0             ND             34.1
                          4,4'DDD (P.P'DDD)             4.3                           36.6                          2.7                          283.4
                          2.4'DDT (O.P'DDT]              1                            1.5                           0.3            J             14.7
                          4.4'DDT (P,P'DD7]             1.8                           3.8                           1                            40


                       PCB # (CLORINATION)
                          NOAA S&T PCBs
                                8 (CL-2)                 0            ND              0             ND              0.2            J              0             ND
                                18 (CL3)                 0            ND              0.8                           0             ND              0             ND
                                28 (CL3)                0.4            J              1.2                           0.2            J             0.5             J
                                44 (CIA)                0.8            J              3.1                           0.2            J              0             ND
                                52 (CIA)                2.1                           4.8                           0.4            J              2
                                66 (CIA)                0.9                           4.6                           0             ND             0.7             i
                                101 (CL5)               5.3                           7.4                           0.9            J             4.8
                                105 (CL5)               0.8            J              1.9                           0.1            J             0.7             J
                           110/77 (CL5/4)                0            ND              0             ND              0             ND              0             ND






                                                          Mussel Watch "ect Year 8 - Pesticides and PCBs Data


                             INVEST#-                PBSP                         CBJB                         CBSR                         CBPP
                                ID:             Pensacola Bay              Choctawhatchee              Choctawhatchee               Choctawhatchee,
                               Srm:              Sabine Point                Joe's Bayou                Off Santa Rosa                 Postil Point
                             LABSAMNO:               K7090                        K7082                        K7084                        K7080
                          SAMPLEITPE:                SAMP                         SAMP                         SAMP                         SAMP
                               UNM.                  ng/g                         ng/g                         ng/g                         ng/g
                              Analyte                Cone       DB QUAL           Cone      DB QUAL            Cone      DB QUAL            Cone      DB QUAL


                      118/108/149(CL5/5/6)            4.3                         6.4                          0.6           1              3.4
                             128 (CL6)                1.2                         0             ND             0.5           1              0            ND
                             138 (CL6)                7.7                         5.9                          2.1                          11.1
                             126 (CL5)                0            ND             0             ND             0            ND              0            ND
                             153 (CL65)               9.5                         6.3                          1.4                          15.6
                             170(CL7)                 0.7           1             1.5                          0.7           1              1.1
                             180 (CL7)                0            ND             0             ND             0.3           1              1.2
                      187/182/159(CL7/7/6)            1.6                         1.6                          0.5           1              6.9
                             195 (CL8)                0            ND             0             ND             0            ND              0            ND
                             206 (CL9)                0            ND             0             ND             0            ND              0            ND
                             209 (CLIO)               0            ND             0             ND             0            ND              0            ND

                       Surrogate Recoveries
                             DBOFB%:                 80.8                         77.5                         77.4                         81.9
                             PCB#103%:               86.7                         77.9                         82.8                         91.5
                             PCB#198%:               82.5                         88.9                         82.6                         83






                                                       Mussel Watch Project Year 8 - Pesticides and PCB9 Data


                             INVEWO.-                PCIJO                       PCMP                      SAWB                         APDB
                               ID:              Panama City                 Panama City                St. Andrew               Apalachicola Bay,
                               STM:            Little Oyster Bar           Municipal Pier            Watson Bayou                       Dry Bar
                             IABSAMNO:               K7092                       K7096                     K7094                        K7098
                         SAMPLE TYPE:                SAMP                        SAMP                      SAMP                         SAMP
                               UNIT:                 ng/g                        ng/g                      ng/g                         ng/g
                             Analyte                 Cone       DB QUAL          Conc      DB QUAL         Cone      DB QUAL            Cone      DB, QUAL  I

                         RECEIVr DATE:               1/13/93                     1113193                   1/13/93                      1/14/93
                             gCBATCH:                M1234                       M1234                     M1234                        M1234
                       EXTRACTION DATE:              9/16/93                     9/16/93                   9/16/93                      9/16/93
                             METHOD:                 GCMS                        GCMS                      GCMS                         GCMS
                        ANALYSIS DATE:               10/28/93                    10/29/93                  10/29/93                     10129/93
                             METHOD:                 GCECD                       GCECD                     GCECD                        GCECD
                        ANALYSIS DATE:               8/23/94                     8/23194                   8/23/94                      8/23/94
                             MATRIX:                 TISSUE                      TISSUE                    TISSUE                       TISSUE
                             SUBMAT,
                             WE'rWrl                 15.31                       15-13                     15.04                        15-M
                             I)Rywr.                 2.83                        2.37                      2.43                         1,49
                             WTUNITS:                GRMS           DRY          GRAMS         DRY         GRAMS        DRY             GRMS         DRY
                             PCTSOlJI)S:             18-500/0                    15.70%                    16.20%                       9 - W/o
                             Upid Weight:
                             TOTAL LIPID:            949                         8.53                      7.16                         6.1
                             LIPID Ulam:             % DRY                       % DRY                     % DRY                        % DRY
                                VOL:
                             VOLUNITS-               LITERS                      LITERS                    LITERS                       LITERS

                             DBOFB-.                 77.3                        82.7                      78.9                         84.6
                             PCB#103:                83.9                        84.7                      81.7                         9Z2
                             PCB#198:                81.3                        88.8                      85.4                         89.1
                             TOTAL BHCs                I             J           I'l           J            1-3          1J             0.8            J
                     TOT CHLORDANES (ALL)             8.5                        20Z                       42.6                         6.3
                    1W CHLORDANES (S&1J               5.4                        9.9                       23.1                         3.9
                             TOTAL DDTs              48.4                        44.6                      108.3                        13
                        TOTAL PCI39 (S&II            40.3                        169.4                     266.4                        19.5           J

                             ALPRA-BHC                0.4                        0.6                        0.6                         0.6            J
                                HCB                    0            ND             0           ND           0            ND             0. i           J
                             BETA-BHC                  0            ND             0            ND          0            ND             0             ND
                             GAMMA-BHC                0.6                        0.5                        0.7                         0.3            J
                             DELTA-BHC                 0            ND             0            ND          0            ND             0             IND
                                                                    114D         0.4           J            0.3          ki             0. i






                                                        Mussel Watch Project Year 8 - Pesticides and PCBs Data


                              tNVESr#:                 PCLO                       PCMP                       SAVIB                     APDB
                                ID:              Panama City                 Panama City                St. Andrew               Apalachicola Bayt
                               Srm:             Little Oyster Bar           Municipal Pier            Watson Bayou                    Dry Bar
                           LABSAMNO:                   K7092                      K7096                      K7094                    K7098
                          SAMPLE IYPE:                 SAMP                       SAMP                       SAMP                      SAMP
                               UNrr:                   ng/g                       ng/g                       ng/g                      ng/g
                              Analyte                  Conc      DB QUAL          Conc      DB QUAL          Conc     DB QUAL          Cone         DB QUAL



                         HEPTA-EPOXIDE                 0.5                        0.6                        1.5                        0.9
                         OXYCHLORDANE                  0.3           J            0.7                        1.5                        0.2
                      GAMMA-CHLORDANE                  2                          7.1                        12.5                       1.2
                      ALPHA-CHLORDANE 0                2.9                        4.9                        11.6                       1.6
                      TRANS-NONACHLOR *                2                           4                         9.7                        1.3
                         CIS-NONACHLOR                 0.8                        2.6                        5.5                         1
                              ALDRIN                   0            ND             0           ND            0.1          J              0             ND
                              DIELDRIN                 1.6                        2.6                        4.1                        2.7
                              ENDRIN                   0            ND             0           ND            0           ND             0.2
                              MIREX                    0            ND             0           ND            0           ND             0.4
                         2NDDE (O,P`DDE)               1                          0.7                        1.3                         0             ND
                         4,4'DDE (P.PIDDE)             32.7                       20.2                       63.2                       9.7
                         2.4'DDD (O.VDDD)              0            ND             3                         4.7                        0.2
                         4,4'DDD (P.FYDDD)             11.7                       15.5                       24.7                       2.5
                         2.4'DDT (O.P'DM               0.9                        1.6                        4.3                         0             ND
                         4,4'DDT (P.P'DEM              2                          3.4                        10                         0.6


                      PCB # (CLORINAIION)
                         NOAA S&T PCBs
                              8 (CL2)                  0            ND            0.7           J            0           ND              0             ND
                              18 (CL3)                 0            ND            1.8                        0           ND              0             ND
                              28 (CL3)                 0.3           J            1.7                        2.5                        0.1             J
                              44 (ClA)                 0.5           J            3.2                        4.6                         0             ND
                              52 (CL4)                 1.2                        5.5                        10.6                       0.4             J
                              66 (CIA)                 0            ND            2.2                        4.1                         0             ND
                              101 (CL5)                2.6                        13.9                       25.3                       0.5             J
                              105 (CL5)                1.4                        13.2                       8.7                        0.2             J
                          110/77 (CL5/4)               0            ND             0           ND            0           ND              0             ND






                                                       Mussel Watch Project Year 8 - Pesticides and PCBs Data


                            INVEST#:                PCLO                        PCMP                        SAWB                      APDB
                               ID:              Panama City                 Panama City                St. Andrew               Apalachicola Bay,
                              SITE:            Little Oyster Bar           Municipal Pier            Watson Bayou                    Dry Bar
                            LABSAMNO:               K7092                       K7096                       K7094                     K7098
                         SAMPLE TYPE:               SAMP                        SAMP                        SAMP                      SAMP
                              LJNM.                 ng/g                        ng/g                        ng/g                      ng/g
                             Analyte                Cone        D13 QUAL        Cone       D13 QUAL         Cone     DB QUAL          Cone         DB QUAL


                     118/108/149(CL5/5/6)             2.6                       14.2                        21.4                        0.6            J
                            128 (CL6)                 0.2           J             0           ND            1.7                         0             ND
                            138 (CL6)                 4.2                       13.2                        21.1                        3.2
                            126 (CL5)                 0            ND             0           ND            0           ND              0             ND
                            153 (CL6)                 5.3                       15.2                        30.3                        1.6
                            170 (CL7)                 0.4           J           0.6            J            0.6          J              0.5            J
                            180 (CL7)                 0            ND             0           ND            0           ND              0             ND
                     187/182/159(CL7/7/6)             1.5                       4.1                         11                          1.4
                            195 (CL8)                 0            ND             0           ND            0           ND              0             ND
                            206 (CL9)                 0            ND             1                         0           ND              0             ND
                            209 (CLIO)                0            ND             0           ND            0           ND              0             ND

                      Surrogate Recoveries
      00                    DBOFB%:                 77.3                        82.7                        78.9                      84.6
                            PCB#103%:               83.9                        84.7                        81.7                      92.2
                            PCB#198%:               81.3                        88.8                        85.4                      89.1






                                                          Mussel Watch Project Year 8 - Pesticides and PCBs Data


                                INVF.Sr#:                 APCP                        AESP                     CKBP                    TBNP
                                   ID:             Apalachicola Bay             Apalachee Bay                  Cedar Kay            Tampa Bay
                                  SITE:              Cat Point Bar               Spring Creek                  Black Point         Navarez Park
                                LABSAMNO:                 K7104                       K7102                    K7100                   K71 10
                                SAMPLE'IYPE:              SAMP                        SAMP                     SAMP                    SAMP
                                  UNM.                    ng/g                        ng/g                     ng/g                    ng/g
                                  Analyte                 Conc       DB QUAL          Conc      DB QUAL        Conc     DB QUAL        Conc      DB Q


                                RECEIPT DATE:             1/14/93                     1/14/93                  1/14/93                 1/15/93
                                QCBATCH:                  M1235                       M1235                    M1234                   M1235
                          EXTRACTION DATE:                9/17/93                     9/17/93                  9/16/93                 9/17/93
                                METHOD@                   GCMS                        GCMS                     GCMS                    GCMS
                           ANALYSIS DATE:                 10/30/93                    10/30/93                 10/29/93                10/30/93
                                METHOD:                   GCECD                       GCECD                    GCECD                   GCECD
                           ANALYSIS DATE:                 8/22/94                     8/22/94                  8/24/94                 8/23/94
                                MATRIX:                   TISSUE                      TISSUE                   TISSUE                  TISSUE
                                SUBMA7%
                                WETWT:                    15.22                       15                       15.16                   15.07
                                DRYWT:                    2.55                        1.49                     2.67                    2.67
                                W1UNITS:                  GRAMS         DRY           GRAMS        DRY         GRAMS       DRY         GRAMS        DRY
                                PCTSOLIDS:                16.80%                      9.900/0                  17.600A                 17.70%
        CD
                                Upid Weight:
                                TOTAL LIPID:              7.16                        4.83                     7.8                     6.96
                                LIPID UNITS:              % DRY                       % DRY                    % DRY                   % DRY
                                  VOL.
                                VOLUNITS:                 LITERS                      IXMRS                    LITERS                  LITERS

                                DBOF13:                   79.1                        83.1         NA          80.3                    66.2
                                PCB#103:                  86.4                        98.7         NA          91.4                    78.3
                                PCB# 198-                 91                          95.7         NA          83.1                    75.1
                                TOTAL BHC9                0.8            J            0.4          J           0.4                      0           ND
                       TOT CHLORDANES (ALL)               6.3                         3                        3                       60.7
                       TOT CHLORDANES, (S&IJ              3.9                         1.8          J           2                       35.1
                                TOTAL DDTs                20.9                        9.4                      3.5                     32.1
                          TOTAL PCBs (S&II                27.4           J            22.3         J           6.9                     179.6

                                ALPHA-BHC                 0.5                         0            ND          0.4                      0           ND
                                  HCB                     0             ND            0.1                      0           J            0           ND
                                BETA-BHC                  0             ND            0.4                      0           ND           0           ND
                                GAMMA-BHC                 0.3            J            0            ND          0           ND           0           ND
                                DELTA-BHC                 0             ND            0            ND          0           ND           0           ND
                             HEPTACHLOR                   0             ND            0            ND          0.1         J            0           ND






                                                          Mussel Watch Project Year 8 - Pesticides and PCBs Data


                                 INVEST#:                 APCP                       AESP                     CKBP                       TBNP
                                   ID:             Apalachicola Bay             Apalachec Bay              Cedar Kay                Tampa Bay
                                 Srm:                Cat Point Bar               Spring Creek              Black Point             Navarez Park
                              LABSAMNO:                   K7104                      K7102                   K7100                       K71 10
                            SAMPLE TYPE:                  SAMP                       SAMP                     SAMP                       SAMP
                                 UNIT:                    ng/g                        ng/g                    ng/g                       ng/g
                                 Analyte                  Conc       DB QUAL          Conc      DB QUAL       Conc      DB QUAL          Conc     DB QUAL


                            HEPTA-EPOXIDE                 0.4            J             0           ND           0.1         J            0.9
                            OXYCHLORDANE                   0            ND             0           ND           0.1         J            2.4
                         GAMMA-CHLORDANE                  1.4                          0.9                      0.7                      12.5
                         ALPHA-CHLA)RDANE                 1.8                          1.1                      1                        13.5
                         TRANS-NONACHLOR                  1.7                          0.7                      0.8                      20.8
                            CIS-NONACHLOR                  1                           0.3          J           0.3         J            10.7
                                 ALDRIN                    0            ND             0           ND           0          ND            0           ND
                                 DIELDRIN                 1.3                          0           ND           0.5                      5.2
                                 ENDRIN                    0            ND             0           ND           0.1         J            0           ND
                                 MIREX                     0            ND             0           ND           0          ND            3.3
                            2.4'DDE (O.P'DDE)             0.6                          0           ND           1.2                      0           ND
                            4.4'DDE (P.P'DDE)             12.5                         7                        2.2                      24.9
                            2.4'DDD (0,P'DDD)             0.6                          1                        0          ND            1.1
       0                    4,4'DDD (P.P'DDD)             5.4                          1.4                      0          ND            5.2
                            2,4'DDT (OX131311              0            ND             0           ND           0          ND            0           ND
                            4,4'DDT (P.P'DDII             1.8                          0           ND           0.1         J            0.9


                         PCB # (CLORINATION)
                            NOAA S&T PCBs
                                 8 (CL2)                   0            ND             0           ND           0          ND            1.1
                                 18 (CL3)                 0.6            J             0.7          J           0.5         J            2.6
                                 28 (CL3)                  0            ND             0           ND           0          ND            0           ND
                                 44 (CIA)                  1                           0           ND           0          ND            3.6
                                 52 (CIA)                 1.3                          0.2          J           0          ND            6.5
                                 66 (CIA)                  0            ND             0.3          J           0          ND            0           ND
                                 101 (CL5)                1.4                          0.2          J           0          ND            9.6
                                 105 (CL5)                 0            ND             0           ND           0           J            2.5
                            110/77 (CL5/4)                 0            ND             0           ND           0          ND            24.4






                                                        Mussel Watch Project Year 8 - Pesticides and PCBs Data


                               INVEST#:                 APCP                        AESP                    CKBP                      TBNP
                                  ID:             Apalachicola Bay             Apalacbee Bay             Cedar Kay               Tarnpa. Bay
                                 Srm:              Cat Point Bar               Spring Creek              Black Point            Navarez Park
                               LABSAMNO:                K7104                       K7102                   K7100                     K7110
                            SAMPLE IYPE:                SAMP                        SAMP                    SAMP                      SAMP
                                 UNrr.-                 ng/g                        ng/g                    ng/g                      ng/g
                                Analyte                 Cone        DB QUAL         Cone      DB QUAL       Cone     DB QUAL          Cone     DB QU


                        118/108/149(CIZ/5/6)             1.4                         0.6          J          0.3         J            10
                               128 (CL6)                 0             ND            0           ND           0          ND           0.7
                               138 (CL6)                 2                           0           ND           0          ND           7.9
                               126 (CL5)                 0             ND            0           ND           0          ND           0           ND
                               153 (CL6)                 2.7                         0.3          J          0.8                      16.7
                               170 (CL7)                 0             ND            1.7                     0.5         J            0           ND
                               180 (CL7)                 1.1                         0           ND           0          ND           0           ND
                        187/182/159(CL7/7/6)             1.4                         0           ND          0.3         J            5.5
                               195 (CL8)                 0             ND            5.7                      0          ND           0           ND
                               206 (CL9)                 0             ND            0           ND           0          ND           0           ND
                               209 (CLIO)                0             ND            0           ND           0          ND           0           ND


       N)                Surrogate Recoveries
                               DBOFB%:                  79.1                        83.1                    80.3                      66.2
                               PCB#103%:                86.4                        98.7                    91.4                      78.3
                               PCB#198%:                 91                         95.7                    83.1                      75.1






                                                         Mussel Watch Project Year 8 - Pesticides and PCBs Data

                   INVF-ST#-                 T13MK                        T13PB                      TBOT                       TBRA                          ITH-B
                     ID:                Tampa Bay                   Tampa Bay                  Tampa Bay                   Tampa Bay                    Tampa Bay
                   SITE:             Mullet Key Bayou              Papys Bayou               Old Tampa Bay                Knigbts Airport              Hillsborougb
                   LkBS,WN0-                 K7106                        K7118                      K7112                      K7108                         K7116
              SAMPLE 7WE:                    SAMP                         SAMP                       SAMP                       SAMP                          SAMP
                   UNrr,                     ng/g                         ng/g                       ng/g                       ng/g                          ngJg
                   Analyte                   Cone       DB QUAL           Cone    DB QUAL            Cone     DB QUAL           Cone       DB QUAL            Cone    DB QUAL


              RECEIPT DATE:                  1/15/93                      1/16/93                    1/15/93                    1/15/93                       1/16/93
                   QCBATCH-.                 M1235                        M1235                      M1235                      M1235                         M1235
            EXTRACTION DATE:                 9/17/93                      9/17/93                    9/17/93                    9/17/93                       9117/93
                   METFIOD:                  GCMS                         GCMS                       Gems                       GCMS                          clc-ms
             ANALYSIS DATE:                  10/30/93                     10/31/93                   10/30/93                   10/30/93                      10/31/93
                   MEMiOD:                   GCECD                        GCECD                      GCECD                      GCECD                         GCECD
             ANALYSIS DATE,                  6/22/94                      8/23/94                    8/23/94                    8/23194                       8/23/94
                   MATRIX:                   TISSUE                       TISSUE                     InSSIJE                    TISSUE                        TISSUE
                   SUBMAT.
                   wETwv-.                   15.13                        15-35                      15.07                      15.28                         14.75
                   bRywr:                    3.7                          2.67                       1.98                       2.91                          2.78
                   wrUNM:                    GRAMS          DRY           GRAMS       DRY            GRAMS        DRY           GRAMS          DRY            GRAMS       DRY
                   PCTSQUIDS@                2 4. W/o                     17.40%                     13.100/0                   19-00%                        18.90%
                   Lipid Weight:
                   TOTAL LIPID:              7.45                         7.62                       5.49                       5.62                          6.97
                   LIPID UNITS-              % DRY                        % DRY                      % DRY                      % DRY                         % DRY
                    VOL:
                   VOLUNITS,                 LITERS                       LrMRS                      LITERS                     LITERS                        LrMRS
                   DBOF13:                   78.5                         74.7                       70.6                       75.1                          72.4
                   PCB#103-.                 91.4                         88.5                       83.6                       86.6                          73.5
                   PCB#198:                  89.6                         85.7                       76.8                       83.5                          80.7
                   TOTAL BHCx                 0              ND           1.7                        0.6           J              1.8                         1.3          J
          TOT CHLORDANM                      8.3                          39.1                       14.5                       70.1                          21.2
          TOT CHLORDANES (S"                 4.9                          22.1                       7.7                        41.1                          11.4
                   TOTAL DDT9                7.2                          13.7                       12                           94                          29.9
             TOTAL PCBs JS&T)                10.7            J            35.7                       30.6          J            315.7                         186.1
                   ALPHA-BHC                  0              ND            0          ND                           ND             0             ND            0.2          J
                     HCB                      0              J             0          ND             0             ND             0A            J             ID          ND
                   BETA-BHC                   0              ND            0          ND             0             ND             0             ND            0           ND
                   GAMMA-BHC                  0              ND           1.7                        0.6                          1.8                         1.1
                   DELTA-Blic                 0              ND            0          ND             0             ND             0             NTD           0           NDI
                                                             vqm                      ND             0             ND             0
                                              0                            0                                                                    Nu            0           D@ru






                                                          Mussel Watch Project Year 8 - Pesticides and PCBs Data


                   INVEST#:                 TBMK                          TBPB                      TBOT                        TBKA                         TBHB
                     ID:                Tampa Bay                   Tampa Bay                  Tampa Bay                    Tampa Bay                  Tampa Bay
                    SITE:            Mullet Key Bayou               Papys Bayou              Old Tampa Bay                Knights Airport              Hillsborough
                LABSAMNO:                   K7106                         K7118                     K7112                       K7108                        K7116
               SAMPLE 7WE:                  SAMP                          SAMP                      SAMP                        SAMP                         SAMP
                   UNIT-                     ng/g                         ng/g                      ng/g                        ng/g                         ng/g
                   Analyte                  Conc        DB QUAL           Conc    DB QUAL           Conc      DB QUAL           Conc       DB QUAL           Conc    DB QUAL


              HEPTA-EPOXIDE                  0.2                          1.2                       0.1           J              1                           0.5
              OXYCHLORDANE                   0.3                          1.6                       0.4           J             2.5                          0.8
           GAMMA-CHLORDANE                   1.7                          7                         3.3                         16.4                         4.2
           ALPHA-CHLORDANE *                 2.3                          8.2                       2.9                         14.8                         3.9
           TRANS-NONACHLOR 0                 2.4                          12.7                      4.7                         25.2                         7
              CIS-NONACHLOR                  1.4                          8.5                       3.1                         10.1                         4.7
                   ALDRIN                    0              ND            0          ND             0             ND             0             ND            0           ND
                   DIELDRIN                  0.9                          3.5                       0.4           J              4                           1.7
                   ENDRIN                    0              ND            0          ND             0             ND             0             ND            0           ND
                   MIREX                     0.5                          3.3                       0.6                         1.4                          2.3
              2.4'DDE (0,FrDDE)              0              ND            0          ND             0             ND            1.4                          0           ND
              4.4'DDE (P.PIDDE)              3.8                          12.2                      10.2                        73.1                         20
              2.4'DDD (O,P'DDD)              0.3             J            0          ND             0             ND            2.5                          0.7
              4.4'DDD (P,P'DDD)              3                            1.5                       1.8                         15.2                         3.8
              2,4'DDT (O,P'DEM               0              ND            0          ND             0             ND             0             ND            2
              4.4'DDT (P.P'DM                0.1             J            0          ND             0             ND            1.8                          3.5


           PCB # (CLORINATION)
              NOAAS&TPCBs
                   8 (CL2)                   0.5             J            0          ND             0             ND             0             ND            0           ND
                   18 (CL3)                  0.2             J            0.4         J             0.7           J             2.7                          0.7          J
                   28 (CL3)                  0              ND            0          ND             2.4                         6.3                          2
                   44 (CIA)                  0.5             J            1.1                       1.1                         6.6                          2.5
                   52 (CIA)                  0.8                          1.3                       1.6                         13.1                         5.3
                   66 (CIA)                  0              ND            0          ND             0             ND             0             ND            0           ND
                   101 (CL5)                 0.4             J            2                         1.1                         17.9                         10.9
                   105 (CL5)                 0              ND            0          ND             0.4           J             3.5                          2.2
               110/77 (CL5/4)                0              ND            0          ND             0             ND            37.7                         27






                                                         Mussel Watch Project Year 8 - Pesticides and. PCBs Data


                  INVFSr#:                   TBMK                       TBPB                     TBOT                         TBKA                        TBHB
                     ID:                Tampa Bay                   Tampa Bay                 Tampa Bay                   Tampa Bay                   Tampa Bay
                    SITE:            Mullet Key Bayou              Papys Bayou              Old Tampa Bay               Knights Airport              Hillsborough
                  LABSAMNO:                  K7106                      K7118                    K7112                        K7108                       K7116
               SAMPLE TYPE:                  SAMP                       SAMP                     SAMP                         SAMP                        SAMP
                    UNIT:                    ng/g                       ng/g                     ng/g                         ng/g                        ng/g
                  Analyte                    Conc       DB QUAL         Conc     DB QUAL         Conc        DB QUAL          Conc       DB QUAL          Conc     DB QUAL

           118/108/149(CL5/5/6)              1                          2.9                        2                          16.9                        11.7
                  128 (CL6)                  0             ND            0          ND             0            ND            0.7                          1
                  138 (CL6)                  0             ND           2.6                        1.7                        13.5                        10.5
                  126 (CL5)                  0             ND            0          ND             0            ND             0             ND            0           ND
                  153 (CL6)                  1.1                        5.5                        2.8                        27.4                        15.1
                  170 (CL7)                  0             ND            0          ND             0            ND             0 -           ND            0           ND
                  180 (CL7)                  0             ND            0          ND             0            ND            4.6                         1.1
          187/182/159(CL7/7/6)               0.4            j           2.4                        1                          9.3                         5.5
                  195 (CL8)                  0             ND            0          ND             0            ND             0             ND            0           ND
                  206 (CL9)                  0             ND            0          ND             0            ND             0             ND            0           ND
                  209 (CLIO)                 0             ND            0          ND             0            ND             0             ND            0           ND

            Surrogate Recoveries
        ba
                  DBOFB%:                    78.5                       74.7                     70.6                         75.1                        72.4
                  PCB# 103%:                 91.4                       88.5                     83.6                         86.6                        73.5
                  PCB#198%:                  89.6                       85.7                     76.8                         83.5                        80.7






                                                         Mussel Watch Project Year 8 - Pesticides and PCBs Data


                                INVEST#:                TBCB                          CBBI                         CBFM                      NBNB
                                   ID:              Tampa Bay                 Charlotte Harbor             Charlotte Harbor              Naples Bay
                                  SITE:           Cockroach Bay                  Bird Island                  Fort Meyers                Naples Bay
                                LABSAMNO:               K7114                         K7128                        K7126                     K7120
                            SAMPLE 7YPE:                SAMP                          SAMP                         SAMP                      SAMP
                                  UNIT:                 ng/g                          ng/g                         ng/g                      ng/g
                                Analyte                 Conc       DB QUAL            Conc      DB QUAL            Conc       1313 QUAL      Conc    DB QUAL



                            RECEIPT DATE:               1/16/93                       1/19/93                      1/19/93                   1/19/93
                                QCBATCH:                M1235                         M1235                        M1235                     M1235
                          EXTRACTION DATE:              9/17/93                       9/17/93                      9/17/93                   9/17/93
                                METHOD:                 GCMS                          GCMS                         GCMS                      GCMS
                           ANALYSIS DATE-               10/31/93                      10/31/93                     10/31/93                  10/31/93
                                METHOD:                 GCECD                         GCECD                        GCECD                     GCECD
                           ANALYSIS DATE:               8/23/94                       8/23/94                      8/23/94                   8/23/94
                                MATRIX:                 TISSUE                        TISSUE                       7ISSUE                    TISSUE
                                SUBMAT:
                                WE1wr:                  15.07                         8.11                         15.11                     14.97
                                DRYWT:                  2.85                          1.11                         2.45                      2.65
                                VrlUNITS:               GRAMS        DRY              GRAMS        DRY             GRAMS        DRY          GRAMS       DRY
        Ln                      PCTSOLIDS:              18.900A                       13.70%                       16.200/6                  17.700/6
                                Lipid Weight:
                                TOTAL LIPID:            8.39                          4.23                         6.95                      6.33
                                LIPID UNITS:            % DRY                         % DRY                        % DRY                     % DRY
                                  VOL:
                                VOLUNITS:               LITERS                        LrIERS                       LITERS                    LITERS

                                DBOF13:                 71.9                          76.6                         78                        75.7
                                PCB# 103:                81                           93.4                         93.4                      85.9
                                PCB#198:                79.2                          89.4                         92.1                      90.4
                                TOTAL BHCs               0            ND              1.5           J              0.7            J          0.5          J
                       T()1T CHLORDANES (ALL)           44.9                          4.6                          35.4                      17.2
                       TOT CHLORDANES (S&II             25.2                          2.6           J              20.9                       10
                                TOTAL DDTs              46.4                          4.8           J              27.2                      8.1
                          TOTAL PCBs (S&TJ              15.8           J              4.5           J              50                        21.3         J

                                ALPHA-BHC                0            ND              0             ND             0             ND           0          ND
                                  HCB                    0            ND              0.1           J              0             ND           0          ND
                                BETA-BHC.                0            ND              1.3                          0             ND           0          ND
                                GAMMA-BHC                0            ND              0.2           J              0.7                       0.5
                                DELTA-BHC                0            ND              0             ND             0             ND           0          ND
                             HEPTACHLOR.                 0            ND              0             ND             0.6                        0          ND






                                                          Mussel Watch Project Year 8 - Pesticides and PCBs Data


                                 INVEST#:                TBCB                        CBBI                           CBFM                      NBNB
                                  ID:               Tampa Bay                  Charlotte Harbor              Charlotte Harbor              Naples Bay
                                 SITE:            Cockroach Bay                   Bird Island                   Fort Meyers                Naples Bay
                             LABSAMNO:                   K7114                       K7128                          K7126                     K7120
                            SAMPLE TYPE:                 SAMP                        SAMP                           SAMP                      SAMP
                                 UNIT:                   ng/g                        ng/g                           ng/g                       ng/g
                                 Analyte                 Conc      DB gUAL           Conc         DB QUAL           Conc        DB QUAL        Conc     DB QUALI


                           HEPTA-EPO)UDE                 0.6                           0             ND             0.6                         0.4          J
                           OXYCHLORDANE                  1.9                           0             ND             1.1                         0.6
                        GAMMA-CHLORDANE                  6.7                          0.8             J              7                          3.3
                        ALPHA-CHLORDANE *                10.7                         1.1                           7.1                         4.1
                        TRANS-NONACHLOR 0                13.9                         1.5                           12.6                        5.6
                           CIS-NONACHLOR                 11.1                         1.1                           6.4                         3.3
                                 ALDRIN                   0            ND              0             ND              0             ND            0          ND
                                 DIELDRIN                1.3                          0.8             J             4.6                         2.5
                                 ENDRIN                   0            ND              0             ND              0             ND            0          ND
                                 MIREX                   6.1                           0             ND              0             ND            0          ND
                           2,4'DDE (O.P'DDE)              0            ND              0             ND              0             ND            0          ND
                           4.4'DDE (P,P'DDE)             42.9                         4.8                           18.3                        6.7
       to                  2,4'DDD (0,7131313)           0.7                           0             ND              1                           0          ND
                           4.4'DDD (P.P'DDD)             2.8                           0             ND             6.4                         1.4
                           2,4*DDT (O.P`DDTJ              0            ND              0             ND              0             ND            0          ND
                           4,4'DDT (P,P'DDTI              0            ND              0             ND             1.6                          0          ND

                        PCB # (CLORINA710N)
                           NOAA S&T PCBs
                                 8 (CL2)                 0.7                          0.9             J             0.2             J            0          ND
                                 18 (CW)                  0            ND              0             ND              0             ND           0.4         J
                                 28 (CL3)                 0            ND              0             ND             0.4             J           0.8
                                 44 (CIA)                0.8                           0             ND             1.5                          1
                                 52 (CIA)                0.8                           0             ND             2.2                         1.9
                                 66 (CIA)                 0            ND              0             ND              0             ND            0          ND
                                 101 (CL5)               0.8                          0.2             J             3.3                         1.7
                                 105 (CL5)                0            ND              0             ND             1.1                          0          ND
                            110/77 (CL5/4)                0            ND              0             ND              0             ND            0          ND






                                                        Mussel Watch Project Year 8 - Pesticides and PCBs Data


                              INVEST#:                TBCB                        CBBI                        CBFM                       NBNB
                                 ID:              Tampa Bay                 Charlotte Harbor            Charlotte Harbor             Naples Bay
                                SITE:            Cockroach Bay                Bird Island                  Fort Meyers               Naples Bay
                              LABSAMNO:               K7114                       K7128                       K7126                      K7120
                           SAMPLE TYPE:               SAMP                        SAMP                        SAMP                       SAMP
                                UNIT.                  ng1g                       ng1g                        ng/g                       ng/g
                               Analyte                 Cone      1313 QUAL        Cone       DB QUAL          Cone        1313 QUAL      Cone    DB QUAL


                       118/108/149(CL5/5/6)            2.6                        0.5            J              4.9                      2.7
                              128 (CL6)                 0           ND             0            ND              0            ND          0          ND
                              138 (CL6)                 1                          0            ND              3.5                      0          ND
                              126 (CL5)                 0           ND             0            ND              0            ND          0          ND
                              153 (CL6)                2.1                         0            ND              5.3                      2.1
                              170 (CL7)                 0           ND             0            ND              0            ND          0          ND
                              180 (CL7)                 0           ND             0            ND              0            ND          0          ND
                       187/182/159(CL7/7/6)             0           ND             0            ND              1.3                      0.9
                              195 (CL8)                 0           ND             0            ND              3.2                      0          ND
                              206 (CL9)                 0           ND             0            ND              0            ND          0          ND
                              209 (CLIO)                0           ND             0            ND              0            ND          0          ND

                         Surrogate Recoveries
                              DBOFB%:                  71.9                       76.6                          78                       75.7
                              PCB#103%-                 81                        93.4                        93.4                       85.9
                              PCB#198%:                79.2                       89.4                        92.1                       90.4







                                                          Mussel Watch Prqject Year 8 - Pesticides and PCB9 Data


                  INVEST#:                 RBHC                         EVFU                       PRBB                         PRBM[                      PRBJ
                     ID:               Rookery Bay                 Everglades                  Puerto Rico                 Puerto Rico                Puerto Rico
                     Srm:           Henderson Creek              Faka. Union Bay           Bahia de Boquieron            Bahia Montalva             Bahia de Jobos
                  LABSAMNO:                K7122                        K7124                      K7130                        K7132                      K7134
               SAMPLE TYPE:                SAMP                         SAMP                       SAMP                         SAMP                       SAMP
                    UNIT:                  ng/g                         ng/g                       ng/g                         ng/g                       ng/g
                  Analyte                  Cone       D13 QUAL          Cone     DB QUAL           Cone        DB QUAL          Cone      1313 QUAL        Cone     DI3 Q



              RECEIPT DATE:                1/19/93                      1/19/93                    1/20/93                      1/21/93                    1/22/93
                  QCBATCH:                 M1235                        M1235                      M1235                        M1235                      M1235
            EXTRACTION DATE:               9/17/93                      9/17/93                    9/17/93                      9/17/93                    9/17/93
                  METHOD:                  GCMS                         GCMS                       GCMS                         GCMS                       GCMS
              ANALYSIS DATE:               10/31/93                     10/31/93                   10/31/93                     10/31/93                   10/31/93
                  METHOD:                  GCECD                        GCECD                      GCECD                        GCECD                      GCECD
              ANALYSIS DATE:               8/23/94                      8/23/94                    8/23/94                      8/23/94                    8/24/94
                  MATRIX:                  TISSUE                       71SSUE                     TISSUE                       TISSUE                     TISSUE
                  SUBMAT:
                  WETWT:                   14.92                        15.16                      9.4                          6.64                       8.22
                  DRYWT:                   2.68                         1.78                       1.89                         1.03                       1.39
                  WTUNITS:                 GRAMS         DRY            GRAMS       DRY            GRAMS          DRY           GRAMS        DRY           GRAMS        DRY
         bo
         OD       PCTSOLIDS:               17.900/6                     11.800A                    20.10%                       15.500/6                   16.90%
                  Lipid Weight:
                  TOTAL LIPID:               6.4                        6.02                       6.2                          2.3                        3.77
                  LIPID UNITS:             % DRY                        % DRY                      % DRY                        % DRY                      % DRY
                     VOL:
                  VOLUNITS:                LITERS                       LITERS                     LITERS                       LITERS                     LITERS

                  DBOFB:                   77.6                         74.1                       73.6                         78.7                       79.8
                  PCB#103:                 94.4                         81.8                       90.1                         89.2                       80.5
                  PCB# 198:                89.5                         81.6                       84.5                         89.1                       87.8
                  TOTAL BHCs                 0            ND            0           ND               0            ND             0           ND            0            ND
          TOT CHLORDANES (A1,U               3.4                        1.7                          0                           0                         0.2
          TOT CHI.A)RDANES (S&II             1.9                        0.9                          0            ND             0           ND            0.2
                  TOTAL DDTs                 3.2                        1.7                          1             1            2.1           1            1.1
             TOTAL PCBs (S8M                 3.7           1            10.5         1             3.8             1            36.1          1            33.6

                  ALPHA-BHC                  0            ND            0           ND               0            ND             0           ND            0            ND
                     F4rR                    0            ND            0.1          j               0            ND             0           ND            0            ND
                  BETA-BHC                   0            ND            0           ND               0            ND             0           ND            0            ND
                  GAMMA-BHC                  0            ND            0           ND               0            ND             0           ND            0            ND
                  DELTA-BHC                  0            ND            0           ND               0            ND             0           ND            0            ND
                HE-r1t'%CHWR                 0            ND            0           LND                           IND            V                         0            ND





                                                         Mussel Watch Project Year 8 - Pesticides and PCBs Data


                 INVEST#:               RBHC                         EVFU                        PRBB                         PRBM                        PRI3J
                   ID:               Rookery Bay                  Everglades                  Puerto Rico                  Puerto Rico                Puerto Fdco
                  SITE:            Henderson Creek             Faka Union Bay             Bahia de Boquieron             Bahia Montalva.            B"ta de Jobos
              LABSAMNO:                 K7122                       K7124                        K7130                       K7132                        K7134
             SAMPLE TYPE:                SAMP                        SAMP                        SAMP                         SAMP                        SAMP
                  UNIT-                  ng/g                        ng/g                         ng/g                        ng/g                        ng/g
                 Analyte                 Cone        DB QUAL         Cone       DB QUAL          Cone         DB QUAL         Cone        DB QUAL         Cone      1313 Q



            HEPTA-EPO)GDE                  0             ND            0           ND               0             ND            0            ND            0            ND
            OXYCHLORDANE                   0             ND            0           ND               0             ND            0            ND            0            ND
         GAMMA-CHLORDANE                  0.7                         0.3           J               0             ND            0            ND            0            ND
         ALPHA-CHLORDANE 0                0.9                         0.5           J               0             ND            0            ND           0.2            J
         TRANS-NONACHLOR 0                 1                          0.5           J               0             ND            0            ND            0            ND
            CIS-NONACHLOR                 0.9                         0.5           J               0             ND            0            ND            0            ND
                 ALDRIN                    0             ND            0           ND               0             ND            0            ND            0            ND
                 DIELDRIN                  0             ND            0           ND               0             ND            0            ND           0.7            J
                 ENDPJN                    0             ND            0           ND               0             ND            0            ND            0            ND
                 MIREX                     0             ND            0           ND               0             ND            0            ND            0            ND
            2.4'DDE (0,P'DDE)              0             ND            0           ND               0             ND            0            ND            0            ND
            4,4'DDE (P,PDDE)              3.2                         1.7                           1                          1.4                        1.1
            2.4'DDD (0,P'DDD)              0             ND            0           ND               0             ND           0.7            J            0            ND
            4,4'DDD (P,P'DDD)              0             ND            0           ND               0             ND            0            ND            0            ND
        (D  2.4*DDT (0,P'DDTI              0             ND            0           ND               0             ND            0            ND            0            ND
            4,4*DDT (P.P'DDTI              0             ND            0           ND               0             ND            0            ND            0            ND


         PCB # (CLORINATION)
            NOAA S&T PC139
                 8 (CL2)                   0             ND           0.6           J               0             ND            0            ND            0            ND
                 IS (CL3)                  0             ND            0           ND               0             ND            0            ND            0            ND
                 28 (CL3)                  0             ND            0           ND               0             ND            0            ND            0            ND
                 44 (CIA)                  0             ND            0           ND               0             ND            0            ND            0            ND
                 52 (CIA)                  0             ND            0           ND               0             ND           0.6            J           0.4            J
                 66 (CIA)                  0             ND            0           ND               0             ND            0            ND            0            ND
                 101 (CL5)                0.1            J             0           ND               0             ND            I             J           0.6            J
                 105 (CIZ)                 0             ND            0           ND               0             ND            0            ND           0.5            J
             110/77(CL5/4)                 0             ND            0           ND               0             ND            0            ND           7.5






                                                       Mussel Watch Project Year 8 - Pesticides and PCBs Data


               INVEST#:                RBHC                       EVFU                       PRBB                        PRBM                      PF@
                  ID:               Rookery Bay                Everglades                 Puerto Rico                Puerto Rico               Puerto Rico
                 SrrE:           Henderson Creek             Faka Union Bay           Bahia dc Boquteron           Bahia Montalva             Bahia de Jobos
               LABSAMNO:               K7122                      K7124                      K7130                       K7132                     K7134
            SAMPLE TYPE:               SAMP                       SAMP                       SAMP                        SAMP                      SAMP
                 UNIT:                 ng/g                       ng/g                       ng/g                        ng/g                      ng/g
                Analyte                Cone        DB QUAL        Cone       DB QUAL         Cone        DB QUAL         Cone       DB QUAL        Cone      DB Q

        118/108/149(CL5/5/6)             0             ND           0           ND             0             ND           0            ND          0.9            J
               128 (CL6)                 0             ND           0           ND             0             ND           0            ND            0          ND
               138 (CL6)                 0             ND           0           ND             0             ND           1.5           J            0          ND
               126 (CL5)                 0             ND           0           ND             0             ND           0            ND            0          ND
               153 (CL6)                0.6            J            0           ND            0.7            J            8.5                      3.6
               170 (CL7)                 0             ND           0           ND             0             ND           0            ND            0          ND
               180 (CL7)                 0             ND           0           ND             0             ND           0            ND            0          ND
        187/182/159(CL7/7/6)             0             ND           0           ND             0             ND           3.9                        1            J
               195 (C118)                0             ND          2.9                         0             ND           0            ND          0.8            J
               206 (CL9)                 0             ND           0           ND             0             ND           0            ND            0          ND
               209(CL10)                 0             ND           0           ND             0             ND           0            ND            0          ND

         Surrogate Recoveries
      0        DBOF'B%:                77.6                       74.1                       73.6                        78.7                      79.8
               PCB#103%:               94.4                       81.8                       90.1                        89.2                      80.5
               PCB#198%:               89.5                       81.6                       84.5                        89.1                      87.8




I
I
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I
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I
I
I                    Pesticide QC Data
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1                           131






                                                                Mussel Watch Year 8 - Pesticide QC Data


                          INVEST#:           LAB QA SAMPLE                 LAB QA SAMPLE                       GBYC                 LAB QA SAMPLE
                              ID:              PROC BLANK                    SPIKE BLANK                 Galveston Bay                      GBYC
                            SITE:                                                                         Yacht Club                 Galveston Bay
                         LABSAMNO:                 Q6336                        Q6337                          K7004                        Q6338
                            UNIT:                   ng/g                           %                           ng/g                         ng/g
                        Analyte (Cont)              Conc        DB QUAL        % RECOV        DB QUAL          Conc     DB QUAL             Conc      D13 g UAL

                        TOTAL BHCs                   0              ND                                         9.5                          10.6
                  TOT CHLORDANES (ALL)               0              ND                                         36.5                         41
                  TOT CHLORDANES (S&T)               0                         AVERAGE                         20.7                         23.3
                        TOTAL DDTs                  0.1             1          % RECOV                         26.2                         32.3
                      TOTAL PCBs (S&Tj              4.3                                                        162.7                        182

                        ALPHA-BHC                    0              ND            65                           2.4                          2.6
                             HCB                     0              1             81.5                         0            1               0
                         BETA-BHC                    0              ND            59.7                         2.9                          3.3
                        GAMMA-BHC                    0              ND            67.2                         3.1                          3.6
                         DELTA-BHC                   0              ND            63.7                         1.1                          1.1
                        HEPTACHLOR                   0              ND            66.1                         0.1           1              0.1
                      HEPTA-EPO)UDE                  0              ND            70.5                         6.9                          8.1
                      OXYCHLORDANE                   0              ND            86.4                         1                            1.1
                    GAMMA-CHLORDANE                  0              ND            76.3                         10                           11
                    ALPHA-CHLORDANE                  0              ND            73.2                         8                            8.8
                    TRANS-NONACHLOR                  0              ND            68.6                         5.8                          6.4
                      CIS-NONACHLOR                  0              ND            77.4                         4.8                          5.6
                           ALDRIN                    0              ND            66.1                         0            ND              0            ND
                          DIELDRIN                   0              ND            62.2                         9.3                          10.9
                           ENDRIN                    0              ND            79.6                         0            ND              0            ND
                           MIREX                     0              ND            82.6                         0.4                          0.4
                      2,4'DDE (0,P'DDE)              0              ND            67.9                         0.3          1               0.4
                      4,4'DDE (P,P'DDE)             0.1             1             65.6                         13.8                         17.9
                      2,4'DDD (0,PDDD)               0              ND            70.1                         1.2                          1.3
                      4.4'DDD (P.P'DDD)              0              ND            63.9                         9.5                          10.7
                      2,4'DlXr (0,P'DEM              0              ND            72.2                         0.8                          1
                      4,4'DDT (P.P'DDII              0              ND            66.4                         0.6                          0.9

                   PCB # (CLORINATION)
                      NOAA S&T PCBs
                           8 (CL2)                  0.1             1             91.6                         0            ND              0            ND
                           18 (CI-3)                 0              ND            86.9                         1.2                          1.8






                                                                  Mussel Watch Year 8 - Pesticide QC Data


                            INVESrr#:          LAB QA SAMPLE                 LAB QA SAMPLE                  -   GBYC                 LAB QA SAMPLE
                              ID:               PROC BLANK                    SPIKE BLANK                 Galveston Bay                      GBYC
                             SrrE:                                                                          Yacht Club                 Galveston Bay
                            LABSAMNO:               Q6336                         Q6337                         K7004                        Q6338
                             UNrr:                    ng/g                          %                           ng/g                         ng/g
                         Analyte (Cont)               Conc       DB QUAL        % RECOV        DB QUAL          Conc      DB QUAL            Conc       DB QUAL

                            28 (CL3)                   0             ND            88.3                         2.6                          2.8
                            44 (CIA)                   0             ND            88.2                         7.2                          7.7
                            52 (CL4)                   0             ND            93.6                         10.4                         11.1
                            66 (CIA)                   0             ND            80.4                         1.5                          1.6
                            101 (CL5)                  0             ND            87.7                          9                           9.3
                            105 (CL5)                  0             ND            79.2                         3.5                          4.1
                        110/77 (CL5/4)                 0             ND            77.8                          8                           9.3
                    118/108/149(CL5/5/6)               0             ND            83.4                         6.1                          6.6
                            128 (CL6)                  0             ND            95.9                         0.7           1              0.8
                            138 (CL6)                  0.2            1            82.2                         8.7                          9.8
                            126 (CL5)                  0             ND            76.7                          0            ND              0             ND
                            153 (CL6)                  0.1            1            61.2                         14.2                         15.7
                            170 (CL7)                  0.5                          83                          0.3           1              0.7
                            180 (CL7)                  0             ND            72.7                         2.6                          3.4
                    187/182/159(CL7/7/6)               0             ND            80.9                         3.4                          3.8
                            195 (CL8)                  0             ND            79.1                          0            ND              0
                            206 (CL9)                  0             ND            71.6                          0            ND              0
                            209 (CLIO)                 0             ND            83.1                          0            ND             0.2


                     Surrogate Recoveries
                            DBOFB%:                   75.5                         76.5                         73.4                         70.1
                            PCB#103%:                  83                          84.6                         75.4                         68.1
                            PCB# 1980/6:              79.7                         76.6                         75.8                         72.6






                                                               Mussel Watch Year 8 - Pesticide QC Data


                         INVESTC            LAB QA SAMPLE                LAB QA SAMPLE                LAB QA SAMPLE                        VBSP
                            ID:                    GBYC                    PROC BLANK                   SPIKE BLANK                 Vennillion Bay
                           SITE:             Galveston Bay                                                                         Southwest Pass
                       LABSAMNO:                   Q6339                      Q6340                         Q6341                          K7046
                           UNIT-                    %                          nglg                           %                            ng/g
                       Analyte (Cont)           % RECOV       DB QUAL          Conc        DB QUAL        % RECOV        1313 QUAL         Conc     DB QUAL

                       TOTAL BHCs                                                0             ND                                          2.2           1
                 TOT CHLORDANES (ALL)                                            0             ND                                          17
                 TOT CHLORDANES (S&Tj          AVERAGE                           0                        AVERAGE                          9.9
                       TOTAL DI)Ts              % RECOV                         0.9                       % RECOV                          52.7
                     TOTAL PCBs (S&T)                                           4.6                                                        87.2

                       ALPHA-BHC                   68.3                          0             ND            61.7                          1.4
                           HC13                    97.5                         0.1             1            82.5                          0            ND
                        BETA-BHC                   63.9                          0             ND            61.2                          0            ND
                       GAMMA-BHC                   73.1                          0             ND             71                           0.8
                       DELTA-BHC                   60.2                          0             ND            61.5                          0            ND
                       HEPTACHLOR                  73.1                          0             ND            75.5                          0.2           1
                     HEPTA-EPOXIDE                 94.2                          0             ND             74                           2.7
                     OXYCHIA)RDANE                 95.7                          0             ND            91.6                          0.5           1
                   GAMMA-CHLORDANE                 84.4                          0             ND            82.3                          3.7
                   ALPHA-CHLORDANE                 83.1                          0             ND            83.1                          3.6
                   TRANS-NONACHLOR                 79.1                          0             ND            81.8                          3.5
                     CIS-NONACHLOR                 86.4                          0             ND            77.6                          2.9
                          ALDRIN                   70.4                          0             ND            70.8                          0            ND
                        DIELDRIN                   72.9                          0             ND             70                           11.5
                          ENDRIN                   76.1                          0             ND             71                           0.8
                           MIREX                   101                           0             ND            97.3                          0.5           1
                     2,4'DDE (0,P'DDE)             67.8                          0             ND            73.1                          0            ND
                     4,4'DDE (P.P'DDE)             92.4                         0.9                          73.3                          30.1
                     2,4'DDD (0,P'DDD)             74.4                          0             ND            75.6                          1.2
                     4,4'DDD (P,P'DDD)             77.7                          0             ND            74.6                          15.4
                     2,4'DDT (O,P'DDTI             81.1                          0             ND            82.6                          1.7
                     4,4'DDT (P,P'DDTI             68.2                          0             ND             78                           4.3


                   PCB # (CLORINATION)
                     NOAA S8rT PCBs
                          8 (CL2)                  109.7                         0             ND            92.6                          0            ND
                          18 (CL3)                 107.7                         0             ND             97                           0            ND






                                                                    Mussel Watch Year 8 - Pesticide QC Data


                            INVESr#:            LAB QA SAMPLE                  LAB QA SAMPLE                  LAB QA SAMPLE                          VBSP
                               ID:                      GBYC                     PROC BLANK                     SPIKE BLANK                   Vernifflon. Bay
                              SrrE:              Galveston Bay                                                                               Southwest Pass
                            LABSAMNO:                   Q6339                       Q6340                           Q6341,                           K7046
                              UNrr:                     %                              ng/g                           %                              ng/g
                         Analyte (Cont)             % RECOV        DB QUAL             Conc        DB QUAL        % RECOV         DB QUAL            Conc       DB QUAL

                            28 (CL3)                    100.9                          0              ND             91.5                            0.3
                            44 (CIA)                    113.8                          0              ND             95.1                            1.3
                            52 (CL4)                    124.8                          0              ND             100.5                           1.8
                            66 (CIA)                    88.5                           0              ND             88.8                            0.6            j
                            101 (CL5)                   107.6                          0              ND             99.1                            4.2
                            105 (CL5)                   90                             0              ND             85.3                            1.7
                        110/77 (CL5/4)                  101.4                          0              ND             97.9                            4.4
                    118/108/149(CL5/5/6)                116.9                          0              ND             88.5                            2.3
                            128 (CL6)                   119.7                          0              ND             76.6                            0             ND
                            138 (CL6)                   106.7                          0.5                           89.4                            10.2
                            126 (CL5)                   101.6                          0              ND             85.7                            0             ND
                            153 (CL6)                   85.2                           0              ND             67.5                            9.6
                            170 (CL7)                   75.9                           0.6                           86.4                            0             ND
                            180 (CL7)                   94.1                           0              ND             80.6                            0             ND
                    187/182/159(CL7/7/6)                108                            0              ND             87.1                            4.6
                            195 (CI,8)                  94.9                           0              ND             83.6                            0             ND
                            206 (CL9)                   87.7                           0              ND             74.1                            0             ND
                            209 (CLIO)                  107                            0              ND             86.9                            0             ND


                     Surrogate Recoveries
                            DBOFB%:                     73.2                           80.3                          73.6                            75.3
                            PCB#103%:                   72.2                           90.5                          85.2                            81.6
                            PCB#198%:                   71.8                           79.4                          75.1                            77






                                                                Mussel Watch Year 8 - Pesticide QC Data


                         INVESTC            LAB QA SAMPLE                LAB QA SAMPLE                LAB QA SAMPLE                 LAB QA SAMPLE
                            ID:                     VBSP                        VBSP                    PROC BLANK                   SPIKE BLANK
                           SITE:             Vermillion Bay               Vermillion Bay
                        LABSAMNO:                 Q6342                        Q6343                        Q6344                        Q6345
                           UNIT:                    ng/g                         %                           ng/g                           %
                      Analyte (Cont)                Conc      DB QUAL        % RECOV        1313 QUAL       Conc         DB QUAL       % RECOV        DB gUAL

                       TOTAL BHCs                   2                                                         0             ND
                 TOT CHLORDANES (ALL)               16.7                                                      0             ND
                TOT CHLORDANES (S&T)                9.9                      AVERAGE                          0                        AVERAGE
                       TOTAL DDTs                   46.4                     % RECOV                          0             ND         % RECOV
                     TOTAL PCBs (S"                 81.2                                                      5


                        ALPHA-BHC                   1.3                         42.9                          0             ND              82.4
                           HCB                      0.1           j             75.6                         0.1             j              99.3
                        BETA-BHC                    0             ND            60.1                          0             ND              70.5
                        GAMMA-BHC                   0.6                         58.8                          0             ND              89.3
                        DELTA-BHC                   0             ND            46.8                          0             ND              79.4
                       HEPTACHLOR                   0.2           j             72.5                          0             ND              87.2
                     HEPTA-EPO)UDE                  2.6                         62.8                          0             ND              85.5
                     OXYCHLORDANE                   0.6                         88.3                          0             ND              103.5
                  GAMMA-CHLORDANE                   3.8                         77.9                          0             ND              89.5
                   ALPHA-CHLORDANE                  3.6                         71.5                          0             ND              92.5
                   TRANS-NONACHLOR                  3.5                         74.1                          0             ND              89
                     CIS-NONACHLOR                  2.4                         71.3                          0             ND              86.4
                         ALDRIN                     0             ND            67.1                          0             ND              85.9
                        DIELDRIN                    10.8                        55.1                          0             ND              80.9
                         ENDRIN                     0.9                         76.2                          0             ND              83.2
                          MIREX                     0.4           1             102.5                         0             ND              105.8
                     2,4'DDE (O.P'DDE)              0.4           1             65.6                          0             ND              82.2
                     4,4'DDE (P,P'DDE)              27                          37             M              0             ND              86.3
                     2,4'DDD (0,P'DDD)              1.1                         69.3                          0             ND              94.6
                     4,4'DDD (P,P'DDD)              13.2                        53.9                          0             ND              84.4
                     2,4'DDT (0,P'DEM               1.3                         75.9                          0             ND              92.4
                     4.4'DDT (P,P'DDTI              3.3                         72.5                          0             ND              90.6


                  PCB # (CLORINATION)
                     NOAA S&T PCBs
                          8 (CL2)                   0             ND            76.6                         0.4                            109
                         18 (CL3)                   0             ND            94.7                          0             ND              105.8






                                                                Mussel Watch Year 8 - Pesticide QC Data


                          INVEST#:          LAB QA SAMPLE                LAB QA SAMPLE                LAB QA SAMPLE                LAB QA SAMPLE
                            ID:                    VBSP                        VBSP                     PROC BLANK                   SPIKE BLANK
                           SITE:             'Vermillion Bay              Vemifflon Bay
                          IABSAMNO:                Q6342                       Q6343                       Q6344                          Q6345
                           UNIT:                   ng/g                          %                          ng/g                           %
                       Analyte (Cont)              Conc       DB QUAL        % RECOV       DB QUAL          Conc        DB QUAL        % RECOV        DB QUAL

                          28 (CL3)                 0.3             1           88.7                           0             ND            105.1
                          44 (CIA)                 1.1                         93.7                           0             ND            104
                          52 (CIA)                 1.9                         100.9                          0             ND            108
                          66 (CIA)                 0.6             1           112.2                          0             ND            100.6
                          101 (CL5)                4.4                         96.9                           0             ND            102.8
                          105 (CL5)                1.2                         86.5                           0             ND            98.4
                      110/77 (CL5/4)               4.6                         127.9                          0             ND            107.5
                  118/108/149(CL5/5/6)             2.2                         91.8                           0             ND            98.8
                          128 (CL6)                 0             ND           84.7                           0             ND            97.8
                          138 (CL6)                8.5                         87.8                           0.4                         98.6
                          126 (CL5)                 0             ND           109.4                          0             ND            99.6
                          153 (CL6)                8.7                         63.8                           0             ND            71.1
                          170 (CL7)                0.8                          92                            0.4                         93.2
                          180 (CL7)                 0             ND           88.9                           0             ND            93.5
        W         187/182/159(CL7/7/6)              4                          85.7                           0             ND            95.7
                          195 (CL8)                 0             ND           85.9                           0             ND            95.6
                          206 (CL9)                 0             ND           76.9                           0             ND            85.1
                          209 (CLIO)                0             ND           91.5                           0             ND            95.3

                    Surrogate Recoveries
                          DBOFBO/b:                75.5                        71.7                         77.4                          73.3
                          PCB#103%:                86.5                        87.5                         87.2                          77.6
                          PCB#198%:                75.6                        75.5                         83.4                          71.8






                                                                 Mussel Watch Year 8 - Pesticide QC Data


                       INVEST#:                    MSPB                   LAB QA SAMPLE                   LAB QA SAMPLE                  LAB QA SAMPLE
                          ID:             Mississippi Sound                       MSPB                          MSPB,                     PROC BLANK
                         SITE:              Pascagoula Bay                Mississippi Sound              Mississippi Sound
                     LABSAMNO:                     K7078                          Q6346                         Q6347                         Q6348
                         UNrP.                     ng/g                           ng/g                            %                            ng/g
                     Analyte (Cont)                Conc        DB QUAL            Conc        DB QUAL        % RECOV         DB QUAL           Conc         DB QUAL


                     TOTAL BHCs                    1.6                            1.5                                                            0             ND
              TOT CHLORDANES (ALL)                 9.1                            11.9                                                           0             ND
              TOT CHLORDANES (S&T)                 5.8                            8.1                        AVERAGE                             0
                     TOTAL DI)Ts                   23.2                           28.7                       % RECOV                             0             ND
                   TOTAL PCBs (S&II                153.6                          202.1                                                         2.2


                     ALPHA-BHC                     1.1                            0.7                           73.8                             0             ND
                         HCB                       0              ND               0             ND             109.4                           0.1             1
                      BETA-BHC                     0              ND              0.2             1             64.5                             0             ND
                     GAMMA-BHC                     0.5                            0.6                           82.9                             0             ND
                     DELTA-BHC                     0              ND               0             ND             68.9                             0             ND
                     HEPTACHLOR                    0.1             1              0.2                           82.1                             0             ND
                   HEPTA-EPO)UDE                   0.7                            0.9                           80.3                             0             ND
                   OXYCHLORDANE                    0.4             1              0.5             1             97.2                             0             ND
                GAMMA-CHLORDANE                    2.9                            3.4                            90                              0             ND
        00      ALPHA-CHLORDANE                    2.6                            3.7                           95.4                             0             ND
                TRANS-NONACHLOR                    2.4                            3.3                           94.3                             0             ND
                   CIS-NONACHLOR                   0              ND               0             ND             116.8                            0             ND
                        ALDRIN                     0              ND               0                            80.5                             0             ND
                      DIELDRIN                     3                              3.3                           81.3                             0             ND
                        ENDRIN                     0              ND               0             ND             97.5                             0             ND
                         MIREX                     0.7                             1                            112.6                            0             ND
                   2,4'DDE (0,P'DDE)               2.5                            3.9                           87.4                             0             ND
                   4ADDE (P,P'DDE)                 13.1                           15.9                          99.4                             0             ND
                   2,4'DDD (O.P'DDD)               1.2                            1.4                           107.5                            0             ND
                   4,4'DDD (P.P'DDD)               4.6                            5.3                           90.9                             0             ND
                   2,4'DDT (0,P'DEM                0.8                            1.3                           94.6                             0             ND
                   4,4'DDT (P,P'DEM                0.9                            0.8                           95.6                             0             ND


                PCB # (CLORINATION)
                   NOAA S&T PCBs
                        8 (CL2)                    0              ND               0             ND             104.8                            0             ND
                       18 (CL3)                    0              ND               0             ND             107.3                            0             ND






                                                                     Mussel Watch Year 8 - Pesticide QC Data


                         INVEST#:                    MSPI3                     LAB QA SAMPLE                    LAB QA SAMPLE                    LAB QA SAMPLE
                            ID:              Mississippi Sound                          MSPB                            MSPB                       PROC BLANK
                           SITE:               Pascagoula Bay                  Mississippi Sound                Mississippi Sound
                         IABSAMNO:                   K7078                              Q6346                           Q6347                         Q6348
                           UNIT:                     ng/g                               ng/g                             %                              ng/g
                      Analyte (Cont)                 Cone          DB QUAL              Cone        1313 QUAL       % RECOV          DB QUAL            Cone         DB QUAL

                         28 (CL3)                     0.5                               0.6                             97.2                             0              ND
                         44 (CL4)                     1.2                               1.4                             94.5                             0              ND
                         52 (CL4)                     2.3                               2.8                             100.2                            0              ND
                         66 (CIA)                     0.9              1                1.3                             116.7                            0              ND
                         101 (CL5)                    4.1                               6.2                             111.5                            0              ND
                         105 (CL5)                   43.1                               53.4                            151.5            M               0              ND
                      110/77 (CL5/4)                   0              ND                0              ND               137                              0              ND
                 118/108/149(CL5/5/6)                  4                                4.8                             109.1                            0              ND
                         128 (CL6)                     0              ND                0              ND               113.2                            0              ND
                         138 (CL66)                   9.6                               11.9                            105.1                            0              ND
                         126 (CL5)                     0              ND                0              ND               124.2                            0              ND
                         153 (CL66)                   6.7                               8                               76.3                             0              ND
                         170 (CL7)                    0.7              1                1.1                             101.4                            0              ND
                         180 (CL7)                     0              ND                0              ND               124.1                            0              ND
                 187/182/159(CL7/7/6)                  0              ND                4.6                             129.2                            0              ND
                         195 (CL8)                     0              ND                0              ND               111.5                            0              ND
                         206 (CL9)                     0              ND                0              ND               101.4                            0              ND
                         209 (CLIO)                    0              ND                0              ND               113                              0              ND


                   Surrogate Recoveries
                         DB0FB0/6:                   82.5                               75                              75.1                             67
                         PCB#103%:                    88                                77.8                            76.1                            63.3
                         PCB# 1980/6:                86.8                               83.7                            84.5                            70.6






                                                                   Mussel Watch Year 8 - Pesticide QC Data


                          INVEST#:            LAB QA SAMPLE                        TBMK                     LAB QA SAMPLE                  IAB QA SAMPLE
                             ID:               SPIKE BLANK                      Tampa Bay                        TBMK                        SPIKE K7106
                            SITE:                                            Mullet Key Bayou                  Tampa Bay                      Tampa Bay
                        LABSAMNO:                   Q6349                         K7106                          Q6350                          Q6351
                            UNIT:                     %                             ng/g                           ng/g                            %
                        Analyte (Cont)            % RECOV        DB QUAL            Conc        DB QUAL            Conc        DB QUAL         % RECOV        DB QUAL

                        TOTAL BHCs                                                   0              ND             0.1
                 TOT CHLORDANES (ALL)                                               8.3                            10.5
                 TOT CHLX)RDANES (S&T)           AVERAGE                            4.9                            6.5                        AVERAGE
                        TOTAL DI)Ts               % RECOV                           7.2                            8.1                        % RECOV
                      TOTAL PCBs (S&T1                                              10.7                           11.1


                        ALPHA-BHC                    98.5                            0              ND             0.1             j               79.9
                            HCB                      107.4                           0               j             0.1             j               88.4
                         BETA-BHC                    75.3                            0              ND              0              ND              84.5
                        GAMMA-BHC                    99.3                            0              ND              0              ND              89.5
                        DELTA-BHC                    79.7                            0              ND              0              ND              76.1
                        HEPTACHLOR                   91.6                            0              ND              0              ND              99.6
                      HEPTA-EPOICIDE                 72.1                           0.2              j             0.4                             85.9
                      OXYCHLORDANE                   111.5                          0.3                            0.5                             105
                    GAMMA-CHLADRDANE                 92.7                           1.7                            2.1                             41.5
                    ALPHA-CHLORDANE                  94.5                           2.3                            3.3                             25.6            M
                    TRANS-NONACHLOR.                 91.8                           2.4                            2.9                             0.6             M
                      CIS-NONACHLOR                  86.8                           1.4                            1.5                             38.5            M
                           ALDRIN                    84.8                            0              ND              0              ND              98
                         DIELDRIN                    81.4                           0.9                            1.1                             68
                           ENDRIN                    85.2                            0              ND              0              ND              97.3
                            MIREX                    106.3                          0.5                            0.6                             87.9
                      2,4'DDE (0,P'DDE)              74.8                            0              ND              0              ND              88.1
                      4,4'DDE (P,P'DDE)              72.9                           3.8                            4.6                             0               M
                      2,4'DDD (0,P'DDD)              87                             0.3              1             0.3                             81.3
                      4.4'DDD (P.P'DDD)              79.7                            3                              3                              31.1            M
                      2,4'DDT (O,P'DM                92.1                            0              ND              0              ND              100
                      4,4'DDT (P,P'DM                94.2                           0.1              j             0.3             j               89.4


                   PCB # (CLORINATION)
                      NOAA S&T PCBs
                           8 (CL2)                   117.5                          0.5              1              0              ND              91.8
                           18 (CL3)                  116.8                          0.2              j             0.4             1               94.5






                                                                  Mussel Watch Year 8 - Pesticide QC Data


                          INVEST#:           LAB QA SAMPLE                       TBMK                    LAB QA SAMPLE                  LAB QA SAMPLE
                             ID:              SPIKE BLANK                     Tampa Bay                        TBMK                       SPIKE K7106
                           SITE:                                           Mullet Key Bayou                 Tampa Bay                      Tampa Bay
                          LABSAMNO:                Q6349                         K7106                         Q6350                          Q6351
                           UNIT:                     %                             ng/g                          ng/g                           %
                       Analyte (Cont)            % RECOV        DB QUAL            Conc       DB QUAL            Conc       DB QUAL        % RECOV         DB QUAL

                          28 (CL3)                   99.5                           0             ND             0.2             1              95.2
                          44 (CIA)                   81.7                          0.5            1              0.7                            92.5
                          52 (CIA)                   108.4                         0.8                           0.6                            79
                          66 (CIA)                   95                             0             ND              0             ND              101.7
                          101 (CL5)                  100                           0.4            1              0.6                            80
                          105 (CL5)                  96.1                           0             ND             0.1             1              94.3
                      110/77 (CL5/4)                 134.4                          0             ND              0             ND              133.5
                  118/108/149(CL5/5/6)               96.2                           1                             1                             73
                          128 (CL6)                  95.8                           0             ND              0             ND              101.4
                          138 (CL6)                  100.1                          0             ND              0             ND              102
                          126 (CL5)                  106                            0             ND              0             ND              118.9
                          153 (CI,66)                75                            1.1                           1.1                            57.2
                          170 (CL7)                  112                            0             ND              0             ND              104.5
                          180 (CL7)                  94.9                           0             ND              0             ND              106.5
                  187/182/159(CL7/7/6)               97.7                          0.4            1              0.3             1              87
                          195 (CL8)                  99.4                           0             ND              0             ND              119.4
                          206 (CL9)                  89.2                           0             ND              0             ND              93.8
                          209 (CL10)                 108.4                          0             ND              0             ND              106.8


                   Surrogate Recoveries
                          DBOFBOA:                   65.9                          78.5                          75.9                           79.2
                          PCB#103%:                  69.4                          91.4                          68.6                           96.6
                          PCB# 1980/6:               69.5                          89.6                          81.5                           98.3




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                                                             Mussel Watch Project Year 8 - Trace Metal

            SITE      LABSAMP        SRMID       ADGDAT     SAMPTYPE         PON      WETWTR       ADWT     % MOIST     MAIXCOD UNITTM UNITQUAL                 Ag


            LMSB    K7031                        6/15/93      SAMP       S&T Oysters     35.89     0.1977     81.44      TISSUE        PPM         DRY         0.96
            CCNB    K7025                        6/15/93      SAMP       S&T Oysters     37.92     0.1991     85.28      TISSUE        PPM         DRY         1.10
            ABLR    K7035                        6/15/93      SAMP       S&T Oysters     37.98     0.1969     85.78      TISSUE        PPM         DRY         0.86
            MBAR    K7033                        6/15/93      SAMP       S&T Oysters     31.11     0.1948     90.00      TISSUE        PPM         DRY         1.01
            SAPP    K7043                        6/15/93      SAMP       S&T Oysters     5.23      0.1905     91.59      TISSUE        PPM         DRY         1.35
            EVFU    K7125                        6/16/93      SAMP       S&T Oysters     28.63     0.1979     90.88      TISSUE        PPM         DRY         0.70
            ESBD    K7045                        6/15/93      SAMP       S&T Oysters     30.97     0.1947     90.70      TISSUE        PPM         DRY         1.61
            MBGP    K7037                        6/15/93      SAMP       S&T Oysters     33.69     0.196      91.78      TISSUE        PPM         DRY         1.44
            MBLR    K7039                        6/15/93      SAMP       S&-T Oysters    29.27     0.1945     89.96      TISSUE        PPM         DRY         2.72
            MBCB    K7041                        6/15/93      SAMP       S&T Oysters     30.31     0.1911     87.03      TISSUE        PPM         DRY         1.57
            MBTP    K7027                        6/15/93      SAMP       S&T Oysters     25.15     0.192      83.90      TISSUE        PPM         DRY         1.67
            MBEM    K7029                        6/15/93      SAMP       S&T'Oysters     33.72     0.1971     84.37      TISSUE        PPM         DRY         1.82
            BRCL    K7003                        6/15/93      SAMP       S&-T Oysters    31.07     0.1983     90.02      TISSUE        PPM         DRY         2.66
            BRFS    K7001                        6/15/93      SAMP       S&,T Oysters    33.76     0.1968     88.71      TISSUE        PPM         DRY         1.34
            GBHR    K7015                        6/15/93      SAMP       S&-T Oysters    21.03     0.1934     82.79      TISSUE        PPM         DRY         2.91
            GBSC    K7009                        6/15/93      SAMP       S&T Oysters     26.28     0.1984     83.98      TISSUE        PPM         DRY         1.50
            GBTD    K7013                        6/15/93      SAMP       S&T Oysters     37.01     0.1915     85.03      TISSUE        PPM         DRY         2.79
            GBYC    K7005                        6/15/93      SAMP       S&-T Oysters    32.97     0.1941     86.87      TISSUE        PPM         DRY         1.68
            GBOB    K7011                        6/15/93      SAMP       S&T Oysters     30.32     0.1973     88.46      TISSUE        PPM         DRY         0.48
            SLBB    K7017                        6/15/93      SAMP       S&-T Oysters    39.06     0.199      88.79      TISSUE        PPM         DRY         3.27
            CLSJ    K7021                        6/15/93      SAMP       S&T Oysters     37.48     0.1985     92.34      TISSUE        PPM         DRY         1.74
            CLLC    K7019                        6/15/93      SAMP       S&T Oysters     32.05     0.1954     85.83      TISSUE        PPM         DRY         1.02
            JHJH    K7023                        6/15/93      SAMP       S&T Oysters     34.09     0.1927     84.95      TISSUE        PPM         DRY         2.21
            VBSP    K7047                        6/15/93      SAMP       S&T Oysters     34.77     0.1952     83.38      TISSUE        PPM         DRY         3.76
            ABOB    K7057                        6/15/93      SAMP       S&T Oysters     34.75     0.1984     85.04      TISSUE        PPM         DRY         1.81
            CLCL    K7059                        6/15/93      SAMP       S&T Oysters     34.5      0.1929     82.72      TISSUE        PPM         DRY         1.14
            TBLB    K7053                        6/15/93      SAMP       S&T Oysters     27.2      0.1963     91.88      TISSUE        Ppm         DRY         0.56
            TBLF    K7055                        6/15/93      SAMP       S&T Oysters     30.51     0.1973     80.73      TISSUE        Ppm         DRY         0.44
            BBSD    K7049                        6/15/93      SAMP       S&T Oysters     29.1      0.1979     83.64      TISSUE        PPM         DRY         1.67
            BBMB    K7051                        6/15/93      SAMP       S&T Oysters     31.46     0.1924     84.36      TISSUE        PPM         DRY         0.32
            MRTP    K7063                        6/15/93      SAMP       S&T Oysters     28.03     0.1989     86.91      TISSUE        PPM         DRY         2.85
            MRPL    K7061                        6/15/93      SAMP       S&T Oysters     30.48     0.1947     90.88      TISSUE        PPM         DRY         4.65
            BSSI    K7073                        6/16/93      SAMP       S&T Oysters     27.84     0.1984     90.27      TISSUE        PPM         DRY         3.43
            BSBG    K7065                        6/16/93      SAMP       S&-T Oysters    26.28     0.1955     85.96      TISSUE        PPM         DRY         0.81
            LBMP    K7067                        6/15/93      SAMP       S&-T Oysters    19.32     0.1974     88.20      TISSUE        PPM         DRY         2.37






                                                                Mussel Watch Project Year 8 - Trace Metal

             SITE      LABSAMP         SRMID       ADGDAT     SAMPTYPE          PON       WETWTR       ADWT     %MOIST MATXCOD UNITTM UNnpUAL                         Ag


             MSPC     K7071                        6/16/93       SAMP       S&T Oysters      35.73     0.1969     85.28      TISSUE         PPM         DRY           3.80
             MSBB     K7069                        6/15/93       SAMP       S&T Oysters      19.5      0.1914     86.67      TISSUE         PPM         DRY           2.88
             MSPB     K7079                        6/16/93       SAMP       S&T Oysters      35.49     0.1965     90.19      TISSUE         PPM         DRY           2.30
             MBCP     K7077                        6/16/93       SAMP       S&T Oysters      27.81     0.1977     85.98      TISSUE         Ppm         DRY           2.01
             MBHI     K7075                        6/16/93       SAMP       S&T Oysters      19.88     0.1985     90.85      TISSUE         PPM         DRY           6.58
             PBPH     K7089                        6/16/93       SAMP       S&T Oysters      26.16     0.1964     89.03      TISSUE         PPM         DRY           2.07
             PBIB     K7087                        6/16/93       SAMP       S&T Oysters      30.7      0.1972     91.30      TISSUE         PPM         DRY           2.86
             PBSP     K7091                        6/16/93       SAMP       S&T Oysters      33.5      0.1972     88.00      TISSUE         PPM         DRY           1.67
             CBJB     K7083                        6/16/93       SAMP       S&T Oysters      33.28     0.1981     84.28      TISSUE         PPM         DRY           0.60
             CBSR     K7085                        6/16/93       SAMP       S&T Oysters      32.64     0.1973     90.38      TISSUE         PPM         DRY           2.37
             CBPP     K7081                        6/16/93       SAMP       S&T Oysters      29.01     0.1984     86.38      TISSUE         PPM         DRY           4.48
             PCLO     K7093                        6/16/93       SAMP       S&T Oysters      29.28     0.1983     85.18      TISSUE         PPM         DRY           0.90
             PCMP     K7097                        6/16/93       SAMP       S&T Oysters      33.13     0.1952     86.51      TISSUE         PPM         DRY           2.14
             SAWB     K7095                        6/16/93       SAMP       S&T Oysters      33.39     0.1965     86.52      TISSUE         PPM         DRY           2.47
             APDB     K7099                        6/16/93       SAMP       S&T Oysters      25.83     0.1975     85.25      TISSUE         PPM         DRY           1.77
             APCP     K7105                        6/16/93       SAMP       S&T Oysters      25.75     0.1987     84.82      TISSUE         PPM         DRY           1.13
             AESP     K7103                        6/16/93       SAMP       S&T Oysters      24.43     0.1964     92.43      TISSUE         PPM         DRY           1.05
             CKBP     K7101                        6/16/93       SAMP       S&T Oysters      19.02     0.1955     85.49      TISSUE         PPM         DRY           0.35
             TBNP     K7111                        6/16/93       SAMP       S&T Oysters      28.95     0.1966     88.26      TISSUE         PPM         DRY           2.07
             TBMK     K7107                        6/16/93       SAMP       S&T Oysters      25.13     0.1964     82.21      TISSUE         PPM         DRY           0.28
             TBPB     K7119                        6/16/93       SAMP       S&T Oysters      34.02     0.1976     84.69      TISSUE         PPM         DRY           1.33
             TBOT     K7113                        6/16/93       SAMP       S&T Oysters      26.18     0.1966     88.24      TISSUE         PPM         DRY           2.11
             TBKA     K7109                        6/16/93       SAMP       S&T Oysters      15.87     0.1984     85.13      TISSUE         PPM         DRY           2.48
             TBHB     K7117                        6/16/93       SAMP       S&T Oysters      21.15     0.1939     82.32      TISSUE         PPM         DRY           1.48
             TBCB     K7115                        6/16/93       SAMP       S&T Oysters      13.59     0.1971     85.50      TISSUE         PPM         DRY           1.38
             CBBI     K7129                        6/16/93       SAMP       S&T Oysters      27.3      0.1959     92.12      TISSUE         PPM         DRY           3.01
             CBFM     K7127                        6/16/93       SAMP       S&T Oysters      19.47     0.1963     86.70      TISSUE         PPM         DRY           3.01
             NBNB     K7121                        6/16/93       SAMP       S&T Oysters      26.98     0.1989     87.51      TISSUE         PPM         DRY           4.37
             RBHC     K7123                        6/16/93       SAMP       S&T Oysters      17.72     0.1994     86.17      TISSUE         PPM         DRY           1.03
             GBCR     K7007                        6/15/93       SAMP       S&T Oysters      34.82     0.193      88.91      TISSUE         PPM         DRY           5.17
             PRBB     K7131                        6/16/93       SAMP       S&T Oysters      26.83     0.1949     87.29      `P- S S T T F. PPM         DRY           0-10
             PRBM     K7133                        6/16/93       SAMP       S&T Oysters      10.71     0.1948     89.26      TISSUE         PPM         DRY           .1.28
             PRBJ     K7135                        6/16/93       SAMP       S&T Oysters      15.66     0.1941     89.66      TISSUE         PPM         DRY           0.52






                                                            Mussel Watch Project Year 8 - Trace Metal


                  SUE       LABSAMP         As         Cd         Cr        CU         Fe         Hg         Ni        Pb         Se         Sn         Zn



                  LMSB     K7031           5.61       2.57       0.29       62         197      0.050       1.02      0.52       2.69       0.09        297
                  CCNB     K7025           6.20       2.94       0.39       152        247      0.158       1.22      1.18       2.90       0.01        3490
                  ABLR     K7035           7.02       2.47       0.46       76         280      0.126       1.39      0.74       3.32       0.11        806
                  MBAR     K7033           10.87      2.39       0.96       103        839      0.163       1.26      0.89       2.02       0.07        1273
                  SAPP     K7043           6.01       3.83       0.49       61         299      0.064       1.28      0.66       3.40       0.07        341
                  EVFU     K7125           5.06       2.44       0.91       60         246      0.216       1.48      0.26       1.38       0.01        1317
                  ESBD     K7045           9.29       3.51       0.57       114        361      0.113       1.65      0.50       3.45       0.05        889
                  MBGP     K7037           5.13       2.81       0.80       117        475      0.355       3.07      0.84       3.29       0.09        1643
                  MBLR     K7039           4.46       5.52       0.59       200        441      0.778       2.31      1.05       4.06       0.14        1455
                  MBCB     K7041           4.57       3.53       0.57       152        276      0.125       2.09      0.55       2.97       0.07        1035
                  MBTP     K7027           5.37       2.91       0.86       116        492      0.077       1.91      0.83       3.06       0.00        896
                  MBEM     K7029           5.55       6.39       0.51       134        324      0.062       1.52      0.49       3.22       0.05        758
                  BRCL     K7003           4.84       3.64       1.58       265        922      0.089       2.29      1.19       2.96       0.07        2017
                  BRFS     K7001           4.89       2.45       1.11       156        599      0.037       2.03      0.72       2.80       0.10        2243
                  GBHR     K7015           4.64       5.98       0.96       165        661      0.082       2.22      0.76       3.70       0.08        1164
                  GBSC     K7009           3.68       3.59       0.89       148        222      0.043       2.15      0.75       3.60       0.65        4630
                  GBTD     K7013           4.40       4.00       0.40       174        245      0.062       1.96      0.56       3.23       0.30        2348
                  GBYC     K7005           3.94       4.21       0.97       127        385      0.055       1.91      0.91       3.10       0.83        2036
                  GBOB     K7011           5.81       0.96       0.27       112        115      0.031       1.21      1.20       2.18       0.06        3389
                  SLBB     K7017           9.95       4.70       0.82       213        415      0.075       1.77      0.58       3.27       0.13        3306
                  CLSJ     K7021           8.62       3.71       0.49       128        315      0.133       2.39      0.45       3.40       0.05        1497
                  CLLC     K7019           5.17       2.34       0.29       153        192      0.108       2.01      0.45       2.86       0.17        3240
                  JHJH     K7023           9.21       4.31       0.32       157        258      0.062       1.49      0.40       3.71       0.00        1753
                  VBSP     K7047           6.36       7.08       0.50       306        298      0.042       2.01      0.48       2.85       0.00        1916
                  ABOB     K7057           6.90       4.40       0.39       184        244      0.047       1.41      0.48       2.37       0.00        2128
                  CLCL     K7059           6.98       4.21       0.83       148        498      0.044       2.26      1.03       2.11       0.00        2242
                  TBLB     K7053           5.76       2.55       0.50       120        353      0.076       1.73      0.56       2.18       0.00        1843
                  TBLF     K7055           6.95       1.99       0.43       118        171      0.042       1.62      0.42       1.78       0.00        1764
                  BBSD     K7049           6.01       3.50       0.56       192        292      0.037       2.44      0.52       1.56       0.01        2202
                  BBMB     K7051           10.40      1.41       0.51       39         336      0.067       1.64      0.48       1.66       0.44        1258
                  MRT?     K7063           4.76       7.93       0.48       271        210      0.076       2.08      0.42       2.31       0.15        2146
                  MRPL     K7061           5.68       13.69      2.59       368        1471     0.091       4.72      1.38       3.22       0.13        2833
                  BSSI     K7073           4.86       12.13      0.46       281        248      0.068       3.59      0.46       2.60       0.13        2785
                  BSBG     K7065           3.88       5.37       0.72       103        577      0.203       2.10      0.68       2.22       0.07        2081
                  LBMP     K7067           4.18       10.85      1.12       343        673      0.269       3.39      0.73       2.36       0.08        5164






                                                           Mussel Watch Project Year 8 - Trace Metal


                 SUE       IABSAMP        As         Cd         Cr         CU         Fe        Hg         Ni         Pb         Se         Sn         Zn


                 MSPC     K7071           5.93       9.35       0.74       172        343      0.092      2.41       0.49       1.97       0.04       3604
                 MSBB     K7069           8.21       7.19       0.68       258        349      0.115      1.45       1.09       2.35       0.15       5620
                 MSPB     K7079           8.90       2.33       0.36       161        197      0.102      1.53       0.34       2.56       0.19       3713
                 MBCP     K7077           4.93       2.93       0.39       97         241      0.138      1.99       0.26       1.97       0.09       1039
                 MBHI     K7075           4.34       8.82       1.19       446        647      0.122      3.24       0.78       2.00       0.17       8879
                 PBPH     K7089           6.82       3.02       0.38       79         258      0.149      1.38       0.47       2.35       0.05       2620
                 PBIB     K7087           6.34       4.22       1.75       97         1248     0.177      2.87       0.89       2.02       0.04       1278
                 PBSP     K7091           11.59      1.99       0.50       70         186      0.150      1.40       0.33       2.44       0.06       1420
                 CBJB     K7083           7.19       2.97       1.00       467        692      0.331      0.82       1.24       2.95       0.43       5631
                 CBSR     K7085           5.97       3.50       0.74       70         480      0.193      1.61       0.39       2.47       0.05       1147
                 CBPP     K7081           5.12       2.42       0.59       93         267      0.334      0.94       11.10      3.12       0.12       3537
                 PCLO     K7093           8.85       1.08       0.27       30         157      0.119      0.52       0.41       2.04       0.07       1789
                 PCMP     K7097           13.53      1.07       0.64       420        181      0.108      0.87       0.68       2.19       0.71       2763
                 SAWB     K7095           11.82      0.71       0.89       385        314      0.082      0.87       1.89       1.91       0.19       6281
                 APDB     K7099           4.30       2.85       1.26       73         846      0.175      1.78       0.62       1.75       0.06       522
                 APCP     K7105           6.03       1.68       1.01       193        620      0.114      1.56       0.62       1.53       0.08       832
                 AESP     K7103           6.58       3.35       0.99       40         261      0.190      1.06       0.50       2.79       0.08       1189
      00.        CKBP     K7101           7.65       1.24       0.67       14         217      0.096      0.99       0.33       1.34       0.02       379
      0)         TBNP     K71 11          44.52      0.94       0.87       115        237      0.153      1.27       1.23       1.27       0.16       2359
                 TBMK     K7107           9.32       1.23       0.56       19         181      0.131      0.81       0.57       1.20       0.01       332
                 TBPB     K7119           4.15       1.37       1.19       62         303      0.266      1.34       1.30       2.13       0.00       2339
                 TBOT     K7113           2.86       2.55       1.91       116        788      0.532      1.89       1.33       1.89       0.02       8023
                 TBKA     K7109           4.05       1.97       0.48       179        149      0.072      1.19       1.93       2.09       0.51       3304
                 TBHB     K7117           4.79       2.73       1.02       82         257      0.127      1.30       0.91       1.81       0.47       2017
                 TBCB     K7115           4.57       3.42       0.99       89         362      0.159      1.31       0.94       1.54       0.28       2092
                 CBBI     K7129           22.96      2.03       2.16       209        427      0.216      1.35       0.72       1.68       0.05       3266
                 CBFM     K7127           5.35       3.73       0.88       203        256      0.125      1.16       0.80       2.30       0.17       3055
                 NBNB     K7121           12.93      0.96       0.92       556        194      0.096      0.80       0.37       1.27       0.13       3705
                 RBHC     K7123           10.75      1.76       1.23       67         247      0.140      0.87       0.33       1.06       0.00       743
                 GBCR     K7007           5.17       3.01       0.69       141        351      0.111      1.51       0.72       2.68       0.21       1970
                 RIRBB    K7131           11.87      0.37       2.07       38         428      0.097      1.82       0.17       2.12       0.07       A17
                 PRBM     K7133           14.23      0.60       0.93       321        272      0.175      1.17       0.20       3.51       0.00       3477
                 PRBJ     K7135           10.01      1.17       0.45       197        320      0.080      1.08       0.17       2.24       0.00       707




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   m m m m m m m m m @ m m m m m m m m M

                                                        Mussel Watch Project Year 8 - Trace Metal QC Data


             SITE        LABSAMP          SIRMID      ADGDAT     SAMFIYPE          PON       WETWTR      ADWT     % MOIST    MATXCOD UNrITM UNITQUAL Ag


             MBTP      K7027                          6/15/93       SAMP       S&T Oysters     25.15     0.192      83.90      TISSUE        PPM         DRY       1.67
             MBTP      K7027-DUP                      6/15/93       LDUP       S&T Oysters               0.199      83.90      TISSUE        PPM         DRY       1.63
             MBEM      K7029                          6/15/93       SAMP       S&T Oysters     33.72     0.1971     84.37      TISSUE        PPM         DRY       1.82
             MBEM      SPIKE                          6/15/93       SPIKE      S&T Oysters                                     TISSUE        PPM         DRY       1.02
             MBEM      K7029-SPK                      6/15/93        MS        S&T Oysters               0.1962     84.37      TISSUE        PPM         DRY       2.60
             GBSC      K7009                          6/15/93       SAMP       S&T Oysters     26.28     0.1984     83.98      TISSUE        PPM         DRY       1.50
             GBSC      SPIKE                          6/15/93       SPIKE      S&T Oysters                                     TISSUE        PPM         DRY       1.01
             GBSC      K7009-SPK                      6/15/93        MS        S&T Oysters               0.1975     83.98      TISSUE        PPM         DRY'      2.23
             VBSP      K7047                          6/15/93       SAMP       S&T Oysters     34.77     0.1952     83.38      TISSUE        PPM         DRY       3.76
             VBSP      K7047-DUP                      6/15/93       LDUP       S&T Oysters                          83.38      TISSUE        Ppm         DRY       3.81
             CLCL      K7059                          6/15/93       SAMP       S&T Oysters       34.5    0.1929     82.72      TISSUE        PPM         DRY       1.14
             CLCL      K7059-DUP                      6/15/93       LDUP       S&T Oysters               0.2004     82.72      TISSUE        PPM         DRY       1.05
             TBLF      K7055                          6/15/93       SAMP       S8(r Oysters    30.51     0.1973     80.73      TISSUE        PPM         DRY       0.44
             TBLF      SPIKE                          6/15/93       SPIKE      S&T Oysters                                     TISSUE        PPM         DRY       1.01
             T13LF     K7055-SPK                      6/15/93        MS        S&T Oysters               0.1989     80.73      TISSUE        PPM         DRY       1.35
             BSBG      K7065                          6/16/93       SAMP       S&T Oysters     26.28     0.1955     85.96      TISSUE        PPM         DRY       0.81
             BSBG      K7065-DUP                      6/16/93       LDUP       S&T Oysters               0.1985     85.96      TISSUE        PPM         DRY       0.82
             MSPB      K7079                          6/16/93       SAMP       S&T Oysters     35.49     0.1965     90.19      TISSUE        Ppm         DRY       2.30
        00
             MSPB      SPIKE                          6/16/93       SPIKE      S&T Oysters                                     TISSUE        PPM         DRY       1.01
             MSPB      K7079-SPK                      6/16/93        MS        S8(r Oysters              0.1979     90.19      TISSUE        PPM         DRY       3.33
             APDB      K7099                          6/16/93       SAMP       S&T Oysters     25.83     0.1975     85.25      TISSUE        PPM         DRY       1.77
             APDB      K7099-DUP                      6/16/93       LDUP       S&T Oysters               0.1982     85.25      TISSUE        PPM         DRY       1.83
             AESP      K7103                          6/16/93       SAMP       S&T Oysters     24.43     0.1964     92.43      TISSUE        Ppm         DRY       1.05
             AESP      K7103-DUP                      6/16/93       LDUP       S8(r Oysters              0.196      92.43      TISSUE        Ppm         DRY       1.00
             TBNP      K7111                          6/16/93       SAMP       S&T Oysters     28.95     0.1966     88.26      TISSUE        PPM         DRY       2.07
             TBNP      SPIKE                          6/16/93       SPIKE      S&T Oysters                                     TISSUE        PPM         DRY       1.03
             TBNP      K711 I-SPK                     6/16/93        MS        S&T Oysters               0.1942     88.26      TISSUE        PPM         DRY       2.98
             TBPB      K7119                          6/16/93       SAMP       S&T Oysters     34.02     0.1976     84.69      TISSUE        PPM         DRY       1.33
             TBPB      SPIKE                          6/16/93       SPIKE      S8(r Oysters                                    TISSUE        PPM         DRY       1.01
             TBPB      K7119-SPK                      6/16/93        MS        S&-T Oysters              0.1989     84.69      TISSUE        Ppm         DRY       2.27






                                                       Mussel Watch Project Year 8 - Trace Metal QC Data


            SrrE        LABSAMP          SRMID ADGDAT SAMPTYPE                    PON       WETWIR ADWr %MOISr MATXCOD UNMM UNrrQUAL Ag


                      SRMLEV           NIST 1566a                 SRMLEV      S&r Oysters                                     TISSUE        PPM         DRY       1.68
                      NBS-OYS-C        NIST 1566a    6/15/93        SRM       S&-T Oysters              0.1968                TISSUE        PPM         DRY       1.63
                      NBS-OYS-D        NIST 1566a    6/15/93        SRM       S&r Oysters               0.192                 TISSUE        PPM         DRY       1.67
                      NBS-OYS-J        NIST 1566a    6/15/93        SRM       S&-T Oysters              0.1966                TISSUE        PPM         DRY       1.61
                      NBS-OYS-P        NIST 1566a    6/16/93        SRM       S&T Oysters               0.1998                TISSUE        PPM         DRY       1.50
                      NBS-OYS-R        NIST 1566a    6/16/93        SRM       S&-T Oysters              0.1977                TISSUE        PPM         DRY       1.66
                      NBS-OYS-W        NIST 1566a    6/16/93        SRM       S&-T Oysters              0.1955                TISSUE        PPM         DRY       1.73
                      BLANK-A                        6/15/93       BLANK      S&T Oysters                                     TISSUE     TOTMCG                   0.00
                      BLANK-B                        6/15/93       BLANK      S&T Oysters                                     TISSUE     TOTMCG                   0.00
                      BLANK-H                        6/15/93       BLANK      S&T Oysters                                     TISSUE     TOTMCG                   0.00
                      BLANK-M                        6/16/93       BLANK      S&-T Oysters                                    TISSUE     TOTMCG                   0.00
                      BLANK-N                        6/16/93       BLANK      S&T Oysters                                     TISSUE     TOTMCG                   0.00
                      BLANK-U                        6/16/93       BLANK      S&T Oysters                                     TISSUE     TOTMCG                   0.00





                                                     Mussel Watch Project Year 8 - Tmce Metal QC Data


                                        SITE       LABSAMP        As Cd Cr           Cu Fe Hg          Ni    Pb    Se     Sn Zn



                                        MBTP     K7027            5.37  2.91 0.86    116  492 0.077 1.91    0.83 3.06    0.00 896
                                        MBTP     K7027-DUP        5.23  3.36 0.84    115  485 0.081   2.13  0.79 2.93    0.09  939
                                        MBEM     K7029            5.55  6.39 0.51    134  324 0.062   1.52  0.49 3.22    0.05  758
                                        MBEM     SPIKE            8.90  2.16  20.39  224  510 0.101   20.39 5.10  20.39  5.10  2141
                                        MBEM     K7029-SPK        14.22 8.44  19.65  364  861 0.143   19.81 5.32  25.51  5.08  2744
                                        GBSC     K7009            3.68  3.59 0.89    148  222 0.043 2.15    0.75 3.60    0.65  4630
                                        GBSC     SPIKE            8.84  2.14  20.25  223  506 0.101   20.25 5.06  20.25  5.06  2127
                                        GBSC     K7009-SPK        12.45 5.52  20.32  354  693 0.154   20.91 5.51  26.55  5.49  6598
                                        VBSP     K7047            6.36  7.08 0.50    306  298 0.042 2.01    0.48 2.85    0.00  1916
                                        VBSP     K7047-DUP        6.34  7.41 0.47    329  284 0.041 2.03    0.48 3.00    0.00  1981
                                        CLCL     K7059            6.98  4.21  0.83   148  498 0.044   2.26  1.03   2.11  0.00  2242
                                        CLCL     K7059-DUP        6.87  4.05  0.89   144  472 0.044   2.28  0.97   2.13  0.00  2192
                                        TBLF     K7055            6.95  1.99  0.43   118  171 0.042   1.62  0.42   1.78  0.00  1764
                                        TBLF     SPIKE            8.78  2.13  20.11  221  503 0.100   20.11 5.03  20.11  5.03  2112
                                        TBLF     K7055-SPK        14.06 3.88  18.13  342  681 0.134   19.01 5.04  21.29  5.02  3741
                                        BSBG     K7065            3.88  5.37 0.72    103  577 0.203 2.10    0.68 2.22    0.07  2081
                                        BSBG     K7065-DUP        4.10  5.11  0.69   102  580 0.209   1.88  0.66 1.97    0.06  1924
                                        MSPB     K7079            8.90  2.33  0.36   161  197 0.102   1.53  0.34   2.56  0.19  3713
                                        MSPB     SPIKE            8.83  2.14  20.21  222  505 0.101   20.21 5.05  20.21  5.05  2122
                                        MSPB     K7079-SPK        17.14 4.48  18.47  397  729 0.193   22.37 5.24  25.33  5.56  5944
                                        APDB     K7099            4.30  2.85  1.26   73   846 0.175 1.78    0.62 1.75    0.06 522
                                        APDB     K7099-DUP        4.31  2.67 1.36    70   825 0.178 1.90    0.57 1.75    0.09 548
                                        AESP     K7103            6.58  3.35  0.99   40   261 0.190   1.06  0.50   2.79  0.08  1189
                                        AESP     K7103-DUP        6.66  3.30  0.88   39   260 0.202   1.12  0.50   2.71  0.09  1199
                                        TBNP     K7111            44.52 0.94  0.87   115  237 0.153   1.27  1.23   1.27  0.16  2359
                                        TBNP     SPIKE            8.99  2.18  20.60  227  515 0.102   20.60 5.15  20.60  5.15  2163
                                        TBNP     K7111-SPK        53.05 3.17  18.46  341  740 0.231   20.87 6.66  22.45  5.79  4305
                                        TBPB     K7119            4.15  1.37 1.19 62      303 0.266 1.34    1.30 2.13    0.00  2339
                                        TBPB     SPIKE            8.78  2.13  20.11  221  503 0.100   20.11 5.03  20.11  5.03  2112
                                        TBPB     K71 19-SPK       12.86 3.51  21.70  293  851 0.342   21.47 6.64  23.16  5.13  4430






                                                     Mussel Watch Project Year 8 - Trace Metal QC Data


                                        SNE          LABSAMP       As Cd Cr          Cu Fe Hg          Ni    Pb     Se    Sn    Zn



                                                  SRMLEV          14.00 4.15   1.43  66   539  0.064  2.25  0.37   2.21         830
                                                  NBS-OYS-C       13.69 4.10   1.45  65   514  0.056  2.30  0.39   2.17  1.90   829
                                                  NBS-OYS-D       13.53 4.02   1.46  64   521  0.063  2.40  0.36   2.19  1.62   854
                                                  NBS-OYS-,J      12.94 3.68   1.26  66   499  0.064  1.93  0.36   2.03  1.88   838
                                                  NBS-OYS-P       12.76 3.70   1.29  65   507  0.060  2.53  0.36   1.90  1.75   836
                                                  NBS-OYS-R       12.14 4.28   1.37  65   515  0.063  2.11  0.35   1.94  1.30   828
                                                  NBS-OYS-W       13.35 3.65   1.28  65   528  0.065  2.05  0.33   1.96  1.21   851
                                                  BLANK-A         0.00  0.01   0.01   0    0   0.001  0.01  0.01   0.00  0.00    0
                                                  BLANK-B         0.00  0.01   0.01   0    0   0.001  0.00  0.01   0.01  0.00    0
                                                  BIANK-H         0.01  0.01   0.01   0    0   0.001  0.00  0.00   0.00  0.00    0
                                                  BLANK-M         0.00  0.01   0.01   0    0   0.001  0.00  0.01   0.01  0.00    0
                                                  BLANK-N         0.01  0.01   0.01   0    0   0.001  0.00  0.00   0.00  0.00    0
                                                  BLANK-U         0.01  0.00   0.01   0    0   0.001  0.00  0.01   0.00  0.00    0




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                                                               St. Johns Core Data - Hydrocarbon Results - Sediment - 1992


                                       INVEST#:               DUPLICATE PROC BLANK SPIKED MATRIX CONTROL                                            CONTROL             CONTROL
                                           ID:                  X-3 4243                 -900              X-3 42-43                 -700                -700                -700
                                       LABSAMNO:                    Q3365                Q3366                Q3367                  W26690              W26691              W26699
                                       METHOD:               GCFIDtCvCMS GCF1D/GCMS GCFID/GCMS GCFID/GCMS GCFID/GCMS GCFID/GCMS
                                       QCBATCH:                     M495                 M495                 M495                   M492                M494                M495
                                       V&-IWT:                      16.66                10.00                16.99                  1.00                1.00                1.00
                                       DRYWT:                       6.03                 10.00                6.15                   1.00                1.00                1.00
                                         LAB:                       GERG                 GERG                 GERG                   GERG                GERG                GERG
                                       MATRIX:               QCSEDIMENT QCBLANK                          SEDIMENT              QCSBLANK QCSBLANK QCSBLANK
                                       SUBMAT:                                                                                       EV OIL              EV OIL              EV OIL


                                         UNIT:                      nglg                 ngfg                    %                   n919                ng/g                ng/g
                                       PNA Analyte                  Conc                 Conc              % Recov                   Conc                Conc                Conc


                                       NAPHTHALENE                  33.6                 0.5                  127.4                  612.0               654.7               633.0
                                CI-NAPHTHALENES                     25.3                 0.7                                         1968.5              1968.3              1962.6
                                C2-NAPHTHALENES                     30.3                 0.0                                         2012.6              2064.1              1863.9
                                C3-NAPHTHALENES                     33.1                 0.0                                         1426.3              1550.4              1100.9
                                C4-NAPHTHALENES                     49.6                 0.0                                         817.4               897.2               587.6
                                       BIPHENYL                     9.7                  0.2                  128.0                  167.0               150.7               216.5
                                ACENAPHTHYLENE                      42.7                 0.1                  117.9                  1.0                 0.9                 0.8
                                       ACENAPHTHENE                 5.5                  0.1                  125.6                  14.7                11.7                16.0
                                       FLUORENE                     15.3                 0.2                  93.5                   77.7                78.7                84.5
                                       CI-FLUORENES                 18.2                 0.0                                         182.8               164.5               195.0
                                       C2-FLUORENES                 29.8                 0.0                                         218.1               218.0               221.0
                                       C3-FLUORENES                 39.0                 0.0                                         218.3               198.8               188.7
                                       PHENANTHRENE                 61.2                 0.3                  98.6                   217.7               198.7               237.6
                                       ANTHRACENE                   53.0                 0.1                  104.9                  2.5                 3.6                 3.9
                                       CJ-PHEN-ANTHR                74.2                 0.0                                         Q2.1                375.1               374.1
                                       C2-PHEN-ANTHR                90.7                 0.0                                         421.0               385.4               389.0
                                       C3-PHEN-ANTHR                65.1                 0.0                                         233.5               213.3               209.4
                                       C4-PHEN.AMI R                45.1                 0.0                                         145.3               118.6               130.8
                                       DIBENZOTH10                  4.6                  0.1                  73.9                   136.8               114.2               163.6
                                       CI-DIBEN                     11.1                 0.0                                         245.3               213.2               241.1
                                       C2-DIBEN                     23.6                 0.0                                         326.1               277.9               304.2
                                       C3-DIBEN                     21.3                 0.0                                         203.8               175.4               191.1
                                       FLUORANTHENE                 186.0                0.1                  109.1                  10.2                8.6                 11.0
                                       PYRENE                       200.6                0.1                  102.9                  13.5                13.7                13.1
                                CI-FLUORAN-PYR                      165.9                0.0                                         56.9                .54.2               56.4
                                BENaANTHRACENE                      145.5                0.1                  86.1                   5.6                 3.3                 4.6
                                       CHRYSENE                     117.3                0.2                  80.7                   55.4                46.5                55.9
                                       CI-CHRYSENES                 137.7                0.0                                         74.9                58.5                59.7
                                       C2-CHRYSENES                 86.2                 0.0                                         96.6                83.2                92.9
                                       C3-CHRYSENES                 16.4                 0.0                                         41.4                45.3                33.6
                                       C4-CHRYSENES                 17.1                 0.0                                         41.8                38.5                41.9
                                       BENbFLUORAN                  119.8                0.0                  109.6                  5.2                 3.7                 3.8
                                       BENkFLUORAN                  35.5                 0.1                  106.1                  4.7                 4.2                 3.7
                                       BENePYRENE                   59.3                 0.1                  83.1                   10.9                8.9                 9.0
                                       BENaPYRENE                   86.1                 0.1                  101.3                  2.4                 2.3                 2.3
                                       PERYLENE                     358.9                0.3                  111.3                  2.0                 2.3                 3.1
                                       I123cdPYRENE                 49.4                 0.1                  113.7                  1.3                 1.0                 1.5
                                       DBahANTHRA                   13.5                 0.0                  72.5                   1.7                 2.0                 2.6
                                       BghiPERYLENE                 46.8                 0.1                  126.6                  4.3                 3.9                 4.1


                                       Totad PAHs                   2264.8               2.9                  NA                     10477.0             10400.8             9711.2









                                                                                                        154







                                                         St. Johns Core Data - Hydrocarbon Results - Sediment - 1992

                                    INVEST#-.           DUPLICATE PROC BLANK SPIKED MATRIX CONTROL                               CONTROL -76NTROL
                                       ID:               X-3 42-43             -900           X-3 42-43             -700             -700             -700
                                 LABSAMNO:                   Q3365             Q3366             Q3367              W26690           W26691           W26699
                                    METHOD:            GCF]DIGCMS GCFID/GCMS GCF1D/GCMS GCFID/GCMS GCFID/GCMS GCFID/G(-MS
                                    QCBATCH:                 M495              M495              M495               M492             M494             M495
                                    WETWT:                   16.66             10.00             16.99              1.00             1.00             1.00
                                    DRYWr:                   6.03              10.00             6.15               1.00             1.00             1.00
                                      LAB:                   GERG              GERG              GERG               GERG             GERG             GERG
                                    MATRIX:            QCSEDIMENT QCBLANK                    SEDIMENT          QCSBLANK QCSBL.ANK QCSBLANK
                                    SUBMAT:                                                                         EV OIL.          EV OEL           EV OIL_j

                                     UNrr:                   ngtg              ng/9                %                ng/g             ng/g             ng/g
                                 Analyte (Cont)              Conc              Conc            % Recov              Conc             Conc             Conc


                               2-U=YLNAPH                    17.5              0.4               90.3               1075.7           1080.4           1080.3
                               1-ME-rHYLNAPH                 7.8               0.3               81.6               892.8            887.9            881.9


                              2,6-DIMETHNAPH                 11.2              0.2               107.0              650.4            612.0            824.4


                             2,3,5-TRDAETHNAPH               9.5               0.3               78.4               349.0            336.1            353.S


                               I-METHYLPHEN                  19.2              0.1               74.4               165.8            153.4            168.2



                             Surrogate Recoveries


                                    NAPHD8:                  99.04             109.15            106.69             91.60            240.96           130.18
                                    ACENDIO:                 92.72             96.98             80.85              90.70            264.87           94.42
                                    PHEND10:                 84.13             80.61             84.44              78.62            236.56           85.07
                                    CHRYD12:                 41.71             62.84             36.00              58.80            158.34           62.14
                                    PERYD12:                 57.98             20.75             59.78              76.28            104.18           65.03


                                                                                   BOLD SURROGATE RECOVERIES               MATRIX INTERFERENCE









































                                                                                             155






                                                          St. Johns Core Data - Hydrocarbon Results - Sediment - 1992



                              M:                     X-3 0-1           X-3 1-2          X-3 3-4          X-3 4-5           X-3 5-6          X-3 6-7          X-3 7-8
                        LABSAMNO:                    C3890             C3891            C3892            C3893             C3894            C3895            C3896
                           MFITIOD:           GCFM/GCMS GCFM/GCMS GCFID/GCMS GCFM/GCMS GCFID/CvCMS GCFM/GCMS GCFID/GCMS
                           QCBATCH:                  M492              M492             M492             M492              M492             M492             M492
                           WETVT:                    6.18              17.79            36.64            22.54             13.95            32.49            27.29
                           DRYWT:                    2.01              6.03             10.04            7.19              3.92             10.04            7.97
                              LAB:                   GERG              GERG             GERG             GERG              GERG             GERG             GERG
                           MATRIX:              SEDIM]ENT SEDWENT SEDWENT SEDPVMNT SEDIMENT SEDWEENT SEDMMNT
                           SUBMAT:


                           Alkanes and
                           Isoprenoids               Conc              Conc             CDnc             Conc              Conc             Conc             Conc
                              UNIT:                  ng/9              ngfg             ng/g             nglg              ng/g             ng/g             ng1g


                              CIO                    275               32               59               21                95               30               55
                              CII                    50                11               21               18                16               19               23
                              C12                    92                16               23               14                33               16               24
                              C13                    48                15               24               12                38               12               18
                              C14                    146               45               41               22                125              23               43
                              C15                    143               66               62               42                129              43               58
                              C16                    73                23               23               13                55               11               27
                              C17                    285               235              245              211               302              318              279
                           PRISTANE                  200               154              149              171               218              313              246
                              cis                    102               64               69               74                116              77               70
                           PHYTANE                   298               214              232              266               400              362              282
                              C19                    501               486              503              445               504              624              426
                              C20                    316               279              290              226               266              315              236
                              C21                    324               324              323              268               332              384              317
                              C22                    328               325              313              292               363              371              347
                              C23                    1071              915              778              802               1102             866              946
                              C24                    773               589              523              560               762              593              612
                              C25                    2014              1707             1490             1301              1985             1671             1742
                              C26                    954               840              729              725               999              811              853
                              C27                    3436              3014             2745             3161              3569             2905             3259
                              C28                    1379              1180             1023             972               1349             1106             1150
                              C29                    4860              4467             4045             4038              5118             4348             4524
                              C30                    1296              1176             1108             1094              1296             1229             1274
                              C31                    4904              5220             4900             4755              5523             5183             5483
                              C32                    572               688              686              683               648              765              714
                              C33                    767               2083             1971             1892              1401             2236             2259
                              C34                    20                173              180              202               105              225              186
                        T0T ALKANES                  25218             24340            22546            22480             26846            24854            25454


                              UNIT:                  Ug/9              Ug/9             Ug/g             U919              ug/9             Ugtg             Ug1g
                              UCNI                   624               W                519              42                631              677              514


                     &wrWu Reooverks                 %                 %                %                %                 %                %                %
                           C12ALKD:                  42.9              78.6             67.0             76.4              81.8             70.7             73.6
                           C20ALKD:                  43.0              65.9             50.3             73.9              84.8             51.4             75.4
                           C24ALKD:                  46.7              92.0             86.4             101.2             96.9             94.9             103.1
                           C30ALKD:                  43.2              91.0             81.8             97.5              96.4             91.4             95.8














                                                                                             156






                                                                St. Johns Core Data - Hydrocarbon Results - Sediment - 1992


                                INVEST#:
                                   ID:                    X-3 0-1            X-3 1-2           X-3 3-4           X-3 4-5            X-3 5-6           X-3 6-7           Y-3 7-8
                                LABSAMNO:                 C3890              C3891             C3892             C3893              C3894             C3895             C3896
                                MMOD:               GCFlI)1GCMS GCFID/GCMS GCF1D/GCMS GCFID/GCMS GCFM/GCMS GCFID/OCMS GCFU)/GCMS
                                QCBATCH:                  M492               M492              M492              M492               M492              M492              14492
                                WETWT:                    6.18               17.79             36.64             22.54              13.95             32.49             27.29
                                DRYWT:                    2.01               6.03              10.04             7.19               3.92              10.01             7.97
                                  LAB:                    GERG               GERG              GERG              GERG               GERG              GERG              GERG
                                MATRIX:              SEDBfENT SEDIMENT SEDIMENT SEDIMENT SEDIMENT SEDIMENT SEDIMENT
                                SUBMAT:


                                 UNIT:                    ng/g               ng/g              ng/g              ft919              ngtg              ngtg              ng/g
                                PNA Analyte               Conc               Conc              Conc              Conc               Conc              Conc              Conc


                                NAPHTHALENE               96.2               80.5              84.8              92.7               104.1             108.0             108.9
                                Cl-NAPHTHALENES           74.6               50.7              54.6              57.7               73.1              64.7              80.3
                                C2-NAPHTHALENES           89.7               50.1              55.6              54.7               74.4              67.0              79.0
                                C3-NAPHTHALENES           113.8              42.9              50.9              52.9               73.5              57.1              72.9
                                C4-NAPHTHALENES           118.7              39.4              45.9              46.2               74.0              47.6              49.1
                                BIPHF24YL                 25.3               17.2              15.3              15.4               26.0              18.2              21.1
                                ACENAPHTHYLENE            35.8               34.3              42.1              46.6               46.1              52.1              47.5
                                ACENAPHTHENE              25.9               23.8              27.6              29.9               29.6              39.0              66.8
                                FLUORENE                  41.8               37.8              42.0              46.9               48.7              58.7              79.5
                                Cl-FLUORENES              33.0               20.2              21.4              25.1               30.7              26.7              30.2
                                C2-FLUORENES              64.2               28.1              28.0              31.0               42.0              30.3              40.9
                                C3-FLUORENES              94.0               39.8              29.5              35.0               63.6              32.5              55.5
                                PHENANTHRENE,             175.9              125.6             129.6             147.7              187.2             137.6             237.2
                                ANTHRACENE                94.8               76.0              88.7              100.3              115.0             110.3             96.6
                                Cl-PHEN-ANTHR             109.6              65.5              65.2              74.5               101.8             71.0              83.8
                                C2-PHEN-ANTHR             109.3              60.3              43.5              58.5               95.3              50.5              75.1
                                C3-PHEN-ANTHR             101.1              44.2              29.2              37.1               69.2              33.4              68.1
                                C4-PHEN-ANTHR             98.9               40.0              25.7              29.2               52.5              27.3              69.0
                                DIBENZOTE90               16.3               10.5              11.1              12.2               15.3              13.6              16.2
                                Cl-DEBEN                  40.3               14.7              13.9              13.2               25.8              13.7              18.5
                                C2-DEBEN                  89.1               28.7              23.4              26.4               59.0              20.0              38.7
                                O-DEBEN                   57.9               23.0              15.4              18.6               43.4              16.2              35.5
                                FLUORANTHENE              326.1              210.8             152.7             167.7              291.9             164.5             329.7
                                PYRENE                    405.7              227.9             155.9             175.3              316.9             152.0             371.6
                                CI-FLUORAN-PYR            202.7              98.0              72.4              92.5               147.6             80.3              168.2
                                BENaANTHRACENE            202.0              170.8             189.4             272.2              269.2             279.4             261.5
                                CHRYSENE                  184.5              166.9             153.2             269.2              289.2             222.2             248.3
                                Cl-CHRYSENES              139.2              110.7             110.9             183.6              181.3             157.3             161.1
                                C2-CHRYSENES              11.7               72-3              73.0              107.3              113.7             99.6              91.4
                                C3-CHRYSENES              35.4               24.9              17.3              36.3               43.6              30.5              33.5
                                C4-CHRYSENES              58.2               18.8              28.2              31.9               30.5              23.8              36.1
                                BENbFLUORAN               269.3              156.0             168.0             241.3              233.3             233.4             228.7
                                BENOLUORAN                87.7               68.5              54.9              113.7              115.8             87.6              86.8
                                BENePYRENE                127.8              81.6              81.6              131.7              126.0             119.3             120.0
                                BENaPYRENE                176.7              108.3             107.8             169.6              163.8             152.6             152.5
                                PERYLENE                  379.6              256.4             194.5             165.6              348.0             150.0             133.0
                                I123cdPYRENE              130.4              78.5              62.1              98.5               124.3             78.4              101.8
                                DBahANTHRA                30.4               17.8              15.7              24.5               30.3              19.5              25.5
                                BghiPERYLENE              121.8              72.8              57.6              96.9               116.2             74.1              100.8

                                Total PAHs                4215.7             2637.8            2443.8            3263.9             4043.6            3069.8            3987.7








                                                                                                     157







                                                           St. Johns Core Data - Hydrocarbon Results - Sediment - 1992



                                 ID:                     X-3 0-1            X-3 1-2           X-3 3-4            X-3 4-5            X-3 5-6           X-3 6-7            X-3 7-8
                           LABSAMNO:                     C3890              C3891             C3892              C3893              C3894             C3895              C3896
                              METHOD:             GCFED/GCMS GCF11D/GCMS GCFH)/GCMS GCFID/GCMS GCFID/GCMS GCFII)/GCMS GCFID/GCMS
                              QCBATCH:                   M492               M492              M492               M492               M492              M492               M492
                              V&-r*N,r:                  6.18               17.79             36.64              22.54              13.95             32.49              27.29
                              DRYWT:                     2.01               6.03              10.04              7.19               3.92              10.04              7.97
                                LAB:                     GERG               GERG              GERG               GERG               GERG              GERG               GERG
                              MATRIX:               SEDIMENT SED54ENT SEDIMENT SEDIMENT SEDIMENT SEDPAENT SEDIMENT
                              SUBMAT:


                                UNIT:                    ng1g               nglg              ngfg               ngtg               0919              ng/g               ng/g
                           Analyte (Cont)                Conc               Conc              Conc               Conc               Conc              Conc               Conc


                          2-NIETHYLNAPH                  50.0               36.4              38.7               41.3               51.1              46.1               56.0
                         1 -METHYLNAPH                   24.6               14.3              15.9               16.4               22.0              18.7               24.3


                         2,6,DIMETHNAPH                  30*0               23*6              24*1               23,8               19,2              30,9               30* 1


                      2,3,5-TRIMETHNAPH                  19.3               10.6              11A                11.7               14.7              13.1               14.6


                          I-METHYIYHEN                   25.5               22.8              15.9               24.2               42.0              17.1               28.7



                       Surropte Recoveries


                              NAPHD8:                    50.80              91.17             84.98              75.59              83.53             77.00              76.69
                              ACEND10:                   55.80              90.32             92.47              82.83              94.40             79.78              80.60
                              PHEND10:                   49.25              90.10             87.68              77.14              85.93             77.03              92.95
                              CHRYD12:                   44.73              29.93             24.42              16.06              26.05             15.86              45.99
                              PERYD12:                   36.79              65.58             92.64              82.65              54.31             92.56              99.71


                                                                                  BOLD SURROGATE RECOVERIES                 MATRIX DITERFERENCE











































                                                                                                    158







                                                            St. Johns Core Data - Hydrocarbon Results - Sediment - 1992


                              U4VEST#-.
                                 M:                    X-3 8-9      X-3 10-11        X-3 13-14        X-3 14-15        X-3 15-16        X-3 16-17        ).*.-3 22-23
                           LABSAMNO:                   C3897            C3898             C3900            C3901           C3902             C3903            C3904
                              ME11101):          GCFIDIGCMS GCFID/GCMS GCFID/GCNIS GCFID/GCMS GCFID/GCMS GCFID/GCMS GC:.M/GCMS
                              QCBATCH:                 M492             M492              M492             M494            M494              M494             M494
                              VAETVT:                  37.14            24.37             28.57            36.21           16.08             45.16            35.14
                              DRYWT:                   9.99             7.31              10.00            10.03           4.60              9.9,8            10.05
                                 LAB:                  GERG             GERG              GERG             GERG            GERG              GERG             GERG
                              MATRIX:             SEDIMENT         SEDNEENT SEDIMENT SEDIMENT                         SEDBMfr          SEDD4ENT         SEDPVIENT
                              SUBMAT:


                              Alkanes and
                              Isoprenoids              Conc             Conc              Conc             Conc            Conc              Conc             Conc
                                 UNIT:                 ngtg             ngtg              ngtg             ng/9            ng/g              ng/g             ng/g


                                 CIO                   33               61                32               35              133               so               26
                                 CII                   17               20                9                9               18                12               17
                                 C12                   16               25                13               17              67                32               66
                                 C13                   12               20                13               12              21                13               2
                                 C14                   30               62                34               25              61                23               34
                                 C15                   43               72                43               39              75                45               37
                                 C16                   17               36                20               16              42                12               4
                                 C17                   448              369               173              253             354               359              255
                              PRISTANE                 243              332               85               162             261               206              79
                                 C18                   79               101               54               95              106               95               18
                              PHYTANE                  386              445               138              253             296               255              74
                                 C19                   514              509               221              311             362               316              266
                                 C20                   304              290               199              281             211               168              120
                                 C21                   430              383               263              423             411               360              382
                                 C22                   415              374               221              337             259               234              222
                                 C23                   989              991               923              1129            1110              1109             1017
                                 C24                   712              656               551              639             712               692              573
                                 C25                   1892             1797              1814             2157            2106              1994             1858
                                 C26                   931              912               819              924             922               849              822
                                 C27                   3291             3327              3237             4554            3176              2835             2591
                                 C28                   1284             1203              1125             1292            834               572              666
                                 C29                   5034             4815              4904             5947            3498              1890             2495
                                 C30                   1023             1029              1050             1073            929               316              412
                                 C31                   4589             4630              5223             5449            2945              1189             1236
                                 C32                   625              603               595              714             284               134              113
                                 C33                   2019             1576              2125             2356            694               289              276
                                 C34                   225              103               176              216             42                16               7
                         TOT ALKANES                   25602            24741             24059            28717           19927             14064            13668


                                 UNIT:                 ug/9             UgIg              Ug/9             Ug/9            Ug1g              ug/g             Ug/g
                                 UcM                   735              720               268              413             246               206              203


                       Surropte Recoveries             %                %                 %                %               %                 %                %
                              C12ALKD:                 67.8             70.7              79.3             79.0            75.2              75.5             114.7
                              C20ALKD:                 49.9             56.0              83.9             74.1            93.3              87.2             81.4
                              C24ALKI):                86.8             89.4              87.2             95.5            88.8              79.2             87.0
                              C30ALKD:                 108.7            102.0             95.0             120.6           72.6              72.1             105.4












                                                                                              159







                                                         St. Johns Core Data - Hydrocarbon Results - Sediment - 1992


                             l[NVEST#'
                                ID:                   X-3 8-9        X-3 10-11         X-3 13-14         X-3 14-15         X-3 15-16         X-3 16-17         X-3 22-23
                             LABSAMNO:                C3897             C3898              C3900             C3901            C3902             C3903              C3904
                             W-MOD:             GCFID/GCMS GCFIID/GCMS GCF]ID/GCMS GCFMVGCMS GCFID/GCMS GCF]DtGCMS GCFID/GCMS
                             QCBAT)CH:                M492              M492               M492              M494             M494              M494               M494
                             WETWT:                   37.14             24.37              28.57             36.21            16.08             45.16              35.14
                             DRYWT:                   9.99              7.31               10.00             10.03            4.60              9.98               10.05
                              LAB:                    GERG              GERG               GERG              GERG             GERG              GERG               GERG
                             A"TRIX:              SEDB4ENT SEDWENT SEDRAENT SEDMENT SEDDIENT SEDVAENT SEDRAENT
                             SUBMAT:                                                                                                                                         f

                              UNIT:                   ng/g              ngtg               ngtg              ng/g             n9t9              ng/g               ng/g
                             PNA Analyte              Conc              Conc               CDnc              Conc             Conc              Conc               Conc


                             NAPHTHALENE              99.6              108.1              51.8              65.4             72A               65.2               106.4
                       CI-NAPHTHALENES                59.1              77.2               31.2              37.1             49.2              42.6               59.1
                       C2-NAPHTHALENES                59.6              73.3               36.6              39.1             53.2              45.7               59.8
                       O-NAPHTHALENES                 55.0              56.6               40.2              35.7             62.1              48.8               63.4
                       C4-NAPHTHALENES                47.1              75.5               40.0              35.1             83.1              54.0               61.2
                             BIPHENYL                 17.4              24.7               9.2               13.7             21.2              15.2               19.4
                       ACENAPHTHYLENE                 46.7              42.2               23.9              41.2             39.5              46.9               40.9
                       ACENAPFITHENE                  30*7              49,8               15*3              23,1             23*7              233                23*7
                             FLUORENE                 49.0              61.8               22.6              30.4             36.6              34.4               37.3
                             CI-FLUORENES             23.1              31.3               15.4              19.2             33.8              26.3               21.5
                             C2-FLUORENES             28.1              37.7               20.5              19.8             53.0              37.7               28.8
                             O-FLUORENES              23,9              63*4               28*8              24*1             72.8              42.7               28.2
                       PHENANTHRENE                   131.4             204.7              86.7              116.8            155.0             131.6              117.0
                             ANTHRACENE               90.3              91.2               48.5              69.5             79.6              79.6               70.8
                       CI-PHEN-ANTHR                  59.0              82.5               50.7              51.9             95.5              70.5               59.1
                       C2-PHEN-ANTHR                  40.4              78.2               46.8              36.4             83.2              56.2               41.6
                       C3-PHEN-ANTHR                  28.4              69.5               30.4              28.8             63.0              40.2               28.3
                       C4-PHEN-ANTHR                  25.2              61.7               28.3              32.5             61.0              35.9               25.2
                             DEBENZOTHIO              11*0              14*6               6,1               9*6              15*1              11,0               10*7
                             CI-DEBEN                 12.0              20.2               10.7              11.4             32.4              13.8               12.8
                             C2-DI]BEN                18.2              48.8               21.6              20.0             61.6              26.4               18.8
                             O-DEBEN                  14.3              41.5               15.3              15.2             41.6              19.5               12.2
                       FLUORANTHENE                   152*4             290*8              111,5             122*1            226*1             187*7              132*6
                             PYRENE                   138.9             334.7              115.5             134.9            265.1             191.1              131.8
                       Cl-FLUORAN-PYR                 68.5              167.6              61.5              56.6             116.2             88.8               59.8
                       BENaANTHRACENE                 235.6             199.8              122.2             122.0            168.8             245.2              85.2
                             CHRYSENE                 180.4             179.8              125.4             120.7            131.9             242.7              90.5
                             CI-CHRYSENES             135.1             127.2              80.3              82.0             95.9              153.7              68.2
                             C2-CHRYSENES             77.9              70.0               47.4              47.7             50.2              86.9               49.6
                             C3-CHRYSENES             34,2              25*2               16*4              15*2             21,1              26*2               20*1
                             C4-CHRYSENES             22.4              29.0               12.5              14.3             26.9              33.4               14.3
                             BENbFLUORAN              198.2             174.7              99.9              111.4            137.5             213.2              90.7
                             BENkFLUORAN              74.6              63.3               42.6              48.8             39.6              79.3               23.6
                             BENePYRENE               100*7             83*9               48*2              57.6             58.4              103.0              45.4
                             BENaPYRENE               124.2             111.5              67.9              76.4             84.3              138.1              56.8
                             PERYLENE                 251.6             344.3              254.7             446.5            417.5             448.7              546.7
                             1123cdPYRENE             63.7              78.7               38.9              34.0             55.2              83.5               30.4
                             DBahANTHRA               16.5              18.5               10.5              8.9              13.9              21.8               7.4
                             BghiPERYLENE             60.6              72.2               35.7              30.0             50.4              77.8               28.5


                             Total PAHs               2653.2            3441.2             1717.4            1859.5           2829.9            2940.0             1881.2








                                                                                                160







                                                             St. Johns Core Data - Hydrocarbon Results - Sediment - 1992


                                WVEST#.
                                    ID:                    X-3 8-9        X-3 10-11         X-3 13-14         X-3 14-15         X-3 15-16          X-3 145-17        X .3 22-23
                              LA,BSAMNO:                   C3897             C3898              C3900             C3901             C3902             C3903              -C3904
                                ME'MOD:             GCFM/GCMS GCFM/GCMS GCFID/GCMS GCMGCMS GCFM/GCMS GCFID/GCMS GCF1D/GCMS
                                QCBATCH:                   M492              M492               M492              M494              M494              M494               M494
                                WETWT:                     37.14             24.37              28.57             36.21             16.08             45.16              35.14
                                DRYWT:                     9.99              7.31               10.00             10.03             4.60              9.98               10.05
                                  LAB:                     GERG              GERG               GERG              GERG              GERG              GERG
                                MATRIX:               SEDIMENT SEDBUNT SEDNENT SEDIMENT SEDIMENT SEDIMENT SEDPAENT
                                SUBMAT:


                                  UNIT:                    n&                ng/g               ng/9              ng/g              ng/g              ng1g               ng/9
                             Analyte (Cont)                Conc              Conc               Conc              Conc              Conc              Conc               Conc


                           2-NEErHYLNAPH                   42.4              54.5               21.7              25.8              33.4              29.6               41.7
                           I-NEETHYINAPH                   16.7              22.7               9.5               11.3              15.9              13.1               17.4


                          2,6-DPAETHNAPH                   26.5              28.8               13.0              19.8              27.3              22.0               25.2


                        2,3,5-TRIMETMNAPH                  12.1              13.8               7.6               9.9               17.3              13.1               15.9


                           I-METHYLPHEN                    14.8              16.8               17.0              15.7              31.2              21.2               14.4



                         Surropte Recoveries


                                NAPHD8:                    76.42             83.75              76.06             113.98            97.90             97.27              94.44
                                ACENDIO:                   82.22             84.68              92.05             98.49             75.99             89.46              96.63
                                PHEND10:                   83.22             94.72              83.00             88.73             69.02             91.30              100.30
                                CHRYD12:                   16.47             58.59              24.22             25A9              31.91             19.34              33.37
                                PERYD12:                   55.44             60.02              59.14             61.42             69.45             41.75              48.40


                                                                                   BOLD SURROGATE RECOVERIES                 MATRIX WIERFERENCE











































                                                                                                  161






                                                         St. Johns Core Data - Hydrocarbon Results - Sediment - 1992


                           ONEST#:
                               ID:               X-3 27-28        X-3 30-31        X-3 32-33        X-3 33-34        X-3 35-36        X-3 36-37        X-3 37-38
                           LABSAMNO:                     C3905        C3906                C3907            C3908            C3909             C3910      C3911
                           METHOD:            GCFIDIGCMS GCFID/GCMS GCFID/GCMS GCMGCMS GCFID/GCMS GCFID/GCMS GCFID/Gcms
                           QCBATCH:                      M494         M494                 M494             M494             M494              M494       M494
                           WETWT:                        26.70        11.16                18.47            22.66            35.59             26.22      4.19
                           DRYWT:                        10.04        4.05                 7.02             10.06            10.00             7.08       0.80
                               LAB:                      GERG         GERG                 GERG             GERG             GERG              GERG       GERG
                           MATRIX:              SEDB4ENT SEDRAENT SEDNENT SEDB4ENT SEDBffNT SEDB4ENT SEDRvMNT
                           SUBMAT:


                           Alkanes and
                           Lsoprenoids                   Conc         Conc                 Conc             Conc             Conc              Conc       Conc
                               UNrr:                     ng/g         ng/g                 ng/g             ng/g             ng/g              ngtg       ngtg

                               CIO                       28           97                   23               19               30                58         232
                               C11                       22           24                   14               10               8                 14         169
                               C12                       63           106                  40               26               45                77         210
                               C13                       6            41                   4                7                2                 1          153
                               C14                       56           140                  40               19               55                58         461
                               C15                       59           127                  64               26               59                98         323
                               C16                       2            19                   23               9                13                10         171
                               C17                       156          247                  151              98               196               198        374
                           PRISTANE                      121          235                  109              57               114               110        304
                               08                        33           62                   4                13               37                29         141
                           PHYTANE                       103          181                  80               43               122               83         212
                               C19                       151          294                  208              90               194               182        311
                               C20                       59           128                  48               47               95                89         118
                               C21                       231          401                  231              155              330               322        426
                               C22                       127          188                  144              91               177               201        290
                               C23                       596          792                  713              394              831               951        1032
                               C24                       373          475                  466              245              488               566        677
                               C25                       1060         1447                 1251             734              1541              1806       1883
                               C26                       475          648                  578              343              697               788        878
                               C27                       1397         2204                 1626             1124             2308              2696       3170
                               C28                       349          668                  382              354              613               712        1091
                               C29                       1262         2813                 1514             1483             2358              2825       5618
                               C30                       222          516                  236              235              418               423        1416
                               C31                       668          2241                 630              963              1186              1632       6995
                               C32                       67           169                  69               93               93                144        853
                               C33                       141          407                  104              220              259               361        2414
                               C34                       5            19                   7                1                6                 8          89
                       TOT ALKANES                       7832         14688                8757             6899             12277             14440      29843
                               UNIT:                     Ugtg         U9/9                 U919             U919             U919              ugtg       ug/g
                               UCNI                      179          293                  270              112              167               192        292

                    Surropte Recoveries                  %            %                    %                %                %                 %          %
                           C12ALKD:                      78.5         78.4                 89.9             79.2             85.0              72.1       78.0
                           C20ALKD:                      94.4         84.4                 82.7             79.5             80.9              86.7       81.8
                           C24ALKD:                      96.4         93.7                 76.6             84.3             94.4              85.2       87.3
                           C30ALKD:                      87.9         86.7                 104.6            89.7             100.7  -93.2                 88.8







                                                                                           162







                                                                St. Johns Core Data - Hydrocarbon Results - Sediment - 1992


                                 INVEST#:
                                     ID:                 X-3 27-28           X-3 30-31          X-3 32-33          X-3 33-34           X-3 35-36          X-3 36-37           X-337-38
                                 LABSAMNO:                  C3905               C3906              C3907               C3908               C3909              C3910              C3911
                                 NWTHOD:              GCFM/GCMS GCFID/GCMS GCFBXGCMS GCFM/GCMS GCFID/GCMS GCFM/GCMS GCFM/GCWIS
                                 QCBATCH:                   M494                M494               M494                M494                M494               M494               M494
                                 WETWT:                     26.70               11.16              18.47               22.66               35.59              26.22              4.19
                                 DRYWT:                     10.04               4.05               7.02                10.06               10.00              7.08               0.80
                                   LAB:                     GERG                GERG               GERG                GERG                GERG               GERG               GERG
                                 MA77JX:                SEMENT SEDMENT SEDRVIENT SED04ENT SEDMENT SEMENT                                                                    SIU)BMW
                                 SUBMAT:


                                  UNIT:                     ng/g                ng/g               ng/g                ng/g                ng1g               ng/g               nglg
                                 PNA Analyte                Cone                Cone               Cone                Cone                Cone               Cone               Cone


                             NAPHTHALENE                    277.5               138.5              144.1               47.3                47.1               58.7               55.1
                         Cl-NAPHTHALENES                    179.3               83.1               83.1                38.7                119.3              44.6               59.3
                         C2-NAPHTHALENES                    109.4               69.9               71.4                33.9                25.7               41.2               94.6
                         C3-NAPHTHALENES                    94.7                80.4               63.7                39.7                35.9               54.1               104.4
                         C4-NAPHTHALENES                    70.4                96.9               56.4                38.8                64.4               60.8               150.0
                                 BIPHENYL                   36.0                22.7               21.8                8.7                 10.1               18.7               22.8
                         ACENAPHTHYLENE                     53.6                40.6               54.5                24.3                31.4               48.7               34.9
                             ACENAPHTHENE                   80.4                30.6               37.0                12.6                6.3                10.7               10.6
                                 FLUORENE                   108.6               49.3               52.6                20.6                13.6               21.6               25.6
                             Cl-FLUORENES                   38.2                30.8               26.3                17.5                19.5               24.4               39.0
                             C2-FLUORENES                   37.2                45.0               29.3                24.3                X 1                35.3               88'2
                             C-3-FLUORENES                  55.1                70.0               35.2                30.2                26.9               54.5               143.4
                             PHENANTHRENE                   464.3               182.6              156.2               87.3                64.6               92.5               104.6
                             ANTHRACENE                     192.7               93.4               97.9                43.3                42.1               65.6               51.8
                             Cl-PHEN-ANTHR                  167.8               100.7              71.5                51.1                62.1               89.7               123.3
                             C2-PHEN@-ANTHR                 134.3               112.2              53.5                45.4                61.4               97.5               157.7
                             C3-PHEN-ANTHR                  94.3                99.8               32.2                27.5                39.2               81.6               142.0
                             C4-PHEN-ANTHR                  75.5                69.0               25.0                20.4                26.4               14.1               106.6
                             DEBENZOTHIO                    34.8                16.2               14.5                6.7                 5.5                7.0                12.9
                                 Cl-DEBEN                   27.0                28.5               15.0                9.6                 13.6               19.3               60.0
                                 C2-DI]BEN                  42.4                70.2               25.4                15.6                24.8               44.2               144.2
                                 O-DEBEN                    35.3                63.7               15.5                11.1                22.6               41.7               101.7
                             FLUORANTHENE                   590.6               282.9              163.5               113.9               104.2              205.9              247.4
                                 PYRENE                     557.6               312.3              170.5               118.9               111.2              257.9              350.0
                         Cl-FLUORAN-PYR                     315.7               155.8              81.6                68.9                90.8               194.5              243.7
                         BENaANTHRACENE                     389.2               200.2              204.6               89.4                228.0              166.8              172.8
                                 CHRYSENE                   292.1               1,50.3             199.2               68.1                193.3              163.0              144.3
                             Cl-CHRYSENES                   252.7               137.0              166.7               72.3                201.6              169.4              185.5
                             C2-CHRYSENES                   160.0               104.1              122.1               48.6                118.8              117.0              147.2
                             O-CHRYSENES                    39.6                36.7               45.8                15.3                44.9               30.3               54.4
                             C4-CHRYSENES                   46.8                31.5               39.5                13.8                27.4               27.1               49.2
                             BENbFLUORAN                    292.7               156.5              186.8               76.7                166.6              130.3              211.2
                             BENkFLUORAN                    74.9                45.0               91.6                23.4                64.8               57.5               68.3
                             BENePYRENE                     144.7               78.3               118.8               41.3                91.5               74.5               121.0
                             BENaPYRENE                     209.2               105.4              145.6               53.6                141.6              111.3              @171.0
                                 PERYLENE                   244.2               456.9              301.3               233.1               361.5              399.9              5 11.7
                             I123odPYRENE                   142.1               74.6               90.2                34.9                533                66.1               :m 18.9
                             DBahANTHRA                     36.2                20.0               22.2                9.2                 14.4               17.7               30.0
                             B&PERYLENE                     137.6               69.7               86.5                35.3                46.4               61.8               112.3

                                 Total PAHs                 6090.3              3544.2             3116.8              1538.0              2497.2             2877.6             4259.6









                                                                                                          163







                                                       St. Johns Core Data - Hydrocarbon Results - Sediment - 1992


                           INVEST#:
                              ID:                X-3 27-28         X-3 30-31         X-3 32-33        X-3 33-34         X-3 35-36         X-3 36-37        X-3 37-38
                         LABSAMNO:                   C3905             C3906            C3907             C3908             C3909            C3910             C3911
                           MET11OD:            GCFID/GCMS GCFID/GCMS GCFID/GCMS GCFID/GCMS GCF1D1GCMS GCF1D/GCMS GCFID/GCMS
                           QCBATCH:                  M494              M494             M494              M494              M494             M494              M494
                                                     26.70             11.16            1 BA7             22.66             35.59            26.22             4.19
                           DRYWT:                    10.04             4.05             7.02              10.06             10.00            7.08              0.80
                             LAB:                    GERG              GERG             GERG              GERG              GERG             GERG              GERG
                           MATRIX:              SEDIMENT SEDIMENT SEDRAENT SEDIMENT SEDWENT SEDIMENT SEDIMENT
                           SUBMAT:


                             UNIT:                   ng/g              nglg             n919              ng/g              ngtg             ng1g              ng/g
                         Analyte (Cont)              Conc              Conc             Conc              Conc              Conc             Conc              Conc


                        2-NfETffYL,NAPH              128.8             59.5             59.1              26.3              21.2             30.3              37.8
                        I-MErHYL.NAPH                50.5              23.6             24.0              12.5              98.1             14.3              21.5


                       2,6-DD*MIINAPH                47*9              11*9             31*7              14*0              9*9              16*1              26*9


                    2,3,5-TRUAETMAPH                 20.3              19.6             15.0              9.2               9.2              11.2              23.4


                        I-]METHYLPHEN                48.0              28.2             21.4              14.2              18.4             30.2              25.9



                     Surropte Recoveries


                           NAPHD8:                   82.78             84.48            91.66             94.06             96.97            73.95             94.21
                           ACENDIO:                  90.62             94.19            95.96             94.19             102.43           73.21             92.82
                           PHEND10:                  73.26             82.73            97.11             85.09             83.06            67.51             88.41
                           CHRYD12:                  41.37             35."             19.01             32.28             14.15            31.17             75.23
                           PERYD12:                  111.49            51.30            73.08             61.43             91.23            70.79             68.89


                                                                            BOLD SURROGATE RECOVERIES                MATRIX INTERFERENCE










































                                                                                              164






                                                             St. Johns Core Data - Hydrocarbon Results - Sediment - 1992


                              INVEST#:
                                   ID:              X-3 38-39        X-3 39-40         X-3 40-41        X-3 42-43        X-3 43-44         X-3 44-45        X-3 45-46
                            LABSAMNO:                    C3912            C3913                C3914        C3915             C3916            C39,17            C3918
                              hIETHOD:           GCFIDtGCMS GCFM1GCMS GCFIDtGCMS GCFID/GCMS GCFID/GCMS GCFID/GCMS GCI1D/GCMS
                              QCBATCH:                   M494             M494                 M495         M495              M495             M495              M495
                              WETWT.                     31.66            30.64                30.06        16.63             30.36            8.08              27.83
                              DRYWT:                     10.13            10.02                10.01        6.02              10.05            2.53              10.02
                                 LAB:                    GERG             GERG                 GERG         GERG              GERG             GERG              GERG
                              MATM:                SEDB4ENT SEDWENT SEDUAENT SEMENT SEDWENT SEDDAENT SEDIMENT
                              SUBMAT:


                              Alkanes and
                              Isoprenoids                Conc             Conc                 Conc         Conc              Conc             Conc              Conc
                                 UNIT:                   ng/g             ng/g                 ngtg         ng/g              ngtg             ngtg              ng/g


                                 CIO                     23               24                   20           37                23               182               23
                                 C11                     9                14                   11           40                12               34                16
                                 C12                     39               46                   37           78                44               119               45
                                 C13                     3                5                    3            39                6                73                6
                                 C14                     32               42                   49           64                23               216               42
                                 C15                     51               39                   55           63                37               252               42
                                 C16                     11               6                    5            24                5                98                14
                                 C17                     169              168                  169          168               133              274               165
                              PRISTANE                   85               151                  259          106               84               281               140
                                 C18                     26               24                   32           38                24               101               57
                              PHYTANE                    62               94                   146          60                51               203               103
                                 C19                     146              145                  133          119               96               254               179
                                 C20                     91               86                   84           89                66               127               92
                                 C21                     281              282                  257          266               214              355               254
                                 C22                     174              164                  154          160               131              231               174
                                 C23                     832              791                  671          686               644              913               744
                                 C24                     496              472                  419          415               417              592               463
                                 C25                     1565             1450                 1240         1306              1235             1662              1388
                                 C26                     728              596                  548          567               547              783               592
                                 C27                     2462             1871                 1604         2134              1795             2526              1857
                                 C28                     568              474                  435          678               524              954               506
                                 C29                     2100             1589                 1567         3282              1992             4649              1896
                                 C30                     397              263                  236          525               293              1139              267
                                 C31                     1066             957                  826          2353              1114             4401              947
                                 C32                     118              68                   85           216               44               498               80
                                 C33                     192              217                  155          564               234              1131              191
                                 C34                     3                18                   1            10                4                20                9
                          TOT ALKANES                    11729            10054                9202         14088             9791             22066             10292


                                 UNTIT:                  u9/9             ug/g                 Ug/9         U919              ug/g             ug1g              Ug/g
                                 UCM                     136              152                  155          126               112              252               163


                       Surrogate Recoveries              %                %                    %            %                 %                %                 %
                              C12ALKD:                   97.9             82.5                 105.3        83.4              101.8            83.2              105.5
                              C20ALKD:                   82.1             94.9                 94.4         79.5              98.3             85.3              83.0
                              C24ALKD:                   80.9             81.9                 95.8         83.5              91.3             87.1              87.6
                              C30ALKD:                   95.2             79.7                 96.1         99.9              109.7            97.8              113.0














                                                                                               165







                                                           St. Johns Core Data - Hydrocarbon Results - Sediment - 1992


                             DqVEST#:
                                 ED:                X-3 38-39          X-3 39-40          X-3 40-41         X-3 42-43          X-3 43-44          X-3 44-45         X-3 45-46
                             LABSAMNO:                  C3912              C3913             C3914              C3915              C3916             C3917              C3918
                             METHOD:              GCFM/GCMS GCFID/GCMS GCFW/GCMS GCFID/GCMS GC7M/GCMS GCFID/GCMS GCFID/GCMS
                             QCBATCH:                   M494               M494              M495               M495               M495              M495               M495
                             WETWT:                     31.66              30.64             30.06              16.63              30.36             9.08               27.83
                             DRYWT:                     10.13              10.02             10.01              6.02               10.05             2-53               10.02
                               LAB:                     GERG               GERG              GERG               GERG               GERG              GERG               GERG
                             MATRIX:               SEMENT SEDUVIENT SEDUVIENT SEDMENT SEDDvWNT SEDDAENT SEDRAENT
                             SUBMAT:


                               UNIT:                    ng/g               ng/g              ng/g               ngIg               ng/g              ngIg               ng/g
                             PNA Analyte                Conc               Conc              Conc               Conc               Conc              Conc               Conc


                             NAPHTHALENE                53.6               94.9              96.0               52.0               50.4              92.0               71.7
                      CI-NAPHTHALENES                   48.3               60.0              69.6               81.0               41.8              70.8               53.9
                      C2-NAPHTHALENES                   43.7               49.6              64.8               198.1              49.4              72.9               53.1
                      C3-NAPHTHALENES                   47.7               52.9              54.0               165.7              54.7              88.8               56.3
                      C4-NAPHTHALENES                   57.7               61.7              72.2               87.3               63.0              124.4              69.0
                             BEPHENYL                   13.3               18.6              21.0               12.8               15.2              24.4               21.3
                      ACENAPHTHYLENE                    35.7               110.4             68.7               46.3               70.7              71.9               95.7
                             ACENAPHTHENE               15*5               17,9              17,9               7*9                10A               13*0               12*1
                             FLUORENE                   22.3               36.7              30.9               40.7               26.4              35.8               36.8
                             CI-FLUORENES               21.7               34.5              30.0               98.0               34.0              38.5               30.9
                             C2-FLUORENES               38.3               52.3              41.5               125.3              50.5              78.6               48.7
                             O-FLUORENES                44.4               52.0              39.1               95.2               66.4              93.9               53.5
                             PHENANTHRENE               76.8               145.1             137.1              132.3              90.0              122.5              114.9
                             ANTHRACENE                 53.5               134.3             95.9               55.5               89.9              116.9              130.6
                             CI-PHEN-ANTHR              78.6               169.3             99.4               220.3              125.1             134.3              94.8
                             C2-PHEN-ANTHR              91.3               170.5             98.3               215.0              145.2             159.6              94.0
                             C3-PHEN-ANTHR              60.7               87.6              60.1               101.1              92.6              123.9              64.7
                             C4-PHEN-ANTHR              43.6               41.8              38.6               550.0              59.3              92A                44.4
                             DIBENZOTFHO                6*0                10*5              13,3               12*9               11*2              13,3               10,1
                             CI-DEBEN                   14.4               28.3              20.5               30.5               16.3              39.0               16.0
                             C2-DEBEN                   28.8               57.9              31.2               39.3               30.4              86.0               27.3
                             O-DEBEN                    23.0               32.8              21.1               26.3               26.7              67.6               21.0
                             FLUORANTHENE               192A               1116*1            171.8              160.7              214.4             294.4              182.1
                             PYRENE                     201.9              207.0             183.5              192.3              241.9             352.8              177.0
                      Cl-FLUORAN-PYR                    167.7              221.2             154.9              198.1              202.6             293.3              157.3
                      BENaANTHRACENE                    97.4               466.2             338.3              132.3              257.7             274.0              185.9
                             CHRYSENE                   96.7               449.8             345.0              172.6              273.2             311.9              196.6
                             CI-CHRYSENES               93.8               482.1             332.8              188.0              289.4             292.4              200.4
                             C2-MYSENES                 59.1               261.3             221.2              147.5              194.1             2D5.4              135.8
                             C3-CHRYSENES               16*7               73*9              42,2               32,2               39,3              62*0               12,2
                             C4-CHRYSENES               11.0               66.7              40.8               26.0               40.3              48.3               28.1
                             BENbFLUORAN                73.9               301.5             291.8              144.8              266.6             333.1              224.9
                             BENkFLUORAN                30.1               137.9             124.3              33.0               107.5             74.4               48.3
                             BENePYRENE                 39.8               185.2             161.9              74.2               148.5             155.5              107.0
                             BENaPYRENE,                56.8               312.5             232.0              99.5               206.3             222.4              146.1
                             PERYLENE                   360.9              349.9             951.5              375.0              355.2             502.7              489.7
                             1123cdPYRENE               35.1               132.0             75.0               49.0               116.1             146.8              62.6
                             DBahANTHRA                 9.5                39.0              19.1               14.1               29.9              37.6               16.1
                             B&PERYLENE                 33.3               114.7             65.8               46.7               106.0             129.5              54.4


                             Total PAHs                 2134.0             5146.4            4021.4             4104.5             3950.0            4994.0             3176.1










                                                                                               166






                                                          St. Johns Core Data - Hydrocarbon Results - Sediment - 1992


                              INVEST#:
                                  ID:               X-3 38-39        X-3 39-40         X-3 4041         X-3 42-43        X-3 43-44         X-3 44-45        X -3 45-46
                            LABSAMNO:                  C3912             C3913            C3914            C3915             C3916            C3917            C3918
                              ME-MOD:            GCFIID/GCMS GCF11D/GCMS GCFID/GCMS GCFID/GCMS GCF]ID/GCMS GCFID/GCMS GCqD/GCMS
                              QCBATCH:                 M494              M494             M495             M495              M495             M495             M495
                              VWETWT:                  31.66             30.64            30.06            16.63             30.36            8.G8             27.83
                              DRYWT:                   10-13             10.02            10.01            6.02              10.05            2.53             10.02
                                LAB:                   GERG              GERG             GERG             GERG              GERG             GERG             GERG
                              MATRIX:              SEDIMENT SEDUvENT SEDB4ENT SEDBAENT SEDPAEW SEDB4ENT SIDMIEN"I'
                              SUBMAT:


                                UNIT:                  ngtg              ngtg             ng/g             ng/g              ng/g             ng/g             ng/g
                           Analyte (Cont)              Conc              Conc             Conc             Conc              Conc             Conc             Conc


                          2-NiETHYLNAPH                32.3              41.2             47.6             36.2              29.1             49.9             39.4
                          1-METHYLJNAPH                16.0              18.9             22.0             44.7              12.7             20.9             14.6


                          2,6-DRAErMNAPH               15.7              24.5             30.3             44.8              23.0             29.2             29.6


                       2,3,5-TRBffi7MAPH               11.6              15.9             16.7             35.9              16.4             21.7             16.9


                           I-METHYLPHEN                13.6              35.0             23.4             53.0              32.8             39.4             26.8



                       &wropte Recoveries


                              NAPHD8:                  88.17             96.13            104.27           93.81             101.95           91.08            95.47
                              ACEND10:                 91.89             83.05            89.07            84.75             85.72            92.06            76.57
                              PHEND10:                 86.23             66.96            60.60            75.34             83.90            85.16            70.63
                              CHRYD12:                 52.19             13.07            12.64            30.94             22.58            39.81            24.53
                              PERYD12:                 72.23             92.01            38.67            69.19             110.83           75.70            81.29


                                                                           BOLD SURROGATE RECOVERIES                  MATRIX INTERFERENCE









































                                                                                             167






                                                         St. Johns Core Data - Hydrocarbon Results - Sediment - 1992


                          INVESTW:                                              PROC BLANK SPIKED MATRIX PROC BLANK ORIGINAL DUPLICATE
                             11):               X-3 46-47        X-3 47-48             -900             X-3 4-5               -900               X-3 4-5           X-3 4-5
                       LABSAMNO:                     C3919             C3920           Q3336              Q3337               Q3338              C3893             Q3339
                          METHOD:            GCMGCMS GCFID/GCMS GCFEWGCMS GCFID/GCMS GCFID/GCMS GCFID/GCMS GCFID/GCMS
                          QMATCH:                    M495              M495            M492               M492                M492               M492              M492
                          WETVT:                     26.27             27.51           10.00              18.84               10.00              22.54             19.00
                          DRYWT:                     9.01              10.04           10.00               6.01               10.00              7.19              6.06
                             LAB:                    GERG,             GERG            GERG,              GERG                GERG               GERG              GERG
                          MATRIX:              SEDIMENT SEDIMENT QCBLANK                            QCSEDIMENT            QCBLANK SEDIMENT SEDIMENT
                          SUBMAT:


                          Alk.anes and
                          Isoprenoids                Conc              Conc            Conc             % Recov               Conc               Conc              Conc
                             UNIT:                   ng/9              ng/g            ng/g                 %                 ng/g               ng1g              ng/g


                             CIO                     31                25                    0              NA                      0            21                21
                             C11                     15                18                    3              NA                      0            18                23
                             C12                     47                46                    0              108                     1            14                16
                             C13                     9                 15                    0              NA                      0            12                12
                             C14                     55                49                    1              NA                      0            22                24
                             C15                     50                56                    1              110                     0            42                44
                             C16                     5                 4                     2              NA                      0            13                18
                             C17                     168               195                   1              114                     1            211               207
                          PRISTANE                   157               182                   0              121                     1            171               143
                             CI8                     38                62                    1              116                     0            74                54
                          PHYTANE                    102               147                   0              NA                      1            266               206
                             C19                     148               165                   1              NA                      1            445               396
                             C20                     53                85                    2              120                     1            226               210
                             C21                     234               277                   3              115                     2            268               240
                             C22                     166               191                   8              NA                      2            292               246
                             C23                     741               807                   7              NA                      2            802               882
                             C24                     473               511                   6              93                      1            560               600
                             C25                     1376              1517                  5              NA                      2            1501              1640
                             C26                     624               663                   7              NA                      1            725               772
                             C27                     1938              2072                  2              NA                      2            3161              2974
                             C28                     545               572                   0              101                     1            972               1114
                             C29                     2136              2130                  2              NA                      2            4038              4253
                             C30                     337               363                   0              119                     1            1094              1084
                             C31                     1216              929                   2              NA                      1            4755              4614
                             C32                     106               44                    0              104                     0            683               601
                             C33                     215               213                   0              NA                      0            1892              1759
                             C34                     9                 7                     0              97                      0            202               175
                      TOT ALKANES                    10996             11346                 54             NA                      24           22480             22326


                             UNIT:                   U919              U919            ug/g                                   ug/9               U919              U9/9
                             UCM                     167               191                   0              NA                      0            462               443


                   Surrogate Recoveries              %                 %                     %              %                       %            %                 %
                          C12ALKD:                   101.2             96.0            75.8                 71.4              80.8               76.4              65.6
                          C20ALKD:                   85.7              71.6            79.1                 74.7              85.0               73.9              72.2
                          C24ALKD:                   83.8              74.7            82.4                 93.9              86.5               101.2             94.0
                          C30ALKD:                   97.1              101.8           61.1                 82.2              57.2               97.5              87.9














                                                                                             168






                                                             St. Johns Core Data - Hydrocarbon Results - Sediment - 1992


                             INVEST#:                                                 PROC BLANK SPIKED MATRIX PROC BLANK ORIGINAL DUPLICATE
                                 11):               X-3 46-47         X-3 47-48              -900                 X-3 4-5             -900              X-3 4-5           X-3 4-5
                             LABSAMNO:                  C3919             C3920              Q3336                Q3337               Q3338             C3893             Q3339
                             MET'HOD:            GCFID/GCMS GCFID/GCMS GCFID/GCMS GCFID/GCMS GCFID/GCMS GCFID1GCMS GCFID/GCMS
                             QCBATCH:                   M495              M495               M492                 M492                M492              M492              M492
                             Wm:                        26.27             27.51              10.00                18.84               10.00             22.54             19.00
                             DRYWT:                     9.01              10.04              10.00                6.01                10.00             7.19              6.06
                               LAB:                     GERG              GERG               GERG                 GERG                GERG              GERG              GERG
                             MATRIX:               SEDWENT SEDIMENT QCBLANK                               QCSEDIMENT             QCBLANK SEDIMENT S:---DIMENT
                             SUBMAT:


                               LTN117:                  ng/g              ng/g               ng/g                 %                   ngtg              njVg              ng/g
                             PNA Analyte                Conc              Conc               Conc                 % Recov             Conc              Conc              Conc


                             NAPHTHALENE                78.4              96.5               0.7                  93.6                1.1               92.7              94.4
                             Cl-NAPHTHALENES            61.3              76.8               0.7                  NA                  0.9               57.7              56.5
                             C2-NAPHTHALENES            60.9              74.1               0.0                  NA                  0.0               54.7              52.6
                             C3-NAPHTHALENES            59.6              83.5               0.0                  NA                  0.0               52.9              45.6
                             C4-NAPHTHALENES            71.6              90.1               0.0                  NA                  0.0               46.2              39.9
                             BIPHENYL                   22.9              25.1               0.3                  129.0               0.0               15.4              17.3
                             ACENAPHTHYLENE             87.8              99.2               0.2                  107.3               0.0               46.6              51.2
                             ACENAPHTHENE               13.7              18.1               0.3                  120.4               0.0               29.9              33.9
                             FLUORENE                   33.6              48.8               0.2                  98.5                0.1               46.9              51.2
                             Cl-FLUORENES               28.0              46.4               0.0                  NA                  0.0               25.1              32.7
                             C2-FLUORENES               37.5              69.1               0.0                  NA                  0.0               31.0              25.6
                             C3-FLUORENES               48.6              65.1               0.0                  NA                  0.0               35.0              39.1
                             PHENANTHRENE               122.0             155.2              0.4                  80.0                0.2               147.7             179.8
                             ANTHRACENE                 137.0             157.2              0.2                  83.2                0.1               100.3             113.3
                             Cl-PHEN-ANTHR              102.1             137.7              0.0                  NA                  0.0               74.5              78.8
                             C2-PHEN-ANTHR              99.9              132.0              0.0                  NA                  0.0               58.5              66.4
                             C3-PHEN_ANTHR              68.7              84.9               0.0                  NA                  0.0               37.1              48.1
                             C4-PHEN-ANTHR              43.5              51.1               0.0                  NA                  0.0               29.2              41.3
                             DIBENZOTHIO                10.2              13.0               0.1                  71.8                0.0               12.2              13.2
                             Cl-DIBEN                   17.0              20.8               0.0                  NA                  0.0               13.2              15*0
                             C2-DIBEN                   33.8              34.3               0.0                  NA                  0.0               26.4              27.8
                             C3-DIBEN                   23.4              25.7               0.0                  NA                  0.0               18.6              22.2
                             FLUORANTHENE               183.4             216.5              0.2                  113.1               0.2               167.7             250.7
                             PYRENE                     178.2             234.6              0.2                  129.0               0.3               175.3             271.0
                             Cl-FLUORAN.PYR             159.6             196.7              0.0                  NA                  0.0               92.5              118.1
                             BENaANTHRACENE             324.7             228.1              0.1                  114.2               0.1               272.2             206.7
                             CHRYSENE                   324.1             185.2              0.1                  105.4               0.1               269.2             214.9
                             Cl-CHRYSENES               337.5             223.0              0.0                  NA                  0.0               183.6             134.6
                             C2-CHRYSENES               232.8             145.9              0.0                  NA                  0.0               107.3             74.5
                             C3-CHRYSENES               72.5              37.1               0.0                  NA                  0.0               36.3              25.7
                             C4-CHRYSENES               39.4              31.7               0.0                  NA                  0.0               31.9              26.8
                             BENbFLUORAN                319.2             203.6              0.2                  71.4                0.2               241.3             174.8
                             BENkFLUORAN                147.7             69.8               0.1                  83.6                0.0               113.7             80.9
                             BENePYRENE                 170.4             103.3              0.1                  109.0               0.1               131.7             96.3
                             BENaPYRENE                 252.7             147.8              0.1                  101.4               0.1               169.6             124.3
                             PERYLENE                   366.3             298.9              OA                   90.3                0.2               165.6             240.7
                             1123edPYRENE               110.0             62.0               0.1                  88.3                0.1               98.5              70.1
                             DBahANTHRA                 29.0              17.6               0.2                  84.0                0.0               24.5              18.4
                             BghiPERYLENE               94.3              55.6               0.1                  106.5               0.1               96.9              70.3

                             Total PAHs                 4236.9            3763.0             4A                   1879.6              3.7               3263.9            3102.8









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                                                           St. Johns Core Data - Hydrocarbon Results - Sediment - 1992


                           INVEST#:                                                 PROC BLANK SPIKED MATRIX PROC BLANK ORIGINAL DUPLICATE
                              ID:                 X-3 46-47         X-3 47-48              -900                X-3 4-5              -900              X-3 4-5           X-3 4-5
                        LABSAMNO:                    C3919              C3920              Q3336               Q3337                Q3338             C3893             Q3339
                           METHOD:             GC1MYGCMS GCFED/GCMS GC]FID/GCMS GCFID/GCMS GCFID/GCh4S GCFID/GCMS GCFID/GCMS
                           QCBATCH:                  M495               M495               M492                M492                 M492              M492              M492
                           WETwr:                    26.27              27.51              10.00               18.84                10.00             22.54             19.00
                           DRYWT:                    9.01               10.04              10.00               6.01                 10.00             7.19              6.06
                             LAB:                    GERG               GERG               GERG                GERG                 GERG              GERG              GERG
                           MATRIX:               SEDIMENT SEDIMENT QCBLANK QCSEDIMENT QCBLANK SEDIMENT SEDIMENT
                           SUBMAT:


                             UNIT:                   ng/g               ng/g               ng1g                 %                   ng/g              ng/g              ng/g
                        Analyte (Cont)               Conc               Conc               Conc                % Recov              Conc              Conc              Conc


                       2-11E11HYLNAPH                41*0               51,7               OA                  91*2                 0*5               41*3              40A
                       1-ME-rHYLNAPH                 18.3               21.1               0.3                 127.0                0.5               16.4              16.1


                      2,6-DIMETRNAPH                 28.2               39.1               0.3                 123.4                0.6               23.8              26.8


                    2,3,5-TRIMETHNAPH                15.5               23.0               0.4                 111.4                0.5               11.7              11.8


                        I-ME'rHYLPHEN                30.8               30.1               0.1                 81.2                 0.1               24.2              28.4



                    Surropte RecDveries


                           NAPHD8:                   101.00             93.40              85.17               93.68                86.47             75.59             96.15
                           ACENDIO:                  95.87              79.94              81.72               94.97                94.46             82.83             86.77
                           PHEND10:                  83.00              72.75              80.81               100.78               93.32             77.14             81.10
                           CHRYD12:                  17.98              29-"               61,07               21,68                92*50             16.06             26-10
                           PERYD12:                  80.17              106.03             39.40               61.02                52.10             82.65             65.20


                                                                             BOLD SURROGATE RECOVERIES                  MATRIX INTERFERENCE










































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                                                         St. Johns Core Data - Hydrocarbon Results - Sediment - 1992


                           INVEST#:           PROC BLANK SPIKED MATRIX PROC BLANK ORIGINAL DUPLICATE PROCBLANK DRIGINAL
                               El):                -900            X-3 32-33                 -900       X-3 32-33        X-3 32-33           -900          X-3 4243
                        LABSAMNO:                  Q3345                Q3346                Q3347          C3907            Q3348           Q3364              C3915
                           METHOD:            GCFID/GCMS GCFID/GCMS GCFID/GCMS GCFID/GCMS GCF1D/GCMS GCFED/GCMS GCFID/GCms
                           QCBATCH:                M494                 M494                 M494           M494             M494            M495               M495
                           WETWT.                  10.00                17.63                10.00          18.47            18.58           10.28              16.63
                           DRYWT:                  10.00                6.70                 10.00          7.02             7.06            10.28              6.02
                             LAB:                  GERG                 GERG                 GERG           GERG             GERG            GERG               GERG
                           MATRIX:             QCBLANK           QCSEDIMENT           QCBLANK          SEDIMENT SEDIMENT QCBLANK                          3EDIMENT
                           SUBMAT:


                           Alkanes and
                           hoprenoids              Conc             % Recov                  Conc           Conc             Conc            Conc               Conc
                             UNIT:                 ng/g                 %                    ng/9           ng/g             ng/g            ng/g               ng/g


                             CIO                      0                 NA                   1              23               25                    0            37
                             C11                      0                 NA                   0              14               17                    0            40
                             C12                      0                 92.3                 1              40               43                    1            78
                             C13                      0                 NA                   0              4                20                    0            39
                             C14                      0                 NA                   0              40               31                    0            64
                             C15                      0                 91.8                 1              64               49                    4            63
                             C16                      2                 NA                   1              23               5                     2            24
                             C17                      2                 94.8                 1              151              152                   0            168
                           PRISTANE                   0                 94.0                 1              109              119                   0            106
                             C18                      2                 99.0                 1              4                25                    0            38
                           PHYTANE                    0                 NA                   1              80               81                    0            60
                             C19                      1                 NA                   2              208              146                   0            119
                             C20                      1                 103.2                3              48               40                    1            89
                             C21                      1                 97.4                 3              231              214                   2            266
                             C22                      2                 NA                   4              144              134                   2            160
                             C23                      2                 NA                   4              713              646                   2            686
                             C24                      0                 88.4                 3              466              440                   0            415
                             C25                      I                 NA                   3              1251             1175                  2            1306
                             C26                      I                 NA                   3              578              552                   2            567
                             C27                      I                 NA                   5              1626             1493                  3            2134
                             C28                      0                 92.1                 2              382              417                   3            678
                             C29                      0                 NA                   5              1514             1412                  3            3282
                             C30                      0                 90.1                 1              236              298                   4            525
                             C31                      0                 NA                   0              630              676                   3            2353
                             C32                      0                 104.2                0              69               65                    2            216
                             C33                      0                 NA                   0              104              110                   0            564
                             C34                      0                 88.2                 0              7                9                     0            10
                       TOT ALKANES                    16                NA                   46             9757             8394                  34           14088


                             UNIT:                 U9/9                                      ugtg           U9/9             ugtg            Ug/g               ugtg
                             UCM                      0                 NA                   0              270              244                   0            126


                    Surropte Recoveries               %                 %                    %              %                %                     %            %
                           C12ALKD:                78.6                 79.3                 78.6           89.9             81.5            76.3               83.4
                           C20ALKD:                79.5                 94.3                 80.5           82.7             98.6            76.1               79.5
                           C24ALKD:                80.6                 89.8                 82.3           76.6             81.5            78.2               83.5
                           C30ALKD:                78.4                 95.0                 65.3           104.6            113.4           73.4               99.9













                                                                                             171






                                                            St. Johns Core Data - Hydrocarbon Results - Sediment - 1992


                          DP*IUT#:             PROC BLANK SPIKED MATRIX PROC BLANK ORIGINAL DUPLICATE PROC BLANK ORIGINAL
                              ID:                     -900              X-3 32-33                 -900           X-3 32-33          X-3 32-33               -900            X-3 4243
                          LABSAMNO:                   Q3345                 Q3346                 Q3347              C3907              Q3348               Q3364               C3915
                          METHOD:              GCMGCMS GCF1D/GCMS GCMGCMS GCFID/GCMS GCFID/GCMS GCFID/GCMS GCFID/GCMS
                          QCBATCH:                    M494                  M494                  M494               M494               M494                M495                M495
                          WETWT:                      10.00                 17.63                 10.00              18.47              18.58               10.28               16.63
                          DRYWT:                      10.00                 6.70                  10.00              7.02               7.06                10.28               6.02
                            LAB:                      GERG                  GERG                  GERG               GERG               GERG,               GERG,               GERG
                          MATRIX:                QCBLANK             QCSEDIMENT             QCBI-ANK.           SEDIMENT SEDIMENT QCBLANK SEDIMENT
                          SUBMAT:


                            UNIT:                     ng/9                   %                    nwg                ng/g               ngtg                ng/g                ng/g
                          PNA Analyte                 Conc               % Recov                  Conc               Conc               Conc                Conc                Conc


                          NAPHTHALENE                 0,6                   124*0                 0*5                144* 1             92,9                0*7                 12*0
                   CI-NAPHTHALENES                    0.5                   NA                    0.7                83.1               59.0                0.7                 81.0
                   C2-NAPHTHALENES                    0.0                   NA                    0.0                71.4               53.0                0.0                 198.1
                   C3-NAPHTHALENES                    0.0                   NA                    0.0                63.7               50.0                0.0                 165.7
                   C4-NAPHTHALENES                    0.0                   NA                    0.0                56.4               65.1                0.0                 87.3
                          BEPHENYL                    0.1                   129.3                 0.3                21.8               15.4                0.3                 12.8
                   ACENAPHTHYLENE                     0.1                   110.9                 0.1                54.5               38.6                0.1                 46.3
                          ACENAPHTHENE                0.2                   116.7                 0.1                37.0               23.0                0.2                 7.9
                          FLUORENE                    0.1                   101.2                 0.1                52.6               36.8                0.5                 40.7
                          CI-FLUORENES                0.0                   NA                    0.0                26.3               23.0                0.0                 98.0
                          C2-FLUORENES                0.0                   NA                    0.0                29.3               33.1                0.0                 125.3
                          C3-FLUORENES                0*0                   NA                    0*0                35,2               47*1                0*0                 95*2
                          PHENANTHRENE,               0.1                   126.9                 1.0                156.2              142.9               2.5                 132.3
                          ANTHRACENE                  0.1                   88.1                  0.1                97.9               79.9                0.2                 55.5
                          CI-PHEN-ANTHR               0.0                   NA                    0.0                71.5               74.9                0.0                 220.3
                          C2-PHEN-ANTHR               0.0                   NA                    0.0                53.5               83.7                0.0                 215.0
                          C3-PHEN_ANT-HR              0.0                   NA                    0.0                32.2               67.1                0.0                 101.1
                          C4-PHEN-ANT-HR              0.0                   NA                    0.0                25.0               62.6                0.0                 550.0
                          DIBENZOTHIO                 0.1                   77.0                  0.2                14.5               11.2                0.3                 12.9
                          CI-DIBEN                    0.0                   NA                    0.9                15.0               15.1                0.0                 30.5
                          C2-DIBEN                    0.0                   NA                    0.0                25.4               34.2                0.0                 39.3
                          C3-DIBEN                    0.0                   NA                    0.0                15.5               28.0                0.0                 26.3
                          FLUORANTHENE                0.1                   89.9                  0.2                163.5              257.3               0.4                 160.7
                          PYRENE                      0.1                   102.2                 0.2                170.5              296.1               0.4                 192.3
                   CI-FLUORAN-PYR                     0.0                   NA                    0.0                81.6               161.0               0.0                 198.1
                   BENaANTHRACENE                     0.1                   96.8                  0.1                204.6              192.8               0.2                 132.3
                          CHRYSENE                    0*1                   74A                   0*2                199,2              131 *7              0,1                 172,6
                          CI-CHRYSENES                0.0                   NA                    0.0                166.7              139.0               0.0                 188.0
                          C2-CHRYSENES                0.0                   NA                    0.0                122.1              112.0               0.0                 147.5
                          C3-CHRYSENES                0.0                   NA                    0.0                45.8               47.9                0.0                 32.2
                          C4-CHRYSENES                0.0                   NA                    0.0                39.5               41.3                0.0                 26.0
                          BENbFLUORAN                 0.0                   96.4                  0.1                186.8              213.0               0.1                 144.8
                          BENkFLUORAN                 0.1                   90.2                  0.1                91.6               47.8                0.1                 33.0
                          BENePYRENE                  0*1                   126*0                 0*1                118*1              113*0               0*2                 14,2
                          BENaPYRENE                  0.1                   128.5                 0.1                145.6              141.6               0.1                 99.5
                          PERYLENE                    0.2                   117.0                 0.1                301.3              254.7               0.3                 375.0
                          1123cdPYRENE                0.1                   96.3                  0.1                90.2               103.1               0.1                 49.0
                          DBahANTHRA                  0,1                   81 *0                 0*1                22*2               25*6                0*2                 14,1
                          B*eERYLENE                  0.1                   112.1                 0.1                86.5               96.9                0.2                 46.7


                          ToW PAHs                    2.6                   NA                    5.2                3116.8             3257.0              7.5                 4104.5









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                                                         St. Johns Core Data - Hydrocarbon Results - Sediment - 1992


                           I[NVEST#-          PROC BLANK SPUCED MATRIX PROC BLANK ORIGINAL DUPLICATE PROC BLANK ORIGINAL
                               a):                  -900               X-3 32-33           -900         X-3 32-33        X-3 32-33            -900          X-3 4243
                         LABSAMNO:                  Q3345              Q3346               Q3347           C3907             Q3348            Q3364            C3915
                           METFIOD:           GCFEDIGCMS GCFID/GCMS GCF1D/GCMS GCFID/GCMS GCFID/GCMS GCFID/GCMS GCF]ID/GCMS
                           QCBATCH:                 M494               M494                M494            M494              M494             M495             M495
                           V&-rwr:                  10.00              17.63               10.00           18.47             18.58            10.28            16.63
                           DRYWT:                   10.00              6.70                10.00           7.02              7.06             10.28            6.02
                             LAB:                   GERG               GERG                GERG            GERG              GERG             GERG             GERG
                           WIATRIX:             QCBLANK          QCSEDIMENT           QCBLANK          SEDIMENT SEDAIENT QCBLANK                           SEDNIENT
                           SUBMAT:


                             UNIT:                  ngtg                %                  og/g            n919              ngtg             ngtg             ng/g
                        Analyte (Cont)              Conc               % Recov             Conc            Conc              Conc             Conc             Conc


                       2-METHYLNAPH                 0.3                123.9               0.3             59.1              41.3             0.3              36.2
                      1 -METHYLNAPH                 0.2                107.5               0.3             24.0              17.7             0.4              44.7


                       2,6-DRAET'HNAPH              0.1                111.9               0.2             31.7              21.2             0.4              44.8


                    2,3,5-TRRAETMAPH                0.1                128.1               0.2             15.0              12.0             0.2              35.9


                       1 -METHYLPHEN                0.1                84.2                0.1             21.4              21.4             0.4              53.0



                    Surropte Recoveries


                           NAPHD8:                  87.20              101.72              88.68           91.66             93.57            95.65            93.isi
                           ACENDIO:                 83.23              99.27               89.62           95.96             92.50            92.92            84.75
                           PHENDIO:                 96.24              108.42              90.50           97.11             89.34            84.04            75.34
                           CHRYD12:                 80.85              26.36               87.26           19.01             59.58            94.86            30.94
                           PERYD12:                 33.30              100.15              58.03           73.08             79.85            40.00            69.19


                                                                            BOLD SURROGATE RECOVERIES                 MATRIX INTERFERENCE








































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                                                      St. Johns Core Data - Hydrocarbon Results - Sediment - 1992


                                 DNM*.               DUPLICATE PROC BLANK SPIKED MATRIX CONTROL                               CONTROL          CONTROL
                                    ID:                X-3 42-43           -900            X-3 42-43              -700            -700              -700
                               LABSAMNO:                   Q3365           Q3366               Q3367              W26690          W26691            W26699
                                 METHOD:            GCFID/GCMS GCFID/GCMS GCF1D/GCMS GCFID/GCMS GCFID/GCMS GCFID/GCMS
                                 QCBATCH:                  M495            M495                M495               M492            M494              M495
                                 WETWT.                    16.66           10.00               16.99              1.00            1.00              1.00
                                 DRYWT:                    6.03            10.00               6.15               1.00            1.00              1.00
                                    LAB:                   GERG            GERG                GERG               GERG            GERG              GERG
                                 MATRIX:            QCSEDMIENT QCBLANK                    SEDWENT           QCSBLANK QCSBLANK QCSBLANK
                                 SUBMAT:                                                                          EV OIL          EV OIL            EV OIL


                                 Alkanes and
                                 Isoprenoids               Cone            Cone             % Recov               Cone            Cone              Cone
                                    UNrr:                  nglg            0919                %                  ng/9            ng/9              ngfg


                                    CIO                    39                    0                                2849            2621              3099
                                    C11                    22                    0                                2980            2586              2749
                                    C12                    74                    0             96                 2639            2279              2507
                                    C13                    25                    0                                2683            2371              2436
                                    C14                    55                    0                                2477            2129              2344
                                    C15                    61                    4             97                 2350            2108              2366
                                    C16                    24                    1                                2209            1908              2105
                                    C17                    130                   0             94                 2399            2261              2481
                                 PRISTANE                  82                    0             95                 1659            1549              1884
                                    C18                    33                    0             94                 1963            1946              1970
                                 PHYTANE                   44                    1                                1156            1117              1112
                                    C19                    88                    1                                1926            2018              1945
                                    C20                    67                    0             100                1941            1581              1688
                                    C21                    231                   1             93                 1607            1663              1701
                                    C22                    128                   2                                1691            1578              1545
                                    C23                    576                   2                                1641            1463              1446
                                    C24                    342                   0             108                1388            1559              1391
                                    C25                    1088                  1                                1273            1235              1200
                                    C26                    490                   1                                1178            1047              1017
                                    C27                    1717                  1                                888             781               790
                                    C28                    602                   0             94                 679             655               652
                                    C29                    2699                  0                                500             605               601
                                    C30                    617                   0             117                524             551               580
                                    C31                    2267                  0                                505             477               469
                                    C32                    224                   0             110                383             430               399
                                    C33                    517                   0                                290             308               287
                                    C34                    6                     0             95                 194             276               192
                             TOT ALKANES                   12250                 15                               41870           39101             40957


                                    UNIT:                  ugtg            U919                ug/8               ugtg            U919              ugtg
                                    UCM                    109                   0                                153             190               212


                          Surrogate Recoveries             %                     %             %                  %                 %                %
                                 C12ALKD:                  88.8            78.2                82.8               100.9           124.2             103.9
                                 C20ALKD:                  87.8            77.7                93.8               96.7            95.2              88.8
                                 C24ALKD:                  92.7            79.4                85.4               97.8            96.7              90.8
                                 C30ALKD:                  94.0            75.4                86.0               91.1            87.9              ".0














                                                                                            174




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                                                       Saint Johns River Core Pesticide and PCB Results - 1992



                      RAW FILE               C3890P C3891P C3892P C3893P C3894P C3895S C3896P C3897P C3898P C3900P C3901P C3902P
                       VVETWT:                 6.18       17.79 36.64 22.54             13.95 32.49 27.29 37.14                  24.37       28.57       36.21       16.08
                       DRYWT:                  2.01       6.03     10.04      7.19      3.92      10.04     7.97      9.99       7.31        10.00       10.03       4.60
                      SAMP TYPE:
                          ID:                X-3 0-1 X-3 1-2 X-3 3-4 X-3 4-5 X-3 5-6 X-3 6-7 X-3 7-8 X-3 8-9                 X-3 10-11 X-3 13-14 X-3 14-15 X-3 15-161
                         UNITS                 (ppb)      (ppb)    (ppb]      (ppb]     (ppb)     (ppb)     (ppb)     (ppb)      (ppb)       (ppb)       (ppb]       (ppb)

                      TOTAL BHC'S              0.18       0.15     0.12       0.11      0.22      0.27      0.16      0.16       0.17        0.07        0.09        0.13
                TOTAL CHLORDANES               1.32       2.00     2.05       1.85      1.58      2.07      2.34      2.08       1.92        1.87        2.68        1.79
                      TOTAL DDT'S              16.93      18.01    15-35      15-64     29.27     21.52     17.10     17.26      19.26       10.90       14.22       15.51
                      TOTAL PCB'S              253.3      247.9    249.2      279.4     344.7     381.6     364.1     331.0      317.5       204.9       240.3       179.4


                      ALPHA-BHC                0.00       0.06     0.05       0.05      0.06      0.09      0.03      0.03       0.04        0.01        0.02        0.08
                         HCB                   0.00       0.01     0.00       0.00      0.00      0.00      0.00      0.00       0.00        0.00        0.00        0.00
                      BETA-BHC                 0.00       0.00     0.00       0.00      0.00      0.03      0.02      0.00       0.00        0.00        0.00        0.00
                      GAMMA-BHC                0.18       0.08     0.06       0.06      0.16      0.09      0.11      0.13       0.14        0.05        0.06        0.00
                      DELTA-BHC                0.00       0.01     0.01       0.00      0.00      0.06      0.01      0.01       0.00        0.01        0.01        0.06
                      HEPTACHLOR               0.07       0.04     0.01       0.01      0.00      0.02      0.02      0.02       0.00        0.01        0.01        0.02
                  HEPTA-EPOMDE                 0.00       0.00     0.01       0.00      0.00      0.00      0.02      0.00       0.00        0.00        0.01        0.00
        -4        OXYCHLORDANE                 0.00       0.20     0.17       0.24      0.20      0.00      0.31      0.00       0.00        0.18        0.28        0.25
        0)      GAMMA-CHLORDANE                0.78       0.84     0.92       0.87      0.80      0.93      1.13      1.12       1.03        0.84        1.27        0.84
                ALPHA-CHLORDANE                0.18       0.31     0.28       0.20      0.19      0.39      0.24      0.34       0.22        0.31        0.36        0.22
                TRANS-NONACHLOR                0.09       0.13     0.08       0.07      0.08      0.13      0.06      0.08       0.07        0.05        0.08        0.08
                  CIS-NONACHLOR                0.19       0.49     0.58       0.44      0.30      0.61      0.565     0.52       0.60        0.47        0.66        0.39
                       ALDRIN                  0.00       0.01     0.01       0.00      0.00      0.03      0.01      0.00       0.00        0.00        0.00        0.00
                      DIELDRIN                 0.12       0.13     0.11       0.09      0.08      0.14      0.08      0.09       0.09        0.08        0.12        0.05
                       ENDRIN                  0.00       0.11     0.00       0.00      0.00      0.00      0.00      0.00       0.00        0.00        0.00        0.00
                         MIREX                 0.00       0.00     0.00       0.00      0.00      0.00      0.00      0.00       0.00        0.00        0.00        0.00
                  2,4'DDE (O.P'DDE)            0.00       0.04     0.03       0.02      0.04      0.12      0.02      0.06       0.06        0.04        0.11        0.03
                  4ADDE (P,P'DDE)              4.35       3.65     3.61       3.44      3.94      5.58      5.66      5.34       5.51        3.97        6.87        8.19
                  2,4'DDD (0,P'DDD)            0.54       1.00     0.98       0.97      0.84      1.50      1.35      1.41       1.31        0.74        1.02        0.72
                  4,4'DDD (P,P'DDD)            11.74      12.87    10.25      10.66     23.48     13.27     9.21      9.86       11.50       5.75        5.75        5.69
                  2,4'DDT (0,P'DM              0.04       0.13     0.13       0.12      0.14      0.30      0.17      0.15       0.21        0.12        0.14        0.23
                  4,4'DDT (P,P'DDTI            0.26       0.33     0.34       0.44      0.83      0.74      0.68      0.44       0.67        0.28        0.33        0.65
                      PCB#8 (CL2)              0.6        0.1       0.1       0.1       0.2       0.1       0.6       0.1        0.1         0.0         0.1         0.0
                      PCB#18 (CL3)             0.2        0.3       0.3       0.5       0.4       0.6       1.4       0.6        1.1         0.3         0.5         0.7
                      PCB#28 (CL,3)            0.9        1.3       1.4       1.2       1.2       1.8       2.4       1.9        2.2         1.0         1.4         2.9
                      PCB#44 (CIA)             2.7        2.8       2.6       3.1       3.4       4.2       4.1       4.0        3.5         2.2         2.3         2.6






                                                     Saint Johns River Core Pesticide and PCB Results - 1992



                     RAW FILE               C3890P C3891P C3892P C3893P C3894P C3895S C3896P C3897P C3898P C3900P C3901P C3902P
                       WETWr:                  6.18      17.79 36.64 22.54           13.95 32.49 27.29 37.14                24.37       28.57       36.21      16-08
                       DRYWr:                  2.01      6.03     10.04     7.19     3.92      10.04    7.97      9.99      7.31        10.00       10.03      4.60
                     SAMP TYPE:
                          ID,               X-3 0-1 X-3 1-2 X-3 3-4 X-3 4-5 X-3 5-6 X-3 6-7 X-3 7-8 X-3 8-9 X-3 10-11 X-3 13-14 X-3 14-15 X-3 15-16
                        UNUS                   (ppb)     (ppb)    (ppb)     (ppb)    (ppb)     (ppb)    (ppb)     (ppb)     (ppb)       (ppb)       (ppb)      (p

                    PCB#52 (CL4)               9.3       10.3     10.5      13.3     12.0      15.9     15.1      14.6      11.6        6.8         7.9        8.6
                    PCB#66 (CL4)               1.2       1.9      1.5       2.0      1.7       2.8      3.1       2.6       2.7         1.2         1.6        1.7
                    PCB# 10 1 (CL5)            11.2      13.3     13.6      15.0     13.6      18.6     18.6      17.4      16.9        11.3        13.8       12.4
                    PCB#105 (CL5)              0.3       0.4      0.7       0.6      0.2       0.6      0.5       0.3       0.6         0.6         0.6        0.4
                PCB# 110/77 (CL5/4)            14.8      17.8     17.9      18.9     16.5      22.7     23.6      21.2      22.6        15.8        19.3       18.7
            PCB# I 18/108/149(CL5/5/6)         5.4       7.7      6.8       8.0      11.3      11.7     10.4      9.8       10.1        6.5         6.0        3.9
                    PCB# 128 (CL6)             1.2       1.6      1.6       1.6      1.6       2.1      1.9       1.4       1.8         1.4         1.6        1.2
                    PCB#138(CL6)               12.2      12.2     12.7      13.8     18.7      15.8     14.2      13.7      14.3        11.6        13.8       9.6
                    PCB#126 (CL5)              0.0       0.0      0.0       0.0      0.0       0.0      0.0       0.0       0.0         0.0         0.0        0.0
                    PCB# 153 (CL6)             33.7      36.1     36.5      43.7     64.9      56.1     57.2      55.0      50.9        30.3        35.6       22.0
                    PCB# 170 (CL7)             18.9      6.0      5.9       4.7      4.8       18.9     11.6      7.7       6.9         6.3         5.5        3.6
                    PCB# 180 (CL7)             8.5       8.8      9.6       9.6      10.6      10.9     12.0      10.4      10.9        7.1         9.9        6.3
            PCB# 187/182/159(CL7/7/6)          5.8       6.0      6.4       6.7      9.1       8.7      8.5       7.9       7.6         4.4         6.2        4.1
                    PCB#195 (CL8)              1.1       1.3      1.2       1.0      1.2       1.8      1.5       1.3       1.2         0.8         1.0        0.5
                    PCB#206 (CL9)              1.3       1.5      1.3       1.5      1.5       2.0      1.9       1.3       1.4         0.6         0.8        0.5
                   PCB#209 (CLIO)              0.2       0.4      0.2       0.2      0.0       0.4      0.3       0.2       0.2         0.1         0.1        0.0






                                                   Saint Johns River Core Pesticide and PCB Results - 1992



                  RAW FILE               C3903P C3904P C3905P C3906P C3907P C3908P C3909P C3910P C3911P C3912P C3913P
                   WETWT:                  45.16       35.14      26.70       11.16      18.47      22.66       35.59      26.22      4.19        31.66       30.64
                   DRYWT:                  9.98        10.05      10.04       4.05       7.02       10.06       10.00      7.08       0.80        10.13       10.02
                  SAMP TWE:
                      ID:               X-3 16-17 X-3 22-23 X-3 27-28 X-3 30-31 X-3 32-33 X-3 33-34 X-3 35-36 X-3 36-37 X-3 37-38 X-3 38-39 X-3 39-40
                     UNn,s                 (ppb)       (ppb)      (ppb)       (ppb)      (ppb)      (ppb)       (ppb)      (ppb)      (ppb)       (ppb)       (ppb)

                  TOTAL BHC'S              0.16        0.07       0.48        0.13       0.19       0.03        0.13       0.69       0.21        0.03        0.00
             TOTAL CHLORDANES              2.04        0.84       1.36        1.39       1.91       0.74        1.39       1.08       0.03        0.04        0.03
                  TOTAL DDTS               17.93       7.34       10.11       14.26      13.07      5.42        8.84       7.00       5.76        8.09        6.43
                  TOTAL PCB'S              246.3       174.1      259.5       243.8      251.0      77.0        34.8       44.0       23.2        54.0        46.0


                  ALPHA-BHC                0.05        0.05       0.38        0.09       0.12       0.02        0.02       0.02       0.00        0.01        0.00
                     HCB                   0.00        0.00       0.00        0.00       0.00       0.00        0.00       0.00       0.00        0.00        0.00
                  BETA-BHC                 0.00        0.00       0.00        0.00       0.01       0.00        0.00       0.00       0.00        0.02        0.00
                  GAMMA-BHC                0.09        0.00       0.08        0.04       0.02       0.01        0.11       0.67       0.21        0.00        0.00
                  DELTA-BHC                0.03        0.02       0.03        0.00       0.03       0.01        0.00       0.00       0.00        0.00        0.00
                  REPTACHLOR               0.03        0.10       0.09        0.00       0.06       0.03        0.04       0.04       0.03        0.02        0.01
               HEPTA-EPOMDE                0.01        0.00       0.01        0.00       0.00       0.00        0.00       0.00       0.00        0.00        0.01
       -4      OXYCHLORDANE                0.21        0.22       0.22        0.26       0.31       0.08        0.01       0.00       0.00        0.02        0.01
      00     GAMMA-CHLORDANE               0.88        0.38       0.80        1.06       1.17       0.57        1.34       1.04       0.00        0.00        0.00
             ALPHA-CHLORDANE               0.26        0.09       0.08        0.01       0.20       0.03        0.00       0.00       0.00        0.00        0.01
             TRANS-NONACHLOR               0.05        0.01       0.00        0.00       0.03       0.00        0.00       0.00       0.00        0.00        0.00
               CIS-NONACHLOR               0.61        0.04       0.15        0.06       0.15       0.02        0.00       0.00       0.00        0.00        0.00
                   ALDRIN                  0.00        0.00       0.00        0.00       0.00       0.00        0.00       0.00       0.00        0.00        0.00
                  DIELDRIN                 0.09        0.03       0.10        0.05       0.09       0.02        0.04       0.04       0.00        0.04        0.09
                   ENDRIN                  0.00        0.00       0.00        0.00       0.00       0.00        0.00       0.00       0.00        0.08        0.00
                     MIREX                 0.00        0.00       0.00        0.00       0.00       0.00        0.00       0.00       0.00        0.00        0.00
               2,4'DDE (O.P'DDE)           0.14        0.00       0.00        0.00       0.00       0.16        0.49       0.25       0.00        0.23        0.14
               4,4'DDE (P,P'DDE)           8.62        1.40       3.25        2.66       3.62       3.03        6.52       5.13       5.15        5.78        4.73
               2.4'DDD (0,P'DDD)           1.10        1.89       1.64        1.59       2.70       0.71        0.47       0.41       0.15        0.33        0.37
               4,4'DDD (P,P'DDD)           7.07        3.88       4.33        9.78       6.03       1.41        1.32       1.18       0.46        1.68        1.18
               2,4'DDT (O.P'DErn           0.29        0.04       0.26        0.00       0.15       0.03        0.00       0.00       0.00        0.03        0.00
               4,4'DDT (P.P'DErD           0.73        0.15       0.63        0.24       0.57       0.08        0.04       0.03       0.00        0.04        0.02
                  PCB#8(CL2)               0.2         0.2        0.6         0.0        0.0        0.0         0.0        0.0        0.0         0.0         0.0
                  PCB#18(CL3)              0.4         0.6        2.8         2.2        1.3        0.4         0.2        0.0        0.0         0.0         0.0
                  PCB#28(CL3)              0.0         0.0        1.9         1.5        1.2        0.3         0.4        0.4        0.0         0.0         0.0
                  PCB#44 (CIA)             2.0         1.1        6.0         4.7        2.5        0.9         0.1        0.1        0.2         0.1         0.1






                                                     Saint Johns River Core Pesticide and PCB Results - 1992



                   FAW FILE                C3903P C3904P C3905P C3906P C3907P C3908P C3909P C3910P C3911P C3912P C3913P
                     V;ETWr:                 45.16       35.14       26.70      11.16      18.47       22.66       35.59      26.22       4.19       31.66       30.64
                     DRYWr:                  9.98        10.05       10.04      4.05       7.02        10.06       10.00      7.08        0.80       10.13       10.02
                   SAMP TYPE:
                        ID:               X-3 16-17 X-3 22-23 X-3 27-28 X-3 30-31 X-3 32-33 X-3 33-34 X-3 35-36 X-3 36-37 X-3 37-38 X-3 38-39 X-3 39-401
                      UNUS                   (ppb)       (ppb)       (ppb)      (ppb)      (ppb)       (ppb)       (ppb)      (ppb)       (ppb)      (ppb)       (ppb)

                  PCB#52 (CIA)               7.9         15.1        33.4       28.6       26.3        8.5         1.4        0.9         1.3        0.5         0.6
                  PCB#66 (CIA)               1.8         0.7         2.5        1.2        0.9         0.4         0.0        0.0         0.0        0.0         0.0
                 PCB#101 (CL5)               16.4        10.5        17.9       16.9       14.0        5.1         4.3        4.3         3.3        5.5         6.6
                 PCB# 105 (CL5)              0.7         0.0         1.4        0.6        0.0         0.1         0.0        0.0         0.0        0.0         0.0
              PCB# 110/77 (CL5/4)            24.1        4.7         16.1       15.3       5.7         3.9         3.4        3.1         2.2        3.1         3.7
          PCB# I 18/108/149(CL5/5/6)         5.9         2.3         6.6        5.3        3.7         1.2         0.6        0.5         0.3        0.5         0.5
                 PCB#128 (CL6)               1.8         2.7         1.8        1.4        3.1         0.9         1.0        0.7         0.6        1.5         1.3
                 PCB# 138 (CLO               13.7        1.6         6.1        8.0        2.1         2.3         1.1        0.7         0.9        1.1         1.0
                 PCB#126 (CL5)               0.5         0.0         0.0        0.0        0.0         0.0         0.5        0.4         0.0        1.0         0.8
                 PCB#153 (CL6)               34.6        25.6        24.8       25.9       37.9        8.9         2.8        2.4         1.0        4.2         4.5
                 PCB# 170 (CL7)              6.4         9.8         3.1        3.2        5.9         1.6         0.7        6.9         0.6        4.4         2.0
                 PCB# 180 (CL7)              10.3        4.7         4.9        6.5        8.2         1.9         0.8        0.7         0.5        1.8         1.5
        -4PCB# 187/182/159(CL7/7/6)          6.6         2.1         2.6        3.5        4.0         0.9         0.5        0.4         0.2        0.8         0.7
        (D       PCB# 195 (CIA               1.0         0.8         0.6        0.5        1.4         0.2         0.2        0.1         0.2        0.5         0.2
                 PCB#206 (CL9)               0.8         0.5         0.4        0.3        0.7         0.1         0.4        0.2         0.3        0.9         0.4
                 PCB#209 (CLIO)              0.9         0.3         0.2        0.1        0.2         0.1         0.5        0.5         0.4        1.9         0.6






                                                           Saint Johns River Core Pesticide and PCB Results - 1992



                         RAW FILE                 C3914P C3915P C3916P C3917P C3918P C3919P C3920P Q3336P Q3337P                                                   Q3338P C3893P.
                          VVETWT:                    30.06        16.63        30.36       8.08        27.83        26.27         27.51      10.00        18.84      10.00 22.54
                          DRYWT:                     10.01        6.02         10.05       2.53        10.02        9.01          10.04      10.00        6.01       10.00       7.19
                         SAMP'IYPE:                                                                                                         BLANK         SPIKE      SAND ORIG
                             ID:                 X-3 40-41 X-3 42-43 X-3 43-44 X-3 44-45 X-3 45-46 X-3 46-47 X-3 47-48                                ofC3893P      BLANK X-3 4-5
                            UNITS                    (ppb)        (ppb]        (ppb]       (ppb)       (ppbj        (ppb]         (ppbl      (ppb)     % Recov       (ppb]       (ppbj

                         TOTAL BHC'S                 0.17         0.00         0.00        0.12        0.02         0.01          0.06       0.00         NA         0.00        0.11
                   TOTAL CHLORDANES                  0.04         0.12         0.00        0.00        0.03         0.08          0.03       0.00         NA         0.00        1.85
                         TOTAL DDT"S                 4.19         1.12         0.82        1.02        0.82         0.92          1.25       0.06         NA         0.11        15.64
                         TOTAL PCB'S                 38.8         14.8         17.7        26.3        25.9         23.0          41.6        2.3         76%         4.0        279.4


                         ALPHA-BHC                   0.10         0.00         0.00        0.00        0.00         0.00          0.04       0.00         1060/6     0.00        0.05
                            HCB                      0.00         0.00         0.00        0.00        0.00         0.00          0.00       0.00         81%        0.00        0.00
                         BETA-BHC                    0.04         0.00         0.00        0.12        0.02         0.01          0.01       0.00         290/6      0.00        0.00
                         GAMMA-BHC                   0.00         0.00         0.00        0.00        0.00         0.00          0.00       0.00         96%        0.00        0.06
                         DELTA-BHC                   0.03         0.00         0.00        0.00        0.00         0.00          0.00       0.00         117%       0.00        0.00
                         HEPTACHLOR                  0.00         0.00         0.00        0.00        0.00         0.04          0.00       0.00         125%       0.00        0.01
                     HEPTA-EPOMDE                    0.01         0.00         0.00        0.00        0.01         0.01          0.01       0.00         91%        0.00        0.00
         00          OXYCHLORDANE                    0.02         0.00         0.00        0.00        0.00         0.00          0.00       0.00         NA         0.00        0.24
                   GAMMA-CHLORDANE                   0.00         0.12         0.00        0.00        0.00         0.00          0.00       0.00         79%        0.00        0.87
                   ALPHA-CHLORDANE                   0.01         0.00         0.00        0.00        0.02         0.03          0.02       0.00         91%        0.00        0.20
                   TRANS-NONACHLOR                   0.00         0.00         0.00        0.00        0.00         0.00          0.00       0.00         83%        0.00        0.07
                     CIS-NONACHLOR                   0.00         0.00         0.00        0.00        0.00         0.00          0.00       0.00         NA         0.00        0.44
                          ALDRIN                     0.00         0.00         0.00        0.00        0.00         0.00          0.00       0.00         128%       0.00        0.00
                         DIELDRIN                    0.07         0.00         0.00        0.03        0.06         0.05          0.05       0.00         82%        0.00        0.09
                          ENDRIN                     0.00         0.24         0.00        0.00        0.00         0.00          0.00       0.00         660/6      0.00        0.00
                            MIREX                    0.00         0.00         0.00        0.00        0.00         0.00          0.00       0.00         72%        0.00        0.00
                     2,4'DDE (0,P'DDE)               0.11         0.00         0.00        0.00        0.00         0.00          0.00       0.00         780/6      0.00        0.02
                     4.4!DDE tP.P'DDE)               3.24         0.93         0.66        0.87        0.59         0.64          0.68       0.06         95%        0.07        3.44
                     2.4'DDD (O,P'DDD)               0.23         0.09         0.09        0.11        0.16         0.13          0.19       0.00         74%        0.01        0.97
                     4,4'DDD (P,P'DDD)               0.55         0.11         0.06        0.04        0.07         0.14          0.26       0.00         99%        0.03        10.66
                     2.4'DDT (O,P'DDTj               0.03         0.00         0.00        0.00        0.00         0.00          0.06       0.00         66%        0.00        0.12
                     4,4'DDT (P,P'D"                 0.02         0.00         0.00        0.00        0.00         0.00          0.06       0.00         106%       0.00        0.44
                         PCB#8 (CL2)                 0.0          0.0          0.0         0.0          0.0          0.0          0.0         0.0         NA          0.0        0.1
                         PCB#18 (CL3)                0.0          0.0          0.0         0.2          0.0          0.1          0.1         0.0         NA          0.0        0.5
                         PCB#28 (CL3)                0.0          0.7          0.0         0.0          0.0          0.0          0.0         0.0         NA          0.0        1.2
                         PCB#44 (CIA)                0.2          0.0          0.1         0.2          0.2          0.2          0.3         0.0         NA          0.0        3.1







                                                     Saint Johns River Core Pesticide and PCB Results - 1992



                      RAW FILE                C3914P C3915P C3916P C3917P C3918P C3919P C3920P Q3336P Q3337P                                      Q3338P C3893
                        V;ETWr:               30.06       16.63       30.36      8.08       27.83       26.27      27.51      10.00      18.84      10.00 22.54
                        DRYWr:                 10.01       6.02       10.05      2.53       10.02        9.01      10.04      10.00       6.01      10.00     7.19
                      SAMP TYPE:                                                                                             BLANK       SPIKE      SAND ORIG
                           ID:              X-3 40-41 X-3 42-43 X-3 43-44 X-3 44-45 X-3 45-46 X-3 46-47 X-3 47-48                     ofC3893P     BLANK X-3 4-5
                         UNITS                 (ppb)       (ppb)      (ppb)      (ppb)       (ppb)      (ppb)       (ppb)     (ppb)    % Recov      (ppb)     (ppb)

                     PCB#52 (CIA)               0.8         0.0        0.2        0.3         0.4        0.8         1.5       0.0        NA         0.0      13.3
                     PCB#66 (CIA)               0.0         0.0        0.0        0.0         0.0        0.0         0.0       0.0        NA         0.0      2.0
                     PCB#101 (CL5)              5.6         2.6        3.6        3.9         4.9        4.4         5.2       0.0        NA         0.1      15.0
                     PCB#105 (CL5)              0.0         0.0        0.0        0.0         0.0        0.0         0.0       0.0        NA         0.0      0.6
                 PCB# 110/77 (CL5/4)            2.5         1.0        0.8        1.0         1.4        1.1         1.7       0.0        NA         0.1      18.9
             PCB# 1 18/108/149(CL5/5/6)         0.3         0.3        0.1        0.1         0.1        0.1         0.2       0.0        NA         0.0      8.0
                     PCB# 128 (CL6)             0.6         0.3        0.4        0.4         0.5        0.5         0.7       0.0        NA         0.0      1.6
                     PCB# 138 (CL6)             1.3         0.3        0.1        0.6         0.2        0.2         0.2       0.0        NA         0.1      13.8
                     PCB# 126 (CL5)             0.0         0.0        0.0        0.0         0.0        0.0         0.0       0.0        NA         0.0      0.0
                     PCB# 153 (CL6)             3.0         0.5        0.6        0.5         0.8        1.0         1.5       0.0        NA         0.1      43.7
                     PCB# 170 (CL7)             1.4         0.3        1.0        3.5         1.6        0.4         6.0       0.0        NA         0.6      4.7
                     PCB# 180 (CL7)             1.0         0.2        0.2        0.2         0.3        0.4         0.4       0.0        NA         0.0      9.6
         OD PCB#187/182/159(CL7/7/6)            0.6         0.1        0.1        0.0         0.2        0.2         0.2       0.0        NA         0.0      6.7
                     PCB# 195 (CL8)             0.3         0.1        0.2        0.1         0.2        0.2         0.2       0.0        NA         0.0      1.0
                     PCB#206 (CL9)              0.6         0.1        0.2        0.3         0.5        0.4         0.3       0.0        NA         0.0      1.5
                     PCB#209 (CLIO)             1.0         0.3        0.3        0.7         0.9        0.5         1.1       0.0        NA         0.0      0.2






                                                           Saint Johns River Core Pesticide and PCB Results - 1992



                       RAW FILE                   Q3339P Q3345P 93346P                 Q3347P C3907P Q3348P Q3364P C3915P Q3365P Q3366P Q3367P
                         VIETWT:                     19.00       10.00        17.63       10.00       18.47        18.58       10.28       16.63         16.66       10.00        16.99
                         DRYWT:                      6.06        10.00        6.70        10.00       7.02         7.06        10.28       6.02          6.03        10.00        6.15
                       SAMP TYPE:                 QA/QC        BLANK          SPIKE       SAND        REP        QA/9C         SAND        ORIG        QA/QC       BLANK          SPIKE
                            ID:                 ofC3893P                 of C3907P     BLANK     X-3 32-33 of C3907P         BLANK     X-3 42-43 of C3915P                    of C3915P
                          UNITS                      (ppb)       (ppbj    % Recov         (ppb)       (ppb)        (ppb)       (ppb)       (ppb)         (ppb)       (ppb)     % Recov

                       TOTAL BHC'S                   0.10        0.00         NA          0.00        0.19         0.10        0.00        0.00          0.00        0.00         NA
                 TOTAL CHLORDANES                    1.89        0.00         NA          0.00        1.91         1.79        0.00        0.12          0.00        0.02         NA
                       TOTAL DDT"S                   18.27       0.13         NA          0.08        13.07        11.58       0.05        1.12          0.80        0.04         NA
                       TOTAL PCB'S                   340.6       2.3          93%         2.2         251.0        237.4       3.4         14.8          14.1        2.8          850/6


                       ALPHA-BHC                     0.05        0.00         109%        0.00        0.12         0.05        0.00        0.00          0.00        0.00         102%
                           HCB                       0.00        0.00         22%         0.00        0.00         0.00        0.00        0.00          0.00        0.00         60/0
                       BETA-BHC                      0.00        0.00         8%          0.00        0.01         0.01        0.00        0.00          0.00        0.00         19%
                       GAMMA-BHC                     0.04        0.00         105%        0.00        0.02         0.01        0.00        0.00          0.00        0.00         97%
                       DELTA-BHC                     0.00        0.00         98%         0.00        0.03         0.02        0.00        0.00          0.00        0.00         1100/0
                       REP TACHLOR                   0.01        0.00         1030/0      0.00        0.06         0.03        0.00        0.00          0.00        0.00         930/0
                   HEPTA-EPO)UDE                     0.00        0.00         81%         0.00        0.00         0.00        0.00        0.00          0.00        0.00         95%
                   OXYCHLORDANE                      0.26        0.00         NA          0.00        0.31         0.28        0.00        0.00          0.00        0.00         NA
                 GAMMA-CHLORDANE                     0.77        0.00         900/0       0.00        1.17         1.16        0.00        0.12          0.00        0.02         82%
                 ALPHA-CHLORDANE                     0.28        0.00         101%        0.00        0.20         0.19        0.00        0.00          0.00        0.00         93%
                 TRANS-NONACHLOR                     0.11        0.00         92%         0.00        0.03         0.02        0.00        0.00          0.00        0.00         84%
                   CIS-NONACHLOR                     0.46        0.00         NA          0.00        0.15         0.11        0.00        0.00          0.00        0.00         NA
                         ALDRIN                      0.00        0.00         99%         0.00        0.00         0.00        0.00        0.00          0.00        0.00         790/6
                       DIELDRIN                      0.10        0.00         96%         0.00        0.09         0.06        0.00        0.00          0.02        0.00         89%
                         ENDRIN                      0.00        0.00         102%        0.00        0.00         0.00        0.00        0.24          0.00        0.00         78%
                          MIREX                      0.00        0.00         870/6       0.00        0.00         0.00        0.00        0.00          0.00        0.00         53%
                   2,4'DDE (O.P'DDE)                 0.06        0.00         84%         0.00        0.00         0.00        0.00        0.00          0.00        0.00         820/6
                   4,4!DDE (P.P'DDE)                 3.91        0.13         1080/0      0.08        3.62         3.22        0.05        0.93          0.64        0.04         75%
                   2,4'DDD (O.P'DDD)                 1.05        0.00         101%        0.00        2.70         2.62        0.00        0.09          0.09        0.00         70%
                   4,4'DDD (P,P'DDD)                 12.77       0.00         105%        0.00        6.03         5.48        0.00        0.11          0.07        0.00         700/6
                   2,4'DDT (O,P'DDII                 0.13        0.00         94%         0.00        0.15         0.07        0.00        0.00          0.00        0.00         780/6
                   4,4'DDT (P,FDEM                   0.34        0.00         95%         0.00        0.57         0.19        0.00        0.00          0.00        0.00         1230/6
                       PCB#8(CL2)                    0.1         0.0          NA          0.0         0.0          0.1         0.0         0.0           0.0         0.0          NA
                       PCB# 18 (CL3)                 0.3         0.0          NA          0.0         1.3          0.8         0.0         0.0           0.0         0.0          NA
                       PCB#28(CL3)                   1.4         0.0          NA          0.0         1.2          1.5         0.0         0.7           0.0         0.0          NA
                       PCB#44 (CIA)                  3.5         0.0          NA          0.0         2.5          2.3         0.0         0.0           0.1         0.0          NA






                                                  Saint Johns River Core Pesticide and PCB Results - 1992


                   RAW FILE                Q3339P Q3345P Q3346P            Q3347P C3907P Q3348P Q3364P C3915P Q3365P Q3366P Q3367P
                     WETWr,.                 19.00      10.00     17.63      10.00      18.47       18.58     10.28      16.63       16.66     10.00     16.99
                     DRYWF:                  6.06       10.00      6.70      10.00      7.02        7.06      10.28      6.02        6.03      10.00       6.15
                   SAMP TYPE:              QA/QC BLANK           SPIKE       SAND       REP       QA/QC       SAND       ORIG      QA/QC BLANK           SPIKE
                        ID:               ofC3893P             ofC3907P     BLANK   X-3 32-33 of C3907P     BLANK    X-3 42-43 of C3915P               of C3915P
                      UNITS                  (ppb)      (ppb)   % Recov      (ppb)      (ppb)       (ppb)     (ppb)      (ppb)       (ppb)     (ppb)    % Recov
                  PCB#52 (CIA)               13.6       0.0        NA        0.0        26.3        23.4      0.0        0.0         0.2       0.0         NA
                  PCB#66 (CIA)               2.2        0.0        NA        0.0        0.9         1.1       0.0        0.0         0.0       0.0         NA
                  PCB#101 (CL5)              16.3       0.0        NA        0.0        14.0        13.1      0.0        2.6         2.6       0.0         NA
                  PCB#105 (CL5)              0.5        0.0        NA        0.0        0.0         0.0       0.0        0.0         0.0       0.0         NA
              PCB# 110/77 (CL5/4)            20.4       0.0        NA        0.0        5.7         5.2       0.0        1.0         0.8       0.0         NA
          PCB# 1 18/108/149(CL5/5/6)         11.8       0.0        NA        0.0        3.7         3.4       0.0        0.3         0.1       0.0         NA
                  PCB#128 (CL6)              2.4        0.0        NA        0.0        3.1         3.1       0.0        0.3         0.3       0.0         NA
                  PCB# 138 (CL6)             18.1       0.0        NA        0.0        2.1         2.1       0.0        0.3         0.0       0.1         NA
                  PCB# 126 (CL5)             0.0        0.0        NA        0.0        0.0         0.0       0.0        0.0         0.0       0.0         NA
                  PCB#153 (CL6)              55.1       0.0        NA        0.0        37.9        36.9      0.0        0.5         0.5       0.0         NA
                  PCB# 170 (CL7)             6.6        0.0        NA        0.0        5.9         5.7       0.6        0.3         0.8       0.2         NA
                  PCB# 180 (CL7)             11.0       0.0        NA        0.0        8.2         8.2       0.0        0.2         0.2       0.0         NA
     00 PCB#187/182/159(CL7/7/6)             8.2        0.0        NA        0.0        4.0         3.8       0.0        0.1         0.1       0.0         NA
                  PCB#195 (CL8)              1.5        0.0        NA        0.0        1.4         1.2       0.0        0.1         0.1       0.0         NA
                  PCB#206 (CL9)              1.8        0.0        NA        0.0        0.7         0.7       0.0        0.1         0.1       0.0         NA
                 PCB#209 (CLIO)              0.3        0.0        NA        0.0        0.2         0.2       0.0        0.3         0.3       0.0         NA



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                                               Antarctic Limpet Samples-Polar Programs- Aromatic Hydrocarbon Data


            INVEST#:               Station 4                   Station 3                  Station 12               Station 12                Station 13
            ID:                    Humble Island               Humble Island              Janus Island             Janus Island              Christine Is
            LABSAMNO:              J1292                       J1825                       J1289                    J1840                    J1312
            UNIT-                              ng/g                       ng/g                     ng/g                      ng/g                      ng/g
            PNA Analyte                        Conc DB QUAL               Conc DB QUAL             Conc DB QUAL              Cone DB QUAL              Conc DB QUAL

            SAMPLE TYPE:                       SAMP                       SAMP                     SAMP                      SAMP                      SAMP
            COLLECTION DATE:                   1989                       1991                     1989                      1991                   1989.00
            RECEIPT DATE:
            QCBATCH:                           M801                       M801                     M801                      M801                      M861
            EXTRACTION DATE:              03/04/93                   03/04/93                 03/04/93                  03/04/93             06/25/93
            METHOD:                            GCMS                       GCMS                     GCMS                      GCMS                      GCMS
            ANALYSIS DATE:                04/06/93                   04/06/93                 04/06/93                  04/06/93             07/25/93
            METHOD:                            GCECD                   GCECD                    GCECD                     GCECD                     GCECD
            ANALYSIS DATE:                05/03/93                   05/03/93                 05/03/93                  05/03/93                  08/02/93
            MATRIX                             TISSUE                  TISSUE                   TISSUE                    TISSUE                    TISSUE
            SUBMAT-
            SAMPLWT:
            WETWr:                             10.274                     8.613                    7.945                     9.764                     4.24
            DRYWn                                2.9                      1.78                     2.06                      2.18                      1.14
            WTUNITS:                           GRAMS                   GRAMS                    GRAMS                     GRAMS                     GRAMS
        OD
        0)  PCTSOLIDS:                         28.2%                      20.7%                    25.90/6                   22.3%                     0.27
            VOL.
            VOLUNITS:                          LITERS                  LITERS                   LITERS                    LITERS                    LITERS

            NAPHTHALENE                        10.96                      16.37                    65.42 Q                   11.33                     19.19
            CI-NAPHTHALENES                    74.88                      14.44                    74.39 Q                   8.90                      111.01
            C2-NAPHTHALENES                    176.30                     16.36                    0.00 Q                    14.12                     157.98
            C3-NAPHTHALENES,                   181.44                     22.34                    0.00  Q                   14.11                     141.65
            C4-NAPHTHALENES                    99.14                      17.27                    0.00  Q                   0.00 ND                   65.79
            BIPHENYL                             8.7                      3.18 J                   3.52 Q                    1.87 J                    7.36
            ACENAPHTHYLENE                     0.13 J                     0.31 J                   11.68 Q                   0.15 1                    0.22 J
            ACENAPHTHENE                       1.27 J                     1.16 J                   15.52 Q                   0.74 J                    1.52 J
            FLUORENE                           1.48 J                     0.91 J                   6.47 Q                    1.38 J                    4.72 J
            CI-FLUORENES,                      52.23                      13.09                    0.00 Q                    4.90 J                    36.85
            C2-F'LUORENES                      67.00                      60.56                    0.00  Q                   12.44                     88.96
            C3-FLUORENES,                      76.42                      59.33                    0.00  Q                   15.45                     85.24
            PHENANTHRENE                       208.37                     7.35                  2429.0   Q                   3.26 J                    205.24
            ANTHRACENE                         19.71                      4.63 J                    461 Q                     1.3 J                    17.00
            CI_pHEN_ANTHR                      249.23                     17.24                    0.00  Q                   9.52                      200.71






                                               Antarctic Limpet Samples-Polar Programs- Aromatic Hydrocarbon Data


            ENVES`r#:              Station 4                   Station 3                  Station 12               Station 12                Station 13
            ID:                    Humble Island               Humble Island               JanusIsland             Janus Island              Christine 18
            LABSAMNO:              J1292                      J1825                       J1289                    J1840                    J1312
            UNIT:                              ng/g                       ng/g                      ng/g                    ng/g                       ng/g
            PNA Analyte                        Conc DB QUAL               Conc DB QUAL              Conc DB QUAL            Conc DB QUAL               Conc DB QUALI

            C2-PHEN_ANTHR                   181-05                      13.26                       0.00 Q                  7.71                     121.01
            C3-PHEN._ANTHR                     92.23                    12.56                       0.00Q                   0.00   ND                  44.89
            C4-PHEN_ANTHR                      32.62                      0.00  ND                  0.00Q                   0.00   ND                  23.58
            DIBENZOTHIO                         1.4 J                     0.56 J                    867 Q                     1.2 J                    2.08 J
            CI-DIBEN                           8.48                       0.00 ND                   0.00Q                   0.00 ND                    0.00 ND
            C2-DIBEN                           20.74                      0.00 ND                   0.00Q                   0.00 ND                    0.00 ND
            C3-DIBEN                           19.32                      0.00  ND                  0.00Q                   0.00   ND                  0.00 ND
            FIXORANTHENE                       2.42 J                     1.15 J                  631.0 Q                   0.73 J                     0.82 J
            PYRENE                             1.57 J                     1.36 J                 1694.0 Q                     0.8 J                    2.57 J
            Cl-FLUORADLPYR                     23.52                      6.42 J                    0.00Q                   4.12 J                     0.00 ND
            BENaANTHRACENE                     1.59 J                     0.61 J                    5.13 Q                  0.09 1                     1.12 J
            CHRYSENE                           32.32                      1.34 J                    8.32 Q                    0.5 J                    25.03
            Cl-CHRYSENES                       17.92                      0.00 ND                   0.00 Q                  0.00 ND                    0.00 ND
            C2-CHRYSENES                       7.12                       0.00 ND                   0.00 Q                  0.00 ND                    0.00 ND
            C3-CHRYSENES                       0.00 ND                    0.00 ND                   0.00Q                   0.00 ND                    0.00 ND
       OD   C4-CHRYSENES                       0.00 ND                    0.00 ND                   0.00Q                   0.00 ND                    0.00 ND
        4   BENbFLUORAN                        0.39 J                     0.33 J                    5.23 Q                  0.11 J                     1.12 J
            BENkF'LUORAN                       0.41 J                     0.35 J                    5.55 Q                  0.12 J                     1.12 J
            BENePYRENE                         0.54 J                     0.32 J                       6 Q                    0.1 1                    6.32 J
            BENaPYRENE                         0.16 J                     0.38 J                    1.71 Q                  0.12 J                     2.68 J
            PERYLENE                           0.47 J                     0.62 J                    7.67 Q                  0.34 J                     1.64 J
            I123cdPYRENE                       0.16 J                     0.13 J                    3.51 Q                  0.23 J                     0.89 1
            DBahANTHRA                         0.111                      0.09 1                    7.25 Q                  0.41 J                     0.41 J
            BghIPERYLENE                       0.14 J                     0.33 J                    4.11 Q                  0.12 J                     1.34 J

            Total PAH's:                     1671.5                     293.7                    6305.8                     115.8                   1378.39
             (w/o Perylene)

            2-METHYLNAPH                       62.55                      8.88                      29.42 Q                 6.04                       92.26
            I-METHYLNAPH                       12.33                      5.56                      44.97 Q                 2.86 J                     18.74

            2,6-DIMETIINAPH                    122.91                     6.09                      14.6 Q                  4.46 J                   147.04

            2.3.5-TRIME-rENAPH                 43.75                      1.75 J                    16.96 Q                 0.66 J                     57.27






                                             Antarctic Limpet Samples-Polar Programs- Aromatic Hydrocarbon Data


            INVEST#:-              Station 4                  Station 3                 Station 12               Station 12               Station 13
            ID:                    Humble Island              Humble Island             Janus Island             Janus Island             Christine Is
            LABSAMNO:              J1292                      J1825                     J 1289                   J1840                    J1312
            UNM                              ng/g                       ng/g                     ng/g                     ng/g                     ng/g
            PNA Analyte                      Cone DB QUAL               Cone DB QUAL             Cone DB QUAL             Cone 1313 QUAL           Cone DB QUAL


            I-METHYLPHEN                       15.6                     3.26 J                    886 Q                   0.89 1                   12.16

            Surrogate Recoveries
            NAPHD8:                          92.2                       73.6                      1.2 Q                   65.5                     40.23
            ACENDIO:                         32.6                       75.4                      3.0 Q                   68.2                     38.74
            PHENDIO:                         73.9                       71.4                      0.0 Q                   61.9                     37.37
            CHRYD12:                         58.4                       55.5                      2.7 Q                   54.0                     36.55
            PERYD12:                         56.6                       55.7                      3.2 Q                   60.9                     23.34






       00
       00






                                                     Antarctic Limpet Samples-Polar Programs- Aromatic Hydrocarbon Data


                INVEST#:                  Station 13                 Station 20                   Station 20                   Transect D-7                  Transect D-7
                ID:                       Christine Is               Cormorant Is                 Cormorant Is                 Hermit Island                 Hermit Island
                LABSAMNO:                  J1842                      J1310                        J1850                       J1344                         J1866
                UNIT:                               ng/g                         ng/g                         ng/g                         ng/g                          ng/g
                PNA Analyte                         Conc DB QUAL                 Conc DB QUAL                 Conc DB QUAL                 Conc DB QUAL                  Conc DB gUAL

                SAMPLE TYPE:                        SAMP                         SAMP                         SAMP                         SAMP                          SAMP
                COLLECTION DATE:                    1991                         1989                         1991                         1989                          1991
                RECEIPT DATE:
                QCBATCH:                            M801                         M801                         M801                         M801                          M802
                EXTRACTION DATE:              03/04/93                     03/04/93                     03/04/93                     03/04/93                      03/04/93
                METHOD:                             GCMS                         GCMS,                        GCMS                         GCMS                          GCMS
                ANALYSIS DATE:                04/06/93                     04/06/93                     04/06/93                     04/06/93                      04/21/93
                METHOD:                         GCECD                            GCECD                    GCECD                        GCECD                         GCECD
                ANALYSIS DATE:                05/03/93                     05/03/93                     05/03/93                     05/03/93                      05/03/93
                MATRIX:                         TISSUE                           TISSUE                   TISSUE                       TISSUE                        TISSUE
                SUBMAT:
                SAMPLWT:
                WETVIT:                             10.991                       8.574                        9.341                        10.393                        10.135
                DRYW]r:                             2.46                         2.08                         2.18                         2.12                          1.78
                WTUNITS:                        GRAMS                            GRAMS                    GRAMS                        GRAMS                         GRAMS
          00
                PCTSOLIDS:                          22.4%                        24.3%                        23.30/6                      20.40/6                       17.60%
                VOL.
                VOLUNITS:                       LITERS                           LITERS                   LITERS                       LITERS                        LITERS


                NAPHTHALENE                         13.6                         14.81                        58.78                        12.26                         19.83
                Cl.-NAPH[THALENES                   13.33                        66.25                        39.84                        31.61                         13.52
                C2-NAPHTHALENES                     22.67                        165.80                       17.41                        45.28                         7.83 J
                C3-NAPHTHALENES                     22.56                        215.91                       17.17                        48.26                         12.29
                C4-NAPHTHALENES                     22.38                        116.03                       0.00 ND                      31.34                         0.00 ND
                BIPHENYL                            2.27 J                       5.85                         4.84 J                       3.04 J                        3.49 J
                ACENAPHTHYLENE                      0.17 J                       0.13 J                       0.42 J                       0.37 J                        0.23 J
                ACENAPHTHENE                         0.5 J                       1.12 J                       0.9 1                        1.33 J                        0.56 J
                FLUORENE                             0.9 1                       2.06 J                       0.61 J                       1. 18 1                       0.84 J
                Cl-FLUORENES                        22.92                        28.82                        4.04 J                       6.16  J                       0.00 ND
                C2-FLUORENES                        80.87                        115.74                       11.18                        27.64                         0.00 ND
                C3-FLUORENES                        76.90                        91.94                        14.53                        29.82                         0.00 ND
                PHENANTHRENE                        12.44                        254.48                       2.21 J                       50.67                          3.6 J
                ANniRPLCENE                         9.98                         26.1-5                       0.66 i                       7.4-3                         0. -3 i J
                Cl-PHEN-ANTHR                       33.24                        311.84                       4.59 J                       63.76                         0.00 ND



                                                                                                                                                                 Mao


                                             Antarctic Limpet Samples-Polar Programs- Aromatic Hydrocarbon Data


            INVEST#:               Station 13               Station 20               Station 20                Transect D-7               Transect D-7
            ID:                    Christine is             Cormorant Is             Cormorant Is               Hermit Island              Hermit Island
            LABSAMNO:              J1842                   J1310                     J1850                     J 1344                     J1866
            UNIT.                          ng/g                       ng/g                      ng/g                      ng/g                       ng/g
            PNA Analyte                    Conc DB QUAL               Conc DB QUAL              Conc 1313 QUAL            Conc 1313 QUAL             Conc 1313 QUAL

            C2-PHEN_ANTHR                 25.61                    209.46                       8.05 J                    42.19                      0.00
            C3-PHEN-ANTHR                  0.00   ND                  90.58                     10.76                     17.60                      0.00 ND
            C4-PHEN@ANTHR                  0.00   ND                  31.14                     8.10 1                    8.73                       0.00 ND
            DIBENZOTHIO                    0.26 J                     1.92 J                    0.64 J                    0.66 J                     0.41 J
            Cl.-DIBEN                      0.00 ND                    8.52 J                    0.00 ND                   3.77 J                     0.00 ND
            C2-DIBEN                       0.00 ND                    31.39                     0.00 ND                   6.18 J                     0.00 ND
            C3-DIBEN                       0.00   ND                  27.85                     0.00  ND                  0.00  ND                   0.00 ND
            FLUORANTHENE                   0.42 J                     2.77 J                    0.37 J                    0.75 J                     0.96 J
            PYRENE                         0.63 J                     2.46 J                    0.39 J                      0.7 J                    2.26 J
            Cl-FLUORAN-PYR                 9.56                       23.90                     4.89 J                    6.33 J                     0.00 ND
            BENaANTHRACENE                 0.09 j                     7.52                       0.2 J                      1.2 J                    0.27 J
            CHRYSENE                       1.36 J                       33                      0.44 J                    8.45                        0.3 J
            Cl.-CHRYSENES                  0.00 ND                    19.30                     0.00 ND                   6.34 ND                    0.00 ND
            C2-CHRYSENES                   0.00 ND                    7.96 ND                   0.00 ND                   4.73  ND                   0.00 ND
            C3-CHRYSENES                   0.00 ND                    0.00 ND                   0.00 ND                   0.00  ND                   0.00 ND
      'D    C4-CHRYSENES                   0.00 ND                    0.00 ND                   0.00 ND                   0.00  ND                   0.00 ND
            BENbFLUORAN                    0.21 J                     0.47 J                    0.05 J                    0.11 j                     0.14 J
            BENkF'LUORAN                   0.22 J                      0.5 1                    0.05 1                    0.12 J                     0.14 J
            BENePYRENE                     0.28 J                     0.16 J                     0.1 J.                   0.21 J                     0.43 J
            BENaPYRENE                     0.18 j                     0.18 j                    0.16 J                    0.05 J                     0.24 J
            PERYLENE                       0.47 J                     0.55 J                    0.42 J                    0.45 J                      0.4 J
            1123cdPYRENE                    0.1 j                     0.16 J                    0.12 J                    0.18 1                     0.44 J
            DBahAN-l7HRA                   0.09 j                     0.06 J                    0.54 J                      0.1 1                    0.05 1
            BghlPERYLENE                   0.23 J                     0.28 J                    0.34 J                      0.2 J                    0.86 J

            Total PAH's*                  374.0                     1916.5                      212.4                     468.8                      69.0
             (w/o Perylene)

            2-METHYLSAPH                   10.43                      54.43                     26.24                     24.88                      8.62
            1-METHYLNAPH                    2.9 J                     11.82                     13.6                      6.73                        4.9 J

            2,6-DIMETHNAPH                 8.34                       105.48                    5.08                      29.43                      3.64 J
                                                                                                                                                                U]AL










            2,3,5-TRIMETHNAPH              1.09 1                     42.4                      1.43 J                    10.47                      1.42 J






                                               Antarctic Limpet Samples-Polar Programs- Aromatic Hydrocarbon Data


             INVEST#:                Station 13               Station 20                Station 20                Transect D-7               Transect D-7
             ID:                     Christine Is             Cormorant Is              Cormorant Is              Hermit Island              Hermit Island
             LABSAMNO:               J1842                    J1310                     J1850                     J1344                      J1866
             UNIT:                           ng/g                      ng/g                       ng/g                       ng/g                       ng/g
             PNA Analyte                     Conc DB QUAL              Cone DB QUAL               Conc DB QUAL               Conc DB QUAL               Conc DB QUALI


             I-METfMPHEN                     0.85 J                    15.86                      0.55 J                     4.21 J                     0.42 J

             Surrogate Recoveries
             NAPHD8:                         55.4                      70.9                       73.5                       77.9                       73.8
             ACEND10:                        60.2                      78.5                       72.8                       79.7                       65.4
             PHEND10:                        57.5                      77.2                       67.2                       73.8                       64.5
             CHRYD12:                        46.7                      58.0                       54.3                       59.5                       58.7
             PERYD12:                        44.7                      70.2                       60.5                       65.0                       47.2








        CD




                                                      M MM M = M M soft --


                                                  Antarctic Limpet Samples-Polar Programs- Aromatic Hydrocarbon Data


              INVEST#:                Transect D- 11              Transect D- 11             Transect D- 12              Transect D- 12              Transect D- 13
              ID:                     0' Palmer Sta.              54' Palmer Sta              0' Palmer Sta.             62' Palmer Sta              0' Palmer Sta
              LABSAMNO:               J 1871                      J 1872                      J1875                      J 1876                      J1881
              UNIT.                              ng/g                        ng/g                        ng/g                        ng/g                       ng/g
              PNA Analyte                        Cone DB QUAL                Cone DB QUAL                Cone DB QUAL                Cone DB QUAL               Cone DB QUAL

              SAMPLE TYPE:                       SAMP                        SAMP                        SAMP                        SAMP                       SAMP
              COLLECT10N DATE:                   1991                        1991                        1991                        1991                       1991
              RECEIPT DATE:
              QCBATCH:                           M802                        M802                        M802                        M802                       M802
              EXTRACTION DATE:              03/04/93                    03/04/93                   03104/93                    03/04/93                    03104/93
              METHOD:                            GCMS                        GCMS                        GCMS                        GCMS                       GCMS
              ANALYSIS DATE:                04/21/93                    04/21/93                    04/21/93                   04/21/93                    04/22/93
              METHOD:                         GCECD                       GCECD                      GCECD                       GCECD                       GCECD
              ANALYSIS DATE:                05/03/93                    05/03/93                   05/03/93                    05/03/93                    05/03/93
              MATRIX:                         TISSUE                      TISSUE                     TISSUE                      TISSUE                      TISSUE
              SUBMAT:
              SAMPLWT-.
              WFTWT.                             10.005                      10.358                      4.194                       10,086                        10
              DRYWT.                             2.15                        2.81                        0.91                        2.01                       2.06
              WrUNITS:                        GRAMS                       GRAMS                      GRAMS                       GRAMS                       GRAMS
           W PCTSOLIDS:                          21.50A                      27.1%                       21.r,,6                     19.90/0                    20.6%
              VOL.
              VOLUNqT`S:                      LITERS                      LITERS                     LITERS                      LITERS                      LITERS


              NAPHTHALENE                        21,94                       9.95                        24.1                        21.65                      53.92
              CI-NAPH7`HALENBS.                  29.71                       11.50                       24.95                       18.64                   207.01
              C2-NAPHTHALENES                    30.04                       5.45 J                      22.12                       8.90  1                 299.36
              C3-NAPHTHALENES                    28.75                       7.72 J                      26.65                       13.55                   391.80
              C4-NAPHTHALENES                    23.31                       3.77 J                      16.27                       6.87  J                 313.62
              BIPHENYL                            2.9 J                        1.6 j                     4.72 J                      3.9 J                      27.11
              ACENAPHTHYLENE                     0.35 J                      0.09 j                      0.31 J                      0.25 J                     1.12 J
              ACENAPHTHENE                       0.57 J                      0.25 J                      0.62 J                      0.25 J                     4.12 J
              FLUORENE                             1.1 j                      0.6 J                      1.15 1                      1.12 J                     9.68
              CI-FLUORENES                       8.63 J                      4.20 J                      7.89 J                      8.37 J                     46.71
              C2-FLUORENES                       45.13                       10.69                       28.16                       14.71                   142.20
              C3-FLUORENES                       29.86                       0.00 ND                     18.53                       0.00 ND                 144-53
              PHENANTHRENE                       15.06                       3.62 J                      13-62                       5.42 J                     18L51
              ANTHRACENE                         3.98 J                      1,14 J                      3.03 J                      0.58 J                     11.96
              Cl-PHEN-ANTHR                      20.23                       8.73                        12.03                       7.92 J                  221.05






                                                Antarctic Limpet Samples-Polar Programs- Aromatic Hydrocarbon Data


            INVEST#:                Transect D- I I             Transect D- 11              Transect D- 12              Transect D- 12               Mransect D- 13
            ID:                     0' Palmer Sta,              54' Palmer Sta              0' Palmer Sta               62' Palmer Sta               0' Palmer Sta
            LABSAMNO:               J1871                       J1872                       J1875                       J1876                        J1881
            UNIT:                              ng/g                         ng/g                        ng/g                        ng/g                        ng/g
            PNA Analyte                        Conc DB QUAL                 Conc DB QUAL                Conc DB QUAL                Conc DB QUAL                Conc DB QUAL

            C2-PFIEN@ANTFIR                   12.10                         4.45 J                      6.89 J                      5.08 1                      170.81
            C3-PHEN-ANMR                       7.72   J                     0.00  ND                    6.37  J                     7.15  J                     79.49
            C4-PHEN_ANTHR                      4.43   J                     0.00  ND                    0.00  ND                    0.00  ND                    30.71
            DIBENZOTHIO                        0.53 J                        0.2 J                       0.5 J                      0.44 J                      5.57
            CI-DIBEN                           1.77 J                       0.67 J                      1.28 J                      1.09 j                      37.20
            C2-DIBEN                           1.99 1                       0.00 ND                     2.22 J                      2.06 J                      88.24
            C3-DIBEN                           1.88   1                     0.00  ND                    0.00  ND                    1.05  j                     60.76
            FLUORAN71HENE                      1.25 J                       0.68 J                      1.32 J                      0.56 J                      2.61 J
            PYRENE                               1.9 1                      1.18 1                      2.73 J                      1.24 J                      5.31
            Cl-FLUORAN-PYR                     3.33 J                       0.00 ND                     0.00 ND                     0.00 ND                     15.47
            BENaANTFiRACENE                    0.52 J                       0.28 J                      0.47 J                      0.29 J                      1.82 J
            CHRYSENE                           2.72 J                       0.99 1                      1.21 J                      0.53 J                      14.93
            CI-CHRYSENBS                       0.00 ND                      0.00 ND                     0.00 ND                     0.00 ND                     4.73 J
            C2-CHRYSENES                       0.00 ND                      0.00 ND                     0.00 ND                     0.00 ND                     5.22 J
            C3-CHRYSENES                       0.00 ND                      0.00 ND                     0.00 ND                     0.00 ND                     0.00 ND
            C4-CHRYSENES                       0.00 ND                      0.00 ND                     0.00 ND                     0.00 ND                     0.00 ND
            BENbFLUORAN                        0.47 J                       0.29 J                      0.42 J                      0.13 J                      2.09 J
            BENkFLUORAN                        0.46 J                       0.28 J                      0.42 J                      0.13 J                      2.08 J
            BENePYRENE                         0.37 J                       0.23 J                      0.44 J                      0.15 1                      1.03 J
            BENaPYRENE                           0.2 J                      0.15 j                       0.3 J                      0.07 J                      0.38 J
            PERYLENE                           0.28 J                       0.83 J                      0.93 J                       0.4 J                       1.5 j
            1123cdPYRENF,                      0.34 J                       0.27 J                      0.47 J                      0.22 J                      1.36 J
            DBahANTHRA                         0.14 J                       0.03 J                       0.2 J                      0.09 j                      0.41 J
            BghIPERYLENE                       0.37 J                       0.43 J                      0.66 J                      0.37 J                      1.66 J

            Total PAH's:                      304.1                         79.4                      230.1                        132.8                        2587.6
             (w/o Perylene)


            2-METHYINAPH                       19.45                        7.13                        16.47                       11.91                       160.57
            1 -METHYLNAPH                      10.26                        4.37 J                      8.48                        6.73                        46.44


            2.6-DIMETHNAPH                     17.13                        2.57 J                      11.36                       4.64 J                      188.59


            2,3,5-TRIME'niNAPH                 7.18                         1.26 J                      4.33 J                      2.36 J                      98.55






                                                Antarctic Limpet Samples-Polar Programs- Aromatic Hydrocarbon Data


            INVEST#:                Transect D- I I             Transect D- I I             Transect D- 12             Transect D- 12               Transect D- 13
            ID:                     0' Palmer Sta               54' Palmer Sta              0' Palmer Sta              62' Palmer Sta               0' Palmer Sta.
            LhBSAMNO:               J 1871                      J 1872                      J 1875                     J 1876                       11881
            UNM.                               ng/g                        ng/g                        ng/g                        ng/g                       ng/g
            PNA Analyte                        Conc DB QUAL                Conc DB QUAL                Conc DB QUAL                Conc DB QUAL               Conc DB QUAL


            I-METIMPHEN                        5.78                        0.63 J                      4.33 J                      0.82 J                     21.62


            Surrogate Recovertes
            NAPHD8:                            73.7                        92.2                        69.2                        86.2                       77.6
            ACENDIO:                           67.8                        72.7                        65.5                        74.3                       72.3
            PHENDIO:                           71.2                        71.0                        69.7                        77.0                       72.2
            CHRYD12:                           59.2                        67.4                        58.9                        67.9                       69.5
            PERYD12:                           45.1                        44.1                        37.5                        35.6                       42.2






                                                Antarctic Urnpet Sarnples-Polar Programs- Aromatic Hydrocarbon Data

            RVEM:                   Transect D- 13              Transect D- 14            Transect D-14               Transect D- 17             Tmnsecf -D- 17
            ID:                     3 V Palmer Sta              O'Old Palmer              30' Old Palmer              01                         60-62'
            LABSAMNO:               J1880                      J1887                      J1883                      J1893                       J1896
            UNIT.                              ng/g                       ng/g                       ng/g                       ng/g                       ng/9
            ,PNA. Analyte                      Cone 1313 QUAL             Cone DB gUAL               Cone DB QUAL               Cone DB QUAL               Cone DB QUALI
            SAMME TYPE:                        SAMP                       SAMP                       SAMP                       SAMP                       SAMP
            COLLECTION DATE:                   1991                       1991                       1991                       1991                       1991
            RECEIPT DATE:
            gCBATCH:                           M802                       M803                       M802                       M803                       M803
            EXT'RACTION DATE:             03/04/93                   03/05/93                   03/04/93                   03/05/93                    03/05/93
            METHOD:                            GCMS                       GCMS                       GCMS                       GCMS                       GCMS
            ANALYSIS DATE:                04/21/93                   04/07/93                   04/22/93                   04/07/93                    04/07/93
            METHOD:                         GCECD                      GCECD                      GCECD                      GCECD                       GCECD,
            ANALYSIS DATE:                05/03/93                   05/03/93                   05/03/93                   05/03/93                    05/03/93
            MATRIX                          TISSUE                     TISSUE                     TISSUE                     TISSUE                      TISSUE
            SUBMAT.,
            SAMPLWn
            WETWT.,                            10.629                     3.744                      10.041                     4.006                      9.939
            DRYWT.                             2.18                         0.7                      1.92                       0.88                       2.66
            V,-rLTNnS-                      GRAMS                      GRAMS                      GRAMS                      GRAMS                       GRAMS
            PCTSOLIDS:                         20.5%                      18.7%                      19.1%                      22.0%                      26.8%
            VOL,
            VOLUNrrS:                       LITERS                     LITERS                     LITERS                     LITERS                      LITERS

            NAPHTHALENE                        10.96                      87.36                      11.07                      65.89                      10.33
            CI-NAPHTHALENES                    10-88                      70.74                      10.28                      57.32                      10.96
            C2-NAPHTHALENES                    11.30                      38.30                      6.92  J                    40.35                      7.16  J
            C3-NAPHTHALENES                    15.53                      54.15                      11.19                      50.63                      10.59
            C4-NAPHTHALENES                    10@29                      42.80                      6.11  J                    28.79                      0.00  ND
            BIPHENYL                           2.29 J                  103.67                        2.08 J                     46.47                      7.76
            ACENAPHTHYLENE                     0.31 1                     3.70 J                     0.17 J                     1.99  j                    0.29  J
            ACENAPHTHENE                       0.32 J                     3.41 J                     0.53 J                     1.95  J                    1.26  J
            FLUORENE                           0.54 J                     4.83 J                     0.66 J                     7.82                       1.48  J
            Cl-FLUORENES                       4.65 J                     17.66                      0.00 ND                    23.86                      4.11  J
            C2-FLUORENES                       14.94                      45.99                      0.00 ND                    65.78                      6.91  1
            C3-FLUORENES                       13.76                      59.91                      0.00 ND                    53.72                      0.00  j
            PHENANTHRENE                       11.53                      26.52                      7.53                       20.10                      1.83  J
            ANTHRACENE                         2.37 J                     7.66                       ?-*33 JJ                   ii.si                      L96   j
            CI-PHEN@ANTHR                      8.61 J                     26.08                      8.16 J                     29.74                      5.27  J



   M M M M M M M M M M M M M M M M M M M

                                              Antarctic Limpet Samples-Polar Programs- Aromatic Hydrocarbon Data


          INVEST#:               Transect D- 13              Transect D- 14             Transect D- 14             Transect D- 17             Transect D- 17
          ID:                    3 1' Palmer Sta             O'Old Palmer               30'Old Palmer              0,                         60-62'
          LABSAMNO:              J1880                       J 1887                     J1883                      J1893                      J1896
          UNIT.                              ng/g                      ng/g                        ng/g                      ng/g                       ng/g
          PNA Analyte                        Cone DB QUAL              Cone DB QUAL                Cone DB QUAL              Cone DB QUAL               Cone DB QUAL,

          C2-PHEN-ANMR                       6.38 J                   21.01                        7.69 J                   22.15                       0.00  ND
          M-PHEN@ANTHR                       5.00  1                   0.00  ND                    0.00  ND                 25.81                       0.00  ND
          C4-PHEN@ANMR                       2.43  J                   0.00  ND                    0.00  ND                  0.00  ND                   0.00  ND
          DIBENZOTHIO                         0.3 J                    4.30  J                     0.24 J                    2.18  J                    0.53  J
          CI-DIBEN                           0.99 1                    0.00  ND                    0.00 ND                   0.00  ND                   0.00  ND
          C2-DIBEN                           1.60 J                    0.00  ND                    0.00 ND                   0.00  ND                   0.00  ND
          C3-DIBEN                           1.52  J                   0.00  ND                    0.00  ND                  0.00  ND                   0.00  ND
          FLUORANTHENE                       1.08 1                    4.50  J                     2.09 J                    3.88  J                    0.57  J
          PYRENE                             1.59 1                    4.52  J                     2.56 J                    3.62  J                    0.90  1
          Cl-FLUORAN-PYR                     1. 53 J                  13.55                        1.98 1                   10.38                       0.00  ND
          BENaANTHRACENE                     0.97 J                    6.32                        1.99 1                    4.34  J                    0.52  J
          CHRYSENE                           2.57 J                   12.33                        3.96 J                    6.57                       0.93  J
          Cl-CHRYSENES                       0.00 ND                   0.00  ND                    0.00 ND                   0.00  ND                   0.00  ND
          C2-CHRYSENES                       0.00 ND                   0.00  ND                    0.00 ND                   0.00  ND                   0.00  ND
      (D C3-CHRYSENES                        0.00 ND                   0.00  ND                    0.00 ND                   0.00  ND                   0.00  ND
      0) C4-CHRYSENES                        0.00 ND                   0.00  ND                    0.00 ND                   0.00  ND                   0.00  ND
          BENbFLUORAN                         0.6 J                    4.21  J                     1.34 J                    2.98  J                    0.33  J
          BENkFLUORAN                        0.59 J                    4.47  J                     1.33 J                    3.16  J                    0.35  J
          BENePYRENE                         0.28 J                    2.27  J                     0.77 J                    2.48  J                    0.41  J
          BENaPYRENE                         0.21 J                    2.88  J                     0.63 J                    1.86  1                    0.51  J
          PERYLENE                           0.86 J                   46.84                        0.59 J                   21.99                       3.62  J
          1123cdPYRENE                       0.35 J                    2.80  J                     0.78 J                    2.39  J                    0.22  J
          DBahANTHRA                         0.19 1                    2.82  J                      0.1 1                    1.99  j                    0.27  J
          BghIPERYLENE                       0.44 J                    2.74  J                      0.8 1                    1.95  J                    0.41  J

          Total PAITs:                      146.9                     681.5                        93.3                     601.7                       75.9
           (w/o Perylene)

          2-METHYLSAPH                        7.1                     45.46                        6.53                     38.02                       7.27
          I-METHYLNAPH                       3.78 J                   25.28                        3.75 J                   19.30                       3.69 J

          2.6-DIMETHNAPH                     5.73                     26.70                            3J                   20.01                       3.50 1

          2.3.5-TRIMETHNAPH                  3.45 J                    6.73                        1.38 J                    6.86                       1.22 J






                                               Antarctic Limpet Samples-Polar Programs- Aromatic Hydrocarbon Data


           INVEST#:                Transect D- 13              Transect. D- 14            Transect D- 14              Transect. D- 17             Tmnsect D- 17
           ID:                     3 1' Palmer Sta             0' Old Palmer               30' Old Palmer              0,                         60-62'
           LABSAMNO:               J1880                       J1887                      J1883                       J1893                       J1896
           UNIT.                              ng/g                        ng/g                        ng/g                       ng/g                        ng/g
           PNA Analyte                        Conc 1313 QUAL              Conc DB QUAL                Conc DB QUAL               Cone DB QUAL                Cone DB QUAL


           I-METHYLPHEN                       0.86 J                      7.53                        0.59 J                     11.41                       1.55  J

           Surrogate Recoveries
           NAPHD8:                            73.4                        58.4                        71.9                       59.7                        65.3
           ACEND10:                           68.5                        52.8                        68.6                       59.2                        65.8
           PHEND10:                           67.3                        46.0                        74.5                       60.9                        63.2
           CHRYD12:                           65.8                        38.6                        69.2                       45.7                        47.0
           PERYD12:                           33.2                        34.8                        63.4                       40.2                        47.0






                                                Antarctic Limpet Samples-Polar Programs- Aromatic Hydrocarbon Data


          INVEST#:                 Transect D- 19              Transect D- 19              Transect D-7               Transect D-7                    Station 12
          ID:                      0' Palmer Sta               42' Palmer Sta              Hermit Island               18' Hermit Island              Janus Island
          LABSAMNO:                J1882                       J1886                       J1866                      J1865                            J1840
          UNIT-                               ng/g                        ng/g                        ng/g                           ng/g                       ng/g
          PNA Analyte                         Conc DB QUAL                Conc DB QUAL                Conc DB QUAL                   Conc DB QUAL               Conc DB QUAL

          SAMPLE TYPE:                        SAMP                        SAMP                        SAMP                           SAMP                       SAMP
          COLLECTION DATE:                    1991                        1991                        1991                           1991                       1991
          RECEIPT DATE:
          QCBATCH:                            M802                        M802                        M802                           M801                       M801
          EXI*RAC1ION DATE:              03/04/93                    03/04/93                    03/04/93                       03/04/93                  03/04/93
          METHOD:                             GCMS                        GCMS                        GCMS                           GCMS                       GCMS
          ANALYSIS DATE:                 04/22/93                    04/22/93                    04/21/93                       04/06/93                  04/06/93
          METHOD:                          GCECD                       GCECD                      GCECD                          GCECD                      GCECD
          ANALYSIS DATE:                 05/03/93                    05/03/93                    05/03/93                       05/03/93                  05/03/93
          MATRIX-                          TISSUE                      TISSUE                     TISSUE                         TISSUE                     TISSUE
          SUBMAT-
          SAMPLW.
          WETWT.                              10.184                      10.116                      10.135                         8.253                      9.764.
          DRYWT-.                               2.1                         2.5                       1.78                           1.47                       2.18
        '""WTUNITS:                        GRAMS                       GRAMS                      GRAMS                          GRAMS                      GRAMS
         (0
        ODPCTSOIADS:                          20.6%                       24.7%                       17.60A                         17.8%                      22.3%
          VOL.,
          VOLUNITS:                        LITERS                      LITERS                     LITERS                         LITERS                     LITERS


          NAPHTHALENE                         15.59                       11.64                       19.83                          19.7                       11.33
          C I -NAPHTHALENES                   19.38                       12.97                       13.52                          14.73                      8.90
          C2-NAPHTHALENES                     22-06                       10.84                       7.83  J                        17.01                      14.12
          C3-NAPHTHALENES,                    24.15                       15.10                       12.29                          23.46                      14.11
          C4-NAPHTHALENES                     16.11                       7.30  J                     0.00  ND                       0.00 ND                    0.00 ND
          BIPHENYL                            2.19 J                      3.13 J                      3.49 J                         3.91 J                     1.87 J
          ACENAPHTHYLENE                      0.82 J                      0.16 J                      0.23 J                         0.53 J                     0.15 J
          ACENAPHTHENE                        0.45 J                      0.38 J                      0.56 J                          2.1 J                     0.74 J
          FLUORENE                            1.39 J                      0.46 J                      0.84 J                          1.7 J                     1.38 1
          CI-FLUORENES,                       64.93                       7.32 J                      0.00 ND                        6.44 J                     4.90 J
          C2-FLUORENES                        0.00 ND                     0.00 ND                     0.00 ND                        13.22                      12.44
          C3-FLUORENES                        0.00 ND                     0.00 ND                     0.00 ND                        26.12                      15.45
          PHENANTHRENE                        21-05                       5.48                         3.6 J                         3.39 J                     3.26 J
          ANTHRACENE                          3.57 J                      0.74 J                      0.31 J                         1.28 J                      1.3 J
          Cl-PHEN_ANTHR                       27-31                       6.98 J                      0.00 ND                        6.44 J                     9.52






                                                 Antarctic I.Ampet Samples-Polar Programs- Aromatic Hydrocarbon Data


            tNVEST#:                Transect D- 19             Transect D-19               Transect D-7               Transect D-7                   Station 12
            ID:                     O'Palmer Sta               42' Palmer Sta              Hermit Island               18'Herndt Island              Janus Island
            LABSAMNO:               J1882                      J1886                       J1866                      J1865                          J1840
            UNIT:                              ng/g                        ng/g                       ng/g                           ng/g                      ng/g
            PNA Analyte                        Conc DB gUAL                Cone DB gUAL               Conc DB QUAL                   Cone DB gUAL              Cone DB QUAL

            MPHEN@ANTHR                      18.48                         5.06 J                     0.00 ND                        9. 53 J                   7.71
            C3-PHEN-ANTHR                    21.19                         0.00 ND                    0.00 ND                        0.00 ND                   0.00 ND
            C4-PHEN_ANTHR                    11.42                         0.00 ND                    0.00 ND                        0.00 ND                   0.00 ND
            DIBENZOTHIO                        0.35 J                      0.44 J                     0.41 J                         0.56 J                     1.2 J
            CI-DIBEN                           0.00 ND                     1. 15 J                    0.00 ND                        0.00 ND                   0.00 ND
            C2-DIBEN                           0.00 ND                     0.00 ND                    0.00 ND                        0.00 ND                   0.00 ND
            C3-DIBEN                           0.00  ND                    0.00 ND                    0.00 ND                        0.00 ND                   0.00 ND
            FLUORANTHENE                       1.12 J                      0.82 J                     0.96 J                         0.87 J                    0.73 J
            PYRENE                             1.74 J                       1.2 J                     2.26 J                         0.77 J                     0.8 J
            Cl-FLUORAN-PYR                     4.86 J                      0.00 ND                    0.00 ND                        5.09 J                    4.12 J
            BENaANTHRACENE                     0.96 J                      0.31 J                     0.27 J                         0.42 J                    0.09 J
            CHRYSENE                           1.97 J                      1.55 J                      0.3 J                         1.11 J                     0.5 J
            CI-CHRYSENES                       0.00 ND                     0.00 ND                    0.00 ND                        0.00 ND                   0.00 ND
            C2-CHRYSENES                       0.00 ND                     0.00 ND                    0.00 ND                        0.00 ND                   0.00 ND
          i.,C3-CHRYSENES                      0.00 ND                     0.00 ND                    0.00 ND                        0.00 ND                   0.00 ND
          tOC4-CHRYSENES                       0.00 ND                     0.00 ND                    0.00 ND                        0.00 ND                   0.00 ND
          CDBENbFLUORAN                        0.33 J                      0.45 J                     0.14 J                         0.14 J                    0.111
            BENkFLUORAN                        0.33 J                      0.44 J                     0.14 J                         0.15 J                    0.12 J
            BENeFYRENE                         0.45 J                      0.32 J                     0.43 J                         0.19 j                     0.1 1
            BENaPYRENE                         0.37 J                      0.15 1                     0.24 J                         0.33 J                    0.12 J
            PERYIENE                           0.53 J                      0.75 J                      0.4 J                         0.41 J                    0.34 J
            1123edPYRENE                       0.27 J                      0.43 J                     0.44 J                         0.13 J                    0.23 J
            DBahANTHRA                         0.12 J                      0.15 J                     0.05 J                         0.52 J                    0.41 J
            BghlPERYLENE                       0.42 J                      0.33 J                     0.86 J                         0.23 J                    0.12 J

            Total PAH's:                     283.4                         95.3                       69.0                          160.1                    11518
             (w/o Perylene)

            2-METHYMAPH                        14.42                       8.07                       8.62                           9.11                      6.04
            I-METHYLNAPH                       4.96 J                       4.9 J                      4.9 J                         5.62                      2.86 J

            2.6-DIMMNAPH                       12.02                       4.93 J                     3.64 J                         5.52                      4.46 J

            2.3,5-TRIMETHNAPH                  3.37 J                      2.91 J                     1.42 J                         2.74 J                    0.66 J



    M M M M M M M M M M M M M M M M M M M

                                             Antarctic Limpet Samples-Polar Programs- Aromatic Hydrocarbon Data


           INVEST#:              Transect D- 19            Transect D- 19            Transect D-7              Transect. D-7                 Station 12
           ID:                   0' Palmer Sta             42' Palmer Sta             Hermit Island             18' Hermit Island            Janus Island
           LABSAMNO:             J 1882                    J 1886                    J1866                     J1865                         J1840
           UNM                             ng/g                       ng/g                      ng/g                        ng/g                      ng/g
           PNA Analyte                     Conc DB QUAL               Conc DB QUAL              Conc DB QUAL                Conc DB QUAL              Conc DB QUAL



           I-METHYLPHEN                    2.65 J                     0.51 J                    0.42 J                       1.28 J                   0.89 J


           Surrogate Recoveries
           NAPHD8:                         69.1                       71.4                      73.8                        67.7                      65.5
           ACENDIO:                        64.5                       66.3                      65.4                        66.3                      68.2
           PHENDIO:                        62.8                       68.7                      64.5                        64.4                      61.9
           CHRYD12:                        64.6                       68.4                      58.7                        53.3                      54.0
           PERYD12:                        54.3                       59.6                      47.2                        50.2                      60.9








        0
       0






                                             Antarctic Limpet Samples-Polar Programs- Aromatic Hydrocarbon Data


                INVEST#:              Transect D- 14                    LAB QA SAMPLE                LAB QA SAMPLE               LAB gA SAMPLE
                ID:                   ANTARC NIST M801                  Station 12                   PROC BLANK                  Station 12
                LABSAMNO:              Q4882                            Q4883                        Q4884                       g4885
                UNIT:                                    ng/g                        ng/g                         ng/g                        ng/g
                PNA Analyte                              Conc DB gUAL                Conc DB gUAL                 Conc DB gUAL                Conc DB

                SAMPLE TYPE:                             SRM               DUP OF J 1840                          BLK                NIS OF J 1840
                COLLECTION DATE:
                RECEIPT DATE:
                QCBATCH:                                 M801                        M801                         M801                        M801
                EXTRACTION DATE:                    03/04/93                     03/04/93                    03/04/93                     03/04/93
                METHOD:                                  GCMS                        GCMS,                       GCMS,                        GCMS,
                ANALYSIS DATE:                      04/06/93                     04/06/93                    04/06/93                     04/06/93
                METHOD:                               GCECD                       GCECD                        GCECD                       GCECD
                ANALYSIS DATE:                      05/03/93                     05/03/93                    05/03/93                     05/03/93
                MATRIX:                               TISSUE                      TISSUE                       TISSUE                      TISSUE
                SUBMAT.-
                SAMPLWT:
                WETWT-                                   5.049                       9.614                           10                       9.896
                DRYWT:                                   0.67                        2.04                            10                       2.14
         t%D    WTUNITS:                              GRAMS                       GRAMS                        GRAMS                       GRAMS
         0      PCTSOLIDS:                               13.3%                       21.2%                     100.0016                       21.60/6
         @.w
                VOL:
                VOLUNITS:                             LITERS                      LITERS                       LITERS                      LITERS


                NAPHTHALENE                              21.02                       12.56                        0.97 J                      61.51
                CI-NAPHTHALENES                          23.76 J                     9.64                         0.95 j                   135.63
                C2-NAPHMFIALENES                         42.97                       13.39                        0.00 ND                     0.00
                C3-NAPHTHALENES                          79.27                       0.00 ND                      0.00  ND                    0.00
                C4-NAPHTHALENES                       180.22                         0.00 ND                      0.00  ND                    0.00
                BIPHENYL                                 6.28 J                      2.21 J                       0.43 J                      46.14
                ACENAPHTHYLENE                           7.06 J                       0.2 J                       0.02 J                      43.59
                ACENAPHTHENE                             9.55 J                      0.79 J                       0.15 j                      44.52
                FLUORENE                                 8.45 J                       0.5 j                       0.11 1                      43.3
                CI-FLUORENES                             37.06                       5.67 J                       0.00 ND                     0.00
                C2-FLUORENES                          157.95                         17.77                        0.00 ND                     0.00
                C3-FLUORENES                          273.55                         19.24                        0.00 ND                     0.00
                PHENANTHRENE                             32.7                        3.65 J                       0.19 j                      45.4
                ANTHR,kCENE                              i3.63 i                     0.89 J                       0.06 J                      14 S. 7
                Cl-PHEN-ANTHR                            76.26                       7.86 J                       0.00 ND                     0.00






                                              Antarctic Limpet Samples-Polar Programs- Aromatic Hydrocarbon Data


                INVESTC                Transect D- 14                     LAB QA SAMPLE                LAB QA SAMPLE                 LAB QA SAMPLE
                ID:                    ANTARC NIST M801                   Station 12                   PROC BLANK                    Station 12
                LABSAMNO:               Q4882                             Q4883                        Q4884                         Q4885
                UNIT:                                     ng/g                          ng/g                         ng/g                         ng/g
                [fNA Analyte                              Conc DB QUAL                  Conc DB QUAL                 Conc DB QUAL                 Conc DB QUAL

                C2-PHEN  -ANTHR                           239.64                        6.84 J                       0.00 ND                      0.00
                C3-PHEN  -ANTHR                           393.59                        0.00 ND                      0.00 ND                      0.00
                C4-PHEN-ANTIiR                            165.99                        0.00 ND                      0.00 ND                      0.00
                DIBENZOTHIO                               5.06 J                        1.21 J                        0.1 1                       38.01
                CI-DIBEN                                  34.76                         0.00 ND                      0.00 ND                      0.00
                C2-DIBEN                                  151.48                        0.00 ND                      0.00 ND                      0.00
                C3-DIBEN                                  171.21                        0.00 ND                      0.00 ND                      0.00
                FLUORANTHENE                              211.31                        0.63 J                       0.04 J                       45.11
                PYRENE                                    209.34                        0.96 J                       0.07 J                       43.47
                Cl-FLUORAN-PYR                            136.42                        5.96 J                       0.00 ND                      0.00
                BENaANTHRACENE                            36.34                         0.44 J                       0.05 1                       53.24
                CHRYSENE                                  112.02                        0.83 J                       0.03 J                       52.55
                CI-CHRYSENES                              78.50                         0.00 ND                      0.00 ND                      0.00
                C2-CHRYSENES                              46.15                         0.00 ND                      0.00 ND                      0.00
                C3-CHRYSENES                              6.20  J                       0.00 ND                      0.00 ND                      0.00
                C4-CHRYSENES,                             13.13 J                       0.00 ND                      0.00 ND                      0.00
                BENbFLUORAN                               33.16                          0.2 J                       0.04 J                       47.09
                BENkFLUORAN                               35.21                         0.21 J                       0.04 J                       50.02
                BENePYRENE                                71.48                         0.27 J                       0.02 J                       50.96
                BENaPYRENE                                14.95                         0.26 J                       0.03 J                       46.46
                PERYLENE                                  8.28 J                        0.55 J                       0.18 j                       54.38
                I123cdPYRENE                              10.21 J                       0.09 1                       0.02 J                       47.46
                DBahAN71-1RA                              2.47 J                        0.23 J                       0.02 J                       49.36
                Bgh1PERYLENE                              18.69                         0.38 J                       0.03                         50.18

                Total PAH's:                              3167.0                      112.9                          3.4                        1028.6
                 (w/o Perylene)

                2-METHYLNAPH                              12.88 J                       6.46                         0.39 J                       79.32
                I-METHYLNAPH                              10.88 1                       3.18 J                       0.56 J                       56.31


                2.6-DIMETFINAPH                           11. 13 J                      5.68                         0.12 J                       47.44

                2.3,5-TRIMETHNAPH                         16.88                         0.89 1                       0.08 J                       48.49






                                              Antarctic Limpet Samples-Polar Programs- Aromatic Hydrocarbon Data


                INVESTC                Transect D- 14                    LAB QA SAMPLE                LAB QA SAMPLE                LAB QA SAMPLE
                ID:                    ANTARC NIST M801                  Station 12                   PROC BLANK                   Station 12
                LABSAMNO:              Q4882                             Q4883                        Q4884                        Q4885
                UNIT.*                                   ng/g                         ng/g                         ng/g                         ng/g
                PNA Analyte                              Conc DB QUAL                 Conc DB QUAL                 Conc DB; QUAL                Conc DB QUAL,


                1-METHYLPHEN                             16.02                        2.78 J                       0.06 J                       42.67


                Surrogate Recoveries
                NAPHD8:                                  71.9                         68.2                         62.4                         67.8
                ACENDIO:                                 76.9                         67.9                         63.7                         73.4
                PHEND10:                                 75.7                         69.4                         62.6                         73.3
                CHRYD12:                                 61.2                         55.4                         50.3                         54.3
                PERYD12:                                 62.4                         64.7                         9.0                          64.7








        0
        W






                                             Antarctic Limpet Samples-Polar Programs- Aromatic Hydrocarbon Data


                 INVEST#:               LAB QA SAMPLE                Transect D- 19           Transect D- 14                    LAB QA SAMPLE
                 ID:                    GERG CHK                     42' Palmer Sta           ANTARC NIST M802                  Transect D- 19
                 LABSAMNO:              W8220                        J1886                     Q4886                            Q4887
                 UNIT:                               ng/g                      ng/g                             ng/g                          ng/g
                 PNA Analyte                         Conc DB QUAL              Conc DB QUAL                     Conc DB QUAL                  Conc DB QUAL

                 SAMPLE TYPE:                    REF OIL                       SAMP                             SRM                DUP OF J 1886
                 COLLECTION DATE:
                 RECEIPT DATE:
                 QCBATCH:                            M801'                     M802                             M802                          M802
                 EXIRACTION DATE:                                         03/04/93                          03/04/93                     03/04/93
                 ME17HOD:                            GCMS                      GCMS                             GCMS                          GCMS
                 ANALYSIS DATE:                 04/06/93                  04/22/93                          04/21/93                     04/21/93
                 METHOD:                          GCECD                     GCECD                             GCECD                       GCECD
                 ANALYSIS DATE:                                           05/03/93                          05/03/93                     05/03/93
                 MATRIX:                          TISSUE                    TISSUE                            TISSUE                      TISSUE
                 SUBMAT-
                 SAMPLW]r.-
                 VIETWT:                                                       10.116                               5                         9.981
                 DRY%WT.                                 1                       2.5                            0.69                          2.53
        to       WTUNITS:                         GRAMS                     GRAMS                             GRAMS                       GRAMS
        0        PCTSOLIDS:                                                    24.7%                            13.8%                         25.3%
                 VOL:
                 VOLUNITS,:                       LITERS                    LITERS                            LITERS                      LITERS


                 NAPHTHALENE                         607.3                     11.64                            17.05                         12.77
                 CI-NAPHTHALENES                  1888.7                       12.97                            18.92  J                      13.20
                 C2-NAPHTHALENES,                 1644.6                       10.84                            26.25  J                      11.13
                 C3-NAPHTHALENES                  1296.2                       15.10                            64.86                         14.76
                 C4-NAPIfrHALENES,                   761.2                     7.30  J                        166.40                          6.14
                 BIPHENYL                            164.5                     3.13 J                           6.32 J                        3.13 J
                 ACENAPHTHYLENE                        1.2                     0.16 J                           3.58 J                        0.12 J
                 ACENAPHTHENE                        14.4                      0.38 J                             6.3 J                       0.66 J
                 FLUORENE                            72.8                      0.46 J                           6.79 J                        0.48 J
                 Cl-FLUORENES,                       199.0                     7.32 J                           37.60                         3.47 J
                 C2-FLUORENES                        276.2                     0.00 ND                        157.11                          12.11
                 C3-FLUORENES,                       269.9                     0.00 ND                        282.09                          0.00 ND
                 PHENANTHRENE                        202.2                     5.48                             31.97                           6.2
                 ANTHRACENE                           3.8                      0.74 J                           10.44 J                       1.15 J
                 CI-PHEN-ANTHR                       441.8                     6.98 J                           97.39                         7.34 J






                                              Antarctic Limpet Samples-Polar Programs- Aromatic Hydrocarbon Data


                 INVEST#:                LAB QA SAMPLE                 Transect D- 19              Transect D- 14                      LAB QA SAMPLE
                 ID:                     GERG CHK                      42' Palmer Sta              ANTARC NIST M802                    Transect D- 19
                 IABSAMNO:               W8220                         J1886                       Q4886                               Q4887
                 UNIT:                                ng/g                         ng/g                               ng/g                           ng/g
                 PNA Analyte                          Cone 1313 QUAL               Cone 1313 QUAL                     Conc DB QUAL                   Cone DB QUALI

                 C2-PHEN_ANTHR                       487.8                         5.06 J                             230.07                         4.89 J
                 C3-PHEN  -ANTHR                     451.8                         0.00 ND                            279.40                         0.00 ND
                 C4-PHEN  -ANTHR                     222.4                         0.00 ND                            128.75                         0.00 ND
                 DIBENZOTHIO                         149.3                         0.44 J                             4.05 J                         0.34 J
                 Cl-DIBEN                            297.6                         1. 15 1                            27.82 J                        0.00 ND
                 C2-DIBEN                            424.8                         0.00 ND                            126.46                         0.00 ND
                 C3-DIBEN                            356.7                         0.00 ND                            133.05                         0.00 ND
                 FLUORANTHENE                           3.7                        0.82 J                             198.58                         0.86 J
                 PYRENE                               12.0                          1.2 J                             220.89                         1.57 J
                 CI-FLUORAN_M                         68.6                         0.00 ND                            106.07                         0.00 ND
                 BENaANTHRACENE                         5.3                        0.31 J                             40.42                          0.75 J
                 CHRYSENE                             42.3                         1.55 J                             103.73                         1.29 J
                 Cl-CHRYSENES                         91.0                         0.00 ND                            65.61                          0.00 ND
                 C2-CHRYSENES                        113.7                         0.00 ND                            30.90                          0.00 ND
                 C3-CHRYSENES                         22.0                         0.00 ND                            3.17  J                        0.00 ND
                 C4-CHRYSENES                         18.9                         0.00 ND                            3.67  J                        0.00 ND
                 BENbFLUORAN                            2.5                        0.45 J                             36.57                          0.48 J
                 BENkFLUORAN                            2.6                        0.44 J                             36.42                          0.48 J
                 BENePYRENE                           10.1                         0.32 J                             71.07                          0.37 J
                 BENaPYRENE                             1.9                        0.15 J                             11.35 J                        0.15 j
                 PERYLENE                               1.3                        0.75 J                             8.79 J                         0.99 j
                 I123cdPYRENE                           1.6                        0.43 J                             10.29 J                        0.42 J
                 DBahANTHRA                             1.1                        0.15 1                              2.6 J                         0.14 J
                 BghtPERYLENE                           3.4                        0.33 J                             17.27                          0.47 J

                 Total PAH'9:                        10635                         95.3                               2821.3                        104.9
                  (w/o Perylene)

                 2-M1rrFIYI,NAPH                     1041.6                        8.07                               10.31 J                        8.05
                 I-METHYLNAPH                        847.2                          4.9 J                             8.61 J                         5.15


                 2.6-DIMETHNAPH                      639.9                         4.93 J                             9.56 J                           4.8

                 2.3,5-TRIMETHNAPH                   333.5                         2.91 J                             17.59                           2.5 J






                                              Antarctic Limpet Samples-Polar Programs- Aromatic Hydrocarbon Data


                 INVEST#:               LAB 9A SAMPLE                Transect D- 19            Transect D- 14                     LAB QA SAMPLE
                 ID:                    GERG CHK                     42' Palmer Sta            ANTARC NIST M802                   Transect D- 19
                 LABSAMNO-              W8220                        J 1886                    Q4886                              Q4887
                 UNrr.                               ng/g                       ng/g                             ng/g                          ng/g
                 PNA Analyte                         Conc DB gUAL               Conc DB gUAL                     Conc DB gUAL                  Cone DB Q UAL


                 I-METHYLPFIEN                       140.7                      0.51 1                           15.08                         0.83 J


                 Surrogate Recoveries
                 NAPHD8:                             88.6                       71.4                             75.5                          54.2
                 ACENDIO:                            91.4                       66.3                             67.0                          49.4
                 PHENDIO:                            92.2                       68.7                             73.7                          48.6
                 CHRYD12:                            77.5                       68.4                             62.8                          44.0
                 PERYD12:                            97.7                       59.6                             41.2                          37.5






                                             Antarctic Limpet Samples-Polar Programs- Aromatic Hydrocarbon Data


       INVEST#:              LAB QA SAMPLE                LAB QA SAMPLE               LAB QA SAMPLE                Transect D- 17            Transect D- 13
       ID:                   PROC BLANK                   Transect D- 19               GERGCHK                     60-62'                     NIST
       LABSAMNO*             Q4888                        Q4889                       W8310                        J1896                      Q4890
       UNIT.                               ng/g                        ng/g                        ng/g                      ng/g                      ng/g
       PNA Analyte                         Conc DB QUAL                Conc DB QUAL                Conc DB QUAL              Conc DB QUAL              Conc DI3 QUALI

       SAMPLE TYPE:                        BLK                 MSOFJ1886                       REF OIL                       SAMP                      SRM
       COLLEC71ON DATE:
       RECEIPT DATE:
       QCBATCH:                           M802                         M802                        M802                      M803                     M803
       EXTRAC'nON DATE:               03/04/93                     03/04/93                                             03/05/93                 03/05/93
       METHOD:                            GCMS                        GCMS                         GCMS                      GCMS                     GICMS
       ANALYSIS DATE:                 04/21/93                     04/21/93                    04/21/93                 04/07/93                 04/07/93
       METHOD:                          GCECD                       GCECD                        GCECD                    GCECD                     GCECD
       ANALYSIS DATE:                 05/03/93                     05/03/93                                             05/03/93                 05/03/93
       MATRIX:                          TISSUE                      TISSUE                       TISSUE                   TISSUE                    TISSUE
       SUBMAT:
       SAMPLW.
       WETWT:                                                         10.006                                                 9.939                    5.069
       DRYWT:                                 10                       2.46                             1                    2.66                      0.67
       *uNrm:                           GRAMS                       GRAMS                        GRAMS                    GRAMS                     GRAMS
       Pi4WLIDS:                                                      24.6%                                                  26.8%                    13.2%
       VOL:
       VOLUNTrS:                        LITERS                      LITERS                       LITERS                   LITERS                    LITERS


       NAPHTHALENE                         0.93 J                      52.63                       616.6                     10.33                    24.35
       CI-NAPHTHALENES                     0.58 j                   116.59                       1907.0                      10.96                    27.39 J
       C2-NAPH717HALENES                   0.00 ND                     0.00                      1724.6                      7.16 J                   41.22
       C3-NAPHTHALENES                     0.00  ND                    0.00                      1560.5                      10.59                    73.82
       C4-NAPHTHALENES                     0.00  ND                    0.00                        814.9                     0.00 ND                136.25
       BIPHENYL                            0.28 J                      42.02                       161.3                     7.76                     20.76
       ACENAPHTHYLENE                      0.03 J                      40.67                         1.1                     0.29 J                    7.44 J
       ACENAPHTHENE                        0.04 J                      38.85                       14.8                      1.26 J                    8.19 j
       FLUORENE                            0.08 j                      40.68                       76.6                      1.48 J                    6.69 J
       CI-FLUORENES                        0.00 ND                     0.00                        157.8                     4.11 J                   54.58
       C2-FLUORENES                        0.00 ND                     0.00                        290.1                     6.91 J                 164.84
       C3-FLUORENES,                       0.00 ND                     0.00                        303.2                     0.00 j                 233.44
       PHENANTHRENE                        0.47 J                      41.62                       198.9                     1.83 J                   34.95
       ANTHRAC.F.W.                        0.02.T                      9.4.3f;                       v;.R                    1 -Ar,j                  13.72 .1
       CI-PHEN-ANTHR                       0.00 ND                     0.00                        419.4                     5.27 J                   84.36




    = = = M M M M M M M M M = M M M M = M



   M = = = = M @ = M = M M = M M M M = M

                                               Antarctic Limpet Samples-Polar Programs- Aromatic Hydrocarbon Data


       INVEST#:                LAB QA SAMPLE                LAB QA SAMPLE                 LAB QA SAMPLE                Transect D- 17             Tran t D- 13
       ID:                     PROC BLANK                   Transect D- 19                GERG CHK                     60-62'                     NIST
       LABSAMNO:               Q4888                        Q4889                         W8310                        J1896                       Q4890
       UNIT:                                 ng/g                         ng/g                         ng/g                      ng/g                       ng/g
       PNA Analyte                           Cone DB QUAL                 Cone DB QUAL                 Cone DB QUAL              Cone DB QUAL               Cone DB

       C2-PHEN_ANTHR                         0.00 ND                      0.00                       466.8                       0.00  ND                249.42
       C3-PHEN@ANTHR                         0.00 ND                      0.00                       371.9                       0.00  ND                388.72
       C4-PHEN@ANMR                          0.00 ND                      0.00                       179.9                       0.00  ND                156.27
       DIBENZOTHIO                           0.03 J                       30.31                      151.0                       0.53  J                    5.70  j
       CI-DIBEN                              0.00 ND                      0.00                       259.1                       0.00  ND                  32.34
       C2-DIBEN                              0.00 ND                      0.00                       359.9                       0.00  ND                153.31
       C3-DIBEN                              0.00 ND                      0.00                       298.4                       0.00  ND                165.31
       FLUORANTHENE                          0.13 J                       36.29                         3.3                      0.57  J                 220.15
       PYRENE                                0.32 J                       40.27                        14.3                      0.90  j                 213.47
       Cl-FLUORAN-PYR                        0.00 ND                      0.00                         58.1                      0.00  ND                129.45
       BENaANTHRACENE                        0.04 J                       41.9                          5.5                      0.52  J                   30.07
       CHRYSENE                              0.09 1                       43.17                        45.9                      0.93  J                 124.92
       CI-CHRYSENES                          0.00 ND                      0.00                         70.8                      0.00  ND                  69.26
       C2-CHRYSENES                          0.00 ND                      0.00                         85.1                      0.00  ND                  40.34
       I-CHRYSENES                           0.00 ND                      0.00                         11.4                      0.00  ND                   6.85  J
       Cat-CHRYSENES                         0.00 ND                      0.00                          5.6                      0.00  ND                  13.51  J
       BENbFLUORAN                           0.01 1                       43.27                         3.2                      0.33  J                   36.52
       BENkFLUORAN                           0.01 j                       43.09                         3.2                      0.35  J                   38.78
       BENePYRENE                            0.03 J                       42.12                        11.0                      0.41  J                   74.19
       BENaPYRENE                            0.08 1                       34.1                          2.2                      0.51  1                   13.06  J
       PERYLENE                              0.13 J                       43.94                         3.4                      3.62  J                   14.81  J
       1123cdFYRENE                          0.03 J                       40.56                         0.7                      0.22  J                   11.06  J
       DBahANTHRA                            0.06 J                       41.09                         1.8                      0.27  J                    2.99  J
       BghIPERYLENE                          0.11 j                       39.91                         4.5                      0.41  J                   17.92

       Total PAH's:                          3.4                         873.5                       10666                       75.9                    3125.6
        (w/o Perylene)

       2-METHYLNAPH                          0.28 J                       68.54                      1055.7                      7.27                      17.57
       1-METHYLNAPH                          0.3 J                        48.05                      851.2                       3.69  J                    9.82 J

       2.6-DIMETHNAPH                        0.14 J                       44.8                       651.9                       3.50  J                   14.71 1

       2.3,5-TRIMETtiNAPH                    0.09 1                       46.12                      357.0                       1.22  J                   16.72






                                            Antarctic Limpet Samples-Polar Programs- Aromatic Hydrocarbon Data


     INVEST#:               LAB QA SAMPLE                LAB QA SAMPLE                LAB QA SAMPLE               Transect D- 17            Transect D- 13
     ID:                    PROC BLANK                   Transect D- 19               GERG CHK                    60-62'                     NIST
     LABSAMNO,.             Q4888                        Q4889                        W8310                       J1896                      Q4890
     UNIT-                                ng/g                        ng/g                        ng/g                      ng/g                      ng/g
     PNA Analyte                          Cone DB; QUAL               Cone DB QUAL                Cone DB QUAL              Cone DB QUAL              Cone DB QUAL


     1-METHYLPHEN                         0.05 J                      36.99                       151.3                     1.55  j                   15.26

     SurTogate Recoveries
     NAPHD8:                              57.8                        79.2                        95.4                      65.3                      70.9
     ACEND10:                             50.3                        68.8                        86.9                      65.8                      70.8
     PHENDIO:                             51.7                        73.0                        92.4                      63.2                      73.9
     CHRYD12:                             36.0                        61.5                        80.2                      47.0                      58.1
     PERYD12:                             25.6                        54.1                        112.2                     47.0                      54.3






       0






                                               Antarctic Limpet Samples-Polar Programs- Aromatic Hydrocarbon Data


                    INVES1`#:              LAB QA SAMPLE                LAB QA SAMPLE               LAB QA SAMPLE                LAB QA SAMPLE
                    ID:                    Transect D- 17               PROC BLANK                  Transect D- 17               GERG CHK
                    LABSAMNO:              Q4891                        Q4892                       Q4893                        W8228
                    UNrr-.                              ng/g                         ng/g                        ng/g                         ng/g
                    PNA Analyte                         Conc DB QUAL                 Conc DB QUAL                Conc DB QUAL                 Conc DB QUAL

                    SAMPLE TYPE:              DUP OF J 1896                          BLK                MS, OF J 1896                      REF OIL
                    COLLECTION DATE:
                    RECEIPT' DATE:
                    QCBATCH:                            M803                         M803                        M803                        M803
                    EXTRACTION DATE:               03/05/93                     03/05/93                    03/05/93
                    ME`I`HOD:                           GCMS                        GCMS,                        GCMS                        GCMS,
                    ANALYSIS DATE-                 04107/93                     04/07/93                    04/07/93                     04/07/93
                    MET'HOD:                         GCECD                        GCECD                       GCECD                        GCECD
                    ANALYSIS DATE:                 05/03/93                     05/03/93                    05/03/93
                    MAITUX:                          TISSUE                       TISSUE                      TISSUE                       TISSUE
                    SUBMAT.
                    SAMPLWP
                    WBI'W:                              10.443                                                   10.492
                    DRYWr:                              2.38                           10                        2.39                             1
                    WTUNrM:                          GRAMS                        GRAMS                       GRAMS                        GRAMS
          0         PCTSOLIDS:                          22.80/6                                                  22.8%
                    VOL.
                    VOLUNII'S:                       LrMRS                        LITERS                      LITERS                       LITERS


                    NAPHTHALENE                         12.72                        0.84 J                      52.33                       632.3
                    C I -NAPHTHALENES                   11.38                        0.76 J                      114.18                    1943.8
                    C2-NAPHTHALENES                     9.18                         0.00 ND                     0.00                      1668.9
                    C3-NAPHTHALENES                     13.23                        0.00 ND                     0.00                      1281.7
                    C4-NAPHTHALENES                     0.00                         0.00 ND                     0.00                        751.3
                    BIPHENYL                            3.96                         0.65 J                      42.55                       169.2
                    ACENAPHTHYLENE                      0.31                         0.02 J                      36.47                         0.4
                    ACENAPHTHENE                        0.95                         0.16 J                      39.62                        16.4
                    FLUORENE                            2.22                         0.13 J                      38.55                        78.3
                    CI-FLUORENES                        7.34                         0.00 ND                     0.00                        196.4
                    C2-FLUORENES                        12.39                        0.00 ND                     0.00                        281.4
                    C3-FLUORENES                        0.00                         0.00 ND                     0.00                        253.7
                    PHENANTHRENE                        2.11                         0.38 J                      36.60                       201.4
                    ANTHRACENE                          1.23                         0.07 J                      17.71                         4.1
                    CI-PHEN-ANTHR.                      6.27                         0.00 ND                     0.00                        456.2






                                               Antarctic Limpet Samples-Polar Programs- Aromatic Hydrocarbon Data


                   INVEST#:                LAB QA SAMPLE                  LAB QA SAMPLE                 LAB QA SAMPLE                  LAB QA SAMPLE
                   ID:                     Transect. D- 17                PROC BLANK                    Transect 13- 17                 GERGCHK
                   LABSAMNO:               Q4891                          Q4892                         Q4893                          W8228
                   UNIT:                                 ng/g                          ng/g                           ng/g                          ng/g
                   PNA Analyte                           Conc 1313 QUAL                Conc DB QUAL                   Conc DB QUAL                  Conc DB QUAL

                   C2-PHEN-ANTHR                         7.34                          0.00  ND                       0.00                         525.7
                   C3-PHEN-ANTI-IR                      12.01                          0.00  ND                       0.00                         444.1
                   C4-PHEN-ANTHR                         9.20                          0.00  ND                       0.00                         201.7
                   DIBENZOTHIO                           0.79                          0.04  J                      30.87                          149.6
                   CI-DIBEN                              0.00                          0.00  ND                       0.00                         309.9
                   C2-DIBEN                              4.22                          0.00  ND                       0.00                         441.7
                   C3-DIBEN                              4.73                          0.00  ND                       0.00                         358.7
                   FLUORANTHENE                          3.27                          0.31  J                      38.58                             3.8
                   PYRENE                                2.76                          0.44  J                      37.06                           12.6
                   Cl-FLUORAN-PYR                        5.07                          0.00  ND                       0.00                          66.5
                   BENaANTHRACENE                        0.82                          0.04  J                      39.68                           .6.0
                   CHRYSENE                              1.98                          0.38  J                      42.26                           44.6
                   Cl-CHRYSENES                          0.00                          0.00  ND                       0.00                          86.1
                   C2-CHRYSENES                          0.00                          0.00  ND                       0.00                         103.5
                   C3-CHRYSENES                          0.00                          0.00  ND                       0.00                          19.6
                   C4-CHRYSENES                          0.00                          0.00  ND                       0.00                          17.4
                   BENbFLUORAN                           0.64                          0.07  J                      37.22                             2.7
                   BENkFLUORAN                           0.68                          0.08  j                      39.52                             2.9
                   BENePYRENE                            0.92                          0.10  1                      41.04                           10.0
                   BENaPYRENE                            0.54                          0.05  1                      30.27                             1.3
                   PERYLENE                              1.59                          0.22  J                      47.50                             1.9
                   I123edPYRENE                          0.41                          0.05  1                      34.83                             0.8
                   DBahAN71-IRA                          0.34                          0.04  J                      36.51                             1.5
                   BghtPERYLENE                          0.55                          0.08  1                      37.76                             3.3

                   Total PAH's:                          139.6                           4.7                        823.6                          10749
                    (w/o PeTylene)

                   2-ME`I1iYLNAPH                        7.32                          0.45  J                      64.93                          1080.9
                   I-METHYLNAPH                          4.06  J                       0.31  J                      49.25                          862.9


                   2.6-DIMETHNAPH                        3.74  J                       0.25  J                      43.43                          682.2


                   2.3.5-TRIMETHNAPH                     0.94  J                       0.22  J                      42.97                          336.6






                                                Antarctic Limpet Samples-Polar Pro9mms- Aromatic HYdrOOarbon Data


                    INVEST#:                LAB QA SAMPLE                 LAB QA SAMPLE                LAB QA SAMPLE                 LAB QA SAMPLE
                    ID:                     Transect D- 17                PROC BLANK                   Transect D- 17                GERGCHK
                    TA 3SAMNO:              Q4891                         Q4892                        Q4893                         W8228
                    UNIT:                                ng/g                          ng/g                         ng/g                          ng/g
                    PNA Analyte                          Conc DB QUAL                  Conc DB QUAL                 Conc DB QUAL                  Conc DB QUAL



                    I-METHYLPHEN                         0.57  J                       0.04 J                       32.65                         130.2
                    Surrogate Recoveries                                                                                                          89.9
                    NAPHD8:                              63.7                          72.0                         65.0
                    ACENDIO:                             64.6                          72.0                         66.1                          88.6
                    PHENDIO:                             61.6                          71.0                         70.0                          88.5
                    CHRYD12:                             52.2                          53.5                         52.0                          74.3
                    PERYD12:                             47.2                          56.1                         44.3                          96.1









          b3




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1                           213






                                Antarctic lAmpet Samples -Polar Programs- Pesticides and PCB's


                   INVEST#:                    Station 4                  Station 3                  Station 12
                   ID:                         Humble Island              Humble Island              JanusIsland
                   IABSAMNO:                   J1292                      J1825                      J1289
                   UNIT.                       ng/g                       ng/g                       ng/g
                  LAnalyte (Cont)              Conc            DB gUAL Conc               DB QUAL Conc              DB QUAL

                   &AWLE TYPE:                 SAW                        SAW                        SAW
                   COIJECTION DATE:            1989                       1991                       1989
                   RECEIPT DATE:
                   QCBATCH:                    M801                       M801                       M801
                   EXTRACTION DATE:            03/04/93                   03/04/93                   03/04/93
                   ME-MOD:                     GCMS                       GICMS                      GCMS
                   ANALYSIS DATE:              04/06/93                   04/06/93                   04/06/93
                   METHOD:                     GCECD                      GCECD                      GCECD
                   ANALYSIS DATE:              05/03/93                   05/03/93                   05/03/93
                   MATRM                       TISSUE                     TISSUE                     TISSUE
                   SUBMAT-
                   SAM[PLWT:
                   WE,rwr:                     10.274                     8.613                      7.945
                   DMW:                        2.9                        1.78                       2.06
                   VVIUNITS:                   GRAMS                      GRAMS                      GRAMS
                   PCTSOLIDS:                  28.2%                      20.7%                      25.90/6
                   VOL:
                   VOLUIMB:                    LITERS                     LITERS                     LITERS


                   TOTAL BHC'S                 0.00            ND         0.00            ND         0.00           ND
                   TOTAL CHLORDANES            0,00            ND         0*45            J          0,00           ND
                   TOTAL DDrS                  5.69                       3.78                       0.00           ND
                   TOTAL PCB'S                 26.5                       9.8                        0.0            ND


                   ALPHA-BHC                   0.00            ND         0.00            ND         0.00           9
                   HCB                         0.42            1          0.57            1          0.00           9
                   BETA-BHC                    0.00            ND         0.00            ND         0.00           Q
                   GAMMA-BHC                   0.00            ND         0.00            ND         0.00           Q
                   DELTA-BHC                   0.00            ND         0.00            ND         0.00           9
                   HEPTACHLOR                  0.00            ND         0.00            ND         0.00           Q
                   HEPTA-EPONME                0.00            ND         0.00            ND         0.00           Q
                   OXYCHLORDANE                0.00            ND         0.00            ND         0.00           Q
                   GAMMA-CHLORDANE             0.00            ND         0.00            ND         0.00           Q
                   ALPHA-CHLORDANE             0.00            ND         0.45            j          0.00           Q
                   TRANS-NONACHLOR             0.00            ND         0.00            ND         0.00           Q
                   CIS-NONACHLOR.              0.00            ND         0.00            ND         0.00           Q
                   ALDRIN                      0.00            ND         0.00            ND         0.00           9
                   DIELDRIN                    0.00            ND         0.00            ND         0.00           9
                   ENDRIN                      0.00            ND         1.38                       0.00           Q
                   WBREX                       0.00            ND         0.00            ND         0.00           Q
                   2,41)DE (O.P'DDE)           0.00            ND         0.00            ND         0.00           Q
                   4,47DDE (P.P'DDE)           0.89            1          0.55            j          0.00           Q
                   2,4`DDD (O,P'DDD)           0.38            j          0.00            ND         0.00           Q
                   4.4DDD (P.P`DDD)            0.00            ND         0.00            ND         0.00           Q
                   2.4'DDT (O.FDDT)            4.42                       1.66                       0.00           9
                   4.4'DDT (P.P'DDT)           0.00            ND         1.57                       0.00           Q

                   PCB # (CLORINAnON)





                                                                      214






                                 Antarctic I.Ampet Samples -Polar Programs- Pesticides and PCB's


                    INVEST#:                   Station 4                  Station 3                 Station 12
                    ID:                        Humble Island              Humble Island             Janus Island
                    IABSAMNO:                  J1292                      J1825                     J1289
                    UNIT.                      ng/g                       ng/g                      ng/g
                    -Analyte (Cont)            Conc            DB gUAL Conc               DB QUAL Conc             DB QUAL

                    8 (CL2)                    0.00            M          0.00            ND        0.00           Q
                    18 (C L.3)                 0.00            ND         0.00            ND        0.00           Q
                    28 (CL3)                   1.48                       0.00            ND        0.00           Q
                    44 (CIA)                   2.59                       1.73                      0.00           Q
                    52 (CIA)                   0.00            ND         0.00            ND        0.00           Q
                    66 (CIA)                   9.73            M          0.47            1         0.00           Q
                    101 (CL5)                  0.00            ND         0.31            1         0.00           Q
                    105 (CL5)                  0.95            1          0.00            ND        0.00           Q
                    110/77 (CL5/4)             0.80            1          0.00            ND        0.00           Q
                    118/108/149(CL5/5/6)       0.57            1          0.00            ND        0.00           Q
                    128 (CL6)                  0.00            ND         0.00            ND        0.00           Q
                    138 (CL6)                  0.86            1          1.16                      0.00           Q
                    126 (CL5)                                  NA                         NA                       NA
                    153 (CL6)                  0.00            ND         0.00            ND        0.00           Q
                    170 (CL7)                  0.00            ND         0.00            ND        0.00           Q
                    180 (CL7)                  1.03            1          0.65            1         0.00           Q
                    187/182/159(CL7/7/6)       0.99            1          0.00            ND        0.00           Q
                    195 (CLS)                  0.00            ND         0.00            ND        0.00           Q
                    206 (CL9)                  0.00            ND         0.00            ND        0.00           Q
                    209 (CLIO)                 0.00            ND         0.00            ND        0.00           Q

                    Surrogate Recoveries
                    DBOFB%:                    63.7                       69.1                      0.2            Q
                    PCB#103%:                  63.8                       73.1                      0.6            Q
                    PCB#198%:                  78.9                       82.7                      0.4            Q


                    OTHER PESTICIDES


                    ENDOSULFAN I
                    ENDOSULFAN 11
                    ENDOSULFAN SULFATE
                    ENDRIN ALDEHYDE


                    PCB #(CHLORINATION)

                    7 (CL2)                    0.00            ND         0.00            ND        0.00           Q
                    15 (CL2)                   0.00            ND         0.00            ND        0.00           Q
                    24 (C1.3)                  0.00            ND         0.00            ND        0.00           Q
                    16/32 (CL3)                0.52            1          0.00            ND        0.00           Q
                    29 (CL3)                   0.00            ND         0.00            ND        0.00           Q
                    26 (CI.3)                  1.14            1          0.00            ND        0.00           Q
                    25 (CL3)                   0.64            1          0.00            ND        0.00           Q
                    50 (CIA)                   1.38            1          0.00            ND        0.00           Q
                    31 (CI.3)                  0.00            ND         0.00            ND        0.00           Q
                    33 (CL3)                   0.00            ND         0.00            ND        0.00           Q
                    22 (CL3)                   0.00            ND         0.00            ND        0.00           Q
                    45 (CIA)                   0.00            ND         0.00            ND        0.00           Q
                    46 (CIA)                   0.00            ND         0.00            ND        0.00           Q
                    49 (CIA)                   0.00            ND         0.09            1         0.00           Q



                                                                      215






                              Antarctic lAmpet Samples -Polar Programs- Pesticides and PCB's


                  INVEST#:                  Station 4                 Station 3                 Station 12
                  ID:                       Humble Island             Humble Island             Janus Island
                  LABSAMNO:                 J1292                     J1825                     J1289
                  UNM                       ng/g                      ng/g                      ng/g
                 jAnalyte (Cont)            Conc            DB QUAL Cone              DB QUAL Conc            DB QUAL

                  47/,W (CIA)               0.00            ND        0.00            ND        0.00          Q
                  37/42 (CIA)               0.00            ND        0.00            ND        0.00          9
                  41/64 (CIA)               0.68            1         3.39                      0.00          Q
                  40 (CIA)                  0.00            ND        0.00            ND        0.00          9
                  100 (CL.5)                0.00            ND        0.00            ND        0.00          9
                  74 (CIA)                  3.02                      0.00            ND        0.00          Q

                  PCB #(CHLORINATION)


                  70 (CIA)                  1.87                      0.00            ND        0.00          9
                  88 (CLS)                  0.00            ND        0.22            1         0.00          9
                  60/56 (CL5)               0.00            ND        0.00            ND        0.00          Q
                  92? (CL5)                 0.00            ND        0.00            ND        0.00          Q
                  84? (CL5)                 0.00            ND        0.00            ND        0.00          Q
                  99 (CL5)                  0.00            ND        0.00            ND        0.00          9
                  83 (CL5)                  0.00            ND        0.00            ND        0.00          Q
                  97 (CIZ)                  0.00            ND        0.00            ND        0.00          Q
                  87 (CL5)                  0.00            ND        0.00            ND        0.00          9
                  85 (CL5)                  0.00            ND        0.00            ND        0.00          Q
                  136 (CL6)                 0.00            ND        0.00            ND        0.00          9
                  82 (CL5)                  0.00            ND        0.00            ND        0.00          9
                  151 (CLAB)                0.50            1         0.00            ND        0.00          9
                  107/108/144(CL5/5/6)      0.00            ND        0.00            ND        0.00          Q
                  149 (CL6)                 0.94            j         0.00            ND        0.00          Q
                  188 (CL7)                 0.00            ND        0.00            ND        0.00          Q
                  146 (CL6)                 0.00            ND        0.00            ND        0.00          9
                  141 (CL6)                 1.88                      0.21            j         0.00          Q
                  137 (CL6)                 1.35            j         0.00            ND        0.00          Q
                  UNK (CL6)                 0.00            ND        0.00            ND        0.00          Q
                  158 (CL7)                 0.83            1         0.00            ND        0.00          9
                  129 (CL6)                 0.00            ND        0.00            ND        0.00          Q
                  178 (CL7)                 0.00            ND        0.00            ND        0.00          Q
                  183 (CL7)                 0.00            ND        0.00            ND        0.00          9
                  167 (CIJ63)               0.00            ND        0.00            ND        0.00          Q
                  185 (CL7)                 0.65            1         0.00            ND        0.00          Q
                  174 (CL7)                 0.51            1         0.00            ND        0.00          Q
                  177 (CL7)                 0.00            ND        0.00            ND        0.00          9
                  156/171/202(CL6/7/8)      0.00            ND        0.00            ND        0.00          9
                  200 (CL8)                 0.00            ND        0.00            ND        0.00          9
                  172 (CL7)                 0.00            ND        0.00            ND        0.00          9
                  191 (CL7)                 0.00            ND        0.00            ND        0.00          Q
                  201 (CL8)                 1.06            j         2.17                      0.00          9
                  196 (CLS)                 0.00            ND        0.00            ND        0.00          Q
                  189 (CL7)                 2.28                      0.00            ND        0.00          Q
                  194 (CL8)                 0.00            ND        0.00            ND        0.00          9
                  205 (CL9)                 0.00            ND        0.00            ND        0.00          Q






                                                                   216






                                      Antarctic Umpet Samples -Polar Programs- Pesticides and PCB's


                          DqVESr#:                      Station 12                   Station 13                 station 13
                          D:):                          Janus Island                 Christine Is               Christine Is
                          LABSAMNO:                     J1840                        J1312                      J1842
                          UNIT.                         ng/g                         ng/g                       ng/g
                          Analyte (Cont)                Conc            DB QUAL Conc               DB QUAL Conc               DB QUAL

                          SAMPLE TYPE:                  SAMP                         SAMP                       SAMP
                          COLLECTION DATE:              1991                         1989                       1991
                          RECEIPT DATE:
                          QCBATCH:                      M801                         M861                       M801
                          EXTRACTION DATE:              03/04/93                     06/25/93                   03/04/93
                          M[ETHOD:                      GCMS                         GCMS                       GCMS
                          ANALYSIS DATE:                04/06/93                     07/25/93                   04/06/93
                          h=OD:                         GCECD                        GCECD                      GCECD
                          ANALYSIS DATE:                05/03/93                     08/02/93                   05/03/93
                          MATRDr_                       TISSUE                       TISSUE                     TISSUE
                          SUBMAT:
                          SAMPLWT:
                          WFIWT:                        9.764                        4.24                       10.991
                          DRYWT.                        2.18                         1.140136                   2.46
                          WIUNITS:                      GRAMS                        GRAMS                      GRAMS
                          PCTSOL1DS:                    22.3%                        26.90/6                    22.40/6
                          VOL.
                          VOLUNITS:                     LITERS                       LITERS                     LITERS


                          TOTAL BHC'S                   2.14                         0.00          ND           0.00          ND
                          TOTAL CHLORDANES              0.00            bm           O.W           J            2.0           J
                          TOTAL DDT"S                   1.81                         6.51                       6.94
                          TOTAL PCB'S                   11.3                         10.4                       17.4


                          ALPHA-BHC                     0.57            J            0.00          ND           0.00          ND
                          HCB                           0.24            J            0.56          1            0.71          1
                          BETA-BHC                      0.00            ND           0.00          ND           0.00          ND
                          GAMMA-BHC                     1.58                         0.00          ND           0.00          ND
                          DELTA-BHC                     0.00            ND           0.00          ND           0.00          ND
                          HEPTACHLOR                    0.00            ND           0.38          J            0.00          ND
                          HEPTA-EPOXIDE                 0.00            ND           0.00          ND           0.71          J
                          OXYCHLORDANE                  0.00            ND           0.00          ND           0.77          J
                          GAMMA-CHLORDANE               0.00            ND           0.00          ND           O.DD          NE)
                          ALPHA-CHLORDANE               0.00            ND           0.00          NE)          0.00          ND
                          TRANS-NONACHLOR               0.00            ND           0.00          ND           0.72          J
                          CIS-NONACHLOR                 0.00            ND           0.00          ND           0.42          J
                          ALDRIN                        0.00            ND           0.00          ND           0.00          ND
                          DIELDRIN                      0.95            j            0.00          ND           0.00          ND
                          ENDRIN                        1.10                         0.00          ND           0.00          ND
                          M[H;tEx                       0.00            ND           0.00          ND           0.00          ND
                          2,413DE (O.PIDDE)             0.00            ND           0.00          ND           0.00          ND
                          4,41)DE (P,PDDE)              0.00            ND           4.68                       1.36
                          2,4'DDD (O,PDDD)              0.00            ND           1.84                       0.00          ND
                          4,413131) (P.P`DDD)           0.00            ND           0.00          ND           0.00          ND
                          2,41)DT (O.FrDEM              1.23                         0.00          ND           2.70
                          -4,4'DDT (P,P'DDTI            0.57            J            0.00          ND           2.78


                          PCB # (CLORINATION)




                                                                               217






                                  Antarctic Limpet Samples -Polar Programs- Pesticides and PCB's


                        UqVEST*:                     Station 12                 Station 13               Station 13
                        ID:                          Janus Island               Christine Is             Christine Is
                        LABSAMNO:                    J1840                      J1312                    J1842
                        UNIT-                        ng/g                       ng/g                     ng/g
                        jAnalyte (Cont)              Conc           DB gUAL Conc              DB QUAL Conc             DB QUAL

                        8 (C12)                      0.45           J           0.00          ND         0.80          J
                        18 (CL3)                     0.00           ND          0.00          ND         0.00          ND
                        28 (CL3)                     0.82           J           0.00          ND         0.65          J
                        44 (CIA)                     1.38                       2.40                     1.66
                        52 (CIA)                     0.00           ND          0.00          ND         0.10          J
                        66 (CIA)                     0.76           J           0.00          ND         0.00          ND
                        101 (CL5)                    0.33           J           0.00          ND         0.12          J
                        105 (CL5)                    0.36           J           0.00          ND         0.34          J
                        110/77 (CL5/4)               0.00           ND          0.98                     0.34          J
                        118/108/149(CL5/5/6)         0.00           ND          0.00          ND         0.00          ND
                        128 (CLAG)                   0.00           ND          0.00          ND         0.00          ND
                        138 (CL6)                    1.47                       1.94                     2.32
                        126 (CL5)                                   NA                        NA                       NA
                        153 (C1,66)                  0.79           J           0.00          ND         1.54
                        170 (CL7)                    0.00           ND          4.52          M          0.00          ND
                        180 (CL7)                    0.44           J           0.00          ND         0.62          J
                        187/182/159(CL7/7/6)         0.00           ND          0.00          ND         0.00          ND
                        195 (CL8)                    0.00           ND          0.00          ND         0.00          ND
                        206 (CL9)                    0.00           ND          0.00          ND         0.00          ND
                        209 (CLIO)                   0.00           ND          0.00          M          0.00          rM


                        Surrogate Rmoveries
                        DBOFB%:                      64.7                       58.0                     61.2
                        PCB# 1030/6:                 72.1                       75.7                     67.2
                        PCB#198%:                    79.3                       92.7                     77.3


                        OTHER PESTICIDES


                        ENDOSULFAN I
                        ENDOSULFAN 11
                        ENDOSULFAN SULFATE
                        ENDRIN ALDEHYDE


                        PCB #(CHLORINAnON)


                        7 (CL2)                      0.00           ND          2.97                     0.00          ND
                        15 (CL2)                     0.00           ND          0.00          ND         0.00          ND
                        24 (CL3)                     0.00           ND          0.85                     0.71          J
                        16/32 (CL3)                  0.00           ND          0.00          ND         0.00          ND
                        29 (CL3)                     0.00           ND          0.00          ND         0.00          ND
                        26 (CL3)                     0.00           ND          0.00          ND         0.00          ND
                        25 (CL3)                     0.00           ND          0.00          ND         0.30          J
                        50 (CIA)                     0.31           J           0.00          ND         0.26          J
                        31 (CL3)                     0.00           ND          0.00          ND         0.00          ND
                        33 (CL3)                     0.00           ND          0.00          ND         0.00          ND
                        22 (CL3)                     0.00           ND          0.00          ND         0.00          ND
                        45 (CIA)                     0.00           ND          0.00          ND         0.00          ND
                        46 (CIA)                     0.00           ND          0.00          ND         0.46          1
                        49 (CIA)                     0.30           J           0.00          ND         0.00          ND



                                                                           218







                                  Antarctic lAmpct Samplcs -Polar Programs- Pcsticides and PCB's


                        INVEST#:                    Station 12                Station 13               Station 13
                        ID:                         Janus Island              Chzistine Is             Christine Is
                        LABSAMNO:                   J 1840                    J 1312                   J1842
                        UNIT:                       ng/g                      ng/g                     ng/g
                        Analyte (Cont)              Conc          DB QUAL Conc             DB QUAL Conc             DB QUAL

                        47/48 (CIA)                 0.00          ND          0.00         ND          0.00         ND
                        37/42 (CIA)                 0.00          ND          0.00         ND          0.00         ND
                        41/64 (CIA)                 0.00          ND          0.00         ND          0.00         ND
                        40 (CIA)                    0.00          ND          0.00         ND          0.00         ND
                        100 (CL5)                   0.00          ND          0.00         ND          0.00         ND
                        74 (CIA)                    0.00          ND          1.03                     0.00         ND


                        PCB #(CHLORINATION)


                        70 (CIA)                    0.37          1           0.00         ND          0.00         ND
                        88 (CL5)                    0.00          ND          0.00         ND          0.20         1
                        60/56 (CL5)                 0.00          ND          0.00         ND          0.00         ND
                        92? (CL5)                   0.00          ND          0.00         ND          0.00         ND
                        84? (CL5)                   0.00          ND          0.24         1           0.00         ND
                        99 (CM                      0.00          ND          0.00         ND          0.00         ND
                        83 (CL5)                    0.00          ND          0.00         ND          0.08         J
                        97 (CL5)                    0.00          ND          0.00         ND          0.00         ND
                        87 (CL5)                    0.00          ND          0.00         ND          0.00         ND
                        85 (CLZ)                    0.00          ND          0.00         ND          0.00         ND
                        136 (CL6)                   0.00          ND          0.00         ND          0.00         ND
                        82 (CL5)                    0.00          ND          0.00         ND          0.00         ND
                        151 (CL6)                   0.00          ND          0.00         ND          0.91         J
                        107/108/144(CL5/5/6)        0.00          ND          0.00         ND          0.00         ND
                        149 (CL6)                   0.00          ND          0.00         ND          0.54         1
                        188 (CL7)                   0.00          ND          0.00         ND          0.00         ND
                        146 (CL6)                   0.00          ND          0.00         ND          0.00         ND
                        141 (CL6)                   0.00          ND          0.00         ND          0.86         1
                        137 (CL6)                   0.00          ND          0.00         ND          0.81         1
                        UNK (CL6)                   0.00          ND          0.00         ND          0.00         ND
                        158 (CL7)                   0.00          ND          0.00         ND          0.00         ND
                        129 (CL6)                   0.00          ND          0.00         ND          0.00         ND
                        178 (CL7)                   0.00          ND          0.00         ND          0.00         ND
                        183 (CL7)                   0.00          ND          0.00         ND          0.00         ND
                        167 (CL6)                   0.00          ND          0.00         ND          0.00         ND
                        185 (CL7)                   0.00          ND          0.00         ND          0.00         ND
                        174 (CL7)                   0.00          ND          0.00         ND          0.00         ND
                        177 (CL7)                   0.00          ND          0.00         ND          0.00         ND
                        156/171/202(CL6/7/8)        0.83          1           0.00         ND          0.66         1
                        200 (CL8)                   0.00          ND          0.00         ND          0.00         ND
                        172 (CL7)                   1.06          1           0.00         ND          1.21         1
                        191 (CL7)                   0.00          NDD         0.00         ND          0.00         ND
                        201 (CLB)                   1.79                      0.00         ND          1.68
                        196 (CL8)                   0.00          NDD         0.00         ND          0.00         ND
                        189 (CL7)                   1.13                      0.00         ND          2.38
                        194 (CL8)                   0.00          ND          0.00         ND          0.00         m
                        205 (CL9)                   0.00          m           0.00         m           0.00         m






                                                                         219






                                Antarctic lAmpct Samplcs -Polar Programs- Pesticidcs and PCB's


                    RTVTW#:                    Station 20                 Station 20                Transect D-7
                    ID:                        Cormorant Is               Cormorant Is              Hermit Island
                    I.&BSAMN0:                 J1310                      J1850                     J1344
                    UNIT-                      ng/g                       ng/g                      ng/g
                    Analytc (Cont)             Conc            DB QUAL Conc              DB QUAL Conc               DB QUAL


                    SAMPLE TYPE:               SAMP                       SAMP                      SAMP
                    COUEC71ON DATE:            1989                       1991                      1989
                    RECEIPT DATE:
                    QCBATCH:                   M801                       M801                      M801
                    EXTRACTION DATE:           03/04/93                   03/04/93                  03/04/93
                    M[ETHOD:                   GCMS                       GCMS                      GCMS
                    ANALYSIS DATE:             04/06/93                   04/06/93                  04/06/93
                    MEMiOD:                    GCECD                      GCECD                     GCECD
                    ANALYSIS DATE:             05/03/93                   05/03/93                  05/03/93
                    MATRD(_                    TISSUE                     TISSUE                    TISSUE
                    SUBMAT:
                    SAMPLWT:
                    WINVT:                     8.574                      9.341                     10.393
                    DRYWT-                     2.08                       2.18                      2.12
                    VVI@S:                     GRAMS                      GRAMS                     GRAMS
                    PCTSOUDS:                  24.3%                      23.3%                     20.4%
                    VOL.
                    VOLUNITS:                  LITERS                     LITERS                    =RS


                    TOTAL BHC'S                0.00            ND         0.00           ND         0.61            1
                    TOTAL CHLORDANES           0.99            j          0.36           1          0.00            ND
                    TOTAL DDT`S                6.01                       4.25                      0.00            ND
                    TOTAL PCB'S                19.9                       16.1                      8.7


                    ALPHA-BHC                  0.00            ND         0.00           ND         0.00            ND
                    HCB                        0.64            j          0.30           1          0.64            1
                    BETA-BHC                   0.00            ND         0.00           ND         0.00            ND
                    GAMMA-BHC                  0.00            ND         0.00           ND         0.00            ND
                    DELTA-BHC                  0.00            ND         0.00           ND         0.61            j
                    HEPTACHLOR                 0.00            ND         0.00           ND         0.00            ND
                    HEPIA-EPO)aDE              0.57            1          0.00           ND         0.00            ND
                    OXYCHLORDANE               0.00            ND         0.00           ND         0.00            ND
                    GAMMA-CHLORDANE            0.00            ND         0.00           ND         0.00            ND
                    ALPHA-CHLORDANE            0.42            1          0.36           1          0.00            ND
                    n?ANS-NONACHLOR            0*00            ND         0,00           ND         0*00            ND
                    CIS-NONACHLOR              0.00            ND         0.00           ND         0.00            ND
                    ALDRIN                     0.00            ND         0.00           ND         0.00            ND
                    DIELDRIN                   0.00            ND         0.53           1          0.00            ND
                    ENDRIN                     0.00            ND         2.08                      0.00            ND
                    NUREX                      0.00            ND         0.00           ND         0.00            ND
                    2,41)DE (O,P`DDE)          0.00            ND         0.00           ND         0.00            ND
                    4,41)DE (P,P'DDE)          0.81            1          0.22           1          0.00            ND
                    2,4DDD (0,P'DDD)           0.41            1          0.09           1          0.00            ND
                    4.4'DDD (P,P'DDD)          0.00            ND         0.00           ND         0.00            ND
                    2.4'DDT (0.P'DDTj          3.60                       1.89                      0.00            ND
                    4,4'DDT (PPDDT)            1.19                       2.05                      0.00            ND


                    PCB # (CLORINATION)





                                                                     220







                                   Antarctic Limpet Samples -Polar Programs- Pesticides and PCB's


                      INVEST#:                     Station 20                  Station 20                 Transect D-7
                      ID:                          Cormorant Is                Cormorant Is               Herinit Islamd
                      LABSAMNO:                    J1310                       J 1850                     J1344
                      UNIT.                        ng/g                        ng/g                       ng/g
                      Analyte (Cont)               Conc            DB QUAL Conc                DB QUAL Conc                DB QUAL

                      8 (CL2)                      2.12                        0.27            1          1.62
                      18 (CL3)                     0.00            ND          0.00            ND         O.W              ND
                      28 (CL3)                     1.27                        0.52            1          1.27
                      44 (CIA)                     2.47                        1.40                       0.92             1
                      52 (CIA)                     0.00            ND          0.00            ND         0.00             ND
                      66 (CIA)                     3.10                        1.31                       0.00             ND
                      101 (CL5)                    1.12                        0.64            1          0.00             ND
                      105 (CL5)                    0.00            ND          0.00            ND         0.00             ND
                      110/77 (CL5/4)               0.55            1           0.00            ND         0.00             ND
                      118/108/149(CL5/5/6)         0.00            ND          0.00            ND         0.00             ND
                      128 (CL6)                    0.00            ND          0.00            ND         0.00             ND
                      138 (CL6)                    1.87                        5.47                       0.65             1
                      126 (CI-5)                                   NA                          NA                          NA
                      153 (CL6)                    0.00            ND          0.00            ND         0.00             ND
                      170 (CL7)                    0.00            ND          0.00            ND         0.00             ND
                      180 (CL7)                    1.24                        0.69            1          0.00             ND
                      187/182/159(CL7/7/6)         0.00            ND          0.50            1          0.00             ND
                      195 (CLS)                    0.00            ND          0.00            ND         0.00             ND
                      206 (CL9)                    0.00            ND          0.00            ND         0.00             ND
                      209 (CLIO)                   0.00            ND          0.00            ND         0.00             ND


                      Surrogate Recoveries
                      DBOFB%:                      67.8                        66.3                       68.7
                      PCB#103%:                    70.4                        72.0                       70.0
                      PCB#198%:                    88.0                        80.8                       81.5


                      OTHER PESTICIDES


                      ENDOSULFAN I
                      ENDOSULFAN H
                      ENDOSULFAN SULFATE
                      ENDRIN ALDEHYDE


                      PCB #(CHLORINATION)


                      7 (CL2)                      0.00            ND          0.00            ND         0.00             ND
                      15 (CL2)                     0.00            ND          0.00            ND         0.00             ND
                      24 (CI-3)                    0.00            ND          0.00            ND         0.00             ND
                      16/32 (CL3)                  0.00            ND          0.00            ND         0.00             ND
                      29 (CL3)                     0.00            ND          0.00            ND         0.00             ND
                      26 (CL3)                     0.00            ND          0.00            ND         0.00             ND
                      25 (CI.3)                    1.39                        0.00            ND         0.37             1
                      50 (CIA)                     0.41            1           0.61            1          0.00             ND
                      31 (CL3)                     0.00            ND          0.00            ND         0.00             ND
                      33 (CL3)                     0.00            ND          1.13                       0.00             ND
                      22 (CL3)                     0.00            ND          1.18                       0.00             ND
                      45 (CIA)                     0.00            ND          0.00            ND         0.00             ND
                      46 (CIA)                     0.00            ND          0.15            1          0.18             1
                      49 (CIA)                     0.00            ND          0.36            1          0.12             1



                                                                          221






                                  Antarctic Limpet Samples -Polar Programs- Pesticides and PCB's


                     NVESN:                       Station 20                  Station 20                  Transect D-7
                     ID:                          Cormorant Is                Cormorant Is                Hermit Island
                     LABSAMNO:                    J1310                       J1850                       J1344
                     UNM                          ng/g                        ng/g                        ng/g
                     Analyte (Cont)               Cone            DB QUAL Cone                DB QUAL Cone                 DB QUAL

                     47/48 (CIA)                  0.00            ND          0.00            ND          0.00             ND
                     37/42 (CIA)                  0.00            ND          0.25            1           0.00             ND
                     41/64 (CIA)                  0.00            ND          0.00            ND          0.00             ND
                     40 (CIA)                     0.00            ND          0.00            ND          0.00             ND
                     100 (CL5)                    0.00            ND          0.00            ND          0.00             ND
                     74 (CIA)                     0.00            ND          0.00            ND          0.00             ND


                     PCB #(CHLORINAMON)


                     70 (CIA)                     0.96            1           0.00            ND          0.00             ND
                     88 (CL15)                    0.00            ND          0.00            ND          0.00             ND
                     60/56 (CL.5)                 0.00            ND          0.00            ND          0.00             ND
                     92? (CL5)                    0.00            ND          0.00            ND          0.00             ND
                     84? (CL5)                    0.00            ND          0.00            ND          0.00             ND
                     99 (CL5)                     0.00            ND          0.00            ND          0.00             ND
                     83 (CL5)                     0.00            ND          0.00            ND          0.00             ND
                     97 (CL5)                     0.00            ND          0.00            ND          0.00             ND
                     87 (CL5)                     0.00            ND          0.00            ND          0.00             ND
                     85 (CL5)                     0.00            ND          0.00            ND          0.00             ND
                     136 (CL6)                    0.00            ND          0.00            ND          0.00             ND
                     82 (CL-5)                    0.00            ND          0.00            ND          0.00             ND
                     151 (CL6)                    0.00            ND          0.00            ND          0.00             ND
                     107/108/144(CL5/5/6)         0.00            ND          0.00            ND          0.00             ND
                     149 (CL6)                    0.00            ND          0.00            ND          0.00             ND
                     188 (CL7)                    0.00            ND          0.00            ND          1.48
                     146 (CL6)                    0.00            ND          0.00            ND          0.00             ND
                     141 (C1.66)                  0.00            ND          0.57            1           0.00             ND
                     137 (CL6)                    2.36                        0.00            ND          0.00             ND
                     UNK (CL6)                    0.00            ND          0.00            ND          0.00             ND
                     158 (CL7)                    0.00            rM          0.00            rM          0.00             M
                     129 (CW)                     0.00            ?w          0.00            M           0.00             NID
                     178 (CL7)                    0.00            ND          0.00            ND          0.00             ND
                     183 (CL7)                    0.00            ND          0.00            ND          0.00             ND
                     167 (CL6)                    0.00            ND          0.00            ND          0.00             ND
                     185 (CL7)                    0.00            ND          0.00            ND          0.00             ND
                     174 (CL7)                    0.00            ND          0.00            ND          0.00             ND
                     177 (CL7)                    0.00            ND          0.00            ND          0.00             ND
                     156/171/202(CL6/7/8)         0.00            ND          0.00            ND          0.00             ND
                     200 (CL8)                    0.00            ND          0.00            ND          0.00             ND
                     172 (CL7)                    0.00            ND          0.00            ND          0.00             ND
                     191 (CL7)                    0.00            ND          0.00            ND          0.00             ND
                     201 (CL8)                    0.00            ND          1.38                        2.06
                     196 (CL8)                    0.00            ND          0.00            ND          0.00             ND
                     189 (CL7)                    2.25                        0.90            j           0.00             ND
                     194 (CL8)                    0.00            ND          0.00            ND          0.00             ND
                     205 (CL9)                    0.00            ND          0.00            ND          0.00             ND







                                                                           222






                                 Antarctic IAmpet Samples -Polar Programs- Pesticides and PCB's


                    INVEST#:                   Transect D-7              Transect D- 11            Transect ]D- I I
                    H):                        Hermit Island             0' Palmer Sta             54' Palmer Sta
                    LABSAMNO:                  J1866                     J1871                     J1872
                    UNrr:                      ng/g                      ng/g                      ng/g
                    Analyte (Cont)             Cone           DB QUAL Cone              DB QUAL Cone               DB QUAL

                    SAMPLE TYPE:               SAMP                      SAMP                      SAMP
                    COLLECTION DATE:           1991                      1991                      1991
                    RECENT DATE:
                    9CBATCH:                   M802                      M802                      M802
                    EXTRACnON DATE:            03/04/93                  03/04/93                  03/04/93
                    hEMOD:                     GCMS                      GCMS                      GCMS
                    ANALYSIS DATE:             04/21/93                  04/21/93                  04/21/93
                    U=OD:                      GCECD                     GCECD                     GCECD
                    ANALYSIS DATE:             05/03/93                  05/03/93                  05/03/93
                    MATRDC-                    TISSUE                    TISSUE                    TISSUE
                    SUBMAT.
                    SAMPLWT:
                                               10.135                    10-005                    10.358
                    DRYWT:                     1.78                      2.15                      2.81
                    WIUNTr`S:                  GRAMS                     GRAMS                     GRAMS
                    -PCTSOUDS:                 17.60/6                   21.5%                     27.1%
                    VOL:
                    VOLUNUS:                   LITERS                    LITERS                    LITERS


                    TOTAL BHC'S                0.00           ND         0.00           ND         0.00            ND
                    TOTAL CHLORDANES,          0.00           ND         0.00           ND         0.00            ND
                    TOTAL DDT"S                0.25           1          0.27           1          0.00            ND
                    TOTAL PCB'S                10.2                      5.1            1          6.1


                    ALPHA-BHC                  0.00           ND         0.00           ND         0.00            ND
                    HCB                        0.20           1          0.09           1          0.08            1
                    BET`A-BHC                  0.00           ND         0.00           ND         0.00            ND
                    GAMMA-BHC                  0.00           ND         0.00           ND         0.00            ND
                    DELTA-BHC                  0.00           ND         0.00           ND         0.00            ND
                    HEPTACHLOR                 0.00           ND         0.00           ND         1.47            M
                    HEPIA-EPOXDE               0.00           ND         0.00           ND         0.00            ND
                    OXYCHLORDANE               0.00           ND         0.00           ND         0.00            ND
                    GAMMA-CHLORDANE            0.00           ND         0.00           ND         0.00            ND
                    ALPHA-CHLORDANE            0.00           ND         0.00           ND         0.00            ND
                    TRANS-NONACHLOR            0.00           ND         0.00           ND         0.00            ND
                    CIS-NONACHLOR              0.00           ND         0.00           ND         0.00            ND
                    ALDRIN                     0.00           ND         0.00           ND         0.00            ND
                    DIELDRIN                   0.00           ND         0.00           ND         0.00            ND
                    ENDRIN                     1.22                      0.00           ND         0.00            ND
                    bE[REX                     0.ob           ND         0.00           ND         0.00            ND
                    2.4'DDE (O.P'DDE)          0.00           DID        0.00           ND         0.00            ND
                    4,4'DDE (P.P'DDE)          0.25           1          0.27           1          0.00            ND
                    2,4'DDD (0,PDDD)           0.00           ND         0.00           ND         0.00            ND
                    4,4'DDD (P,PIDDD)          0.00           ND         0.00           ND         0.00            ND
                    2.4'DDT (0,PIDM            0.00           ND         0.00           ND         0.00            ND
                    4.4'DDT (P,P`DDT)          0.00           ND         0.00           ND         0.00            ND


                    PCB # (CLORINATION)




                                                                     223






                                  Antarctic I.Ampet. Samples -Polar Programs- Pesticides and PCB's


                    HiVEST#:                     Transect D-7                Transect D- 11               Transect D- 11
                    ID:                          Hermit Island               0'Palmer Sta                 54' Palmer Sta
                    L4BSAI*UIO:                  J11166                      J1871                        J1872
                    UNIT:                        ng/g                        ng/g                         ng/g
                    jAnalyte (Cont)              Conc            DB QUAL Conc                 DB QUAL Conc                DB QUAL

                    8 (CL2)                      2.36                        0.00             ND          1.78            M
                    18 (CL3)                     0.00            ND          0.00             ND          0.00            ND
                    28 (CL,3)                    0.14            j           0.20             j           0.00            ND
                    44 (CIA)                     0.00            ND          0.00             ND          0.00            ND
                    52 (CIA)                     0.00            ND          0.00             ND          0.00            ND
                    66 (CIA)                     0.21            j           0.82             1           2.01
                    101 (CL5)                    0.00            ND          0.00             ND          0.00            ND
                    105 (CL5)                    0.22            1           0.00             ND          0.00            ND
                    110/77(CL5/4)                0.05            j           0.08             j           0.00            ND
                    118/108/149(CL5/5/6)         0.00            ND          0.00             ND          0.18            1
                    128 (CLQ                     0.00            ND          0.00             ND          0.00            ND
                    138 (CL6)                    0.29            j           0.40             1           1.02            j
                    126 (CL5)                                    NA                           NA                          NA
                    153 (CL6)                    0.00            ND          0.00             ND          0.00            ND
                    170 (CL7)                    0.00            ND          0.00             ND          0.00            ND
                    180 (CL7)                    0.00            ND          0.47             j           0.00            ND
                    187/182/159(CL7/7/6)         0.00            ND          0.44             j           0.43            j
                    195 (CLB)                    0.00            ND          0.00             ND          0.00            ND
                    206 (CL9)                    0.00            ND          0.00             ND          0.00            ND
                    209 (CLIO)                   0.00            ND          0.00             ND          0.00            ND


                    Surrogate Recoveries
                    DBOFB%:                      68.0                        67.0                         65.4
                    PC13#103%:                   71.4                        70.2                         71.9
                    PCB#198%:                    71.0                        77.7                         84.9


                    OTHER PESTICIDES


                    ENDOSULFAN I
                    ENDOSULFAN 11
                    ENDOSULFAN SULFATE
                    ENDRIN ALDEHYDE


                    PCB #(CHLORINATION)

                    7 (CL2)                      0.00            ND          0.00             ND          0.00            ND
                    15 (CL2)                     0.00            ND          0.00             ND          0.00            ND
                    24 (CL3)                     0.99                        0.62             1           0.00            ND
                    16/32 (CL3)                  0.00            ND          0.14             j           0.00            ND
                    29 (CL3)                     0.00            ND          0.00             ND          0.00            ND
                    26 (CL3)                     0.67            1           0.34             j           0.00            ND
                    25(CL3)                      0.00            ND          0.28             j           0.00            ND
                    50 (CIA)                     0.17            1           0.14             j           0.00            ND
                    31 (CL3)                     0.00            ND          0.00             ND          0.00            ND
                    33(CL3)                      0.00            ND          0.00             ND          0.00            ND
                    22 (CL-3)                    0.00            ND          0.00             ND          0.00            ND
                    45 (CIA)                     0.00            ND          0.00             ND          0.00            ND
                    46 (CIA)                     4.13                        1.31                         1.18            1
                    49 (CIA)                     0.08            ND          0.07             j           0.05            j



                                                                         224






                                 Antarctic Limpet Samples -Polar Programs- Pesticides and PCB'E.



                                                                                                   Mransect D- 11
                    ID:                       Hermit Island             0' Palmer Sta              54' Palmer Sta
                    RiVESTM                   Transect D-7              Transect D- I I


                    TARSAMNO:                 J1866                     J1871                      J1872
                    UNM                       ng/g                      ng/g                       ng/g
                    Analyte (Cont)            Conc            DB QUAL Conc              DB QUAL Coric             DB QUAL

                    47/48 (CIA)               0.00            ND        0.00            ND         O.GD           ND
                    37/42 (CIA)               0.00            ND        0.00            ND         O.OD           ND
                    41/64 (CIA)               0.00            ND        0.00            ND         0.00           ND
                    40 (CIA)                  0.00            ND        0.00            ND         0.00           ND
                    100 (CL5)                 0.00            ND        0.00            ND         0.00           ND
                    74 (CIA)                  0.00            NE)       0.00            ND         0.00           ND


                    PCB #(CHLORINATION)


                    70 (CIA)                  0.00            NE)       0.00            ND         0.00           ND
                    88 (CL5)                  0.00            ND        0.00            ND         0.00           ND
                    60/56 (CL5)               0.00            ND        0.00            ND         0.00           ND
                    92? (CL5)                 0.00            ND        0.00            ND         0.00           ND
                    84? (CL5)                 0.38            1         0.16            1          0.00           NE)
                    99 (CL5)                  0.00            ND        0.00            ND         0.00           ND
                    83 (CL5)                  0.00            ND        0.00            ND         0.00           ND
                    97 (CL5)                  0.07            1         0.00            ND         0.00           ND
                    87 (CL5)                  0.07            1         0.00            NE)        0.00           ND
                    85 (CL5)                  0.00            ND        0.00            ND         0.00           ND
                    136 (CL6)                 0.00            ND        0.00            ND         0.00           ND
                    82 (CL5)                  0.00            ND        0.00            ND         0.00           NID
                    151 (CL6)                 0.00            ND        0.00            ND         0.00           ND
                    107/108/144(CL5/5/6)      0.00            NE)       0.00            ND         0.00           ND
                    149 (CL6)                 0.34            1         0.00            ND         0.48           1
                    188 (CL7)                 0.00            ND        0.00            ND         0.00           ND
                    146 (CLQ                  0.00            ND        0.00            ND         0.00           ND
                    141 (CL6)                 0.00            ND        0.00            ND         1.1.9          1                 1
                    137 (CL6)                 0.00            ND        0.44            j          0.00           ND
                    UNK (CL6)                 0.00            ND        0.00            ND         0.00           ND
                    158 (CL7)                 0.00            ND        0.00            ND         0.00           ND
                    129 (CL6)                 0.06            1         0.00            ND         0.00           ND
                    178 (CL7)                 0.00            ND        0.00            ND         0.00           NE)
                    183 (CL7)                 0.00            ND        0.00            ND         0.00           ND
                    167 (CL6)                 0.00            ND        0.00            ND         0.00           ND
                    185 (CL7)                 0.00            ND        0.00            ND         0.00           ND
                    174 (CL7)                 0.00            ND        0.11            j          0.00           ND
                    177 (CL7)                 0.00            ND        0.00            ND         0.00           ND
                    156/171/202(CL6/7/8)      0.00            ND        0.00            ND         0.00           ND
                    200 (CL8)                 0.00            ND        0.00            ND         0.00           ND
                    172 (CL7)                 0.00            ND        0.00            ND         0.00           ND
                    191 (CL7)                 0.00            ND        0.00            ND         0.00           ND
                    201 (CL8)                 0.00            ND        0.00            ND         0.00           ND
                    196 (CL8)                 0.00            ND        0.00            ND         0.00           ND
                    189 (CL7)                 0.00            ND        0.00            ND         0.00           ND
                    194 (CLS)                 0.00            ND        0.00            ND         0.00           ND
                    205 (CL9)                 0.00            ND        0.00            ND         0.00           ND






                                                                     225






                                  Antarctic I.Ampet Samples -Polar Programs- Pesticides and PCB's


                   INVES`r#:                   Transect D- 12             Transect D- 12             Transect D- 13
                   ID:                         0' Palmer Sta              62' Palmer Sta             0' Palmer Sta
                   LABSAMNO:                   J1875                      J1876                      J1881
                   UNIT-                       ng/g                       ng/g                       ng/g
                   [Analyte (Cont)             Conc           DB QUAL Conc                DB QUAL Conc              1313 QUAL

                   SAMPLE TYPE:                SAMP                       SAMP                       SAMP
                   COLLECTION DATE:            1991                       1991                       1991
                   RECEIFT DATE:
                   QCBATCH:                    M802                       M802                       M802
                   EXTRACI710N DATE:           03/04/93                   03/04/93                   03/04/93
                   METHOD:                     GCMS                       GCMS                       G4CM[S
                   ANALYSIS DATE:              04/21/93                   04/21/93                   04/22/93
                   MDMOD:                      GCECD                      GCECD                      GCECD
                   ANALYSIS DATE:              05/03/93                   05/03/93                   05/03/93
                   MATRDr-                     TISSUE                     TISSUE                     TISSUE
                   SUBMAT
                   SAMPLWT:
                   WFIVT:                      4.194                      10.086                     10
                   DRYWT.                      0.91                       2.01                       2.06
                   Vi'TUNITS:                  GRAMS                      GRAMS                      GRAMS
                   PCTSOLIDS:                  21.7%                      19.946                     20.60/6
                   VOL:
                   VOLUNITS:                   LJTERS                     =RS                        LUERS

                   TOTAL BHC'S                 0.00           ND          0.00            ND         0.00           ND
                   TOITALCHLORDANES            0.00           NI)         0.00            ND         0.74           1
                   TOTAL DDrS                  0.66           j           0.72            1          3.07
                   TOTAL PCB'S                 4.6                        4.0             j          52.0


                   ALPHA-BHC                   0.00           ND          0.00            ND         0.00           ND
                   HCB                         0.11           1           0.49            1          0.18           1
                   BETA-BHC                    0.00           ND          0.00            ND         0.00           ND
                   GAMMA-BHC                   0.00           ND          0.00            ND         0.00           ND
                   DELTA-BHC                   0.00           ND          0.00            ND         0.00           ND
                   HEPTACHLOR                  0.00           ND          0.00            ND         0.00           ND
                   HEPrA-EP02UDE               0.00           ND          0.00            ND         0.00           ND
                   OXYCHLORDANE                0.00           ND          0.00            ND         0.21           j
                   GAMMA-CHLORDANE             0.00           ND          0.00            ND         0.00           ND
                   ALPHA-CHLORDANE             0.00           ND          0.00            ND         0.00           ND
                   TRANS-NONACHLOR             0,00           ND          0*00            ND         0,20           J
                   CIS-NONACHLOR               0.00           ND          0.00            ND         0.33           j
                   ALDRIN                      0.00           ND          0.00            ND         0.00           ND
                   DIELDRIN                    0.00           ND          0.00            ND         0.00           ND
                   ENDRIN                      0.00           ND          0.00            ND         0.00           ND
                   M[IREX                      0.00           ND          0.00            ND         0.27           1
                   2.4'DDE (0,P'DDE)           0.00           ND          0.00            ND         0.00           ND
                   4,4'DDE (P,IYDDE)           0.66           1           0.00            ND         1.37
                   2.4'DDD (0,P`DDD)           0.00           ND          0.00            ND         0.27           1
                   4.4'DDD (P.FYDDD)           0.00           ND          0.72            1          0.83           j
                   2.4'DDT (0,VDEM             0.00           ND          0.00            ND         0.00           ND
                   4.4'DDT (P,IYDEM            0.00           ND          0.00            ND         0.60           1

                   PCB # (CLORINATION)




                                                                      226







                                   Antarctic Umpet Samples -Polar Programs- Pesticides and. PCB'!3


                     IN'VEST'#:                  TYansect D- 12              Transect, D- 12             Thmsect 13-13
                     ID:                         0' Palmer Sta               62' Palmer Sta              0' Palmer Sta
                     T A RSAMNO:                 J1875                       J1876                       J1881
                     UNM                         ng/g                        ng/g                        ng/g
                     Analyte (Cont)              Cone             DB QUAL Cone                DB QUAL Cone                DB QUAL

                     8 (CL2)                     0.69             1          0.00             ND         0.00             ND
                     18 (CL3)                    0.00             ND         0.00             ND         0.00             ND
                     28 (CIS)                    0.00             ND         0.00             ND         0.00             ND
                     44 (CIA)                    0.00             ND         0.00             ND         1.48
                     52 (CIA)                    0.00             ND         0.00             ND         0.40             1
                     66 (CIA)                    0.00             ND         0.00             ND         0.47             1
                     101 (CL5)                   0.00             ND         0.00             ND         3.37
                     105 (CL5)                   0.00             ND         0.00             ND         1.14
                     110/77(CL5/4)               0.00             ND         0.00             ND         3.27
                     118/108/149(CL5/5/6)        0.00             ND         0.00             ND         3.26
                     128(CL6)                    0.00             ND         0.00             ND         0.63             1
                     138(CL6)                    0.74             1          0.69             1          5.14
                     126(CL5)                                     NA                          NA                          NA
                     153 (CL6)                   0.00             ND         0.00             ND         8.68
                     170(CL7)                    0.00             ND         0.00             ND         0.00             ND
                     180(CL7)                    1.25                        0.37             1          7.37
                     187/182/159(CL7/7/6)        0.88             1          0.40             1          6.17
                     195 (CL8)                   0.00             ND         0.14             1          0.68             1
                     206 (CL9)                   0.00             ND         0.00             ND         0.79             1
                     209 (CLIO)                  0.00             ND         0.00             ND         0.00             ND


                     Surrogate Recoveries
                     DBOFB0/6:                   62.8                        65.7                        68.6
                     PCB#103%:                   69.4                        71.7                        76.0
                     PCB#198%:                   68.8                        83.4                        97.8


                     OMER PESTICIDES


                     ENDOSULFAN I
                     ENDOSULFAN B
                     ENDOSULFAN SULFATE
                     ENDRIN ALDEHYDE


                     PCB *(CHLORINATION)


                     7 (C12)                     0.00             ND         0.00             ND         0.00             ND
                     15 (CL2)                    0.00             ND         0.00             ND         0.00             ND
                     24 (CL3)                    0.00             ND         0.40             1          0.47             1
                     16/32 (CL3)                 0.00             ND         0.00             ND         0.00             ND
                     29 (CL3)                    0.00             ND         0.00             ND         0.00             ND
                     26(CL3)                     0.00             ND         0.00             ND         0.00             ND
                     25 (CL3)                    0.00             ND         0.40             1          0.65             1
                     50 (CIA)                    0.46             1          0.21             1          0.30             1
                     31 (CL3)                    0.00             ND         0.00             ND         0.00             ND
                     33 (CL3)                    0.00             ND         0.00             ND         0.00             ND
                     22 (CL3)                    0.00             ND         0.00             ND         0.00             ND
                     45 (CIA)                    0.00             ND         0.00             ND         0.00             ND
                     46 (CIA)                    1.04                        0.97             1          0.65             1
                     49 (CL4)                    0.00             ND         0.08             1          0.24             1



                                                                          227






                                 Antarctic Limpet Samples -Polar Programs- Pesticides and PCB's


                    D4VEST#:                   Transect D- 12             Transect D- 12             Transect D- 13
                    ID:                        0' Palmer Sta              62' Palmer Sta             0' Palmer Sta
                    LABSAMNO:                  J1875                      J 1876                     J1881
                    UNM                        ng/g                       ng/g                       ng/g
                    ,Analyte (Cont)            Conc            DB QUAL Conc               DB QUAL Conc               DB QUAL

                    47/48 (CIA)                0.00            ND         0.00            ND         0.00            ND
                    37/42 (CIA)                0.00            ND         0.00            ND         0.00            ND
                    41/64 (CIA)                0.00            ND         0.00            ND         0.00            ND
                    40 (CIA)                   0.00            ND         0.00            ND         0.00            ND
                    100 (CL5)                  0.00            ND         0.00            ND         0.00            ND
                    74 (CIA)                   0.00            ND         0.10            j          0.58


                    PCB #(CHLORINATION)


                    70 (CIA)                   0.00            ND         0.00            ND         0.70
                    88 (CL5)                   0.00            ND         0.00            ND         0.14
                    60/56 (CL5)                0.00            ND         0.00            ND         0.00            ND
                    92? JCL5)                  0.00            ND         0.00            ND         0.98            j
                    84? (CL5)                  0.00            ND         0.00            ND         0.67
                    99 (CL5)                   0.00            ND         0.00            ND         0.72
                    83 (CL5)                   0.00            ND         0.00            ND         0.31
                    97 (CL5)                   0.00            ND         0.00            ND         0.64
                    87 (CL5)                   0.00            ND         0.00            ND         1.40
                    85 (CL5)                   0.00            ND         0.00            ND         0.45
                    136 (CLQ                   0.00            ND         0.00            ND         0.00            ND
                    82 (CIZ)                   0.00            ND         0.00            ND         0.00            ND
                    151 (CLQ                   0.00            ND         0.00            ND         1.77
                    107/108/144(CLS/5/6)       0.00            ND         0.00            ND         0.00            ND
                    149 (CL6)                  0.00            ND         0.00            ND         2.95
                    188 (CL7)                  0.00            ND         0.00            ND         0.00            ND
                    146 (CL6)                  0.00            ND         0.00            ND         0.00            ND
                    141 (CL6)                  0.00            ND         0.00            ND         2.32
                    137 (CL6)                  0.00            ND         0.00            ND         0.58            j
                    UNK (CL6)                  0.00            ND         0.00            ND         0.22            j
                    158 (CL7)                  0.00            ND         0.00            ND         0.00            ND
                    129 (CL6)                  0.00            ND         0.00            ND         0.00            ND
                    178 (CL7)                  0.00            ND         0.00            ND         0.00            ND
                    183 (CL7)                  0.00            ND         0.10            j          0.00            ND
                    167 (CL6)                  0.00            ND         0.00            ND         0.00            ND
                    185 (CL7)                  0.33            1          0.16            j          0.49            j
                    174 (CL7)                  0.29            1          0.00            ND         3.58
                    177 (CL7)                  0.26            1          0.00            ND         1.97
                    156/171/202(CL6/7/8)       0.00            ND         0.00            ND         0.37
                    200 (CL8)                  0.00            ND         0.00            ND         0.00            ND
                    172 (CL7)                  0.73                       0.39            1          1.41
                    191 (CL7)                  0.00            ND         0.00            ND         0.00            ND
                    201 (CL8)                  0.00            ND         0.00            ND         4.63
                    196 (CL8)                  0.00            ND         0.51            j          2.17
                    189 (CL7)                  0.00            ND         0.00            ND         0.00            ND
                    194 (CL8)                  0.00            ND         0.00            ND         1.45
                    205 JCL9)                  0.00            ND         0.00            ND         0.00            ND






                                                                      228






                                  Antarctic Limpet Samples -Polar Programs- Pesticides and PCB's


                    INVEST#:                    Transect D- 13             Transect D- 14             Transect D-
                    ID:                         3 1' Palmer Sta            0' Old Palmer              30' Old Ralmer
                    LABSAMNO:                   J1880                      J1887                      J1883
                    UNIT.                       nglg                       ng/g                       ng/g
                    Analyte (Cont)              Conc            DB QUAL Conc              DB QUAL Conc               DB QUAL

                    SAMPLE IYPE:                SAMP                       SAMP                       SAMP
                    COLLE=ON DATE:              1991                       1991                       1991
                    RECEIPr DATE:
                    QCBATCH:                    M802                       M803                       M802
                    EXTRACTION DATE:            03/04/93                   03/05/93                   03/04/93
                    M=OD:                       GCMS                       GCM[S                      GCMS
                    ANALYSIS DATE:              04/21/93                   04/07/93                   04/22/93
                    M=OD:                       GCECD                      GCECD                      GCECD
                    ANALYSIS DATE:              05/03/93                   05/03/93                   05/03/93
                    MATRDC                      TISSUE                     TISSUE                     TISSUE
                    SUBMAT.
                    SAMPLWT:
                    WETVT-                      10.629                     3.744                      10.041
                    DRYWT:                      2.18                       0.7                        1.92
                    VVTLJNITS:                  GRAMS                      GRAMS                      GRAMS
                    PCTSOLIDS:                  20.5%                      18.7%                      19.1%
                    VOL.
                    VOLUNITS:                   LUERS                      =RS                        LITERS


                    TOTAL BHC'S                 0.00            ND         3.46                       0.00           ND
                    TOTAL CHLORDANES,           0.00            ND         5.05                       0.82           1
                    TOTAL DDTS                  0.76            1          2.47           1           2.12
                    TOTAL PCB'S                 7.0                        37.1                       5.9


                    AIYHA-BHC                   0.00            ND         0.00           ND          0.00           ND
                    HCB                         0.25            1          0.69           1           0.17           1
                    BETA-BHC                    0.00            ND         0.00           ND          0.00           ND
                    GAAUAA-BHC                  0.00            ND         1.73                       0.00           ND
                    DELTA-BHC                   0.00            ND         1.73                       0.00           ND
                    HEPTACHLOR                  0.00            ND         0.62                       0.00           ND
                    HEFrA-EPO=E                 0.00            ND         0.72                       0.29           1
                    OXYCHLORDANE                0.00            ND         0.00           ND          0.27           1
                    GAMMA-CHLORDANE             0.00            ND         1.22                       0.00           ND
                    ALPHA-CHLORDANE             0.00            ND         1.14                       0.00           ND
                    TRANS-NONACHLOR             0.00            ND         1.35                       0.18           j
                    CIS-NONACHLOR               0.00            ND         0.00           ND          0.08           1
                    ALDRIN                      0.00            ND         0.00           ND          0.00           ND
                    DIELDRIN                    0.00            ND         2.00                       0.00           ND
                    ENDRIN                      0.00            ND         2.06                       1.50
                    M[IREX                      0.00            ND         0.00           ND          0.21           1
                    2,4DDE (O,FDDE)             0.00            ND         0.00           ND          0.00           ND
                    4ADDE (P,P'DDE)             0.36            1          1.10           1           0.00           ND
                    2.4'DDD (O.P'DDD)           0.00            ND         0.00           ND          0.00           ND
                    4.4DDD (PP'DDD)             0.40            j          0.00           ND          0.81           1
                    2,4DDT (0,FYDEM             0.00            ND         1.36           1           0.00           ND
                    4,4'DDT (P,P'DIM            0.00            ND         0.00           ND          1.31


                    PCB 0 (CLORINATION)





                                                                       229






                                  Antarctic Limpet Samples -Polar Programs- Pesticides and PCB's


                    INVESTC                      Transect D- 13              Transect D- 14              Transect D- 14
                    ID:                          3 1' Palmer Sta             O'Old Palmer                30' Old Palmer
                    IA@NO:                       J18110                      J1887                       J1883
                    UNM                          ng/g                        ng/g                        ng/g
                    jAnalyte (Cont)              Conc            DB QUAL Conc                DB QUAL Conc                 DB QUAL

                    8 (CL2)                      0.00            ND          0.00            ND          0.00             ND
                    18 (CL3)                     0.00            ND          0.00            ND          0.00             ND
                    28 (CL3)                     0.00            ND          0.73                        0.00             ND
                    44 (CIA)                     0.00            ND          2.65                        0.55             1
                    52 (CIA)                     0.00            ND          1.39                        0.00             ND
                    66 (CIA)                     0.00            ND          0.07            j           0.00             ND
                    101 (CL5)                    0.00            ND          1.23                        0.00             ND
                    105 (CL5)                    0.00            ND          0.51                        0.00             ND
                    110/77 (CL5/4)               0.00            ND          0.47                        0.28             j
                    118/108/149(CL5/5/6)         0.61            1           2.59                        0.84             1
                    128 (CL65)                   0.06            1           3.74                        0.00             ND
                    138 (CL6)                    1.27                        9.85                        1.31
                    126 (CM                                      NA                          NA                           NA
                    153 (CL6)                    1.15                        3.19                        2.24
                    170 (CL7)                    0.00            ND          0.00            ND          0.00             ND
                    180 (CL7)                    1.07            j           4.53                        0.82             j
                    187/182/159(CL7/7/6)         1.03            1           5.59                        0.61             1
                    195 (CL8)                    0.00            ND          2.02                        0.00             ND
                    206 (CL9)                    0.00            ND          2.70                        0.00             ND
                    209 (CL10)                   0.00            ND          0.00            ND          0.00             ND


                    Surrogate Recoveries
                    DBOFB%:                      67.4                        57.8                        68.5
                    PCB#103%:                    73.0                        50.6                        73.8
                    PCI1# 198%:                  81*5                        43.8                        84.0


                    OTHER PES11CIDES,


                    ENDOSULFAN I
                    ENDOSULFAN 11
                    ENDOSULFAN SULFATE
                    ENDRIN ALDEHYDE


                    PCB #(CHLORINATION)

                    7 (CL2)                      0.00            ND          0.00            ND          0.00             ND
                    15 (CL2)                     0.00            ND          0.00            ND          0.00             ND
                    24 (M)                       0.00            ND          0.00            ND          0.00             ND
                    16/32 (CL3)                  0.00            ND          0.00            ND          0.00             ND
                    29 (CL3)                     0.00            ND          0.52                        0.00             ND
                    26 (CM)                      0.00            ND          0.00            ND          0.00             ND
                    25 (CL3)                     0.00            ND          0.00            ND          0.00             ND
                    50 (CIA)                     0.23            j           1.79            M           0.29             1
                    31 (CL3)                     0.00            ND          0.00            ND          0.00             ND
                    33 (CL3)                     0.00            ND          0.00            ND          0.00             ND
                    22 (CIS)                     0.00            ND          0.00            ND          0.05             1
                    45 (CIA)                     0.00            ND          0.00            ND          0.07             1
                    46 (CIA)                     0.48            j           0.00            ND          0.00             ND
                    49 (CIA)                     0.00            ND          0.00            ND          0.00             ND



                                                                        230







                                      Antarctic Limpet Samples -Polar Programs- Pesticides and PCB's


                       INVESM                        Transect D- 13                 Transect D- 14                Transect 13-14
                       ID:                           3 1' Palmer Sta                0' Old Palmer                 30' Old Palmer
                       IABSAMNO:                     J1880                          J1887                         J1883
                       UNIT'.                        ng/g                           ng/g                          ng/g
                       Analyte (Cont)                Conc               DB QUAL Conc                  DB QUAL Conc                  DB QUAL

                       47/48 (CIA)                   0.00               ND          0.00              ND          0.00              ND
                       37/42 (CIA)                   0.00               ND          0.00              ND          0.00              ND
                       41/64 (CIA)                   0.00               ND          0.00              ND          0.00              ND
                       40 (CIA)                      0.00               ND          0.00              ND          0.00              ND
                       100 (CL5)                     0.00               ND          0.00              ND          0.00              ND
                       74 (CIA)                      0.14               1           0.00              ND          0.112             1


                       PCB #(CHLORINATION)


                       70 (CIA)                      0.00               ND          0.15              1           0.00              ND
                       88 (CL5)                      0.00               ND          0.33              1           0.00              ND
                       60/56 (CL5)                   0.00               ND          0.00              ND          0.00              ND
                       92? (CL5)                     0.00               ND          0.00              ND          0.00              ND
                       84? (CL5)                     0.00               ND          0.00              ND          0.00              ND
                       99 (CL5)                      0.00               ND          0.00              ND          0.00              ND
                       83 (CL5)                      0.00               ND          0.00              ND          0.00              ND
                       97 (CI-5)                     0.00               ND          0.00              ND          0.00              ND
                       87 (CI.5)                     0.00               ND          1.12                          0.00              ND
                       85 (CIZ)                      0.00               ND          0.00              ND          0.00              ND
                       136 (CL6)                     0.00               ND          0.00              ND          0.00              ND
                       82 (CL5)                      0.00               ND          0.00              ND          0.00              ND
                       151 (CL6)                     0.00               ND          0.00              ND          0.09              1
                       107/108/144(CL5/5/6)          0.00               ND          0.00              ND          0.00              ND
                       149 (CL6)                     0.61               1           1.08                          0.66              1
                       188 (CL7)                     0.00               ND          6.28                          0.00              ND
                       146 (CL6)                     0.00               ND          0.00              ND          0.00              ND
                       141 (CL6)                     0.24               1           1.46                          0.39              1
                       137 (CL6)                     0.23               1           0.00              ND          0.21              1
                       UNK (CL6)                     0.00               ND          0.00              ND          0.00              ND
                       158 (CL7)                     0.00               ND          0.00              ND          0.00              ND
                       129 (CL6)                     0.00               ND          0.00              ND          0.00              ND
                       178 (CL7)                     0.00               ND          0.00              ND          0.00              ND
                       183 (CL7)                     0.00               ND          0.00              ND          0.00              ND
                       167 (CL6)                     0.00               ND          2.91                          0.00              ND
                       185 (CL7)                     0.00               ND          0.00              ND          0.00              ND
                       174 (CL7)                     0.41               1           0.00              ND          0.31              1
                       177 (CL7)                     0.27               1           0.00              ND          0.22              1
                       156/171/202(CL6/7/8)          0.00               ND          0.00              ND          0.00              ND
                       200 (CL8)                     0.00               ND          0.00              ND          0.00              ND
                       172 (CL7)                     0.35               1           0.00              ND          0.53              1
                       191 (CL7)                     0.00               ND          0.00              ND          0.00              ND
                       201 (CL8)                     1.45                           0.00              ND          0.00              ND
                       196 (CL8)                     0.48               1           0.00              ND          0.00              ND
                       189 (CL7)                     0.00               ND          0.00              ND          0.00              ND
                       194 (CL8)                     0.16               1           0.00              ND          0.00              ND
                       205 (CL9)                     0.00               ND          0.00              ND          0.00              ND






                                                                               231






                             Antarctic Limpet Samples -Polar Programs- Pesticides and PCB's


                 INVEST#:                  Transect D- 17          Transect D- 17          Transect D- 19
                 ID:                       0,                      60-62'                  0' Palmer Sta
                 LABSAMNO:                 J11193                  J1896                   J1882
                 UNIT.                     ng/g                    ng/g                    ng/g
                 jAnalyte (Cont)           Conc          DB QUAL Conc            DB QUAL Conc             DB QUAL

                 SAMPLE TYPE:              SAMP                    SAMP                    SAMP
                 COLLEC71ON DATE:          1991                    1991                    1991
                 RECEIPT DATE:
                 QCBATCH:                  M803                    M803                    M802
                 EXTRAC71ON DATE:          03/05/93                03/05/93                03/04/93
                 METHOD:                   GCM[S                   GCMS                    GCM[S
                 ANALYSIS DATE:            04/07/93                04/07/93                04/22/93
                 METHOD:                   GCECD                   GCECD                   GCECD
                 ANALYSIS DATE:            05/03/93                05/03/93                05/03/93
                 MATRIX                    TISSUE                  TISSUE                  TISSUE
                 SUBMAT:
                 SAMPLWT:
                 WETWT:                    4.006                   9.939                   10.184
                 DRYWT:                    0.88                    2.66                    2.1
                 VIIIJNrrS:                GRAMS                   GRAMS                   GRAMS
                 PCTSOLIDS:                22.00/6                 26.8%                   20.6%
                 VOL:
                 VOLUNITS:                 L=RS                    =RS                     LnERS


                 TOTAL BHC'S               0.00          ND        0.00          ND        0.00           ND
                 TOTAL CHLORDANES          2.10          j         1.01          1         0.45           j
                 TOTAL DDrS                0.81          j         0.76          1         6.24
                 TOTAL PCB'S               18.1                    10.0                    9.3


                 ALPHA-BHC                 0*00          ND        0*00          ND        0*00           ND
                 HCB                       1.10                    0.15          1         0.26           j
                 BETA-BHC                  0.00          ND        0.00          ND        0.00           ND
                 GAADAA-BHC                0.00          ND        0.00          ND        0.00           ND
                 DELTA-BHC                 0.00          ND        0.00          ND        0.00           ND
                 HEPTACHLOR                0.79          1         0.47          j         0.00           ND
                 HEPTA-EPO)(lDE            0.00          ND        0.00          ND        0.00           ND
                 OXYCHLORDANE              0.33          1         0.23          j         0.00           ND
                 GAMMA-CHLORDANE           0.00          ND        0.00          ND        0.00           ND
                 ALPHA-CHLORDANE           0.00          ND        0.00          ND        0.00           ND
                 TRANS-NONACHLOR           0,911         J         0,31          j         0,45           J
                 CIS-NONACHLOR.            0.00          ND        0.00          ND        0.00           ND
                 ALDRIN                    0.00          ND        0.00          ND        0.00           ND
                 DIELDRIN                  1.50                    0.00          ND        0.00           ND
                 ENDRIN                    0.87          j         0.00          ND        5.79           M
                 M[IREX                    0.00          ND        0.00          ND        0.00           ND
                 2,41)DE (O,P`DDE)         0.00          ND        0.00          ND        0.00           ND
                 4,4`DDE (P,P'DDE)         0.00          ND        0.45          j         0.00           ND
                 2,4'DDD (O.P'DDD)         0.81          1         0.31          1         0.00           ND
                 4,4`DDD (P.P'DDD)         0.00          ND        0.00          ND        2.33
                 2,4'DDT (O,P'DDT)         0.00          ND        0.00          ND        0.00           ND
                 4.4'DDT (P,P'DDT)         0.00          ND        0.00          ND        3.90


                 PCB # (CLORINATION)




                                                               232







                                    Antarctic I.Ampet Samples -Polar Programs- Pesticides and PCB's


                      WEST#:                      Transect D- 17              Transect D-17               Trwisect 13-19
                      ID:                         0.                          60-62'                      0' ]Palmer Sta
                      IABSAMNO:                   J1893                       J1896                       J1882
                      UNIT:                       ng/g                        ng/g                        nglg
                      ,Analyte (Cont)             Conc             DB QUAL Conc               DB QUAL Conc                DB,;)UAL

                      8 (CL2)                     0.00             ND         0.00            ND          0.00            ND
                      18 (CL3)                    0.00             ND         0.00            ND          0.00            ND
                      28 (CL3)                    0.64                        0.00            ND          0.00            ND
                      44 (CIA)                    3.77                        0.74            1           1.03            1
                      52 (CIA)                    0.53                        0.00            ND          0.00            ND
                      66 (CIA)                    0.00             ND         0.00            ND          0.00            ND
                      101 (CL5)                   0.00             ND         0.00            ND          0.00            ND
                      105 (CL5)                   0.32             1          0.00            ND          0.00            ND
                      110/77 (CL5/4)              0.00             ND         0.00            ND          0.24            1
                      118/108/149(CL5/5/6)        0.61                        0.00            ND          0.00            ND
                      128 (CL6)                   2.06                        0.00            ND          0.00            ND
                      138 (CL6)                   5.08                        1.39                        1.47
                      126 (CL5)                                    NA                         NA                          NA
                      153 (CL6)                   0.00             ND         0.00            ND          0.00            ND
                      170 (CL7)                   0.00             ND         0.00            ND          0.00            ND
                      180 (CL7)                   2.86                        0.80            1           0.68            1
                      187/182/159(CL7/7/6)        5.76                        1.27                        1.61
                      195 (CL8)                   1.45                        0.00            ND          0.00            ND
                      206 (CL9)                   1.10                        0.00            ND          0.00            ND
                      209 (CLIO)                  0.00             ND         0.00                        0.00            ND


                      Surrogate Recoveries
                      DBOFB%:                     61.0                        55.0                        63.4
                      PCB#103%:                   64.8                        63.1                        71.8
                      PCB#198%:                   84.1                        70.3                        85.1


                      OTHER PESTICIDES


                      ENDOSULFAN I
                      ENDOSULFAN 11
                      ENDOSULFAN SULFATE
                      ENDRIN ALDEHYDE


                      PCB #(CHLORIMAITON)


                      7 (CL2)                     0.00             ND         0.00            ND          0.00            ND
                      15 (CL2)                    0.00             NDD        0.00            ND          0.00            ND
                      24 (CL3)                    0.00             ND         0.00            ND          0.80            1
                      16/32 (CL3)                 0.00             ND         0.00            ND          0.00            ND
                      29 (CL3)                    0.00             ND         0.33            1           0.00            ND
                      26 (C1.3)                   0.00             ND         0.00            ND          0.00            ND
                      25 (CL3)                    0.53                        0.00            ND          0.00            ND
                      50 (CIA)                    0.00             ND         0.00            ND          0.84            1
                      31 (CI.3)                   0.00             ND         0.00            ND          0.00            ND
                      33 (CL3)                    0.00             ND         0.00            ND          0.00            ND
                      22 (CL3)                    0.00             ND         0.00            ND          0.00            ND
                      45 (CIA)                    0.00             ND         0.00            ND          0.25            1                   1
                      46 (CIA)                    0.00             ND         0.25            1           0.00            ND
                      49 (CIA)                    0.00             ND         0.00            ND          0.00            ND



                                                                         233






                                Antarctic I.Ampet Samples -Polar Programs- Pesticides and PCB's


                    UfVESr#:                   Transect D- 17            7Yansect D- 17             Transect D_ 19
                    ID:                        0,                        60-62'                     0' Ndmer Sta
                    1. A B,"- @ 0:             J1893                     J1896                      J1882
                    UNM                        ng/g                      ng/g                       ng/g
                    lAnalyte (Cont)            Conc            DB QUAL Conc              DB gUAL Conc               DB gUAL

                    47/48 (CIA)                0.00            ND        0.00            ND         0.00            ND
                    37/42 (CIA)                0.00            ND        0.00            ND         0.00            ND
                    41/64 (CIA)                0.00            ND        0.00            ND         0.00            ND
                    40 (CIA)                   0.00            ND        0.00            ND         0.00            ND
                    100 (CL5)                  0.00            ND        0.00            ND         0.00            ND
                    74 (ClA)                   0.00            ND        0.00            ND         0.83            1


                    PCB #(CHLORINAIION)


                    70 (CIA)                   0.00            ND        0.22            1          0.00            ND
                    88 (CL5)                   0.00            ND        0.05            1          0.00            ND
                    60/56 (CL5)                0.00            ND        0.00            ND         0.00            ND
                    92? (CL5)                  0.00            ND        0.00            ND         0.00            ND
                    84? (CL5)                  0.00            ND        0.00            ND         0.00            ND
                    99 (CL5)                   0.00            ND        0.15            1          0.00            ND
                    83 (CL5)                   0.00            ND        0.00            ND         0.00            ND
                    97 (CL5)                   0.00            ND        0.00            ND         0.00            ND
                    87 (CL5)                   0.57            j         0.00            ND         0.00            ND
                    85 (CL5)                   0.00            ND        0.00            ND         0.00            ND
                    136 (CL6)                  0.00            ND        0.00            ND         0.24            1
                    82 (CL5)                   0.00            ND        0.00            ND         0.00            ND
                    151 (CL6)                  0.00            ND        0.00            ND         0.00            ND
                    107/108/144(CL5/5/6)       0.00            ND        0.00            ND         0.00            ND
                    149 (CL6)                  0.86                      0.00            ND         0.00            ND
                    188 (CL7)                  0.00            ND        4.61                       0.00            ND
                    146 (CL6)                  0.00            ND        0.00            ND         0.00            ND
                    141 (CL6)                  0.00            ND        0.00            ND         0.00            ND
                    137 (CL6)                  0.00            ND        0.88            1          1.87
                    UNK (CL6)                  0.00            ND        0.00            ND         0.00            ND
                    158 (CL7)                  0.00            ND        0.00            ND         0.00            ND
                    129 (CL6)                  0.00            ND        0.34            j          0.55            1
                    178 (CL7)                  0.00            ND        0.47            1          0.00            ND
                    183 (CL7)                  0.00            ND        0.00            ND         0.00            ND
                    167 (CL6)                  1.30                      0.00            ND         0.00            ND
                    185 (CL7)                  0.00            ND        0.00            ND         0.00            ND
                    174 (CL7)                  0.00            ND        0.00            ND         0.13            1
                    177 (CL7)                  1.82                      0.00            ND         0.00            ND
                    156/171/202(CL6/7/8)       0.00            ND        0.00            ND         0.00            ND
                    200 (CLB)                  0.00            ND        0.59            1          0.00            ND
                    172 (CL7)                  0.00            ND        0.00            ND         0.85            1
                    191 (CL7)                  0.00            ND        0.00            ND         0.00            ND
                    201 (CLB)                  0.00            ND        0.00            ND         0.00            ND
                    196 (CLS)                  0.00            ND        0.00            ND         0.00            ND
                    189 (CL7)                  0.00            ND        0.00            ND         0.00            ND
                    194 (CL8)                  0.00            ND        0.00            ND         0.18            j
                    205 (CL9)                  0.00            ND        0.00            ND         0.00            ND







                                                                      234







                                   Antarctic Limpet Samples -Polar Programs- Pesticides and PCB's


                   If4VEST#:
                                                Transect D- 19             Transect D-7                Transect D-7
                   ID:                          42' Palmer Sta             Hermit Island               18'Hermit Island
                   IABSAMNO:                    J1886                      J1866                       J1865
                   UNIT:                        ng/g                       ng/g                        ng/g
                   ,Analyte (Cont)              Conc            DB QUAL Conc               DB QUAL Conc                   DB QUAL


                   SAWIF, TYPE:                 SAMP                       SAMP                        SAMP
                   CO1JX=ON DATE:               1991                       1991                        1991
                   RECEIFT DATE:
                   QCBATCH:                     M802                       M802                        M801
                   EXTRACTION DATE:             03/04/93                   03/04/93                    03/04/93
                   METHOD:                      GCM[S                      GCMS                        GCMS
                   ANALYSIS DATE:               04/22/93                   04/21/93                    04/06/93
                   METHOD:                      GCECD                      GCECD                       GCECD
                   ANALYSIS DATE:               05/03/93                   05/03/93                    05/03/93
                   MATRIK                       TISSUE                     TISSUE                      TISSUE
                   SUBMAT:
                   SAMPLWr:
                   VVE`INff:                    10.116                     10.135                      8.253
                   DRYWr:                       2.5                        1.78                        1.47
                   V7IUNn'S:                    GRAMS                      GRAMS                       GRAMS
                   PCT'SOIJDS:                  24.7%                      17.6%                       17.8%
                   VOL:
                   VOL,UNTrS:                   1=RS                       =RS                         LnERS


                   TOTAL BHC'S                  0.00            ND         0.00            ND          0.00               ND
                   TOTAL CHLORDANES             0.24            1          0.00            ND          0.00               ND
                   TOTAL DDTS                   1.82            1          0.25            1           0.00               ND
                   TOTAL PCB'S                  7.0             1          7.9                         4.8


                   ALPHA-BHC                    0.00            ND         0.00            ND          0.00               NJ)
                   HCB                          0.24            1          0.20            j           0.45               1                1
                   BETA-BHC                     1.53            M          0.00            ND          0.00               ND
                   GAMMA-BHC                    0.00            ND         0.00            ND          0.00               ND
                   DELTA-BHC                    0.00            ND         0.00            ND          0.00               ND
                   HEPTACHLOR                   0.24            1          0.00            ND          0.00               ND
                   HEP`IA-EPOXIDE               0.00            ND         0.00            ND          0.00               ND
                   OXYCHLORDANE                 0.00            ND         0.00            ND          0.00               ND
                   GAMMA-CHLORDANE              0.00            ND         0.00            ND          0.00               ND
                   ALPHA-CHLORDANE              0.00            ND         0.00            ND          0.00               ND
                   TRANS-NONACHLOR              0.00            ND         0.00            ND          0.00               ND
                   CIS-NONACHLOR                0.00            ND         0.00            ND          0.00               ND
                   ALDRIN                       0.00            ND         0.00            ND          0.00               ND
                   DIELDRIN                     0.00            ND         0.00            ND          0.00               M)
                   ENDRIN                       0.00            ND         1.22                        0.00               M3
                   M[IREX                       0.00            ND         0.00            ND          0.00               M3
                   2.4'DDE (O,FDDE)             0.00            ND         0.00            ND          0.00               M:)
                   4.4'DDE (P,P'DDE)            0.42            j          0.25            1           0.00               M3
                   2,4`DDD (O.FYDDD)            0.00            ND         0.00            ND          0.00               M3
                   4,4`DDD (P,FDDD)             0.54            1          0.00            ND          0.00               M:)
                   2,4'DDT (O.VDEM              0.00            ND         0.00            ND          0.00               M:)
                   4.4'DDT (P.PID"              0.86            1          0.00            ND          0.00               M3


                   PCB # (CLORINATION)





                                                                        235






                                Antarctic IAmpet, Samples -Polar Programs- Pesticides and PCB's


                 INVEST#:                   Transect D- 19             Transect D-7               Transect, D-7
                 ID:                        42' Palmer Sta             Hermit Island              18'Herrrdt Island
                 LABSWNO:                   J11186                     J1866                      J1865
                 UNIT:                      ng/g                       ng/g                       ng/g
                 ,Analyte (Cont)            Conc             DB QUAL Conc              DB QUAL Conc                  DB QUAL,

                 8 (CI.2)                   0.00             ND        2.36            M          0.00               ND
                 18 (CL3)                   0.00             ND        0.00            ND         0.00               ND
                 28 (CL3)                   0.00             ND        0.14            j          1.01
                 44 (CIA)                   0.00             ND        0.00            ND         0.76               j
                 52 (CIA)                   0.00             ND        0.00            ND         0.00               ND
                 66 (CIA)                   0.00             ND        0.21            j          0.00               ND
                 101 (CLZ)                  0.00             ND        0.00            ND         0.00               ND
                 105 (Ciz)                  0.00             ND        0.22            j          0.00               ND
                 110/77(CL5/4)              0.20             j         0.05            j          0.00               ND
                 118/108/149(CIZ/5/6)       0.63             j         0.00            ND         0.00               ND
                 128 (CL6)                  0.00             ND        0.00            ND         0.00               ND
                 138 (CL6)                  0.80             j         0.29            j          0.00               M
                 126 (CIZ)                                   NA                        NA                            NA
                 153 (CL6)                  0.67             j         0.00            ND         0.00               ND
                 170 (CL7)                  0.00             ND        0.00            ND         0.00               ND
                 180 (CL7)                  0.74             j         0.00            ND         0.77
                 187/182/159(CL7/7/6)       0.56             j         0.00            ND         0.00               ND
                 195 (CLB)                  0.08             j         0.00            ND         0.00               ND
                 206(CL9)                   0.00             ND        0.00            ND         0.00               ND
                 209(CLIO)                  0.00             ND        0.00            ND         0.00               ND

                 Surrogate Recoveries
                 DBOFB%:                    64.0                       68.0                       63.9
                 PCB#103%:                  73.9                       71.4                       67.5
                 PCB#198%:                  117*0                      71.0                       70.5


                 OTHER PESTICIDES


                 ENDOSULFAN I
                 ENDOSULFAN B
                 ENDOSULFAN SULFATE
                 ENDRIN ALDEHYDE


                 PCB #(CHLORINATION)


                 7 (CL2)                    0.00             ND        0.00            ND         0.00               ND
                 15 (CL2)                   0.00             ND        0.00            ND         0.00               ND
                 24 (CL3)                   0.37             j         0.99                       0.00               ND
                 16/32 (CL3)                0.00             ND        0.00            ND         0.00               ND
                 29 (CL3)                   0.00             ND        0.00            ND         0.00               ND
                 26 (CL3)                   0.00             ND        0.67            j          0.00               ND
                 25 (CL3)                   0.00             ND        0.00            ND         0.00               ND
                 50 (CIA)                   0.40             j         0.17            j          0.97
                 31 (CL3)                   0.00             ND        0.00            ND         0.00               ND
                 33 (CL3)                   0.00             ND        0.00            ND         0.00               ND
                 22(CL3)                    0.00             ND        0.00            ND         0.00               ND
                 45 (CIA)                   0.00             ND        0.00            ND         0.00               ND
                 46 (CIA)                   0.61             j         4.13                       0.00               ND
                 49 (CIA)                   0.13             j         0.08            j          0.11



                                                                    236







                                   Antarctic Limpet Samples -Polar Programs- Pesticides and PCB's


                   INVEST#:                     Transect D- 19              Transect D-7                 Transect D-7-
                   ID:                          42' Palmer Sta.             Hermit Island                18'Hermit Island
                   LABSAMNO:                    J1886                       J1866                        J1865
                   UNM                          ng/g                        ng/g                         ng/g
                   Analyte (Cont)               Conc             DB QUAL Conc                DB QUAL Conc                    DB_QUAL

                   47/48 (CIA)                  0.00             ND         0.00             ND          0.00                ND
                   37/42 (CIA)                  0.00             ND         0.00             ND          0.00                ND
                   41/64 (CIA)                  0.00             ND         0.00             ND          0.00                NID
                   40 (CIA)                     0.00             ND         0.00             ND          0.00                NID
                   100 (CL5)                    0.00             ND         0.00             ND          0.00                NID
                   74 (CIA)                     0.00             ND         0.00             ND          0.00                ND


                   PCB #(CHLORINATION)


                   70 (CIA)                     0.00             ND         0.00             ND          0.00
                   88 (CL5)                     0.00             ND         0.00             ND          0.00                NE,
                   60/56 (CL5)                  0.00             ND         0.00             ND          0.00                DMI
                   92? (CL5)                    0.00             ND         0.00             ND          0.00                NE,
                   84? (CL5)                    0.00             ND         0.38             1           0.00                NE,
                   99 (CL5)                     0.00             ND         0.00             ND          0.00                NE,
                   83 (CL5)                     0.00             ND         0.00             ND          0.00                NE,
                   97 (CL5)                     0.00             ND         0.07             1           0.00                NEI
                   87 (CL5)                     0.00             ND         0.07             1           0.00                NE,
                   85 (CL.5)                    0.00             ND         0.00             ND          0.00                NEI
                   136 (CL66)                   0.00             ND         0.00             ND          0.00                NID
                   82 (CL5)                     0.00             ND         0.00             ND          0.00                NE,
                   151 (CL66)                   0.00             ND         0.00             ND          0.00                NEI
                   107/108/144(CL5/5/6)         0.00             ND         0.00             ND          0.00                NEI
                   149 (CL6)                    0.66             1          0.34             1           0.00                NEI
                   188 (CL7)                    0.00             ND         0.00             ND          0.00                NEI
                   146 (CL6)                    0.00             ND         0.00             ND          0.00                NEI
                   141 (CL6)                    0.00             ND         0.00             ND          0.00                NEI
                   137 (CL6)                    0.61             1          0.00             ND          0.00                NEI
                   UNK (CL6)                    0.00             ND         0.00             ND          0.00                NEI
                   158 (CL7)                    0.00             ND         0.00             ND          0.00                NEI
                   129 (CL6)                    0.22             1          0.06             j           0.00                NEI
                   178 (CL7)                    0.00             ND         0.00             ND          0.00                NEI
                   183 (CL7)                    0.00             ND         0.00             ND          0.00                NID
                   167 (CL6)                    0.00             ND         0.00             ND          0.00                NEI
                   185 (CL7)                    0.00             ND         0.00             ND          0.00                NEI
                   174 (CL7)                    0.32             1          0.00             ND          0.00                ND
                   177 (CL7)                    0.00             ND         0.00             ND          0.00                NEI
                   156/171/202(CL6/7/8)         0.00             ND         0.00             ND          0.00                NEI
                   200 (CLB)                    0.00             ND         0.00             ND          0.00                ND
                   172 (CL7)                    0.56             1          0.00             ND          0.00                NEI
                   191 (CL7)                    0.00             ND         0.00             ND          0.00                NEI
                   201 (CL8)                    0.88             1          0.00             ND          1.91
                   196 (CL8)                    0.39             1          0.00             ND          0.00                NEI
                   189 (CL7)                    0.00             ND         0.00             ND          0.00                NEI
                   194 (CL8)                    0.23             1          0.00             ND          0.00                NEI
                   205 (CL9)                    0.00             ND         0.00             ND          0.00                NEI






                                                                          237






                                Antarctic Limpet Samples -Polar Programs- Pesticides and PCB's


              INVESTC                     Station 12               Transect D- 14                      LAB QA SAMPLE
              ID:                         Janus Island             ANIARC NIST      M801               Station 12
              IABSAMNO:                   J1840                    Q4882                               Q4883
              UNM.                        ng/g                     ng/g                                ng/g
              Analyte (Cont)              Conc          DB QUAL Conc                       DB QUAL Conc                  DB QUAL


              SAMPIE TYPE:                SAMP                     SRM                                 DUP OF J1840
              COLLECTION DATE:            1991
              RECEIFT DATE:
              QCBATCH:                    M801                     M801                                M801
              EXTRACTION DATE:            03/04/93                 03/04/93                            03/04/93
              WSMiOD:                     GCMS                     GCMS                                GCMS
              ANALYSIS DATE:              04/06/93                 04/06/93                            04/06/93
              W&MiOD:                     GCECD                    GCECD                               GCECD
              ANALYSIS DATE:              05/03/93                 05/03/93                            05/03/93
              MATREK-                     TISSUE                   TISSUE                              TISSUE
              SUBMAT:
              SAMPLWr:
              WETwr.                      9.764                    5.049                               9.614
              DRYWr:                      2.18                     0.67                                2.04
              V#IIJNrrS:                  GRAMS                    GRAMS                               GRAMS
              PCTWLJDS:                   22.3%                    13.3%                               21.2%
              VOL:
              VOLUNITS:                   lXrERS                   LMERS                               LXMRS


              TOTAL BHC'S                 2.14                     10.78                               3.02
              TOTAL CHLORDANES            0.00          ND         78.74                               0.00              ND
              WIAL DDTS                   1.81                     123.18                              1.01
              TOTAL PCB'S                 11.3                     2190.7                              12.5


              ALPHA-BHC                   0*57          J          3,79                                0.92
              HCB                         0.24          1          0.09                    1           0.32
              BErA-BHC                    0.00          ND         2.43                                0.00
              GAMMA-BHC                   1.58                     0.00                    ND          2.10
              DELTA-BHC                   0.00          ND         4.56                                0.00              ND
              HEFTACHLOR                  0.00          ND         0.00                    ND          0.00              ND
              HEFTA-EPOME                 0.00          ND         0.00                    ND          0.00              ND
              OXYCHIA)RDANE               0*00          ND         9*90                                0.00              ND
              GAMMA-CHLORDANE             0.00          ND         17.16                               0.00              ND
              ALPHA-CHLORDANE             0.00          ND         21.01                               0.00              ND
              TRANS-NONACHLOR             0.00          ND         18.94                               0.00              ND
              CIS-NONACHLOR               0.00          ND         11.73                               0.00              ND
              ALDRIN                      0.00          ND         0.00                    ND          0.00              ND
              DIELDRIN                    0.95          1          11.43                               0.00              ND
              ENDRIN                      1.10                     0.00                    ND          1.55
              AGREX                       0.00          ND         0.46                                0.00              ND
              2.41DDE (O,P'DDE)           0.00          ND         3.64                                0.00              ND
              4,473DE (P.VDDE)            0.00          ND         46.98                               0.00              ND
              2.49DDD (O.VDDD)            0.00          ND         7.55                                0.00              ND
              4.4DDD (P.FDDD)             0.00          ND         50.53                               0.00              ND
              2.41)DT (O.P'DDT)           1.23                     7.86                                1.01
              4.41)DT (PP'DDT)            0.57          1          6.63                                0.00              ND


              PCB # (CLA)RINATION)




                                                                      238






                                 Antarctic Iimpet Samples -Polar Programs- Pesticides and PCB'S


               WEST#:                    StaUon 12               Transect D- 14                    IAB QA
               ED:                       Janus Island            ANTARC NIST M801                  Station 12
               LABSAMNO:                 J1840                   Q4882                             Q4883
               UNIT:                     ng/g                    ng/g                              ng/g
               jAnalyte (Cont)           Conc           DB QUAL Conc                    DB QUAL Conc                 DB QUAL

               8 (CL2)                   0.45           1        7.84                              0.79              1
               18 (CL3)                  0.00           ND       15.46                             0.00              ND
               28 (CL3)                  0.82           J        84.51                             :1.37
               44 (CIA)                  1.38                    76.63                             :1.36
               52 (CIA)                  0.00           ND       92.31                             0.51
               66 (CIA)                  0.76           1        114.94                            0.00              ND
               101 (CL5)                 0.33           1        109.85                            0.82              1
               105 (CL5)                 0.36           1        41.90                             0.16              J
               110/77(CL5/4)             0.00           ND       125.29                            0.00              ND
               118/108/149(CIZ/5/6)      0.00           ND       112.35                            0.00              ND
               128 (CL6)                 0.00           ND       15.80                             0.00              ND
               138 (CL6)                 1.47                    117.34                            1.05
               126 (CIZ)                                NA                                                           NA
               153 (CL6)                 0.79           1        138.89                            0.00              ND
               170 (CL7)                 0.00           ND       0.00                   ND         0.00              ND
               180 (CL7)                 0.44           1        16.58                             0.33              1
               187/182/159(CL7/7/6)      0.00           ND       30.87                  ND         0.00              ND
               195 (CLB)                 0.00           ND       0.00                   1          0.00              ND
               206 (CL9)                 0.00           ND       0.78                              0.00              ND
               209 (CLIO)                0.00           ND       0.00                   ND         0.00              ND

               Sumogate Recoveries
               DBOFB%:                   64.7                    66.3                              63.8
               PCB#103%:                 72.1                    69.4                              69.9
               PCB#198%:                 79.3                    77.5                              76.0

               OTHER PESMCIDES,


               ENDOSULFAN I
               ENDOSULFAN II
               ENDOSULFAN SULFATE
               ENDRIN ALDEHYDE


               PCB #(CHLORINAnON)

               7 (CL2)                   0.00           ND       0.00                   ND         0.00              ND
               15 (CL2)                  0.00           ND       41.16                             0.00              ND
               2 4 (C 1,43)              0.00           ND       9.02                              0.00              ND
               16/32(CL3)                0.00           ND       22.76                             0.00              ND
               29 (CL3)                  0.00           ND       0.00                   ND         0.00              ND
               26 (CIZ)                  0.00           ND       13.99                             0.00              ND
               25 (CL3)                  0.00           ND       14.62                             0.00              ND
               50 (CIA)                  0.31           1        29.70                             0.63              1          1
               31 (CL3)                  0.00           ND       0.00                   ND         0.00              ND
               33 (CI.3)                 0.00           ND       9.15                              1.98
               22 (CL3)                  0.00           ND       13.57                             0.00              ND
               45 (CIA)                  0.00           ND       10.45                             0.00              ND
               46 (CIA)                  0.00           ND       3.82                              0.18              1
               49 (CIA)                  0.30           J        101.62                            0.36              1



                                                                    239






                                Antarctic I.Ampet Samples -Polar Programs- Pesticides and PCB's


              uqvEsr#:                    Station 12               TTansect D- 14                     LAB QA SAMPLE
              ID:                         Janus Island             AWARC NIST       M801              Station 12
              IABSAMNO:                   J1840                    g4882                              Q4883
              UNTP                        ng/g                     ng/g                               ng/g
              lAnalyte (Cont)             Conc          DB QUAL Cone                       DB QUAL Cone                  DB QUAL

              47/48 (CIA)                 0.00          ND         85.82                              0.00               ND
              37/42 (CIA)                 0.00          ND         49.16                              0.00               ND
              41/64 (CIA)                 0.00          ND         67.32                              0.00               ND
              40 (CIA)                    0.00          ND         12.44                              0.00               ND
              100 (CL5)                   0.00          ND         0.00                    ND         0.00               ND
              74 (CIA)                    0.00          ND         71.86                              0.00               ND


              PCB #(CHLORINAIION)


              70 (CIA)                    0.37          1          112.95                             0.60               1
              88 (CL5)                    0.00          ND         22.81                              0.00               ND
              60/56 (CL5)                 0.00          ND         70.91                              0.00               ND
              92? (CL5)                   0.00          ND         30.87                              0.00               ND
              84? (CL5)                   0.00          ND         32.77                              0.00               ND
              99 (CL5)                    0.00          ND         68.84                              0.00               ND
              83 (CL5)                    0.00          ND         13.96                              0.00               ND
              97 (CL5)                    0.00          ND         40.18                              0.00               ND
              87 (CL5)                    0.00          ND         59.10                              0.00               ND
              85 (CL5)                    0.00          ND         27.71                              0.00               ND
              136 (CL6)                   0.00          ND         0.00                    ND         0.00               ND
              82 (CL5)                    0.00          ND         18.02                              0.00               ND
              151 (CL6)                   0.00          ND         24.15                              0.52               1
              107/108/144(CL5/5/6)        0.00          ND         0.00                    ND         0.00               ND
              149 (CL6)                   0.00          ND         62.76                              0,00               ND
              188 (CL7)                   0.00          ND         0.00                    ND         0.00               ND
              146 (CL6)                   0.00          ND         19.58                              0.00               ND
              141 (CL6)                   0.00          ND         8.54                               0.00               ND
              137 (CLQ                    0.00          ND         1.82                               0.00               ND
              UNK (CL6)                   0.00          ND         10.06                              0.00               ND
              158 (CL7)                   0.00          ND         16.77                              0.54               1
              129 (CL6)                   0.00          ND         0.00                    ND         0.00               ND
              178 (CL7)                   0.00          ND         6.24                               0.00               ND
              183 (CL7)                   0.00          ND         17.18                              0.00               ND
              167 (CL6)                   0.00          ND         4.52                               0.00               ND
              185 (CL7)                   0.00          ND         0.00                    ND         0.00               ND
              174 (CL7)                   0.00          ND         0.00                    ND         0.00               ND
              177 (CL7)                   0.00          ND         14.20                              0.00               ND
              156/171/202(CLro/7/8)       0.83          1          7.19                               0.00               ND
              200 (CL8)                   0.00          ND         5.34                               0.00               ND
              172 (CL7)                   1.06          J          10.27                              0.00               ND
              191 (CL7)                   0.00          NDD        1.31                               0.00               ND
              201 (CLS)                   1.79                     5.63                               0.90
              196 (CL8)                   0.00          NDD        4.85                               0.00               ND
              189 (CL7)                   1.13                     0.00                    ND         0.78
              194 (CL8)                   0.00          ND         1.55                               0.00               ND
              205 (CL9)                   0.00          ND         0.00                    ND         0.00               ND






                                                                         240






                                 Antarctic Limpet Samples -Polar Programs- Pesticides and PCB's


            DPIESr#:                   LAB GA SAMPLE                 LAB QA SAMPLE                           Transect D - 19
            ID:                        PROC BLANK                    Station 12                              4.2' Palmer Sta
            LABSAMNO:                  Q4884                         g4885                                   J 1886
            UNrr.                      ng/g                          ng/g                                    101g/g
            ,Analyte (Cont)            Conc               DB QUAL Conc                 DB gUAL               Conc            DB QUAL

            SAMPLE TYPE:               BLK                           MS OF J 1840                 REF OIL    SAMP
            COLLECTION DATE:
            RECEIFT DATE:
            QCBATCH:                   M801                          M801                         M801       M802
            EXTRACIION DATE:           03/04/93                      03/04/93                                03/04/93
            NETHOD:                    G4CMS                         GCMS                         GCMS       GCMS
            ANALYSIS DATE:             04/06/93                      04/06/93                     04/06/93 04/22/93
            ME'niOD:                   GCECD                         GCECD                        GCECD      GCECD
            ANALYSIS DATE:             05/03/93                      05/03/93                                05/03/93
            MATRDC                     TISSUE                        TISSUE                       TISSUE     TISSUE
            SUBMAT:
            SAMPLWr-
            VIETwr:                    10                            9.896                                   10.116
            DRYWr-                     10                            2.14                         1          2.5
            Vi-f UNIT!S:               GRAMS                         GRAMS                        GRAMS      GRAMS
            PCI'SOLIDS:                100.0%                        21.6%                                   24.7%
            VOL:
            VOLUNTTS:                  LUERS                         lXrERS                       LITERS     LITERS

            TOTAL BHC'S                0.00               ND                           NA                    0.00            ND
            TOTAL CHLORDANES,          0.00               ND                           NA                    0.24            1
            TOTAL DDT"S                0.00               ND                           NA                    1.82            1
            TOTAL PCB'S                3.4                1                            NA                    7.0             j

            AI,PHA-BHC                 0.00               ND         77.0                                    0.00            ND
            HCB                        0.00               ND         99.0                                    0.24            1
            BETA-BHC                   0.00               bm         29.0                                    1.53            M
            GAMMA-BHC                  0.00               ND         88.0                                    0.00            ND
            DELTA-BHC                  0.00               ND         85.0                                    0.00            ND
            HEPTACHLOR                 0.00               ND         94.0                                    0.24            1
            HEPTA-EPOME                0.00               ND         82.0                                    0.00            ND
            OXYCHLORDANE               0.00               ND                           NA                    0.00            ND
            GAMMA-CHLORDANE            0.00               ND         89.0                                    0.00            ND
            ALPHA CHLORDANE            0.00               ND         81.0                                    0.00            ND
            TRANS-NONACHLOR            0.00               ND         90.0                                    0.00            ND
            CIS-NONACHLOR              0.00               ND                           NA                    0.00            ND
            ALDRIN                     0.00               ND         89.0                                    0.00            ND
            DIELDRIN                   0.62               1          89.0                                    0.00            ND
            ENDRIN                     0.00               ND         96.0                                    0.00            ND
            ACF.EX                     0.00               ND         95.0                                    0.00            ND
            2,41)DE (O,PDDE)           0.00               ND         83.0                                    0.00            ND
            4.41)DE (P,P`DDE)          0.00               ND         92.0                                    0.42            1
            2,41)DD (O,P`DDD)          0.00               ND         110.0                                   0.00            ND
            4,41)DD (P,FDDD)           0.00               ND         127.0                                   0.54            1
            2,4*DDT (O,PDEM            0.00               ND         71.0                                    0.00            ND
            4.4'DDT (P,PDEM            0.00               ND         91.0                                    0.86            1
                                                                                                                                 4JUAL











            PCB # (CLORINAMON)




                                                                        241






                                 Antarctic I.Ampet Samples -Polar Programs- Pesticides and PCB's


           INVESr*:                    LAB gA SAMPLE                   LA13 QA SAMPLE                            Transect D- 19
           ID:                         PROC BLANK                      Station 12                                42' Palmer Sta
           LABSAMNO:                   Q4884                           Q4885                                     J1886
           UNIT:                       ng/g                            ng/g                                      ng/g
           Analyte (Cont)              Conc                DB QUAL Conc                   DB QUAL                Cone             DB QUAL

           8 (CL2)                     0.00                ND          80.0                                      0.00             ND
           18 (CL3)                    0.00                ND          50.0                                      0.00             ND
           28 (CL3)                    0.00                ND          102.0                                     0.00             ND
           44 (CIA)                    0.74                j           109.0                                     0.00             ND
           52 (CIA)                    0.00                ND          109.0                                     0.00             ND
           66 (CIA)                    0.00                ND          123.0                                     0.00             ND
           101 (CL5)                   0.00                ND          98.0                                      0.00             ND
           105 (CL5)                   0.00                ND          108.0                                     0.00             ND
           110/77(CL5/4)               0.00                ND          78.0                                      0.20             1
           118/108/149(CL5/5/6)        0.00                ND          108.0                                     0.63             j
           128 (CL6)                   0.00                ND          110.0                                     0.00             ND
           138 (CL6)                   0.45                1           114.0                                     0.80             1
           126 (CL5)                                       NA                             NA                                      NA
           153 (CL6)                   0.00                ND          96.0                                      0.67             1
           170 (CL7)                   0.00                ND          123.0                                     0.00             ND
           180 (CL7)                   0.00                ND          116.0                                     0.74             1
           187/182/159(CL7/7/6)        0.00                ND          110.0                                     0.56             1
           195 (CLB)                   0.00                ND          117.0                                     0.08             1
           206 (CL9)                   0.00                ND          107.0                                     0.00             ND
           209 (CL10)                  0.00                ND          113.0                                     0.00             ND


           Surrogate Recoveries
           DBOFB%:                     65.2                            64.9                                      64.0
           PCB#103%:                   68.8                            72.6                                      73.9
           PCB#198%:                   69.0                            80.9                                      87.0


           OTHER PESMCIDES


           ENDOSULFAN I
           ENDOSULFAN 13
           ENDOSULFAN SULFATE
           ENDRIN ALDEHYDE


           PCB #(CHLORINATION)


           7 (CL2)                     0.00                ND                             NA                     0.00             ND
           15 (CL2)                    0.00                ND                             NA                     0.00             ND
           24 (CW)                     0.00                ND                             NA                     0.37             1
           16/32 (CL3)                 0.00                ND                             NA                     0.00             ND
           29 (CL3)                    0.00                ND                             NA                     0.00             ND
           26 (CL3)                    0.00                ND                             NA                     0.00             ND
           25 (CL3)                    0.00                ND                             NA                     0.00             ND
           50 (CIA)                    0.00                ND                             NA                     0.40             1
           31 (CL3)                    0.00                ND                             NA                     0.00             ND
           33 (CI-3)                   0.00                ND                             NA                     0.00             ND
           22 (CL3)                    0.00                ND                             NA                     0.00             ND
           45 (CIA)                    0.00                ND                             NA                     0.00             ND
           46 (CIA)                    0.00                ND                             NA                     0.61             1
           49 (CL4)                    0.10                1                              NA                     0.13             1



                                                                          242






                                   Antarctic IAmpet Samples -Polar Programs- Pesticides and PCB's


             WVESN:                     LAB QA SAMPLE                 LAB QA SAMPLE                             Transect D.. 19
             ED:                        PROC BLANK                    Station 12                                42' Palmer Sta
             LABSAMNO:                  Q4884                         Q4885                                     J1886
             UNrr:                      ng/g                          ng/g                                      ng/g
             Analyte (Cont)             Conc               DB QUAL Conc                   DB QUAL               Gonc            DELOUAL

             47/48 (CIA)                0.00               ND                             NA                    0.00            ND
             37/42 (CIA)                0.00               ND                             NA                    0.00            ND
             41/64 (CIA)                0.00               ND                             NA                    0.00            ND
             40 (CIA)                   0.00               ND                             NA                    0.00            NIE)
             100 (CL5)                  0.00               ND                             NA                    0.00            ND
             74 (CIA)                   0.00               ND                             NA                    0.00            ND


             PCB #(CHLORINAnON)


             70 (CIA)                   0.00               ND                             NA                    0.00            ND
             88 (CL5)                   0.00               ND                             NA                    0.00            ND
             60/56 (CL5)                0.00               ND                             NA                    0.00            ND
             92? (CL5)                  0.00               ND                             NA                    0.00            ND
             84? (CL5)                  0.00               ND                             NA                    0.00            ND
             99 (CL5)                   0.00               ND                             NA                    0.00            ND
             83 (CL5)                   0.00               ND                             NA                    0.00            ND
             97 (CL5)                   0.00               ND                             NA                    0.00            ND
             87 (CL5)                   0.00               ND         130.0                                     0.00            ND
             85 (CL5)                   0.00               ND                             NA                    0.00            ND
             136 (CLQ                   0.00               ND                             NA                    0.00            ND
             82 (CL5)                   0.00               ND                             NA                    0.00            ND
             151 (CL6)                  0.00               ND                             NA                    0.00            ND
             107/108/144(CL5/5/6)       0.14               1                              NA                    0.00            ND
             149 (CL6)                  0.00               ND                             NA                    0.66            1
             188 (CL7)                  0.00               ND                             NA                    0.00            ND
             146 (CL6)                  0.00               ND                             NA                    0.00            ND
             141 (CL6)                  0.00               ND                             NA                    0.00            ND
             137 (CL6)                  0.00               ND                             NA                    0.61            1
             UNK (CL6)                  0.00               ND                             NA                    0.00            ND
             158 (CL7)                  0.00               ND                             NA                    0.00            ND
             129 (CL6)                  0.00               ND                             NA                    0.22            1
             178 (CL7)                  0.00               ND                             NA                    0.00            ND
             183 (CL7)                  0.00               ND                             NA                    0.00            ND
             167 (CL6)                  0.00               ND                             NA                    0.00            ND
             185 (CL7)                  0.00               ND                             NA                    0.00            ND
             174 (CL7)                  0.00               ND                             NA                    0.32            1
             177 (CL7)                  0.00               ND                             NA                    0.00            ND
             156/171/202(CL6/7/8)       0.00               ND                             NA                    0.00            ND
             200 (CL8)                  0.00               ND                             NA                    0.00            ND
             172 (CL7)                  0.68               1                              NA                    0.56            1
             191 (CU)                   0.00               ND                             NA                    0.00            ND
             201 (CL8)                  1.31                                              NA                    0.88            j
             196 (CLS)                  0.00               ND                             NA                    0.39            1
             189 (CL7)                  0.00               ND                             NA                    0.00            ND
             194 (CL8)                  0.00               to                             NA                    0.23            1
             205 (CL9)                  0.00               bm                             NA                    0.00            M
                                                                                                                                    )JUAL







                                                                        243






                               Antarctic I.Ampet Samples -Polar Programs- Pesticides and PCB's


           INVEST#:                   Transect D- 14                    LAB QA SAMPLE                 LAB QA  SAMPLE
           ID:                        ANTARC NIST M802                  Thansect D- 19                PROC BLANK
           IABSAMNO:                  Q4886                             Q4887                         Q4888
           UNIT.                      ng/g                              ng/g                          ng/g
           Analyte (Cont)             Conc                    DB QUAL Conc                 DB QUAL Conc                 DB QUAL

           &AhUqZ TYPE:               SRM                               DUP OF J 1886                 BLK
           COUECTION DATE:
           RECEEPIT DATE:
           9CHATCH:                   M802                              M802                          M802
           EXTRACTION DATE:           03/04/93                          03/04/93                      03/04/93
           METHOD:                    G4CMS                             GICMS                         GCMS
           ANALYSIS DATE:             04/21/93                          04/21/93                      04/21/93
           Mffi'THOD:                 GCECD                             GCECD                         GCECD
           ANALYSIS DATE:             05/03/93                          05/03/93                      05/03/93
           MATRDC-                    nSSUE                             'nSSUE                        'nSSUE
           SUBMAT:
           SAWLWT:
           WETWT:                     5                                 9.981
           DRrWr.                     0.69                              2.53                          10
           WTUNITS:                   GRAMS                             GRAMS                         GRAMS
           PCTSOLIDS:                 13.8%                             25.3%
           VOL:
           VOLUNITS:                  1JTERS                            =RS                           LzTERS


           TOTAL BHUS                 6.88                              0.60               1          0.00              ND
           TOTAL CHLORDANES           75.19                             0.50               1          0.00              ND
           TOTAL DDT"S                131.86                            2.19                          0.00              ND
           TOTAL PCB'S                2263.6                            7.6                           0.5               1


           ALPHA-BHC                  0.00                    ND        0.00               ND         0.00              ND
           HCB                        0.05                    1         0.75                          0.00              ND
           BETA-BHC                   2.27                              0.60                          0.00              ND
           GAMMA-BHC                  0.00                    ND        0.00               ND         0.00              ND
           DELTA-BHC                  4.62                              0.00               ND         0.00              ND
           HEPTACHLOR                 0.00                    ND        0.40               1          0.00              ND
           HEPTA-EPO)ME               0.00                    ND        0.00               ND         0.00              ND
           OXYCHLORDANE               8.83                              0.00               ND         0.00              ND
           GAMMA-CHLORDANE            15.26                             0.00               ND         0.00              ND
           ALPHA-CHLORDANE            21.56                             0.00               ND         0.00              ND
           TRANS-NONACHLOR            18.36                             0.00               ND         0.00              ND
           CIS-NONACHLA)R             11.18                             0.10               1          0.00              ND
           ALDRIN                     3.27                              0.00               ND         0.00              ND
           DIELDRIN                   8.86                              0.00               ND         0.00              ND
           ENDRIN                     0.00                    ND        0.00               ND         0.00              ND
           M[IREX                     0.59                    1         0.00               ND         0.00              ND
           2.4'DDE (O,VDDE)           4.52                              0.00               ND         0.00              ND
           4.4'DDE (P,FIDDE)          49.80                             0.41               1          0.00              ND
           2.41)DD (O.PDDD)           8.35                              0.00               ND         0.00              ND
           4,4`DDD (PI-DDD)           54.89                             0.55               1          0.00              ND
           2.4'DDT (O.P`DDT)          7.24                              0.00               ND         0.00              ND
           4.4'DDT (P,PDM             7.06                              1.23                          0.00              ND

           PCB # (CLORINATION)




                                                                    244







                                   Antarctic Limpet Samples -Polar Programs- Pesticides                anti PCB's


              UVESTC                      Transect. D- 14                     LAB QA SAMPLE                 LAB (TA S-AMPLE
              ID:                         ANTARC NIST M802                    Transect D- 19                PROCBLANK
              LABSAMNO:                   Q4886                               Q4887                         Q4888
              UNIT-                       ng/g                                ng/g                          ng/g
              Analyte (Cont)              Conc                     DB QUAL Conc                  DB gUAL Conc-                  DB QUAL

              8 (CL2)                     6.69                                0.00               ND         0.00                ND
              18 (CL3)                    13.75                               0.00               ND         0.00                ND
              28 (CL3)                    81.40                               0.00               ND         0.00                ND
              44 (CLA)                    74.52                               0.00               ND         0.00                ND
              52 (CLA)                    90.91                               0.00               ND         0.00                ND
              66 (CIA)                    112.32                              0.00               ND         0.00                ND
              101 (CL5)                   114.46                              0.00               ND         0.00                ND
              105 (CL5)                   43.95                               0.00               ND         0.00                ND
              110/77 (CL5/4)              128.93                              0.23               j          0.00                ND
              118/108/149(CL5/5/6)        110.51                              0.51               1          0.00                ND
              128 (CL6)                   15.75                               0.00               ND         0.00                ND
              138 (CL6)                   118.68                              2.11                          0.00                ND
              126 (CL5)                                            NA                            NA                             NA
              153 (CL6)                   141.78                              0.94               1          0.00                ND
              170 (CL7)                   0.00                                0.00               ND         2.03
              180 (CL7)                   16.44                               0.55               1          0.00                ND
              187/182/159(CL7/7/6)        33.42                               0.63               1          0.00                ND
              195 (CL8)                   0.00                                0.00               ND         0.00                ND
              206 (CL9)                   0.00                                0.00               ND         0.00                ND
              209 (CL10)                  0.00                                0.00               ND         0.00                ND


              Surrogate Recoveries
              DBOFB%:                     63.3                                45.4                          43.2
              PCB#103%:                   68.5                                54.7                          50.9
              PCB#198%:                   79.9                                59.9                          44.9


              OTHER PEST[CIDES


              ENDOSULFAN I
              ENDOSULFAN 11
              ENDOSULFAN SULFATE
              ENDRIN ALDEHYDE


              PCB #(CHLORINATION)


              7 (CL2)                     0.00                     ND         0.00               ND         0.00                ND
              15 (CL2)                    38.01                               0.00               ND         0.00                ND
              24 (CL3)                    8.32                                0.24               j          0.00                ND
              16/32 (CL3)                 21.02                               0.00               ND         0.00                ND
              29 (CL3)                    0.00                     ND         0.17               1          0.00                ND
              26 (CL3)                    11.86                               0.00               ND         0.00                ND
              25 (CL3)                    12.49                               0.00               ND         0.00                ND
              50 (CIA)                    27.70                               0.57               1          0.21                1          1
              31 (CL3)                    0.00                     ND         0.00               ND         0.00                ND
              33 (CLS)                    8.11                                0.00               ND         0.00                ND
              22 (CL3)                    10.26                               0.00               ND         0.00                ND
              45 (CIA)                    8.36                                0.00               ND         0.00                ND
              46 (CIA)                    5.14                                0.49                          0.00                ND
              49 (CIA)                    102.39                              0.17                          0.09                1



                                                                          245






                                 Antarctic lAmpet Samples -Polar Programs- Pesticides and PCB's


                                        Transs&ct D- 14                      LAB QA SAMPLE                  LAB QA SAMPLE
            ID:                         ANTARC NIST M802                     Transect D- 19                 PROC BLANK
            LABSAMNO:                   Q4886                                Q4887                          Q4888
            UNIT'.                      ng/g                                 ng/g                           ng/g
            Analyte (Cont)              Conc                     DB QUAL Conc                    DB gUAL Conc                   DB QUALI

            47/48 (CIA)                 89.53                                0.00                ND         0.00                ND
            37/42 (CIA)                 45.36                                0.00                ND         0.00                ND
            41/64 (CIA)                 78.70                                0.00                ND         0.00                ND
            40 (CIA)                    14.45                                0.00                ND         0.00                ND
            100 (CL5)                   0.00                     ND          0.00                ND         0.00                ND
            74 (CIA)                    70.47                                0.00                ND         0.00                ND


            PCB #(CHLORINATION)


            70 (CIA)                    114.40                               0.00                ND         0.00                ND
            88 (CL5)                    25.94                                0.00                ND         0.00                ND
            60/56 (CL5)                 75.47                                0.00                ND         0.00                ND
            92? (CL5)                   36.91                                0.00                ND         0.00                ND
            84? (CL5)                   34.71                                0.00                ND         0.00                ND
            99 (CL5)                    75.05                                0.00                ND         0.00                ND
            83 (CL5)                    14.64                                0.00                ND         0.00                ND
            97 (CL5)                    44-05                                0.00                ND         0.00                ND
            87 (CL5)                    64.04                                0.00                ND         0.00                ND
            85 (CL5)                    30-14                                0.00                ND         0.00                ND
            136 (CL6)                   0.00                     ND          0.00                ND         0.00                ND
            82 (CL5)                    19.18                                0.00                ND         0.00                ND
            151 (CL6)                   25.92                                0.00                ND         0.00                ND
            107/108/144(CL5/5/6)        30.82                                0.00                ND         0.00                ND
            149 (CL6)                   72.01                                0.65                j          0.00                ND
            188 (CL7)                   0.00                     ND          0.00                ND         0.00                ND
            146 (CL6)                   30.84                                0.00                ND         0.00                ND
            141 (CL6)                   11.16                                0.00                ND         0.00                ND
            137 (CL6)                   1.68                                 0.35                1          0.00                ND
            UNK (CL6)                   7.71                                 0.00                ND         0.00                ND
            158 (CL7)                   16.42                                0.00                ND         0.00                ND
            129 (CL6)                   0.00                     ND          0.00                ND         0.00                ND
            178 (CL7)                   2.45                                 0.00                ND         0.00                ND
            183 (CL7)                   19.05                                0.00                ND         0.00                ND
            167 (CL6)                   5.32                                 0.00                ND         0.00                ND
            185 (CL7)                   0.00                     ND          0.00                ND         0.00                ND
            174 (CL7)                   0.00                     ND          0.36                j          0.00                ND
            177 (CL7)                   14.94                                0.11                1          0.00                ND
            156/171/202(CL6/7/8)        9.14                                 0.00                ND         0.00                ND
            200 (CL8)                   4.93                                 0.00                ND         0.00                ND
            172 (CL7)                   7.23                                 0.44                1          0.22                j
            191 (CL7)                   0.00                     ND          0.00                ND         0.00                ND
            201 (CL8)                   0.00                     ND          1.21                           0.00                ND
            196 (CLS)                   4.41                                 0.00                ND         0.00                ND
            189 (CL7)                   0.00                     ND          0.00                ND         0.00                ND
            194 (CL8)                   1.13                                 0.00                ND         0.00                ND
            205 (CL9)                   0.00                     ND          0.00                ND         0.00                ND






                                                                         246







                                   Antarctic I.Ampet Samples -Polar Programs- Pesticides and PCB's


              INVEST#:                    LAB gA SAMPLE                             Tharmect D - 17            Trunsect D-  3
              ID:                         Transect D- 19                            60-62'                     NI14-31'
              LABSAMNO:                   Q4889                                     J1896                      Q4890
              UNrP                        ng/g                                      ng/g                       ng/9
              ta@._ (Cont)                Cone               DB QUAL                Cone            DB QUAL Cone               DB QUAL

              SAbOnE TYPE:                MS OF J 1886                   REF OIL,   SAMP                       SRM
              COUZC71ON DATE:
              RECEWr DATE:
              QCBATCH-                    M802                           M802       M803                       M803
              EXTRACTION DATE:            03/04/93                                  03/05/93                   03/05/93
              bwMOD:                      GCMS                           GCMS       GCMS                       GCMS
              ANALYSIS DATE:              04/21/93                       04/21/93 04/07/93                     04/07/93
              WWMOD:                      GCECD                          GCECD      GCECD                      GCECD
              ANALYSIS DATE:              05/03/93                                  05/03/93                   05/03/93
              MATPJX:                     TISSUE                         TISSUE     TISSUE                     TISSUE
              SUBMAT-
              SAMPLWr:
              WL,Iwr:                     10.006                                    9.939                      5.069
              DRYWr-                      2.46                           1          2.66                       0.67
              V.IuNrrs:                   GRAMS                          GRAMS      GRAMS                      GRAMS
              PCTSOLIDS:                  24.6%                                     26.8%                      13.2%
              VOL:
              VOLUNrM:                    =RS                            =RS        =RS                        LXrERS


              TOTAL BHC'S                                    NA                     0.00            ND         4.32
              TOTAL CHLORDANES,                              NA                     1.01            j          74.89
              TOTAL DDrS                                     NA                     0.76            j          128.59
              TOTAL PCB'S,                                   NA                     10.0                       2220.5


              ALPHA-BHC                   81.0                                      0.00            ND         0.00            ND
              HCB                         45.0                                      0.15            j          0.29            j
              BETA-BHC                    24.0                                      0.00            ND         0.00            ND
              GAMMA-BHC                   96.0                                      0.00            ND         0.00            ND
              DELTA-BHC                   95.0                                      0.00            ND         4.32
              HEPTACHLOR                  93.0                                      0.47            j          0.00            ND
              HEPTA-EPO)CIDE              90.0                                      0.00            ND         0.00            ND
              OXYCHLORDANE                                   NA                     0.23            j          5.27
              GAMMA-CHLORDANE             87.0                                      0.00            ND         18.60
              "HA-CHLORDANE               73.0                                      0.00            ND         20.91
              TRANS-NONACHWR              91.0                                      0.31            1          18.13
              CIS-NONACHLOR                                  NA                     0.00            ND         11.98
              ALDRIN                      89.0                                      0.00            ND         0.00            ND
              DIELDRIN                    96.0                                      0.00            ND         10.13
              ENDRIN                      114.0                                     0.00            ND         0.00            ND
              WHREX                       99.0                                      0.00            ND         0.78            j
              2.4'DDE (O,VDDE)            89.0                                      0.00            ND         0.00            ND
              4,4'DDE (P.FDDE)            100.0                                     0.45            j          43.73
              2,4'DDD (O.PDDD)            111.0                                     0.31            1          6.16
              4,41)DD (P.FDDD)            132.0                                     0.00            ND         64.16
              2.41)DT (O,VDDI)            81.0                                      0.00            ND         7.06
              4,4'DDT (P,VD=              94.0                                      0.00            ND         7.48


              PCB # (CLORINAIION)




                                                                          247






                                 Antarctic IAmpet Samples -Polar Programs- Pesticides and PCB's


             U4VEST#:                    LAB QA SAMPLE                              Transect D-17               Transect D- 13
             ID:                         Transect D- 19                             60-62'                      NIST
             IABSAMNO:                   g4889                                      J1896                       g4890
             UNIT:                       ng/g                                       ng/g                        ng/g
             Analyte (Cont)              Conc                DB gUAL                Conc            DB gUAL Conc                DB QUAL

             8 (CL2)                     84.0                                       0.00            ND          1.23
             is (CL3)                    56.0                                       0.00            ND          10.90
             28 (CL3)                    113.0                                      0.00            to          W. 12
             " (CL4)                     111.0                                      0.74            j           69.23
             52 (C")                     106.0                                      0.00            ND          95.19
             66 (CIA)                    111.0                                      0.00            ND          113.35
             101 (CL5)                   99.0                                       0.00            ND          116.80
             105 (CL5)                   99.0                                       0.00            ND          34.32
             110/77(CL5/4)               75.0                                       0.00            ND          116.96
             118/108/149(CL5/5/6)        112.0                                      0.00            ND          106.96
             128 (CL6)                   119.0                                      0.00            ND          15.01
             138 (CL6)                   116.0                                      1.39                        115.20
             126(CL5)                                        NA                                     NA                          NA
             153 (CL66)                  102.0                                      0.00            ND          145.25
             170(CL7)                    131.0                                      0.00            ND          0.00            ND
             180 (CL7)                   119.0                                      0.80            j           15.12
             187/182/159(CL7/7/6)        118.0                                      1.27                        38.55
             195 (CL8)                   120.0                                      0.00            ND          0.00            ND
             206 (CL9)                   111.0                                      0.00            M           0.76
             209 (CLIO)                  114.0                                      0.00                        0.00            M

             Sumgate Recovetles
             DBOFB%:                     62.5                                       55.0                        67.1
             PCB#103%:                   72.6                                       63.1                        73.2
             PCB#198%:                   85.6                                       70.3                        87.5


             OTHER PESMCIDES


             ENDOSULFAN I
             ENDOSULFAN 11
             ENDOSULFAN SULFATE
             ENDRIN ALDEHYDE


             PCB #(CHLORINATION)


             7 (CL2)                                         NA                     0.00            ND          0.00            ND
             15 (CL2)                                        NA                     0.00            ND          28.73
             24 (CL3)                                        NA                     0.00            ND          4.82
             16/32 (CL3)                                     NA                     0.00            ND          18.32
             29 (CL3)                                        NA                     0.33            j           0.00            ND
             26 (CL3)                                        NA                     0.00            ND          11.55
             25 (CL3)                                        NA                     0.00            ND          12.85
             50 (CIA)                                        NA                     0.00            ND          45.41
             31 (CIZ)                                        NA                     0.00            ND          0.00            ND
             33(CL3)                                         NA                     0.00            ND          0.00            ND
             22 (CL3)                                        NA                     0.00            ND          8.12
             45 (CIA)                                        NA                     0.00            ND          7.29
             46 (CIA)                                        NA                     0.25            1           3.20
             49 (CIA)                                        NA                     0.00            M           97.76



                                                                         248







                                   Antarctic I.Ampet Samples -Polar Programs- Pesticides and PCB's
                                                                                                                      . .             __    I
             INVEM:                       LAB 9A S"PLE                               Transect D- 17              Trmsect D-:@3
             ID:                          Transect D- 19                             60-62'                      N13T
             LABSAMNO:                    Q4889                                      J1896                       Q4090
             UNM.                         ng/g                                       ng/g                        ng/g
             Analyte (Cont)               Conc                DB QUAL                Conc            DB QUAL Conc             _RB QUAL

             47/48 (CIA)                                      NA                     0.00            ND          81.47
             37/42 (CIA)                                      NA                     0.00            ND          41.57
             41/64 (CIA)                                      KA                     0.00            ND          225.49
             40 (CIA)                                         NA                     0.00            ND          10.62
             100 (CL5)                                        NA                     0.00            ND          0.00
             74 (CIA)                                         NA                     0.00            ND          63.,97


             PCB #(CHLORINATION)


             70 (CIA)                                         NA                     0.22            1           101.00
             88 (CL5)                                         NA                     0.05            j           21.08
             60/56 (CL5)                                      NA                     0.00            ND          59.23
             92? (CL5)                                        NA                     0.00            ND          32.67
             84? (CL5)                                        NA                     0.00            ND          34.86
             99 (CL5)                                         NA                     0.15            1           71.02
             83 (CL5)                                         NA                     0.00            ND          11.46
             97 (CL5)                                         NA                     0.00            ND          36.30
             87 (CL5)                     120.0                                      0.00            ND          51.98
             85 (CL5)                                         NA                     0.00            ND          22.33
             1-36 (CLQ                                        NA                     0.00            ND          9.01
             82 (CL5)                                         NA                     0.00            ND          14.09
             151 (CL6)                                        NA                     0.00            ND          24.08
             107/108/144(CL5/5/6)                             NA                     0.00            ND          17.56
             149 (CL6)                                        NA                     0.00            ND          69.64
             188 (CL7)                                        NA                     4.61                        8.35
             146 (CL6)                                        NA                     0.00            ND          15.07
             141 (CL6)                                        NA                     0.00            ND          0.00            ND
             137 (CL6)                                        NA                     0.88            1           0.00            ND
             UNK (CL66)                                       NA                     0.00            ND          7.69
             158 (CL7)                                        NA                     0.00            ND          19.00
             129 (CL6)                                        NA                     0.34            1           0.00            ND
             178 (CL7)                                        NA                     0.47            1           9.46
             183 (CL7)                                        NA                     0.00            ND          18.72
             167 (CL6)                                        NA                     0.00            ND          5.25
             185 (CL7)                                        NA                     0.00            ND          0.00            ND
             174 (CL7)                                        NA                     0.00            ND          0.00            ND
             177 (CL7)                                        NA                     0.00            ND          14.02
             156/171/202(CL6/7/8)                             NA                     0.00            ND          0.00            ND
             200 (CL8)                                        NA                     0.59            1           0.00            ND
             172 (CL7)                                        NA                     0.00            ND          0.00            ND
             191 (CL7)                                        NA                     0.00            ND          0.00            ND
             201 (CLS)                                        NA                     0.00            ND          0.00            ND
             196 (CL8)                                        NA                     0.00            ND          2.97
             189 (CU)                                         NA                     0.00            ND          0.00            ND
             194 (CLS)                                        NA                     0.00            ND          1.24
             205 (CL9)                                        NA                     0.00            ND          0.00






                                                                          249






                                Antarctic I.AmPet Samples -Polar Programs- Pesticides and PCB's


              INVESTC                    LAB QA SAMPLE                 LAB QA SAMPLE                 LAB QA SAMPLE
              ID:                        Transect D- 17                PROC BLANK                    Transect D- 17
              LABSAMNO:                  Q4891                         Q4892                         Q4893
              UNIT.                      ng/g                          ng/g                          ng/g
              [Analyte (Cont)            Conc               DB, QUAL Conc                 DB QUAL Conc                 DB QUAL

              MMPLE TYPE:                DUP OF J 1896                 BLK                           MS OF J 1896
              CO1,LECTION DATE:
              RECEIPT DATE:
              QCBATCH:                   M803                          M803                          M803
              EXTRACTION DATE:           03/05/93                      03/05/93                      03/05/93
              METHOD:                    G4CmS                         GCMS                          Gems
              ANALYSIS DATE:             04/07/93                      04/07/93                      04/07/93
              METHOD:                    GCECD                         GCECD                         GCECD
              ANALYSIS DATE:             05/03/93                      05/03/93                      05/03/93
              MATRDC                     TISSUE                        TISSUE                        TISSUE
              SUBMAT:
              SAMPLWT:
              VVETWT.                    10.443                                                      10.492
              DRYWT:                     2.38                          10                            2.39
                                         GRAMS                         GRAMS                         GRAMS
              PCTSOLIDS:                 22.8%                                                       22.8%
              VWO, @L::
              VOLUNITS:                  LITERS                        LITERS                        LITERS


              TOTAL BHC'S                0.00               ND         0.00               ND                           NA
              TOTAL CHLORDANES           1.98                          0.24               1                            NA
              TOTAL DD1rS                0*97               J          0*311              J                            NA
              TOTAL PCB'S                15.5                          12.8                                            NA


              ALPHA-BHC                  0.00               ND         0.00               ND         71.0
              HCB                        0.16               1          0.00               ND         73.0
              BETA-BHC                   0.00               ND         0.00               ND         32.0
              GAMMA-BHC                  0.00               ND         0.00               ND         86.0
              DELTA-BHC                  0*00               ND         0*00               ND         117*0
              HEPTACHLOR                 0.42               1          0.00               ND         89.0
              HEPTA-EPOXIDE              0.00               ND         0.00               ND         95.0
              OXYCHLORDANE               0.51               1          0.00               ND                           NA
              GAMMA-CHLORDANE            0.00               ND         0.00               ND         90.0
              ALPHA-CHLORDANE            0.00               ND         0.00               ND         72.0
              TRANS-NONACHLOR            1.05                          0.24               1          88.0
              CIS-NONACHLOR              0,00               ND         0*00               ND                           NA
              ALDRIN                     0.00               ND         0.00               ND         86.0
              DIELDRIN                   0.00               ND         0.00               ND         87.0
              ENDRIN                     0.00               ND         0.00               ND         96.0
              M[IREX                     0.00               ND         0.00               ND         93.0
              2.41)DE (O,PDDE)           0.00               ND         0.00               ND         89.0
              4,41)DE (P.P'DDE)          0.69                          0.38               1          84.0
              2,4'DDD (O,P'DDD)          0.28                          0.00               ND         90.0
              4.4DDD (P,P'DDD)           0.00               ND         0.00               ND         95.0
              2.41)DT (O,P'DIM           0.00               ND         0.00               ND         76.0
              4.4DDT (P,P'DD1j           0.00               ND         0.00               ND         108.0


              PCB # (CLORINA710N)




                                                                       250







                                   Antarctic I.Ampet Samples -Polar Programs- Pesticides and'PCB's


                UqVEST#:                     LAB QA SAMPLE                   LAB QA SAMPLE                  LAB QA SAMPLE
                ID:                          Transect D- 17                  PROC BLANK                     Mransect D- 17
                LABSAMNO:                    Q4891                           Q4892                          Q4893
                UNrP                         ng/g                            ng/g                           ng/g
                Anabrte (Cont)               Cone                DB QUAL Cone                    DB QUAL Cone                   DB QUAL.

                8 (CL2)                      0.00                ND          0.00                ND         84.0
                18 (CL3)                     0.00                ND          0.00                ND         41.0
                28 (CL3)                     0.00                ND          0.79                1          98.0
                44 (CIA)                     0.77                1           1.14                           90.0
                52 (CIA)                     1.65                            0.83                1          91.0
                66 (CIA)                     0.00                ND          0.36                1          81.0
                101 (CL5)                    0.00                ND          0.83                1          815.0
                105 (CIZ)                    0.17                1           0.17                j          79.0
                110/77 (CL5/4)               0.00                ND          0.00                ND         61.0
                118/108/149(CIZ/5/6)         1.28                            0.71                1          84.0
                128 (CL6)                    0.22                1           0.00                ND         90.0
                138 (CL66)                   2.52                            2.06                           103.0
                126 (CL5)                                        NA                              NA                             NA
                153 (CL6)                    0.00                ND          1.06                           97.0
                170 (CL7)                    0.00                ND          0.00                ND         47.0
                180 (CL7)                    0.49                1           0.00                ND         108.0
                187/182/159(CL7/7/6)         1.53                            0.87                j          122.0
                195 (CL8)                    0.00                ND          0.00                ND         105.0
                206 (CL9)                    0.00                ND          0.00                ND         97.0
                209 (CLIO)                   0.00                ND          0.00                ND         106.0

                Surrogate Recoveries
                DBOFB%:                      60.5                            68.6                           57.7
                PCB#1030/6:                  71.4                            71.8                           69.4
                PCB#198%:                    71.0                            72.3                           82.4


                OTHER PESMCIDES


                ENDOSULFAN I
                ENDOSULFAN 11
                ENDOSULFAN SULFATE
                ENDRIN AIDEHYDE


                PCB #(CHLORINATION)

                7 (CL2)                      0.00                ND          0.00                ND                             NA
                15 (CL2)                     0.00                ND          0.00                ND                             NA
                24 (CL3)                     0.00                ND          0.00                ND                             NA
                16/32 (CL3)                  0.00                ND          0.19                1                              NA
                29 (CL3)                     0.00                ND          0.00                ND                             NA
                26 (CL3)                     0.00                ND          0.00                ND                             NA
                25 (CL3)                     0.96                1           0.00                ND                             NA
                50 (CIA)                     0.00                ND          1.15                                               NA
                31 (CL3)                     0.00                ND          0.00                ND                             NA
                33 (CL3)                     0.00                ND          0.00                ND                             NA
                22 (CL3)                     0.00                ND          0.00                ND                             NA
                45 (CIA)                     0.00                ND          0.00                ND                             NA
                46 (CIA)                     0.00                ND          0.00                ND                             NA
                49 (CL4)                     0.00                ND          0.80                                               NA



                                                                            251






                                  Antarctic Limpet Samples -Polar Programs- Pesticides and PCB's


               INV&ST#:                     LAB QA SAWLE                   LAB QA SAWLE                    LAB QA SAI"LE
               ID:                          Transed D- 17                  PROC BLANK                      Transect D- 17
               LABSAMNO:                    Q4891                          Q4892                           Q4893
               UNM.                         ng/g                           ng/9                            ng/g
              tAnalyte (Cont)               Conc                DB QUAL Conc                   DB gUAL Conc                    DB QUAL

               47/48 (CIA)                  0.00                ND         0.00                ND                              NA
               37/42 (CIA)                  0.00                ND         0.00                ND                              NA
               41/64 (CIA)                  0.00                ND         0.00                ND                              NA
               40 (CIA)                     0.00                ND         0.00                ND                              NA
               100 (CL5)                    0.00                ND         0.00                ND                              NA
               74 (ClA)                     0.00                ND         0.29                1                               NA


               PCB #(CHLORINAMON)


               70 (CIA)                     0.00                           0.59                1                               NA
               88 (CL5)                     0.54                           0.14                1                               NA
               60/56 (CL5)                  0.00                           0.00                ND                              NA
               92? (CL5)                    0.00                           0.29                1                               NA
               84? (CL5)                    0.00                           0.00                ND                              NA
               99 (CL5)                     1.34                           0.59                1                               NA
               83 (CL15)                    0.00                           0.00                ND                              NA
               97 (C1.5)                    0.00                           0.28                1                               NA
               87 (CLS)                     0.00                           0.28                1           0.0
               85 (CIZ)                     0.16                           0.12                1                               NA
               136 (CL66)                   0.00                           0.00                ND                              NA
               82 (CL5)                     0.00                           0.00                ND                              NA
               151 (CL6)                    0.00                           0.00                ND                              NA
               107/108/144(CL5/5/6)         0.00                           0.00                ND                              NA
               149 (CL6)                    1.20                           0.62                1                               NA
               188 (CL7)                    3.74                           0.50                j                               NA
               146 (CL66)                   0.00                           0.00                ND                              NA
               141 (CLQ                     0.00                           0.00                ND                              NA
               137 (CL66)                   0.00                           0.00                ND                              NA
               UNK (CL6)                    0.00                           0.00                ND                              NA
               158 (CL7)                    0.39                           0.00                ND                              NA
               129 (CL66)                   0.00                           0.00                ND                              NA
               178 (CL7)                    0.00                           0.00                ND                              NA
               183 (CL7)                    0.00                           0.00                ND                              NA
               167 (CL6)                    0.00                           0.00                ND                              NA
               185 (CL7)                    0.00                           0.00                ND                              NA
               174 (CU)                     0.00                           0.00                ND                              NA
               177 (CL7)                    0.34                           0.00                ND                              NA
               156/171/202(CL6/7/8)         0.00                           0.00                ND                              NA
               200 (CLS)                    0.18                           0.00                ND                              NA
               172 (CL7)                    0.00                           0.07                1                               NA
               191 (CL7)                    0.00                           0.00                ND                              NA
               201 (CL8)                    0.00                           0.00                ND                              NA
               196 (CL8)                    0.00                           0.00                ND                              NA
               189 (CL7)                    0.00                           0.00                ND                              NA
               194 (CL8)                    0.00                           0.00                ND                              NA
               205 (CL9)                    0.00                           0.00                ND                              NA







                                                                           252



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                                                           Antarctic Limpet Samples -Polar Programs- Metal Data


                   INVFSr#:               Station 4              Station 3              Station 12           Station 12            Station 13          Station 13
                   ID:                    Humble Island          Humble Island          Janus Island         Janus Island          Christine Is        Christine Is
                   LABSAMNO:              J 1292                 J 1825                 J1289                J 1840                J1312               J1842


                   SAMPLE TYPE:           SAMP                   SAMP                   SAMP                 SAMP                  SAMP                SAMP
                   COLLECTION DATE:       1989                   1991                   1989                 1991                  1989                1991
                   MATRIX:                TISSUE                 TISSUE                 TISSUE               TISSUE                TISSUE              TISSUE
                   ADGDAT                 10/13/92               10/13/92               10/13/92             10/13/92              10/13/92            10/13/92
                   HGDGDAT                                       10/09/92               10/09/92             10/09/92              10/09/92            10/09/92
                   SAMPTYPE               SAMP                   SAMP                   SAMP                 SAMP                  SAMP                SAMP
                   Acid Digest Wt:        0.197                  0.193                  0.169                0.197                 0.199               0.207
                   Hg Digest Wt                                  0.200                  0.196                0.202                 0.197               0.191
                   WI'UNIT'S:             GRAMS           DRY GRAMS               DRY GRAMS            DRY GRAMS            DRY    GRAMS         DRY GRAMS           DRY


                   UNrr:                  (Ppm)                  (Ppm)                  (Ppm)                (Ppm)                 (Ppm)               (Ppm)

                   Ag                     0.973                  1.843                  1.062                1.665                 1.008               1.373
                   As                     11.6                   9.7                    5.2                  2.2                   2.6                 10.9
                   Cd                     6.44                   11.50                  7.85                 13.85                 7.75                9.50
                   Cr                     22.6                   31.1                   2.5                  1.2                   7.4                 4.2
                   Cu.                    8.26                   8.90                   8.04                 8.85                  8.35                10.18
         Ul        Fe                     1053                   1693                   308                  442                   588                 915
                   Hg                                     IS     0.088                  0.014                0.039                 0.032               0.125
                   Nt                     16.4                   18.8                   4.97                 3.94                  5.86                3.05
                   Pb                     0.57                   0.58                   0.46                 0.43                  0.39                0.34
                   Se                     2.70                   1.75                   1.91                 1.47                  2.69                2.69
                   Sn                     0.00            ND     0.08                   0.03                 0.00           ND     0.00          ND    0.00          ND
                   Zn                     70                     72                     71                   70                    16                  69






                                                        Antarctic Limpet Samples -Polar Programs- Metal Data


               INVEST#:              Station 20           Station 20           Transect D-7         Transect D-7         Transect D- 11        Transect D- I I
               ID:                   Cormorant Is         Cormorant Is         Hermit Island        Hermit Island        0' Palmer Sta         54' Palmer Sta
               LABSAMNO:             J1310                J1850                J 1344               J1866                J 1871                J 1872


               SAMPLE TYPE:          SAMP                 SAMP                 SAMP                 SAMP                 SAMP                  SAMP
               COLLECTION DATE:      1989                 1991                 1989                 1991                 1991                  1991
               MATRIX:               TISSUE               TISSUE               TISSUE               TISSUE               TISSUE                TISSUE
               ADGDAT                10/13/92             10/13/92             10/13/92             10/13/92             10/13/92              10/13/92
               HGDGDAT               10/09/92             10/09/92             10/09/92             10/09/92             10/09/92              10/09/92
               SAMPTYPE              SAMP                 SAMP                 SAMP                 SAMP                 SAMP                  SAMP
               Acid Digest Wt:       0.197                0.191                0.193                0.196                0.198                 0.192
               Hg Digest Wt          0.197                0.196                0.198                0.189                0.205                 0.206
               VVITUNITS:            GRAMS          DRY   GRAMS          DRY GRAMS            DRY   GRAMS          DRY   GRAMS          DRY    GRAMS          DRY

               UNIT.                 (Ppm)                (Ppm)                (Ppm)                (Ppm)                (Ppm)                 (Ppm)

               Ag                    0.837                1.333                2.156                2.839                0.686                 0.673
               As                    22.8                 11.2                 10.9                 30.3                 10.4                  11.7
               Cd                    7.69                 12.66                18.6                 20.59                8.70                  4.04
               Cr                    12.3                 5.5                  4.0                  6.0                  24.4                  83.8
               Cu                    11.6                 10.12                2.71                 7.65                 23.43                 33.43
               Fe                    850                  590                  691                  716                  2913                  10564
               Hg                    0.056                0.043                0.042                0.073                0.070                 0.027
               Ni                    7.75                 4.95                 3.95                 5.45                 14.2                  49.7
               Pb                    0.56                 0.59                 3.30                 0.94                 1.89                  2.18
               Se                    2.30                 2.16                 2.16                 2.34                 2.04                  1.82
               Sn                    0.00           ND    0.12                 0.00           ND    0.00           ND    0.17                  0.06
               Zn                    70                   69                   80                   83                   62                    59






                                                            Antarctic Limpet Samples -Polar Programs- Metal Data


              INVEST#:                Transect D- 12          Transect D- 12          Transect D- 13         Transect D- 13          Transect D- 14         Transect D- 14
              ID:                     0' Palmer Sta.          62' Palmer Sta          0' Palmer Sta          3 1' Palmer Sta.        O'Old Palmer           30'Old Palmer
              LABSAMNO:               J1875                   J1876                   J1881                  J1880                   J1887                  J1883


              SAMPLE TYPE:            SAMP                    SAMP                    SAMP                   SAMP                    SAMP                   SAMP
              COLLECTION DATE:        1991                    1991                    1991                   1991                    1991                   1991
              MATRIX:                 TISSUE                  TISSUE                  TISSUE                 TISSUE                  TISSUE                 TISSUE
              ADGDAT                  10/13/92                10/13/92                10/13/92                                       10/13/92               10/13/92
              HGDGDAT                 10/09/92                10/09/92                10/09/92               10/09/92                10/09/92               10/09/92
              SAMPTYPE                SAMP                    SAMP                    SAMP                   SAMP                    SAMP                   SAMP
              Acid Digest Wt:         0.195                   0.200                   0.197                  0.192                   0.091                  0.198
              Hg Digest Wt            0.187                   0.187                   0.203                  0.202                   0.183                  0.207
              WIUNITS:                GRAMS            DRY    GRAMS            DRY    GRAMS           DRY GRAMS               DRY GRAMS              DRY    GRAMS            DRY


              UNIT:                   (Ppm)                   (PPM)                   (PPM)                  (1313m)                 (1313m)                (PPM)

              Ag                      1.094                   1.506                   1.035                  1.401                   2.397                  2.234
              As                      9.1                     15.8                    10.2                   11.6                    11.4                   3.0
              Cd                      8.04                    13.12                   9.79                   11.66                   13.02                  16.17
              Cr                      14.6                    16.8                    19.9                   19.4                    10.2                   22.3
              Cu                      29.29                   13.74                   26.72                  14.14                   9.75                   9.72
              Fe                      1929                    2658                    3006                   3896                    2593                   2518
              Hg                      0.074                   0.051                   0.094                  0.087                   0.091                  0.085
              Ni                      9.39                    9.92                    12.9                   12.2                    6.04                   13.8
              Pb                      3.64                    0.91                    6.64                   2.75                    7.06                   1.67
              Se                      2.58                    2.42                    1.88                   1.57                    1.86                   2.07
              Sn                      0.15                    0.05                    0.31                   0.00             ND     0.22                   0.00             ND
              Zn                      72                      75                      85                     67                      74                     60






                                                        Antarctic Limpet Samples -Polar Programs- Metal Data


             INVEST#:             Transect D- 17        Transect D- 17       Transect D- 19       Transect D- 19        Transect D-7         Transect D-7
             ID:                  0.                    60-62'               0' Palmer Sta        42' Pahner Sta        Hermit Island        18' Hermit Island
             LABSAMNO:            J 1893                J1896                J 1882               J 1886                11866                J1865


             SAMPLE TYPE:         SAMP                  SAMP                 SAMP                 SAMP                  SAMP                 SAMP
             COLLEC11ON DATE:     1991                  1991                 1991                 1991                                       1991
             MATRIX:              TISSUE                TISSUE               TISSUE               TISSUE                TISSUE               TISSUE
             ADGDAT               10/13/92              10/13/92             10/13/92             10/13/92              10/13/92             10/13/92
             HGDGDAT              10/09/92              10/09/92             10/09/92             10/09/92              10/09/92             10/09/92
             SAMPTYPE             SAMP                  SAMP                 SAMP                 SAMP                  SAMP                 SAMP
             Acid Digest Wt:      0.189                 0.193                0.192                0.193                 0.196                0.194
             Hg Digest Wt         0.203                 0.205                0.192                0.200                 0.189                0.190
             WUNITS:              GRAMS           DRY   GRAMS          DRY GRAMS            DRY GRAMS            DRY GRAMS             DRY GRAMS               DRY


             UNIT:                (Ppm)                 (Ppm)                (PPM)                (PPM)                 (Ppm)                (PPM)

             Ag                   1.419                 0.939                1.287                1.446                 2.839                2.638
             As                   10.2                  11.9                 10.7                 18.2                  30.3                 11.0
             Cd                   11.26                 4.49                 10.92                7.06                  20.59                30.44
             Cr                   14.7                  36.3                 69.4                 38.3                  6.0                  6.1
             Cu                   12.19                 11.64                27.84                13.93                 7.65                 7.36
             Fe                   1693                  2905                 2678                 2730                  716                  979
             Hg                   0.014                 0.041                0.074                0.091                 0.073                0.075
             Ni                   9.17                  22.8                 53.6                 23.2                  5.45                 4.48
             Pb                   14.7                  0.76                 1.14                 2.09                  0.94                 0.83
             Se                   2.53                  1.63                 1.78                 1.59                  2.34                 2.91
             Sn                   0.00            ND    0.09                 0.01                 0.04                  0.00           ND    0.06
             Zn                   71                    58                   70                   68                    83                   69






                                                         Antarctic Limpet Samples -Polar Programs- Metal Data


              INVEST#:              Station 12              Transect D- 14                    LAB QA SAMPLE LAB QA SAMPLE           LAB QA SAMPLE      LAB QA SAMPLE
              ID:                   JanusIsland             ANTARC NIST M801                  Station 12         PROC BLANK         Station 12         GERGCHK
              LABSAMNO:             J1840                   Q4882                             Q4883              Q4884              Q4885              W8220

              SAMPLE TYPE:          SAMP                    SRM                               DUP OF J 1840      BLK                MS, OF J 1840      REF OIL
              COLLECTION DATE:      1991
              MATRIX:               TISSUE                  'TISSUE                           TISSUE             TISSUE             TISSUE             TISSUE
              ADGDAT                                                                                                                10/13/92
              HGDGDAT                                                                                                               10/09/92
              SAMPTYPE                                                                                                              LDUP
              Acid Digest Wt:                                                                                                       0.202
              Hg Digest Wt                                                                                                          0.198
              VVTUNITS:             DRY            GRAMS DRY                         GRAMS GRAMS                 GRAMS              GRAMS              GRAMS

              UNIT:                 (PPM)                   (PPM)                             (PPM)              (PPM)              (PPM)              (PPM)

              Ag                                                                                                                    1.540
              As                                                                                                                    18.2
              Cd                                                                                                                    7.22
              Cr                                                                                                                    39.4
              Cu                                                                                                                    13.18
        Cil
        Go    Fe                                                                                                                    2902
              Hg                                                                                                                    0.048
              Ni                                                                                                                    22.8
              Pb                                                                                                                    1.54
              Se                                                                                                                    1.81
              Sn                                                                                                                    0.09
              Zn                                                                                                                    68






                                                         Antarctic Limpet Samples -Polar Programs- Metal Data

                         INVEST#:              Transect D- 19             Transect D- 14                    LAB QA SAMPLE                 LAB QA SAMPLE
                         ID:                   42' Pahner Sta             ANTARC NIST M802                  Transect D- 19                PROC BLANK
                         LABSAMNO:             J1886                      Q4886                             Q4887                         Q4888
                         SAMPLE TYPE:          SAMP                       SRM                               DUP OF J 1886                 BLK
                         COLLECTION DATE:
                         MATRIX:               TISSUE                     TISSUE                            TISSUE                        TISSUE
                         ADGDAT                10/13/92        10/13/92 10/13/92                  10/13/92 10/13/92            10/13/92 10/13/92
                         HGDGDAT               10/09/92        10/09/92 10/09/92                  10/09/92 10/09/92            10/09/92 10/09/92
                         SAMPTYPE              SAMP            SPIKE      MS                      SAMP      LDUP               SAMP       LDUP
                         Acid Digest Wt:       0.211                      0.195                   0.203     0.195              0.195      0.203
                         Hg Digest Wt          0.204                      0.209                   0.192     0.188              0.204      0.192
                         V*7UNITS:             GRAMS                      GRAMS                             GRAMS                         GRAMS
                         UNIT.                 (PPM)                      (PPM)                             (PPM)                         (PPM)
                         Ag                    0.000           1.024      0.940                   0.113     0.055              0.000      0.000
                         As                    2.5             10.2       13.2                    4.9       5.1                12.9       13.3
                         Cd                    0.04            5.12       5.09                    2.05      2.03               1.63       1.46
         tQ              Cr                    2.2             25.6       27.7                    0.3       0.3                2.5        8.6
         01              Cu                    1.08            25.60      26.36                   3.03      3.25               3.22       3.27
         (D              Fe                    36.3            512        525                     126       126                85         147
                         Hg                    0.226           1.14       1.46                    0.182     0.178              0.517      0.622
                         Ni                    1.14            25.6       25.5                    0.29      0.47               3.66       4.61
                         Pb                    0.06            25.6       26.1                    0.02      0.01               0.03       0.00
                         Se                    2.17            25.6       38.2                    6.39      6.37               5.72       5.80
                         Sn                    0.00            0.28       0.22                    0.04      0.01               0.00       0.10
                         Zn                    38              128        168                     84        87                 89         87






                                                            Antarctic Limpet Samples -Polar Programs- Metal Data


                         INVESr#:                           LAB QA SAMPLE                 LAB QA SAMPLE                  Transect D- 17              Transect D- 13
                         ID:                                Transect D- 19                GERG CHK                       60-62'                      NIST
                         LABSAMNO:                          Q4889                         W8310                          J1896                       Q4890


                         SAMPLE TYPE:                       MSOFJ1886                     REF OIL                        SAMP                        SRM
                         COLLECTION DATE:
                         MATRDC_                            TISSUE                        TISSUE                         TISSUE                      TISSUE
                         ADGDAT                 10/13/92 10/13/92              10/13/92 10/13/92              10/13/92 10/13/92           10/13/92 10/13/92
                         HGDGDAT                10/09/92 10/09/92              10/09/92 10/09/92              10/09/92 10/09/92           10/09/92 10/09/92
                         SAMPTYPE               SAMP        LDUP               SAMP       SPIKE               MS         SAMP             SPIKE      MS
                         Acid Digest Wt:        0.202       0.198              0.207                          0.199      0.203                       0.206
                         Hg Digest Wt           0.192       0.205              0.190                          0.186      0.193                       0.199
                         VV7UNITS:                          GRAMS                         GRAMS                          GRAMS                       GRAMS


                         UNrr:                              (PPM)                         (PPM)                          (PPM)                       (PPM)

                         Ag                     0.244       0.249              0.000      1.070               0.909      0.000            0.973      0.847
                         As                     5.9         6.0                5.5        10.1                15.8       0.7              9.7        11.1
                         Cd                     5.12        4.19               0.02       5.03                4.91       0.02             4.87       4.34
        ba               Cr                     2.2         1.3                1.4        25.2                28.2       1.1              24.3       23.1
        0)               Cu                     4.66        4.25               0.48       25.16               26.10      1.18             24.33      22.14
                         Fe                     317         270                13.6       503                 517        28.5             487        462
                         Hg                     0.124       0.109              0.218      1.28                1.36       0.372            1.24       1.27
                         N1                     2.07        1.65               0.98       25.2                25.5       0.76             24.3       24.2
                         Pb                     0.13        0.14               0.05       25.2                25.5       0.14             24.3       23.1
                         Se                     7.91        8.32               3.21       25.2                33.8       0.60             24.3       27.4
                         Sn                     0.00        0.00               0.01       0.28                0.37       0.00             0.27       0.28
                         Zn                     81          82                 21         126                 151        36               122        149






                                                         Antarctic Limpet Samples -Polar Programs- Metal Data


                           INVEST#:                        LAB QA SAMPLE               LAB QA SAMPLE                LAB QA SAMPLE LAB QA SAM
                           ID:                             Transect D- 17              PROC BLANK                   Transect D- 17    GERG CHK
                           LABSAMNO:                       Q4891                       Q4892                        Q4893             W8228

                           SAMPLE TYPE:                    DUP OF J 1896               BLK                          MS OF J 1896      REF OIL
                           COLLECTION DATE:
                           MATRIX:                         TISSUE                      TISSUE                       TISSUE            TISSUE
                           ADGDAT                10/13/92 10/13/92           10/13/92 10/13/92            10/13/92
                           HGDGDAT               10/09/92 10/09/92           10/09/92 10/09/92            10/09/92
                           SAMPTYPE              SAMP      SPIKE             NIS       SAMP               LDUP
                           Add Digest Wt:        0.200                       0.195     0.209              0.203
                           Hg Digest Wt          0.187                                 0.198              0.193
                           VVTUNITS:                       GRAMS                       GRAMS                        GRAMS             GRAMS


                           UNIT:


                           Ag                    1.917     1.025             2.757     0.047              0.111
                           As                    19.9      10.3              33.4      23.9               23.4
                           Cd                    23.14     5.13              28.34     0.63               0.61
                           Cr                    27.6      25.6              51.3      36.3               40.6
          tQ               Cu                    15.14     25.63             41.42     3.04               2.81
          0)               Fe                    9578      513               10654     775                891
                           Hg                    0.026                                 0.129              0.144
                           Ni                    20.7      25.6              42.9      8.86               10.4
                           Pb                    0.95      25.6              26.9      0.31               0.24
                           Se                    16.3      25.6              41.8      4.52               3.99
                           Sn                    0.00      0.28              0.25      0.10               0.13
                           Zn                    186       128               316       79                 81




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               McMurdo Sediment Aromatic
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                                   Antarctic McMurdo's Sediments Aromatic Hydrocarbon Data


                    INVEST#:                BERNACCHIBAY                   BAY OF SAILS                WQB
                    ID:                     100,                           100,                        60'
                    Lll@NO:                 J2034                          J2037                       J2042
                    UNIT:                   ng/g                           ng/g                        ng/g
                    JPNA Analyte            Conc                DB QUAL Conc               DB QUAL Conc             DB QUAL

                    SAMPLE TYPE:            SAMP                           SAMP                        SAMP
                    COLLECTION DATE:        01/09/91                       12/21/90                    12/10/90
                    RECEIPT DATE:
                    QCBATCH:                M607                           M607                        M607
                    EXTRACTION DATE:
                    METHOD:                 GCFID                          GCFID                       GCFID
                    ANALYSIS DATE:
                    METHOD:                 GCMS                           GCMS                        GCMS
                    ANALYSIS DATE:          02/26/93                       02/26/93                    02/27/93
                    METHOD:                 GCECD                          GCECD                       GCECD
                    ANALYSIS DATE:          04/23/93                       04/23/93                    04/23/93
                    MATRIK                  SEDIMENT                       SEDIMENT                    SEDIMENT
                    SUBMAT:
                    SAMPLWT:
                    WETWT:                  16.49                          15.83                       17.57
                    DRYWT:                  11.39                          10.19                       9.99
                    VnUNITS:                GRAMS               DRY        GRAMS           DRY         GRAMS        DRY
                    PCTSOLIDS:
                    VOL.
                    VOLUNITS:               LITERS                         LITERS                      LITERS


                    NAPHTHALENE             2.10                           1.97                        67.74
                    Cl-NAPHTHALENES         6.07                           4.74                        217.45
                    C2-NAPHTHALENES         12.27                          11.21                       286.34
                    C3-NAPHTHALENES         15.19                          17.19                       409.67
                    C4-NAPHTHALENES         16.38                          19.21                       320.17
                    BIPHENYL                1.13                           1.01                        30.92
                    ACENAPHTHYLENE          0*25                J          0,36            1           3* 17
                    ACENAPHTHENE            0.41                           0.92            1           4.81
                    FLUORENE                1.25                           1.36                        10.77
                    Cl-FLUORENES            6.42                           6.13                        27.08
                    C2-FLUORENES            19.82                          23.54                       59.14
                    C3-FLUORENES            36.22                          39.09                       80.06
                    PHENANTHRENE            7.80                           9.08                        43.65
                    ANTHRACENE              1.00                           1.59                        11.66
                    CI-PHEN-ANTHR           7.77                           8.26                        36.63
                    C2-PHEN-ANTHR           10.80                          13.28                       66.11
                    C3-PHEN-ANTHR           10.73                          13.16                       115.62
                    C4-PHEN-ANTHR           8.25                           9.07                        77.36
                    DIBENZOTHIO             0.57                           0.91            1           5.89
                    Cl-DI13EN               4.05                           4.22                        18.40
                    C2-DIBEN                7.76                           7.18                        53.79
                    C3-DIBEN                8.58                           7.45                        96.70
                    FLUORANTHENE            2.57                           3.18                        30.95
                    PYRENE                  9.87                           11.77                       44.71
                    Cl-FLUORAN-PYR          0.00                ND         0.00            ND          34.42
                    BENaANTHRACENE          0.04                           0.08            1           21.48
                    CHRYSENE                0.24                           0.05            1           26.55
                    Cl-CHRYSENES            0.00                ND         0.00            ND          23.70



                                                                       263






                                    Antarctic McMurdo's Sediments Aromatic Hydrocarbon Data


                     IT4VEST#:                BERNACCHIBAY                   BAY OF SAILS                WQB
                     ID:                      100,                           100,                        60'
                     LABSAMNO:                J2034                          J2037                       J2042
                     UNrr-                    ng/g                           ng/g                        ng/g
                     PNA Analyte              Conc               DB QUAL Conc                DB QUAL Conc             DB QUAL


                     C2-CHRYSENES             0.00               ND          0.00            ND          27.54
                     C3-CHRYSENES             0.00               ND          0.00            ND          4.58
                     C4-CHRYSENES             0.00               ND          0.00            ND          5.32
                     BENbFLUORAN              0.07               1           0.09            1           10.56
                     BENkFLUORAN              0.07               1           0.09            1           10.56
                     BENePYRENE               0.22               1           0.20            j           10.94
                     BENaPYRENE               0.06               1           0.04            j           8.90
                     PERYLENE                 0.03               1           0.17            j           4.92
                     1123edPYRENE             0.05               1           0.10            1           5.71
                     DBahANTHRA               0.05               1           0.06            j           1.44
                     B&WERYLENE               0.26               1           0.30            j           6.43


                     =AL PAH's                198.3                          216.9                       2316.9
                        (W/O PERYLENE)


                     2-NIETHYLNAPH            3.44                           2.81                        157.16
                     1-NEETHYLNAPH            2.63                           1.93                        60.29


                     2,6-DINM-FHNAPH          4.34                           4.20                        182.69


                     2,3,5-TRIME'rHNAPH       2.93                           3.27                        68.36


                     1-NEETHYLPHEN            1.61                           1.91                        6.93


                     Surrogate Recoveries
                     NAPHD8:                  76.1                           78.2                        71.0
                     ACEND10:                 73.4                           71.6                        64.9
                     PHEND10:                 90.0                           84.6                        72.7
                     CHRYD12:                 84.8                           86.7                        39.3
                     PERYD12:                 73.1                           47.1                        63.9






























                                                                        264






                                 Antarctic McMurdo's Sediments Aromatic Hydrocarbon Data



                    INVEST#:               OLJTFALL                CAPE ARMITAGE                 OLITFALL,
                    ID:                    30'                     60'                           30,
                    LABSAMNO:              J2049                   J2056                         J2057
                    UNIT:                  ng/g                    ng/g                          ng/g
                    PNA Aralyte            Conc         DB QUAL Conc                  DB QUAL Cone            DB QUAL


                    SAWLE IYPE:            SAMP                    SAMP                          SAMP
                    COLLEC'nON DATE:       11/30/90                12/14/90                      12/13/91
                    RECEIPT DATE:
                    QCBATCH:               M608                    M608                          M608
                    EXTRAC`TION DATE:
                    METHOD:                GCFID                   GCFID                         GCFID
                    ANALYSIS DATE:
                    METHOD:                GCMS                    GCMS                          GCMS
                    ANALYSIS DATE:         02/28/93                02/28/93                      02/28/93
                    METHOD:                GCECD                   GCECD                         GCECD
                    ANALYSIS DATE:         03/20/93                03/20/93                      03/20/93
                    MATRIX:                SEDIMENT                SEDIMENT                      SEDIMENT
                    SUBMAT:
                    SAMPLWT:
                    VVEINW:                13.21                   16.96                         16.25
                    DRYWT:                 10.09                   10.39                         10.43
                    VVTUNITS:              GRAMS        DRY        GRAMS              DRY        GRAMS        DRY
                    PCTSOLIDS:
                    VOL:
                    VOLUNITS:              LITERS                  LITERS                        LITERS


                    NAPHTHALENE            31.25                   3.08                          19.36
                    Cl-NAPHTHALENES        81.97                   8.17                          76.40
                    C2-NAPHTHALENES        107.52                  17.22                         82.63
                    C3-NAPHTHALENES        75.42                   21.13                         45.90
                    C4-NAPHTHALENES        42.83                   17.38                         61-00
                    BIPHENYL               9.88                    1.35                          6.65
                    ACENAPHTHYLENE         1.24                    0.47               1          0.89         1
                    ACENAPHTHIENE          1.25                    0.58               1          1.24
                    FLUORENE               3.95                    1.43                          2.77
                    CI-FLUORENES           9.04                    5.01                          6.42
                    C2-FLUORENES           25.57                   18.50                         23.15
                    C3-FLUORENES           43.01                   30.71                         43.94
                    PHENANTHRENE           19.58                   5.74                          11.12
                    ANTHRACENE             3.38                    0.83               1          4.90
                    CI-PHEN-ANTHR          16.83                   8.60                          12.45
                    C2-PHEN-ANTHR          32.66                   11.74                         28.55
                    C3-PHEN-ANTHR          104.17                  15.40                         45.75
                    C4-PHEN-ANTHR          51.03                   6.99                          37.56
                    DIBENZOTHIO            2.23                    0.97               1          1.25
                    CI-DIBEN               6.87                    3.52                          5.84
                    C2-DIBEN               26.42                   6.94                          18.55
                    C3-DIBEN               45.56                   9.05                          34.26
                    FLUORANTHENE           12.29                   2.71                          12.31
                    PYRENE                 20.55                   8.23                          20.22
                    CI-FLUORAN-PYR         13.85                   2.08                          12.49
                    BENaANTHRACENE         4.32                    0.50               1          5.69
                    CHRYSENE               9.03                    0.48               1          10.46
                    CI-CHRYSENES           7.04                    0.84               1          8.46



                                                                   265






                                    Antarctic McMurdo's Sediments Aromatic Hydrocarbon Data


                      INVEST#:                 OLTIYALL                CAPE ARMITAGE                   OUTFALL
                      ID:                      30'                     60'                             30'
                      LABSAMNO:                J2049                   J2056                           J2057
                      UNIT.                    ng/g                    ng/g                            ng/g
                      PNA Analyte              Cone         DB QUAL Cone                    DB QUAL Cone             DB QUAL


                      C2-CHRYSENES             11.57                   1.50                            10.78
                      C3-CHRYSENES             5.46                    1.16                            5.51
                      C4-CHRYSENES,            1.15                    1.29                            1.92         1
                      BENbFLUORAN              3.77                    0.46                            3.94
                      BENkFLUORAN              3.77                    0.46                            3.94
                      BENeFYRENE               4.00                    0.48                            3.46
                      BENaPYRENE               2.40                    0.38                            2.73
                      PERYLENE                 2.38                    0.28                            1.92
                      I123cdPYRENE             1.78                    0.39                            1.61
                      DBahANTHRA               0.36         1          0.08                            0.42
                      BghiPERYLENE             2.69                    0.60                            2.67

                      TOTAL PAH's              845.7                   216.5                           677.2
                         (W/O, PERYLENE)


                      2-METHYLNAPH             54.80                   5.15                            51.49
                      1-METHYLNAPH             27.17                   3.02                            24.91


                      2,6-DIMETHNAPH           56.67                   8.38                            43.14


                      2,3,5-TRIMETHNAPH        11.12                   3.15                            10.76


                      1-METHYLPHEN             3.87                    1.75                            3.13


                      Surrogate Recoveries
                      NAPHD8:                  82.3                    84.2                            76.9
                      ACENDIO:                 84.8                    82.3                            86.6
                      PHENDIO:                 84.6                    81.1                            87.2
                      CHRYD12:                 62.7                    82.2                            70.1
                      PERYD12:                 70.9                    82.1                            84.5





























                                                                         266






                                 Antarctic McMurdo's Sediments Aromatic Hydrocarbon Data


           INVEST#:               OLrrFALL                WQB                     WQB                      PD-9-92 -15-
           ID:                    60'                     30'                     60'                      0
           LABSAMNO:              J2058                   J2062                   J2063                    J 1942
           UNIT:                  ng/g                    ng/g                    ng/g                     ng/g
           PNA Analyte            Conc         DB QUAL Conc            DB QUAL Conc             DB QUAL Conc             DB QUAL


           SAMPLE TYPE:           SA24P                   SAMP                    SAMP                     SAMP
           COLLECTION DATE:       12/12/91                12/11/91                12/11/91
           RECEWT DATE:
           QCBATC-H:              M609                    M609                    M609                     JP042
           EXTRACTION DATE:                                                                                08/01/92
           METHOD:                GCFID                   GCFID                   GCFID                    GCFID
           ANALYSIS DATE:
           METHOD:                GCMS                    GCMS                    GCMS                     GCMS,
           ANALYSIS DATE:         03/02/93                03/02/93                03/02/93                 08/18/92
           METHOD:                GCECD                   GCECD                   GCECD                    GCECD
           ANALYSIS DATE:         03/12/93                03/12/93                03/12/93                 08/02/93
           MATRIX:                SEDIMENT                SEDIMENT                SEDIMENT                 SED
           SUBMAT:
           SAMPLWT-
           VVETWT:                17.11                   24.43                   13.59                    26.7
           DRYWT:                 10.14                   10.21                   10.24                    10.35
           VVTLTNITS:             GRAMS        DRY        GRAMS        DRY        GRAMS        DRY         GRAMS         DRY
           PCTSOLIDS:
           VOL:
           VOLUNITS:              LITERS                  LITERS                  LITERS                   LITERS


           NAPHTI-LkLENE          47.24                   98.86                   13.88                    1.59
           Cl-NAPHTHALENES        134.51                  390.79                  39.98                    3.90
           C2-NAPHTHALENES        122.27                  547.45                  68.24                    6.99
           C3-NAPHTHALENES        99,55                   548.15                  116.03                   8.67
           C4-NAPHTHALENES        86.96                   298.46                  102.03                   10.69
           BIPHENYL               21.30                   44.27                   7.15                     1.07
           ACENAPHTHYLENE         3.65                    4.83                    0.62         1           0.15          1
           ACENAPHTHENE           2.41                    13.46                   1.14                     0.22          1
           FLUORENE               7.10                    18.73                   2.80                     0.83          1
           Cl-FLUORENES           12.47                   29.92                   8.78                     2.38
           C2-FLUORENES           35.72                   63.50                   24.00                    5.45
           C3-FLUORENES           61.11                   89.57                   33.14                    5.36
           PHENANTHRENE           28.79                   94.28                   12.33                    1.88
           ANTHRACENE             9.64                    18.57                   2.62                     0.20
           Cl-PHEN_ANTHR          28.80                   60.58                   14.65                    4.41
           C2-PHEN@ANTI-IR        48.59                   91.75                   29.80                    6.88
           C3-PHEN-ANTHR          105.06                  130.14                  39.12                    4.35
           C4-PHEN-ANTHR          74.50                   101.65                  28.30                    2.29
           DIBENZOTHIO            5.61                    10.38                   2.50                     0.56
           Cl-DI13EN              16.23                   28.55                   9.49                     2.41
           C2-DIBEN               48.57                   81.94                   28.28                    5.10
           C3-DIBEN               92.36                   126.44                  44.63                    5.13
           FLUORANTHENE           18.09                   85.54                   9.31                     0.44          1
           PYRENE                 28.44                   89.66                   11.92                    1.22
           Cl-FLUORAN-PYR         26.93                   21.29                   7.67                     0.97          1
           BENaANTHRACENE         14.09                   37.10                   2.08                     0.44          1
           CHRYSENE               21.41                   48.76                   3.26                     0.49          1
           CI-CHRYSENES           43*66                   45.57                   4.42                     0.56          1



                                                                    267






                                    Antarctic McMurdo's Sediments Aromatic Hydrocarbon Data


             UqVEST#:                OLJTFALL                WQB                      WQB                     N)-9-92 -15-
             ID:                     60'                     30'                      60'                     0
             LABSAMNO:               J2058                   J2062                    J2063                   J1942
             UNIT:                   ng/g                    ng/g                     ng/g                    ng/g
             I PNA Ana@yte           Conc         DB QUAL Conc             DB QUAL Conc            DB QUAL Conc              DB Qu,.@L

             C2-CHRYSENES            60.53                   45.52                    7.07                    0.00           ND
             C3-CFWSENES             6.90                    6.45                     1.35         1          0.00           ND
             C4-CHRYSENES            2.45                    5.02                     1.41         1          0.00           ND
             BENbFLUORAN             9.40                    20.96                    1.45                    0.49           1
             BENkFLUORAN             9.40                    20.96                    1.44                    0.12           1
             BENePYRENE              17.02                   16.95                    1.91                    0.32           1
             BENaPYRENE              11.59                   19.66                    1.14                    0.34           1
             PERYLENE                4.17                    5.98                     0.49         1          1.29
             I123edPYRENE            6.25                    13.72                    1.06                    0.19           1
             DBabANTHRA              1.98                    2.74                     0.31         j          0.05           1
             B&PERYLENE              13.34                   14.90                    1.62                    0.38           1


             TOTAL PAH's             1383.9                  3387.1                   686.9                   86.5
               (W/O PERYLENE)


             2-METHYLNAPH            101.45                  255.37                   28.49                   2.30
             1-A4ETHYLNAPH           33.06                   135.42                   11.49                   1.60


             2,6-DRMETHNAPH          76.11                   303.53                   32.12                   2.50


             2.3,5-TFJA=NAPH         18.95                   81.51                    16.33                   2.45


             I-NUETHYLPHEN           6.76                    11.44                    3.99                    1.28


             Surrogate Recoveries
             NAPHD8:                 80.6                    84.9                     66.4                    74.5
             ACEND10:                79.2                    87.2                     72.5                    82.6
             PHEND10:                85.7                    83.1                     71.5                    105.0
             CHRYD12:                36.0                    40.0                     61.9                    103.6
             PERYD 12:               67.2                    85.7                     63.7                    50.5





























                                                                         268






                                  Antarctic McMurdo's Sediments Aromatic Hydrocarbon Data



                                  INVEST#:                PD-21-92 -23-             PD-31-92 -4-
                                  ID:                     0                         0
                                  LABSAMNO:               J 1949                    J1956
                                  UNIT:                   ng/g                      ng/g
                                  I PNA Analyte           Conc           DB QUAL Conc             DB QUAL


                                  SAMPLE TYPE:            SAMP                      SAMP
                                  COLLECTION DATE:
                                  RECEIPT DATE:
                                  QCBATCH:                JP042                     JP045
                                  EXTRACTION DATE:        08/01/92                  09/01/92
                                  METHOD:                 GCFID                     GCFID
                                  ANALYSIS DATE:
                                  METHOD:                 GCMS                      GCMS
                                  ANALYSIS DATE:          08/18/92                  09/24/92
                                  METHOD:                 GCECD                     GCECD
                                  ANALYSIS DATE:          08/02/93                  08/02/93
                                  MATRIX:                 SED                       SED
                                  SUBMAT:
                                  SAMPLWT:
                                  VVE-TWT:                17.9                      15.2
                                  DRYWT:                  10.14                     10.11
                                  WTUNITS:                GRAMS          DRY        GRAMS         DRY
                                  PCTSOLIDS:
                                  VOL:
                                  VOLUNITS:               LITERS                    LITERS


                                  NAPHTHALENE             1.23                      1.14
                                  Cl-NAPHTHALENES         3.41                      1.87
                                  C2-NAPHTHALENES         6.31                      3.14
                                  C3-NAPHTHALENES         10.43                     6.18
                                  C4-NAPHTHALENES         16.57                     6.30
                                  BIPHENYL                0.92           1          0.51          1
                                  ACENAPHTHYLENE          0.09           j          0.06          1
                                  ACENAPHTHENE            0.22           j          0.31          1
                                  FLUORENE                0.97           1          0.42          j
                                  Cl-FLUORENES,           3.33                      1.59
                                  C2-FLUORENES            11.73                     5.69
                                  C3-FLUORENES            15.48                     10.94
                                  PHENANTHRENE            2.53                      1.82
                                  ANTHRACENE              0.26           1          0.25          1
                                  Cl-PHEN-ANTHR           8.34                      6.87
                                  C2-PHEN-ANTHR           12.51                     14.67
                                  C3-PHEN-ANTHR           7.37                      11.28
                                  C4-PHEN-ANTHR           4.31                      4.24
                                  D113ENZOTHIO            0.82           1          0.59          1
                                  Cl-DIBEN                4.77                      5.08
                                  C2-DIBEN                11.72                     16.76
                                  C3-DI]BEN               8.58                      17.68
                                  FLUORANTHENE            0.46           j          1.42
                                  PYRENE                  2.13                      3.90
                                  Cl-FLUORAN-PYR          1.00                      1.56
                                  BENaANTHRACENE          0.17           1          0.50          j
                                  CHRYSENE                0.23           1          0.48          1
                                  CI-CHRYSENES            0.30           1          0.63          1



                                                                      269






                                    Antarctic McMurdo's Sediments Aromatic Hydrocarbon Data


                                    U4VEST#:                PD-21-92 -23-              PD-31-92 -4-
                                    ID:                     0                          0
                                    LABSAMNO:               J1949                      J1956
                                    UNIT:                   ng/g                       ng/g
                                    PNA Analyte             Conc           DB QUAL Conc              DB gUAL

                                    C2-CHRYSENES            0.00           ND          0.90          j
                                    C3-CHRYSENES            0.00           ND          0.00          ND
                                    C4-CHRYSENES            0.00           ND          0.00          ND
                                    BENbFLUORAN             0.09           1           0.45          1
                                    BENkFLUORAN             0.02           j           0.21          1
                                    BENePYRENE              0.08           1           0.30          1
                                    BENaPYRENE              0.06           1           0.27          1
                                    PERYLENE                1.08                       1.92
                                    1123cdPYRENE            0.02           1           0.27          1
                                    DBahANTHRA              0.02           1           0.05          1
                                    BghiPERYLENE            0.10           1           0.32          j

                                    TOTAL PAH's             136.6                      128.7
                                      CW/0 PERYLENE)


                                    2-NM-FHYLNAPH           2.06                       1.17
                                    1-bffi-lliYLNAPH        1.35                       0.70          1


                                    2.6-DIbEETHNAPH         2.72                       0.99          1


                                    2,3,5-TRD4ETHNAPH       2.91                       1.27


                                    1-NIETHYLPHEN           1.96                       1.91


                                    Surrogate Recoveries
                                    NAPHD8:                 76.8                       80.6
                                    ACEND10:                89.1                       108.1
                                    PHEND10:                120.0                      133.6         Q
                                    CHRYD12:                116.2                      118.8
                                    PERYD12:                70.2                       87.0




























                                                                        270



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               McMurdo Sediment Pesticides
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                                      Antarctic McMurdo's Sediment Pesticide and PCB Data



                  INVEST#:                   BERNACCHIBAY                  BAY OF SAILS                         WQB
                  ID:                                       100,                       100,                        60'
                  LABSAMNO:                               J2034                      J2037                      J2042
                  UNIT:                                   ng/g                       ng/g                       ng/g
                  Analyte (Cont)                          Conc DB QUAL               Conc DB QUAL               Conc DB QUAL


                  SAMPLE TYPE:                            SAMP                       SAMP                       SAMP
                  COLLECMON DATE:                    01/09/91                    12/21/90                  12/10/90
                  RECEIPT DATE:
                  QCBATCH:                                M607                       M607                       M607
                  EXTRACTION DATE:
                  M=OD:                                   GCFID                      GCFID                      GCFID
                  ANALYSIS DATE:
                  M=OD:                                   GCMS                       GCMS                       GCMS
                  ANALYSIS DATE:                     02/26/93                    02/26/93                  02/27/93
                  METHOD:                               GCECD                      GCECD                      GCECD
                  ANALYSIS DATE:                     04/23/93                    04/23/93                  04/23/93
                  MATRIX:                           SEDIMENT                    SEDIMENT                  SEDIMENT
                  SUBMAT:
                  SAMPLWT:
                  V&-fwr:                         16.48574323                 15.83281541               17.56637946
                  DRYWT:                                  11.39                      10.19                      9.99
                  VVTUNrf`S:                           GRAMS DRY                  GRAMS DRY                  GRAMS DRY
                  PCTSOLIDS:
                  VOL:
                  VOLUNITS:                             LITERS                      UrERS                     LITERS


                  TOTAL BHUS                              0.16  J                    0.00   ND                  0.68  J
                  TOTAL CHLORDANES,                       0.09  j                    0.02   J                   3.22
                  TOTAL DDTS                              0.03  J                    0.00   1                   5.71
                  TOTAL PCB'S                               0.7 J                       0.7 J                   484.9


                  ALPHA-BHC                               0.00  ND                   0.00   ND                  0.00  ND
                  HCB                                     0.01  1                    0.02   J                   0.52  J
                  BETA-BHC                                0.00  ND                   0.00   ND                  0.11  1
                  GAMMA-BHC                               0.16  J                    0.00   ND                  0.57  J
                  DELTA-BHC                               0.00  ND                   0.00   ND                  0.00  ND
                  HEPTACHLOR                              0.00  ND                   0.00   ND                  0.00  ND
                  HEPIA-EPOXIDE                           0.00  ND                   0.00   ND                  0.00  ND
                  OXY'CHLORDANE                           0.00  ND                   0.00   ND                  0.06  ND
                  GA@-CHLORDANE                           0.06  ND                   0.00   ND                  0.00  ND
                  ALPHA-CHLORDANE                         0.03  J                    0.02   J                   0.25  J
                  TRANS-NONACHLOR                         0.00  ND                   0.00   ND                  0.05  J
                  CIS-NONACHLOR                           0.00  ND                   0.00   ND                  2.86
                  ALDRIN                                  0.00  ND                   0.00   ND                  0.00  ND
                  DIELDRIN                                0.00  ND                   0.00   ND                  0.00  ND
                  ENDRIN                                  0.00  ND                   0.00   ND                  0.00  ND
                  M[IREX                                  0.00  ND                   0.00   ND                  0.00  ND
                  2,4-DDE (O,P'DDE)                       0.00  ND                   0.00   ND                  0.00  ND
                  4,4'DDE (P,P'DDE)                       0.01  1                    0.00   ND                  0.00  ND
                  2,4'DDD (O,P'DDD)                       0.01  1                    0.00   ND                  0.53  J
                  4,4-DDD (P,P'DDD)                       0.00  ND                   0.00   ND                  1.47
                  2,4'DDT (0,P'DDT)                       0.00  ND                   0.00   ND                  3.03
                  4,4'DDT (P,P'DDT)                       0.00  ND                   0.00   ND                  0.68  ND





                                                                      272








                                         Antarctic McMurdo's Sediment Pesticide and PCB Data



                    INVEST#:                     BERNACCHIBAY                    BAY OF SAILS                          WQB
                    ID:                                         100,                         100,                         60'
                    LABSAMNO:                                J2034                        J2037                       J2042
                    UNIT:                                     ng/g                         ng/g                        ;rlg/g
                    Analyte (Cont)                            Conc DB QUAL                 Cone DB QUAL                Conc DB QUAL

                    PCB # (CLORINATION)


                    8 (CL2)                                   0.12  J                      0.13  J                     0.39  J
                    18 (CL3)                                  0.06  J                      0.05  J                     0.54  J
                    28 (CL3)                                  0.00  ND                     0.09  1                     2.67
                    44 (CIA)                                  0.07  J                      0.06  J                     1.89
                    52 (CIA)                                  0.04  J                      0.05  J                     4.92
                    66 (CIA)                                  0.00  ND                     0.00  ND                   26.68
                    101 (CL5)                                 0.00  ND                     0.00  ND                   17.48
                    105 (CL5)                                 0.00  ND                     0.00  ND                   12.84
                    110/77 (CL5/4)                            0.00  ND                     0.00  ND                    0.00  ND
                    118/108/149(CL5/5/6)                      0.00  ND                     0.00  ND                    8.15
                    128(CL6)                                  0.00  ND                     0.00  ND                    5.40
                    138 (CL6)                                 0.16                         0.09  1                    68.54
                    126 (CL5)                                       NA                           NA                          NA
                    153 (CL6)                                 0.00  ND                     0.00  ND                   64.34
                    170 (CL7)                                 0.00  ND                     0.00  ND                    0.00  ND
                    180 (CL7)                                 0.00  ND                     0.00  ND                   74.80
                    187/182/159(CL7/7/6)                      0.00  ND                     0.00  ND                   42.02
                    195 (CL8)                                 0.00  ND                     0.00  ND                    7.14
                    206 (CL9)                                 0.00  ND                     0.00  ND                    4.01
                    209 (CLIO)                                0.00  ND                     0.00  ND                    0.00  ND


                    Surrogate Recoveries
                    DBOFB0/b:                                 81.1                         76.9                        47.3
                    PCB#103%:                                 88.3                         80.4                        52.8
                    PCB#198%:                                102.8                         90.5                        56.2


                    PCB #(CHLORINATION)


                    7 (CL2)                                   0.00  ND                     0.00  ND                    0.00  ND
                    15 (CL2)                                  0.04  J                      0.05  J                     2.06
                    24 (CI-3)                                 0.00  ND                     0.00  ND                    0.00  ND
                    16/32 (CL3)                               0.11  1                      0.00  ND                    0.95  J
                    29 (CI,3)                                 0.00  ND                     0.00  ND                    0.00  ND
                    26 (CL3)                                  0.00  ND                     0.00  ND                    0.22  J
                    25(CL3)                                   0.01  1                      0.01  1                     0.14  J
                    50 (CIA)                                  0.00  ND                     0.00  ND                    1.30
                    31 (CL3)                                  0.00  ND                     0.00  ND                    0.00  ND
                    33 (CI,3)                                 0.00  ND                     0.00  ND                    0.34  J
                    22 (CI-3)                                 0.00  ND                     0.00  1@m                   0.27  J
                    45 (CL4)                                  0.00  ND                     0.02  J                     0.24  J
                    46 (CIA)                                  0.00  ND                     0.00  ND                    0.11  1
                    49 (CIA)                                  0.08  J                      0.09  1                     1.20
                    47/48 (CIA)                               0.00  ND                     0.00  ND                    0.00  ND
                    37/42 (CIA)                               0.05  J                      0.04  J                     1.13
                    41/64 (CIA)                               0.00  ND                     0.00  ND                    0.00  ND
                    40 (CL4)                                  0.00  ND                     0.00  ND                    0.39  J
                    100 (CL5)                                 0.00  ND                     0.00  ND                    0.00  ND



                                                                            273







                                      Antarctic McMurdo's Sediment Pesticide and PCB Data



                  INVEST#:                   BERNACCHI BAY                  BAY OF SAILS                         WQB
                  ID:                                       100,                        100,                        60'
                  LABSAMNO:                              J2034                       J2037                      J2042
                  UNIT:                                   ng/g                        ng/g                       ng/g
                  Analyte (Cont)                          Conc DB QUAL                Conc DB QUAL               Conc DB QUAL


                  74 (CIA)                                0.00 ND                     0.00 ND                    0.00 ND


                  PCB #(CHLORINATION)


                  70 (CIA)                                0.00  ND                    0.00  ND                   2.06
                  88 (CL5)                                0.00  ND                    0.00  ND                   1.59
                  60/56 (CL5)                             0.00  ND                    0.00  ND                   0.88  J
                  92? (CL5)                               0.00  ND                    0.00  ND                   2.76
                  84? (CL5)                               0.00  ND                    0.00  ND                   3.89
                  99 (CL5)                                0.00  ND                    0.01  1                    2.98
                  83 (CL5)                                0.00  ND                    0.00  ND                   0.61  J
                  97 (CL5)                                0.00  ND                    0.00  ND                   2.58
                  87 (CL5)                                0.00  ND                    0.00  ND                   5.14
                  85 (CL5)                                0.00  ND                    0.00  ND                   1.05
                  136 (CIJ63)                             0.00  ND                    0.00  ND                  12.29
                  82 (CL5)                                0.00  ND                    0.00  ND                   1.12
                  151 (CL6)                               0.00  ND                    0.00  ND                  27.29
                  107/108/144(CL5/5/6)                    0.00  ND                    0.00  ND                   0.00  ND
                  149 (CL6)                               0.00  ND                    0.00  ND                  56.34
                  188 (CL7)                               0.00  ND                    0.00  ND                   0.00  ND
                  146 (CL6)                               0.00  ND                    0.00  ND                  10.54
                  141 (CL6)                               0.00  ND                    0.00  ND                   0.00  ND
                  137 (CL6)                               0.00  ND                    0.00  ND                  36.12
                  UNK (CL6)                               0.00  ND                    0.00  ND                   0.00  ND
                  158 (CL7)                               0.00  ND                    0.00  ND                   7.12
                  129 (CL6)                               0.00  1@m                   0.00  DO                   0.00  DM
                  178 (CL7)                               0.00  DM                    0.00  l*M                  8.92
                  183 (CL7)                               0.00  ND                    0.00  ND                  20.68
                  167 (CL6)                               0.00  ND                    0.00  ND                   1.61
                  185 (CL7)                               0.00  ND                    0.00  ND                   5.56
                  174 (CL7)                               0.00  ND                    0.00  ND                  33.67
                  177 (CL7)                               0.00  ND                    0.00  ND                  20.27
                  156/171/202(CL6/7/8)                    0.00  ND                    0.00  ND                   0.00  ND
                  200 (CLS)                               0.00  ND                    0.00  ND                   2.89
                  172 (CL7)                               0.00  ND                    0.00  ND                   6.63
                  191 (CU)                                0.00  ND                    0.00  ND                   0.00  ND
                  201 (CL8)                               0.00  ND                    0.00  ND                  16.95
                  196 (CLB)                               0.00  ND                    0.00  ND                  18.68
                  189 (CL7)                               0.00  ND                    0.00  ND                   1.21
                  194 (CLB)                               0.00  ND                    0.00  ND                  15.63
                  205 (CL9)                               0.00  ND                    0.00  ND                   1.00













                                                                        274







                                      Antarctic McMurdo's Sediment Pesticide and PCB Data



                   INVEST#:                      OUTFALL               CAPE ARMITAGE                     OUTFALL,
                   ID:                                  30'                            60'                      30'
                   LABSAMNO:                         J2049                          J2056                     J2057
                   UNIT:                             ng/g                           ng/g                      ng/g
                   Analyte (Cont)                    Conc DB QUAL                   Conc DB QUAL              Conc DB QUAL


                   SAMPLEWPE:                        SAMP                           SAMP                      ELAW
                   COLLECTION DATE:              11/30/90                       12/14/90                 12/13/91
                   RECEWT DATE:
                   QCBATCH:                          M608                           M608                      M608
                   EXTRACTION DATE:
                   METHOD:                           GCFID                          GCFID                     GCFID
                   ANALYSIS DATE:
                   METHOD:                           GCMS                           GCMS                      GCMS
                   ANALYSIS DATE:                02/28/93                       02/28/93                 02/28/93
                   METFIOD:                        GCECD                          GCECD                     GCECD
                   ANALYSIS DATE:                03/20/93                       03/20/93                 03/20/93
                   AIATRIX-                     SEDIMENT                      SEDIMENT                  SEDIMENT
                   SUBMAT:
                   SAMPLWT:
                   WETWT:                     13.21026447                    16.96326531              16.24610592
                   DRYWT.                            10.09                          10.39                     10.43
                   VVTUNITS:                      GRAMS DRY                      GRAMS DRY                 GRAMS DRY'
                   PCTSOLIDS:
                   VOL:
                   VOLUNITS:                        LITERS                        LITERS                    LITERS


                   TOTAL BHC'S                       0.47  J                        1.18  1                   0.03 J
                   TOTAL CHLORDANES                  14.62                          0.39  J                   0.85 J
                   TOTAL DDTS                        16.64                          0.48  J                   3.19 J
                   TOTAL PCB'S                       574.8                          54.4                      96.0


                   ALPHA-BHC                         0.00  ND                       0.34  J                   0.00 ND
                   HCB                               0.51  J                        0.13  J                   0.33 J
                   BETA-BHC                          0.04  J                        0.00  ND                  0.03 J
                   GAM[MA-BHC                        0.42  J                        0.65  J                   0.00 ND
                   DELTA-BHC                         0.00  ND                       0.20  J                   0.00 ND
                   HEPTACHLOR                        0.00  ND                       0.00  ND                  0.00 ND
                   HEPTA-EPOXIDE                     0.00  ND                       0.00  ND                  0.00 ND
                   OXYCHLORDANE                      0.56  J                        0.00  ND                  0.09 1
                   GAMMA-CHLORDANE                   0.00  ND                       0.00  ND                  0.10 1
                   ALPIM-CHLORDANE                   0.00  ND                       0.05  J                   0.06 J
                   TRANS-NONACHLOR                   0.00  ND                       0.02  J                   0.05 J
                   CIS-NONACHLOR                     14.07                          0.33  J                   0.54 J
                   ALDRIN                            0.00  ND                       0.00  ND                  0.00 ND
                   DIELDRIN                          0.00  ND                       0.00  ND                  0.21 J
                   ENDRIN                            0.00  ND                       0.00  ND                  0.00 ND
                   bffllEX                           0.00  ND                       0.00  ND                  0.00 ND
                   2.4'DDE (O,P'DDE)                 0.00  ND                       0.00  ND                  0.00 ND
                   4.4'DDE (P,P'DDE)                 0.00  ND                       0.00  ND                  0.81 J
                   2.4'DDD (0,P'DDD)                 0.00  ND                       0.03  J                   0.19 1
                   4,4'DDD (P,P'DDD)                 1.39                           0.09  1                   0.80 J
                   2,4'DDT (O.P'DDT)                 14.81                          0.36  J                   0.72 J
                   4,4'DDrr (P,P'DDTI                0.44  ND                       0.00  ND                  0.67 J




                                                                      275







                                        Antarctic McMurdo's Sediment Pesticide and PCB Data



                    UfVEST#:                        0LJTFALL               CAPE ARMITAGE                        OUFFALL
                    ID:                                    30'                              60'                         30'
                    LABSAMNO:                          J2049                            J2056                      J2057
                    UNIT:                               ng/g                             ng/g                        ng/g
                  .Analyte (Cont)                       Conc DB QUAL                     Conc DB QUAL                Conc DB QUAL,

                    PCB # (CLORINATION)


                    8 (CL2)                             0.95  1                          0.08  J                     0.09  1
                    18 (CL3)                            2.29                             0.46  J                     0.14  J
                    28 (CW)                             6.06                             0.21  J                     1.21
                    44 (CIA)                            6.93                             0.14  J                     0.44  J
                    52 (CIA)                           17.36                             0.23  J                     1.27
                    66 (CIA)                            6.75                             0.11  1                     0.39  J
                    101 (CL5)                          19.50  D                          1.56                        4.42
                    105 (CL5)                           2.90  D                          2.15                        3.41
                    110/77 (CL5/4)                     12.80  D                          1.19                        3.53
                    118/108/149(CL5/5/6)               39.44                             0.81  J                     1.94
                    128 (CL6)                          33.26                             0.54  J                     0.86  J
                    138 (CL6)                          40.20  D                          8.40                      13.36
                    126 (CL5)                                 NA                               NA                          NA
                    153 (CL6)                          44.00  D                          8.39                      13.22
                    170 (CL7)                           0.00  ND                         3.78                      29.55
                    180 (CL7)                          28.50  D                          8.94                      13.07
                    187/182/159(CL7/7/6)               17.70  D                          4.90                        6.66
                    195 (CLB)                           3.40  D                          1.03                        1.48
                    206 (CL9)                          21.93                             0.46  J                     1.19
                    209 (CLIO)                          0.99  1                          0.02  J                     0.00  ND


                    Surrogate Recoveries
                    DBOFB%:                             41.3                             43.5                        32.8
                    PCB#103%:                           61.8                             58.7                        49.8
                    PCB#198%:                           97.6                             61.3                        48.5


                    PCB #(CHLORINATION)


                    7 (CL2)                             0.00  ND                         0.00  ND                    0.00  ND
                    15 (CL2)                            2.47                             0.12  J                     0.12  J
                    24 (CL3)                            0.12  J                          0.00  ND                    0.00  ND
                    16/32 (CL3)                         2.14                             0.00  ND                    0.14  J
                    29 (CL3)                            0.00  ND                         0.00  ND                    0.00  ND
                    26 (CL3)                            0.68  J                          0.00  ND                    0.00  ND
                    25 (CL3)                            0.40  J                          0.00  ND                    0.05  J
                    50 (CIA)                            3.41                             0.00  ND                    0.00  ND
                    31 (CI,3)                           0.00  ND                         0.00  ND                    0.00  ND
                    33 (CL3)                            2.70                             0.03  J                     0.15  J
                    22 (CL3)                            1.95                             0.02  J                     0.06  J
                    45 (CIA)                            0.99  1                          0.00  ND                    0.07  J
                    46 (CL4)                            0.43  J                          0.00  ND                    0.11  j
                    49 (CIA)                            4.51                             0.10  j                     0.25  J
                    47/48 (CIA)                         1.69                             0.00  ND                    0.00  ND
                    37/42 (CIA)                         4.32                             0.11  1                     0.18  1
                    41/64 (CIA)                         5.08                             0.04  J                     0.28  J
                    40 (CIA)                            1.14                             0.00  ND                    0.00  ND
                    '00  (CL5)                          0.00  ND                         0.00  ND                    0.00  ND



                                                                          276








                                         Antarctic McMurdo's Sediment Pesticide and PCB Data



                    INVEST#:                         OUTFALL                CAPE ARMITAGE                        OUTF-ALL
                    ID:                                     30'                              60'                         30'
                    LABSAMNO:                           J2049                            J2056                       J2057
                    UNIT:                                ng/g                             ng/g                        719/9
                    Analyte (Cont)                       Conc DB QUAL                     Conc DB QUAL                Conc DB QUAL

                    74 (CIA)                             6.00                             0. 16 J                     0.21 J


                    PCB #(CHLORINATION)


                    70 (CIA)                            13.61                             0.15  J                     0.69  J
                    88 (CL,5)                            1.67                             0.08  J                     0.23  J
                    60/56 (CL5)                         12.79                             0.00  ND                    0.30  J
                    92? (CL5)                           20.80                             0.21  J                     0.77  J
                    84? (CL5)                            9.04                             0.18  1                     0.51  J
                    99 (CL5)                             5.32                             0.30  J                     0.62  J
                    83 (CL5)                             1.15                             0.04  J                     0.09  1
                    97 (CL5)                             7.96                             0.22  J                     0.62  J
                    87 (CI-5)                           33.08                             0.45  J                     1.28
                    85 (CL5)                             3.30                             0.08  J                     0.22  J
                    136 (CL6)                            4.10  D                          0.78  J                     1.70
                    82 (CL5)                             3.13                             0.06  J                     0.20  J
                    151 (CL6)                           16.40  D                          2.20                        4.10
                    107/108/144(CL5/5/6)                18.60  D                          1.58                        3.13
                    149 (CL6)                           26.40  D                          5.57                        9.60
                    188 (CL7)                            0.00  ND                         0.00  ND                    0.00  ND
                    146 (CL6)                            6.20  D                          1.05                        2.00
                    141 (CL6)                           29.80  D                          2.23                        4.21
                    137 (CL6)                            0.95  J                          0.04  J                     0.10  1
                    UNK (CL6)                           10.91                             0.11  1                     0.25  J
                    158 (CL7)                            3.10  D                          0.75  J                     1.25
                    129 (CL6)                            0.00  ND                         0.11  1                     0.28  J
                    178 (CL7)                            3.80  D                          1.04                        1.60
                    183 (CL7)                           10.50  D                          2.36                        3.29
                    167 (CL6)                            9.77                             0.18  1                     0.31  J
                    185 (CL7)                            3.60  D                          0.70  J                     1.09
                    174 (CL7)                           14.60  D                          4.29                        6.01
                    177 (CL7)                            8.90  D                          2.66                        3.58
                    156/171/202(CL6/7/8)                 2.30  D                          2.10                        2.30
                    200 (CL8)                           14.03                             0.37  J                     0.44  J
                    172 (CL7)                            3.90  D                          0.89  J                     1.29
                    191 (CL7)                            9.89                             0.27  J                     0.60  J
                    201 (CL8)                            8.10  D                          2.03                        3.15
                    196 (CL8)                            9.50  D                          2.41                        3.62
                    189 (CL7)                            7.94                             0.20  J                     0.31  J
                    194 (CL8)                            7.10  D                          2.11                        3.28
                    205 (CL9)                            6.03                             0.19  1                     0.31  J











                                                                            277







                                   Antarctic McMurdo's Sediment Pesticide and PCB Data



                   INVEST#:                    OUTFALL                       WQB                     WQB
                   ID:                                 60'                     30,                      60'
                   LABSAMNO:                        J2058                    J2062                   J2063
                   UNIT:                            ng/g                     ng/g                    ng/g
                   Anabrte (Cont)                   Conc DB QUAL             Conc DB QUAL            Conc DB QUAL


                   SAWLE TYPE:                      SAMP                     SAMP                    SAMP
                   COLLECTION DATE:            12/12/91                  12/11/91                 12/11/91
                   RECEIFr DATE:
                   QCBATCH:                         M609                     M609                    M609
                   EXTRACTION DATE:
                   METHOD:                          GCFID                    GCFID                   GCFID
                   ANALYSIS DATE:
                   METHOD:                          GCMS                     GCMS                    GCMS
                   ANALYSIS DATE:              03/02/93                  03/02/93                03/02/93
                   METHOD:                        GCECD                    GCECD                     GCECD
                   ANALYSIS DATE:              03/12/93                  03/12/93                03/12/93
                   MATRIX:                     SEDIMENT                SEDIMENT                 SEDIMENT
                   SUBMAT:
                   SAMPLWT:
                   WETWT.                    17.11103611             24.42583732              13.58630755
                   DRYVrr:                          10.14                    10.21                   10.24
                   vv,I@S:                       GRAMS DRY                GRAMS DRY                  GRAMS DRY
                   PCTSOLIDS:
                   VOL:
                   VOLUNITS:                      LITERS                   LITERS                    LITERS


                   TOTAL BHC'S                      0.26  J                  0.13 J                  0.00  ND
                   TOTAL CHLORDANES                 5.04                     1.44                    0.28  J
                   TOTAL DDTS                       7.25                     3.98                    0.80  J
                   TMAL PCB'S                       685.6                    414.6                   103.6


                   ALPHA-BHC                        0.22  J                  0.01 j                  0.00  ND
                   HCB                              4.68  D                  0.67 J                  0.03  J
                   BETA-BHC                         0.00  ND                 0.01 1                  0.00  ND
                   GAMM[A-BHC                       0.04  J                  0.11 1                  0.00  ND
                   DELTA-BHC                        0.00  ND                 0.00 ND                 0.00  ND
                   HEPTACHLOR                       0.00  ND                 0.00 ND                 0.00  ND
                   HEPTA-EPOXIDE                    0.00  ND                 0.01 j                  0.00  ND
                   OXYCHLORDANE                     0.16  J                  0.03 J                  0.02  J
                   GAMMA-CHLORDANE                  0.00  ND                 0.15 J                  0.01  1
                   ALPHA-CHLORDANE                  0.00  ND                 0.05 J                  0.01  j
                   TRANS-NONACHLOR                  0.02  J                  0.05 J                  0.00  ND
                   CIS-NONACHLOR                    4.86                     1.15                    0.25  J
                   ALDRIN                           0.00  ND                 0.00 ND                 0.00  ND
                   DIELDRIN                         0.02  J                  0.26 J                  0.06  J
                   ENDRIN                           0.00  ND                 0.00 ND                 0.00  ND
                   NUREX                            0.00  ND                 0.00 ND                 0.00  ND
                   2,4'DDE (0,P'DDE)                0.00  ND                 0.00 ND                 0.01  1
                   4,4'DDE (P,P'DDE)                0.85  J                  0.75 J                  0.14  J
                   2.4'DDD (0,P'DDD)                0.24  J                  0.17 J                  0.05  J
                   4,4'DDD (P,P'DDD)                2.62                     1.19                    0.38  J
                   2,4'DDT (O,P'DDT)                3.19                     0.99 j                  0.19  1
                   4.4'DDT (P,P'DDT)                0.34  J                  0.88 1                  0.01  j




                                                                  278








                                         Antarctic McMurdo's Sediment Pesticide and PCB Data



                       INVES`r#:                        OUTFALL                        WQB                         WQB
                       ID:                                     60'                        30'                         601
                       LABSAMNO:                          J2058                       J2062                      J2063
                       UNrr.                                ng/g                       ng/g                        ng/g
                       Analyte (Cont)                       Conc DB QUAL               Conc DB QUAL                Cmic DB QUAL

                       PCB # (CLORINATION)


                       8 (CL2)                              2.82                       0.45  J                     0.27  J
                       18 (CL3)                             6.30                       1.31                        0.64  J
                       28 (CL3)                             3.50                       1.87                        0.70  J
                       44 (CL4)                             4.15                       3.78                        1.23
                       52 (CIA)                           10.83                       11.88                        3.22
                       66 (CIA)                             3.56                       0.93  J                     0.34  J
                       101 (CL5)                          80.00                       22.59                        6.42
                       105 (CL5)                            3.03                       1.42                        1.11
                       110/77(CL5/4)                      60.10                       25.60                      10.06
                       118/108/149(CL,5/5/6)              17.55                        6.41                        3.02
                       128 (CL6)                          15.03                        3.61                        1.14
                       138 (CL6)                          19.40   D                   54.27                      12.31
                       126 (CL5)                                  NA                         NA                          NA
                       153 (CL6)                          24.30   D                    6.50  D                   16.43
                       170 (CL7)                            9.50  D                   22.06                        4.59
                       180 (CL7)                          17.00   D                   46.06                        9.76
                       187/182/159(CL7/7/6)                 8.50  D                   32.88                        5.93
                       195 (CL8)                          28.02                        3.69                        0.77  J
                       206(CL9)                           12.02                        1.55                        0.32  J
                       20.9 (CL10)                          0.50  J                    0.33  J                     0.00  ND

                       Surrogate Recoveries
                       DBOFB%:                              68.0                       65.8                        68.1
                       PCB#103%:                            50.0                       57.3                        80.7
                       PCB# 1980/6:                         43.9                       31.1                        58.9


                       PCB #(CHLORINAIION)


                       7 (CL2)                              0.00  ND                   0.00  ND                    0.00  ND
                       15 (CL2)                             2.54                       1.24                        0.47  J
                       24 (CL3)                             0.04  J                    0.22  J                     0.03  J
                       16/32(CL3)                           1.25                       0.36  J                     0.24  J
                       29 (CL3)                             0.00  ND                   0.00  ND                    0.00  ND
                       26 (CI-3)                            0.35  J                    0.13  J                     0.07  J
                       25 (CL3)                             1.01                       0.33  J                     0.11  1
                       50 (CIA)                             4.23                       0.62  J                     0.11  1
                       31 (CL3)                             0.00  ND                   0.00  ND                    0.00  ND
                       33 (CL3)                             1.83                       1.00                        0.43  J
                       22 (CW)                              1.37                       0.69  J                     0.34  J
                       45 (CIA)                             0.37  J                    0.25  J                     0.08  j
                       46 (CIA)                             0.12  J                    0.09  1                     0.00  ND
                       49 (CIA)                             4.63                       2.14                        1.04
                       47/48 (CIA)                          1.56                       0.79  J                     0.20  J
                       37/42 (CIA)                          7.73                       1.95                        0.72  J
                       41/64 (CIA)                          0.00  ND                   1.80                        0.68  J
                       40 (CIA)                             1.72                       0.68  J                     0.20  J
                       100 (CL5)                            0.00  ND                   0.00  ND                    0.00  ND



                                                                            279







                                       Antarctic McMurdo's Sediment Pesticide and PCB Data



                      INVEST#:                        OLITFALL                       WQB                         WQB
                      ID:                                    60'                        30'                         60'
                      LABSAMNO:                          J2058                      J2062                       J2063
                      UNIT:                               ng/g                       ng/g                        ng/g
                    lAnalyte (Cont)                       Conc DB QUAL               Conc DB QUAL                Conc DB QUAL

                      74 (CIA)                            4.39                       1.41                        0.85 J


                      PCB #(CHLORINATION)


                      70 (CIA)                            9.85                       4.72                        2.59
                      88 (CL5)                            2.15                       1.25                        0.46  J
                      60/56 (CL,5)                        9.88                       3.60                        1.74
                      92? (CL5)                          11.38                       3.42                        1.02
                      84? (CL5)                           6.47                       3.46                        1.25
                      99 (CL5)                            6.75                       3.29                        1.53
                      83 (CL5)                            0.96                       0.58  J                     0.21  J
                      97 (CL5)                            8.41                       3.20                        1.41
                      87 (CL5)                           21.18                       9.02                        3.75
                      85 (CL5)                            3.23                       1.52                        0.77  J
                      136 (CL6)                          30.14                       6.58                        1.13
                      82 (CL5)                            2.89                       2.09                        0.64  J
                      151 (CL6)                           4.40  D                   23.97                        3.96
                      107/108/144(CL5/5/6)                0.00  ND                   0.00  ND                    0.00  ND
                      149 (CL6)                           9.40  D                   49.04                        8.59
                      188 (CL7)                           0.00  ND                   0.00  ND                    0.00  ND
                      146 (CL6)                          43.42                       9.21                        1.71
                      141 (CL66)                         16.74  D                   39.84                        7.07
                      137 (CL6)                           1.06                       0.39  J                     0.21  J
                      UNK (CLQ                            7.10                       1.64                        0.40  J
                      158 (CL7)                          20.05                       3.75                        0.91  j
                      129 (CL6)                           4.89                       1.08                        0.30  J
                      178 (CL7)                          24.29                       4.43                        0.77  J
                      183 (CL7)                           4.40  D                   12.11                        2.22
                      167 (CL6)                           6.87                       1.22                        0.30  J
                      185 (CL7)                          22.01                       3.76                        0.69  J
                      174 (CL7)                           7.00  D                   19.47                        3.54
                      177 (CL7)                          10.66  D                    9.99                        1.87
                      156/171/202(CLro/7/8)              76.86                      11.79                        1.84
                      200 (CL8)                           7.71                       1.10                        0.16  J
                      172 (CL7)                          22.74                       3.47                        0.72  J
                      191 (CL7)                           4.47                       0.62                        0.11  j
                      201 (CLS)                           3.80  D                    8.81                        1.75
                      196 (CL8)                           4.80  D                   10.21                        2.12
                      189 (CL7)                           3.38                       0.41  J                     0.08  J
                      194 (CL8)                           4.00  D                    7.48                        1.70
                      205 (CL9)                           2.82                       0.27  J                     0.06  J













                                                                          280








                                      Antarctic McMurdo's Sediment Pesticide and PCB Data



                      INVEST#:                 PD-9-92 -15-             PD-21-92 -23-             PD-31-92 -4-
                      ID:
                      LABSAMNO:                         J1942                     J1949                   J1956
                      UNIT.                             ng/g                      ng/g                     ng/g
                      Analyte (Cont)                    Conc DB QUAL              Conc DB QUAL             Com DB QUAL


                      SAMPLE TWE:                       SAMP                      SAMP                    SAMP
                      COLLECTION DATE:
                      RECEIPT DATE:
                      QCBATCH:                          JP042                     JP042               JP045
                      EXTRACTION DATE:         08/01/92                 08/01/92                   09/01/92
                      METHOD:                           GCFID                     GCFID                  GCFID
                      ANALYSIS DATE:
                      METHOD:                           GCMS                      GCMS                    GCMS
                      ANALYSIS DATE:           08/18/92                 08/18/92                   09/24/92
                      METHOD:                        GCECD                     G-CECD                   GCECD
                      ANALYSIS DATE:               08/02/93                  08/02/93                 08/02/93
                      MATRIX:-                          SED                       SED                      SED
                      SUBMAT:
                      SAMPLWT:
                      VIETWT:                           26.7                      17.9                     15.2
                      DRYWT:                            10.35                     10.14                   10.11
                      WI@S:                         GRAMS DRY                 GRAMS DRY                 GRAMS DRY
                      PCTSOLIDS:
                      VOL:
                      VOLUNITS:                       Ln`ERS                    LITERS                  Ln`ERS


                      TOTAL BHC'S                       0.17 J                    0.20 J                   0.13 J
                      TOTALCHLORDANES                   0.10 1                    0.07 J                   0.06 J
                      TOTAL DDTS                        0.71 J                    0.76 J                   0.46 J
                      TOTAL PCB'S                        1.9 1                     2.8 J                    3.9 J


                      ALPHA-BHC                         0.00 ND                   0.00 ND                  0.00 ND
                      HCB                               0.34 J                    0.19 1                   0.00 ND
                      BETA-BHC                          0.00 ND                   0.00 ND                  0.00 ND
                      GAMMA-BHC                         0.17 J                    0.20 J                   0.13 J
                      DELTA-BHC                         0.00 ND                   0.00 ND                  0.00 ND
                      HEPTACHLOR                        0.10 1                    0.00 ND                  0.00 ND
                      HEPTA-EPOXIDE                     0.00 ND                   0.00 ND                  0.00 ND
                      OXYCHLORDANE                      0.00 ND                   0.00 ND                  0.00 ND
                      GAMMA-CHLORDANE                   0.00 ND                   0.07 J                   O.GO ND
                      ALPHA-CHLORDANE                   0.00 ND                   0.00 ND                  0.00 ND
                      TRANS-NONACHLOR                   0.00 ND                   0.00 ND                  0.06 J
                      CIS-NONACHLOR                     0.00 ND                   0.00 ND                  0.00 ND
                      ALDRIN                            0.00 ND                   0.00 ND                  0.05 1
                      DIELDRIN                          0.00 ND                   0.00 ND                  0.00 ND
                      ENDRIN                            0.00 ND                   0.00 ND                  0.00 ND
                      MIREX                             0.00 ND                   0.00 ND                  0.00 ND
                      2,41)DE (0,P'DDE)                 0.00 ND                   0.00 ND                  0.00 ND
                      4,41)DE (P,P'DDE)                 0.22 J                    0.00 ND                  0.00 ND
                      2,41)DD (0,P'DDD)                 0.00 ND                   0.00 ND                  0.00 ND
                      4,4'DDD (P.P'DDD)                 0.00 ND                   0.00 ND                  0.00 ND
                      2,4'DDT (O,P'DDT)                 0.00 ND                   0.00 ND                  0.00 ND
                      4,4'DDrr (P,P'DEM                 0.49 J                    0.76 J                   0.46 J




                                                                        281







                                        Antarctic McMurdo's Sediment Pesticide and PCB Data



                       INVEST#:                  PD-9-92 -15-                PD-21-92 -23-               PD-31-92 -4-
                       ID:
                       LABSAMNO:                         J 1942                       J1949                      J1956
                       UNIT:                               ng/g                        ng/g                       ng/g
                       Analyte (Cont)                      Conc DB QUAL                Conc DB QUAL               Conc DB QUAL

                       PCB # (CLORINATION)


                       8 (CL2)                             5.57  M                     0.00   M                   0.17   J
                       18 (CL3)                            0.00  ND                    0.01   1                   0.01   j
                       28 (CL3)                            0.00  ND                    0.00   ND                  0.03   J
                       44 (CIA)                            0.00  ND                    0.00   ND                  0.13   J
                       52 (CIA)                            0.00  ND                    0.06   J                   0.23   J
                       66 (CIA)                            0.00  ND                    0.00   ND                  0.00   ND
                       101 (CL5)                           0.16  J                     0.00   ND                  0.39   J
                       105 (CL5)                           0.00  ND                    0.00   ND                  0.00   ND
                       110/77 (CL5/4)                      0.00  ND                    0.00   ND                  0.00   ND
                       118/108/149(CL5/5/6)                0.00  ND                    0.00   ND                  0.22   J
                       128 (CL6)                           0.00  ND                    0.00   ND                  0.04   J
                       138 (CL66)                          0.10  j                     0.15   J                   0.21   J
                       126 (CL5)                                 NA                           NA                         NA
                       153 (CL6)                           0.00  ND                    0.00   ND                  0.23   J
                       170 (CL7)                           1.77  M                     0.00   M                   0.00   M
                       180 (CL7)                           0.00  ND                    0.00   ND                  0.08   J
                       187/182/159(CL7/7/6)                0.00  ND                    0.00   ND                  0.07   J
                       195 (CL8)                           0.00  ND                    0.00   ND                  0.00   ND
                       206 (CL9)                           0.00  ND                    0.00   ND                  0.00   ND
                       209 (CLIO)                          0.00  ND                    0.00   ND                  0.00   ND

                       SurTogate Recoveries
                       DBOFB%:                            107.0                        125.2                     128.1
                       PCB#103%:                           84.4                        99.5                      108.7
                       PCB# 1980/o:                        73.9                        116.0                     118.7


                       PCB #(CHLORINATION)


                       7 (CL2)                             0.17  J                     0.20   J                   0.09   j
                       15 (CL2)                            0.00  ND                    0.23   J                   0.00   ND
                       24 (CL3)                            0.00  ND                    0.02   J                   0.02   J
                       16/32 (CL3)                         0.00  ND                    0.00   ND                  0.00   ND
                       29 (CI-3)                           0.00  ND                    0.00   ND                  0.00   ND
                       26 (CL3)                            0.00  ND                    0.00   ND                  0.03   J
                       25 (CL3)                            0.09  1                     0.00   ND                  0.09   1
                       50 (CIA)                            0.59  J                     0.06   J                   0.12   J
                       31 (CL3)                            0.00  ND                    0.00   ND                  0.00   ND
                       33 (CL3)                            0.00  ND                    0.00   ND                  0.00   ND
                       22 (CL3)                            0.00  ND                    0.00   ND                  0.00   ND
                       45 (CIA)                            0.00  ND                    0.02   J                   0.00   ND
                       46 (CIA)                            0.00  ND                    0.06   J                   0.00   ND
                       49 (CIA)                            0.10  1                     0.00   ND                  0.15   J
                       47/48 (CIA)                         0.80  J                     1.07                       0.79   J
                       37/42 (CIA)                         0.00  ND                    0.00   ND                  0.00   ND
                       41/64 (CIA)                         0.00  ND                    0.00   ND                  0.00   ND
                       40 (CIA)                            0.00  ND                    0.00   ND                  0.00   ND
                       100 (CL5)                           0.00  ND                    0.00   ND                  0.00   ND



                                                                           282







                                      An&,wctic McMurdo's Sediment Pesticide and PCB Data



                      INVEST#:                 PD-9-92 -15-            PD-21-92 -23-             PD-131-92 -4-
                      ID:
                      LABSAMNO:                       J1942                     J1949                    J19,96
                      UNIT:                            ng/g                      ng/g                    ng/g
                      Analyte (Cont)                   Conc DB QUAL              Conc DB QUAL            Com DB QUAL

                      74 (CIA)                         0.22 J                    0.00 ND                 0.00 ND


                      PCB #(CHLORINATION)


                      70 (CIA)                         0.00 ND                   0.00 ND                 0.08  J
                      88 (CL5)                         0.00 ND                   0.00 ND                 0.04  J
                      60/56 (CL5)                      0.00 ND                   0.00 ND                 0.00  ND
                      92? (CL5)                        0.00 ND                   0.00 ND                 0.00  ND
                      84? (CL5)                        0.28 J                    0.49 J                  0.32  J
                      99 (CL5)                         0.00 ND                   0.00 ND                 0.11  1
                      83 (CIZ)                         0.31 J                    0.19 j                  0.00  ND
                      97 (CIZ)                         0.23 J                    0.00 ND                 0.14  J
                      87 (CL5)                         0.00 ND                   0.00 ND                 0.00  ND
                      85 (CIZ)                         0.00 ND                   0.00 ND                 0.00  ND
                      136 (CL6)                        0.00 ND                   0.00 ND                 0.00  ND
                      82 (CL5)                         0.00 ND                   0.00 ND                 0.00  ND
                      151 (CL6)                        0.00 ND                   0.00 ND                 0.00  ND
                      107/108/144(CL,5/5/6)            0.00 ND                   0.00 ND                 0.00  ND
                      149 (CL6)                        0.00 ND                   0.00 ND                 0.15  1
                      188 (CL7)                        0.00 ND                   0.00 ND                 0.00  ND
                      146 (CL6)                        0.00 ND                   0.00 ND                 0.00  ND
                      141 (CL6)                        0.00 ND                   0.00 ND                 0.02  J
                      137 (CL6)                        0.00 ND                   0.00 ND                 0.00  ND
                      UNK (CL6)                        0.00 ND                   0.07 J                  0.00  ND
                      158 (CL7)                        0.00 ND                   0.05 j                  0.00  ND
                      129 (CL6)                        0.00 ND                   0.00 ND                 0.00  ND
                      178 (CL7)                        0.00 ND                   0.00 ND                 0.00  ND
                      183 (CL7)                        0.00 ND                   0.00 ND                 0.00  ND
                      167 (CL6)                        0.00 ND                   0.00 ND                 0.00  ND
                      185 (CL7)                        0.00 ND                   0.00 ND                 0.00  ND
                      174 (CL7)                        0.40 J                    0.00 ND                 0.01  1
                      177 (CL7)                        0.00 ND                   0.00 ND                 0.00  ND
                      156/171/202(CL6/7/8)             0.00 ND                   0.00 ND                 0.00  ND
                      200 (CL8)                        0.05 J                    0.00 ND                 0.00  ND
                      172 (CL7)                        0.13 J                    0.00 ND                 0.12  J
                      191 (CL7)                        0.00 ND                   0.08 J                  0.14  J
                      201 (CL8)                        0.00 ND                   0.00 ND                 0.00  ND
                      196 (CLB)                        0.00 ND                   0.00 ND                 0.00  ND
                      189 (CL7)                        0.00 ND                   0.00 ND                 0.00  ND
                      194 (CL8)                        0.00 ND                   0.09 1                  0.00  ND
                      205 (CL9)                        0.00 ND                   0.00 ND                 0.00  ND












                                                                       283




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                                                                Antarctic McMurdo's Sediments Metal Data


           INVEST#:               BERNACCHIBAY                  BAY OF SAILS                      WQB                  OLJTFALL              CAPE ARMITAGE
           ID:                                  100,                       100,                      60'                      30'                            60'
           LABSAMNO:                            J2034                      J2037                  J2042                     J2049                         J2056

           SAMPLE TYPE:                         SAMP                       SAMP                   SAMP                      SAMP                          SAMP
           COLLEC'nON DATE:               01/09/91                    12/21/90                12/10/90                 11/30/90                       12/14/90
           MATRIX:                       SEDIMENT                    SEDIMENT                SEDIMENT                SEDIMENT                        SEDIMENT
           ADGDAT                 03/18/93                      03/18/93                   11/29/93                 11/29/93                11/29/93
           HGDGDAT                03/25/93                      03/25/93                   12/09/93
           OTHDGDAT               04/06/93                      04/06/93                                NA                       NA                             NA
           Add Digest Wt:                       0.199                      0.208                  0.209                     0.210                         0.207
           Hg Digest Wt                         0.195                      0.194                  0.192                     0.212                         0.193
           NAA Digest Wt                        0.494                      0.498                        NA                       NA                             NA
           v*rIUNITS:                       GRAMS DRY                  GRAMS DRY                GRAMS DRY               GRAMS DRY                       GRAMS DRY

                                                Conc DB QUAL               Conc DB QUAL           Conc DB QUAL              Conc DB QUAL                  Conc DB QUAL
           UNIT-                                (ppm)                      (ppm)                  (ppm)                     (ppm)                         (ppm)

           Al                                   78613                      75917                  80864                     81619                         88983
           Ag                                   0.133                      0.172                  0.628                     1.027                         0.150
       oo  As                                   5.4                        3.2                      7.9                     11.0                            4.8
       U1  Cd                                   0.16                       0.10                   1.439                     1.029                         0.405
           Cr                                   166                        155                      160                     154                             204
           CU                                   17.1                       14.0                   92.6                      120.0                         22.7
           Fe                                   50128                      48046                  63225                     87134                         39999
           Hg                                   0.014J                     0.014J                 0.103                     0.165                         0.036 J
           Mn                                   922                        921                    1307                      1386                          1240
           N1                                   64.4                       55.7                   72.7                      77.3                          106.2
           Pb                                   9.00                       9.56                     64.9                    55.2                            11.2
           Sb                                   0.26 J                     0.00 ND                  5.56                    3.27                            0.51 J
           Se                                   0.20 J                     0.17 J                   0.39 J                  0.28 J                          0.28 J
           Sn                                   1.68                       1.73                     6.98                    25.1                            2.16
           Zn                                   79.1                       79.8                   164.0                     171.0                         98.0







                                                                     Antarctic McMurdo's Sediments Metal Data



                                  INVEST#:                    OUfFALL                   OUTFALL                        WQB                        WQB
                                  ID:                                30'                       60'                        30'                       60'
                                  LABSAMNO:                        J2057                     J2058                     J2062                      J2063


                                  SAMPLE TYPE:                     SAMP                      SAMP                      SAMP                       SAMP
                                  COLLECTION DATE: 12/13/91                             12/12/91                  12/11/91                   12/11/91
                                  MATRIX                    SEDIMENT                  SEDIMENT                   SEDIMENT                  SEDIMENT
                                  ADGDAT                  03/18/93                  03/18/93                  03/18/93                   03/18/93
                                  HGDGDAT                 03/25/93                  03/25/93                  03/25/93                   03/25/93
                                  OTHDGDAT                04/06/93                  04/06/93                  04/06/93                   04/06/93
                                  Acid Digest Wt-                  0.202                     0.195                     0.196                      0.210
                                  Hg Digest Wt                     0.207                     0.199                     0.192                      0.197
                                  NAA Digest Wt                    0.502                     0.503                     0.500                      0.506
                                  VWTUNITS:                    GRAMS DRY                 GRAMS DRY                  GRAMS DRY                 GRAMS DRY


                                                                   Conc DB QUAL              Conc DB QUAL              Conc DB QUAL               Conc DB QUAL
                                  UNIT:                            (ppm)                     (ppm)                     (ppm)                      (ppm)

                                  Al                               78512                     76750                     76216                      79013
                                  Ag                               0.228                     1.27                      0.695                      0.212
                                  As                                 4.1                       6.2                       8.0                        3.0
         00                       Cd                               0.35                      1.51                      0.94                       0.28
         M                        Cr                               240                        185                        176                      252
                                  CU                               48.1                      62.4                      102.2                      35.1
                                  Fe                               70257                     73566                     71469                      81498
                                  Hg                               0.117                     0.107                     0.095                      0.031 J
                                  Mn                               1398                      1400                      1241                       1411
                                  Ni                               84.6                      69.0                      rag. 4                     71.1
                                  Pb                               19.1                      38.8                      89.6                       12.6
                                  Sb                               0.81                      4.81                      7.31                       0.90
                                  Se                               0.02  J                   0.24  J                   0.27  J                    0.00  ND
                                  Sn                               4.50                      9.60                      12.3                       3.00
                                  Zn                               1214.4                    150.2                     210.0                      123.5







                                                                 Antarctic McMurdo's Sediments Metal Data



                                          INVEST`#:              PD-9-92 -15-             PD-21-92 -23-              PD-31-92 -4-
                                          ID:
                                          LABSAMNO:                       J1942                     J1949                      J1956


                                          SAMPLE TYPE:                    SAMP                      SAMP                       SAMP
                                          COLLECTION DATE:
                                          MATRIX:                         SED                       SED                        SED
                                          ADGDAT                 03/18/93                 03/18/93                   03/18/93
                                          HGDGDAT                03/25/93                 03/25/93                   03/25/93
                                          OTHDGDAT               04/06/93                 04/06/93                   04/06/93
                                          Acid Digest Wt:                 0.195                     0.207                      0.208
                                          Hg Digest Wt                    0.199                     0.193                      0.196
                                          NAA Digest Wt                   0.501                     0.489                      0.506
                                          VVTUNrI`S:                  GRAMS DRY                 GRAMS DRY                 GRAMS DRY


                                                                          Conc DB QUAL              Conc DB QUAL               Conc DB QUAL
                                          UNIT:                           (ppm)                     (ppm)                      (ppm)


                                          Al                              71254                     73726                      77194
                                          Ag                              0.164                     0.132                      0.139
                                          As                              4.5                       4.1                        4.7
        00                                Cd                              0.10                      0.05                       0.06
         4                                Cr                              38                          46                       51
                                          CU                              19.4                      16.1                       25.5
                                          Fe                              28302                     30884                      34679
                                          Hg                              0.021J                    0.016J                     0.017J
                                          Mn                              605                       608                        789
                                          Ni                              15.3                      17.1                       18.1
                                          Pb                              7.48                      7.07                       7.92
                                          Sb                              0.53                      0.33 J                     0.39
                                          Se                              0.43J                     0.27 J                     0.27J
                                          Sn                              0.83                      0.87                       0.93
                                          Zn                              56.9                      54.6                       63.3



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          Palmer Fish Aromatic Hydrocarbon Data
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a                          288






                                                 Antarctic Palmer Fish Samples Aromatic Hydrocarbon Data


                   INVEST#:              C.NEGLECTA                CORIICEPS                C.ACERATUS               N. GIBBERIFRONS
                   ID:                   LOWE ISLAND               LOATE ISLAND             LOW ISLAND               DALLMAN BAY
                   LkBSAMNO-.            32013                     J2014                    J2015                    J2016
                   UNrr:                 ng/g                      ng/g                     ng/g                     ng/g
                   PNA Analyte           Cone           DB QUAL, Cone             DB QUAL Cone             DB QUAL Cone                  DB QUAL,

                   INVEST#:              C.NEGLECTA                CORIICEPS                C. ACERATIJS             N. GIBBERIFRONS
                   ID:                   LOWE ISLAND               LOWE ISLAND              LOWE ISLAND              DALLMAN BAY
                   LABSAMNO:             J2013                     J2014                    J2015                    J2016
                   SAMPLE TYPE:          SAMP                      SAMP                     SAMP                     SAMP
                   COLLECTION DATE:      03/28/92                  03/28/92                 03128/92                 04/05/92
                   RECEIPT DATE:
                   QCBATCH:              M827                      M778                     M778                     M778
                   EXTRACTION DATE:      04/26/93
                   ME'n-IOD:             GCFID                     GCFID                    GCFID                    GCFID
                   ANALYSIS DATE:
                   MEMOD:                GCMS                      GCMS                     GCMS                     GCMS,
                   ANALYSIS DATE:        05/24/93                  03/03/93                 03/03/93                 03/03/93
                   METHOD:               GCECD                     GCECD                    GCECD                    GCECD
                   ANALYSIS DATE:        06102/93                  03/15/93                 03/15/93                 03/15/93
     w             MATRIX:               TISSUE                    TISSUE                   TISSUE                   TISSUE
     00            SUBMAT:               MUSCLE                    LIVER                    LIVER                    LIVER
     CD
                   SAMPLWT:
                   VJETWT:               5.184                     0.727                    0.517                    0.657
                   DRYWT:                1.26                      0.20                     0.14                     0.25
                   V*7UNITS:             GRAMS          DRY        GRAMS          DRY       GRAMS          DRY       GRAMS               DRY
                   PCTSOLIDS:
                   VOL:
                   VOLUNI'TS:            LITERS                    LITERS                   LITERS                   LITERS


                   NAPHITIALENE          23.52                     53.83          B         85.12          B         70.01               B
                   CI-NAPHTHALENES       27.63                     58.61          B         153.43         B         86.35               B
                   C2-NAPHTHALENES       14.72          1          0              ND        0              ND        0                   ND
                   C3-NAPHTHALENES       24.69                     0              ND        0              ND        0                   ND
                   C4-NAPHTHALENES       0              ND         0              ND        0              ND        0                   ND
                   BIPHENYL              5.63           1          38.32          1         71.52                    27.60
                   ACENAPHTMLENE         0.84           1          6.23           1         10.83          1         27.79
                   ACENAPHTHENE          3.25           1          11.07          1         29.98          1         20.95
                   FLUORENE              3.37           1          9.39           1         15.93          1         25.24
                   CI-FLUORENES          0              ND         0              ND        0              ND        0                   ND






                                                  Antarctic Palmer FIsh Samples Aromatic Hydrocarbon Data


                    INVEST#:               C. NEGLECTA               CORIICEPS                 C.ACERATUS                N. GIBBERIFRONS
                    ID:                    LOWE ISLAND               LOWE ISLAND               LOWE ISLAND               DALLMAN BAY
                    IABSAMNO:              J2013                     J2014                     J2015                     J2016
                    UNIT-                  ng/g                      ng/g                      ng/g                      ng/g
                    PNA Analyte            Cone           DB QUAL Cone              DB QUAL Cone              DB QUAL Cone                   DB QUAL

                    C2-FLUORENES           0              ND         0              ND         0              ND         0                   ND
                    C3-FLUORENES           0              ND         0              ND         0              ND         0                   ND
                    PHENANTHRENE           2.95           1          17.36          1          20.23          1          25.19
                    ANTHRACENE             0.92           1          9.65           1          20.39          1          23.06
                    Cl-PHEN-ANTHR          0              ND         0              ND         0              ND         0                   ND
                    C2-PHEN-ANTUR          0              ND         0              ND         0              ND         0                   ND
                    U-PHEN-ANTHR           0              ND         0              ND         0              ND         0                   ND
                    C4-PHEN-ANTHR          0              ND         0              ND         0              ND         0                   ND
                    DIBENZOTHIO            1.25           1          6.34           1          12.22          1          17.18               1
                    CI-DIBEN               0              ND         0              ND         0              ND         0                   ND
                    C2-DIBEN               0              ND         0              ND         0              ND         0                   ND
                    C3-DIBEN               0              ND         0              ND         0              ND         0                   ND
                    FLUORANTHENE           1.82           1          6.56           1          14.66          1          19.50
                    PYRENE                 2.20           1          17.33          1          16.68          1          18.10
                    CI-FLUORAN-PYR         0              ND         0              ND         0              ND         0                   ND
      0             BENaANTHRACENE         0.58           1          2.15           1          5.25           1          10.26
                    CHRYSENE               0.62           1          2.93           1          11.59          1          15.49               1
                    CI-CHRYSENES           0              ND         0              ND         0              ND         0                   ND
                    C2-CHRYSENES           0              ND         0              ND         0              ND         0                   ND
                    C3-CHRYSENES           0              ND         0              ND         0              ND         0                   ND
                    C4-CHRYSENES           0              ND         0              ND         0              ND         0                   ND
                    BENbFLUORAN            0.47           1          4.18           1          8.92           1          11.26               1
                    BENkFLUORAN            0.47           1          2.57           j          6.45           1          9.75                1
                    BENePYRENE             0.50           1          5.40           1          4.17           1          13.04               1
                    BENaPYRENE             0.41           1          2.39           1          8.03           1          12.44               1
                    PERYLENE               0.39           1          4.53           1          9.06           1          16.88               1
                    1123edPYRENE           0.26           1          7.60           1          12.09          1          7.97
                    DBahANTHRA             0.37           1          3.96           1          10.21          1          5.66
                    BghIPERYLENE           0.46           1          12.09          1          20.55          1          1.1.n')

                    TOTAL PAH's            116.9                     278.0                     538.3                     459.9
                      (W/O PERYLENE)
                    2-M=1 MELIiAPH         17.70                     32.77          j          65.99                     38.35               j
                    I-METHYLNAPH           9.93                      25.84          1          87.44                     48.00






                                                Antarctic Palmer Fish Samples Aromatic Hydrocarbon Data


                   INVEST#:               C.NEGLECTA                CORIICEPS                C.ACERATUS                N. GIBBERIFRONS
                   ID:                    LOWE ISLAND               LOWE ISLAND              LOWE ISLAND               DALLNM BAY
                   LABSAMNO:              J2013                     J2014                    J2015                     J2016
                   UNM                    ng/g                      ng/g                     ng/g                      ng/g
                   PNA Analyte            Cone           DB QUAL Cone              DB QUAL Cone              DB QUAL Cone                  DB QUAL,


                   2.6-DIMETHNAPH         5.96           1          16.57          1         36.09           1         22.66


                   2.3.5-TRIMETHNAPH      5.41           1          12.59          1         21.54           1         18.11


                   I-METHYLPHEN           0.66           1          9.39           1         17.60           1         28.54


                   Surrogate Recoveries
                   NAPHD8:                47.6                      56.6                     41.8                      46.7
                   ACENDIO:               59.2                      58.9                     44.9                      49.2
                   PHENDIO:               74.6                      58.0                     49.1                      54.9
                   CHRYD12:               76.5                      55.0                     47.3                      55.3
                   PERYD12:               40.9                      60.1                     52.3                      58.2






                                                   Antarctic Palmer Fish Samples Aromatic Hydrocarbon Data


                INVEST#:                N. GIBBERIFRONS               CORIICEPS                    CORIICEPS                    CORIICEPS
                ID:                     DALLMAN BAY                   BAHIA PARAISO                BAHIA PARAISO                PALMER STATION
                LABSAMNO:               J2017                         J2018                        J2019                        J2020
                UNIT:                   ng/g                          ng/g                         ng/g                         ng/g
                PNA Analyte             Conc               DB QUAL Conc                 DB QUAL Conc                  DB QUAL Conc                  DB QUAL

                INVEST#:                N. GIBBERIFRONS               CORIICEPS                    CORIICEPS                    CORIICEPS
                ID:                     DALLMAN BAY                   BAHIA PARAISO                BAHIA PARAISO                PALMER STATION
                LABSAMNO:               J2017                         J2018                        J2019                        J2020
                SAMPLE 7YPE:            SAMP                          SAMP                         SAMP                         SAMP
                COLLECTION DATE:        04/05/92                      04/22/92                     04/22/92                     03/29/92
                RECEIPT DATE:
                QCBATCH:                M827                          M778                         M827                         M778
                EXTRACTION DATE:        04/26/93                                                   04/26/93
                METHOD:                 GCFID                         GCFID                        GCFID                        GCFID
                ANALYSIS DATE:
                METHOD:                 GCMS                          GCMS                         GCMS                         GCMS
                ANALYSIS DATE:          05/24/93                      03/03/93                     05/24/93                     03/03/93
                METHOD,                 GCECD                         GCECD                        GCECD                        GCECD
                ANALYSIS DATE:          06/02/93                      03/15/93                     06/02/93                     03/15/93
      K)        MATRIX:                 TISSUE                        TISSUE                       TISSUE                       TISSUE
      (D
      w         SUBMAT.-                MUSCLE                        LIVER                        MUSCLE                       LIVER
                SAMPLWT.,
                WETWT:                  5.034                         0.514                        5.196                        0.501
                DRYWT.                  1.06                          0.17                         1.17                         0.18
                ViTUNITS:               GRAMS              DRY        GRAMS             DRY        GRAMS              DRY       GRAMS                DRY
                PCTSOLIDS:
                VOL:
                VOLUNITS:               LITERS                        LITERS                       LITERS                       LITERS


                NAPHTHALENE             15.82                         76.65                        18.89                        120.45
                CI-NAPHTHALENES         12.72                         99.16                        22.04                        204.69
                C2-NAPHTHALENES         0.00               ND         0                 ND         0.00               ND        0                     ND
                C3-NAPHTHALENES         0                  ND         0                 ND         0                  ND        0                     ND
                C4-NAPHTHALENES         0                  ND         0                 ND         0                  ND        0                     ND
                BIPHENYL                5.53                          61.68                        5.84               j         54-30
                ACENAPHTHYLENE          0.90                          18.71             1          0.55                         5.55
                ACENAPHTHENE            2.11                          32.59             1          1.48                         16.29
                                                                                                                                                     T
                FLUOREENE               i. 6 C-                       9.6!               T         ri. ILI I          T          7. 9
                C I -FLUORENES          0                  ND         0                 ND         0                  ND        0                     ND






                                                     Antarctic Palmer Fish Samples Aromatic Hydrocarbon Data


                 INVEST#:                N. GIBBERIFRONS                CORUCEPS                       CORIICEPS                     CORIICEPS
                 ID:                     DALLMAN BAY                    BAHIA PARAISO                  BAHIA PARAISO                 PALMER STA77ON
                 LABSAMNO:               J2017                          J2018                          J2019                         J2020
                 UNIT-                   ng/g                           ng/g                           ng/g                          ng/g
                 PNA Analyte             Conc                DB QUAL Conc                  DB QUAL Conc                  DB QUAL Conc                     DB QUAL

                 C2-FLUORENES,           0                   ND         0                  ND          0                 ND          0                    ND
                 C3-FLUORENES            0                   ND         0                  ND          0                 ND          0                    ND
                 PHENANTHRENE            3.41                1          24.08              1           3.40              1           23.19                1
                 ANT`HRACENE             0.58                1          22.13              1           1.15              1           12.99                1
                 CI-PHEN  -ANTHR         0                   ND         0                  ND          0                 ND          0                    ND
                 C2-PHEN  -ANTHR         0                   ND         0                  ND          0                 ND          0                    ND
                 C3-PHEN   ANTHR         0                   ND         0                  ND          0                 ND          0                    ND
                 C4-PHEN  -ANTHR         0                   ND         0                  ND          0                 ND          0                    ND
                 DIBENZOTHIO             1.14                1          21.28              1           1.05              1           9.40                 1
                 CI-DIBEN                0                   ND         0                  ND          0                 ND          0                    ND
                 C2-DIBEN                0                   ND         0                  ND          0                 ND          0                    ND
                 C3-DIBEN                0                   ND         0                  ND          0                 ND          0                    ND
                 FLUORANTHENE            1.69                j          6.17               j           1.11              1           12.51                1
                 PYRENE                  2.12                j          25.64              1           1.67              1           9.94                 1
                 C I -FLUORAN   PYR      0                   ND         0                  ND          0                 ND          0                    ND
       CD        BENaANTHRACENE          0.58                1          3.56               1           0.54              j           2.98                 1
       Co        CHRYSENE                0.57                1          4.98               1           0.52              1           8.04                 1
                 CI-CHRYSENES            0                   ND         0                  ND          0                 ND          0                    ND
                 C2-CHRYSENES            0                   ND         0                  ND          0                 ND          0                    ND
                 C3-CHRYSENES            0                   ND         0                  ND          0                 ND          0                    ND
                 C4-CHRYSENES            0                   ND         0                  ND          0                 ND          0                    ND
                 BENbFLUORAN             0.52                1          4.72               1           0.45              1           4.78                 1
                 BENkFLUORAN             0.52                1          3.27               j           0.45              1           4.78                 j
                 BENePYRENE              0.78                1          6.27               1           0.55              1           1.61
                 BENaPYRENE              0.67                1          5.17               1           0.45              j           21.18
                 PERYLENE                0.21                1          8.81               1           0.46              1           2.11
                 1123cdPYRENE            0.34                1          10.87              1           0.39              1           8.39
                 DBahANTHRA              0.48                1          8.57               j           0.27              1           4.56                 j
                 BghIPERYLENE            0.61                1          12.51              1           0.16              1           12.20                j

                 TOTAL PAH's             52.8                           457.6                          63.6                          555.8
                   (WIO PERYLENE)
                 2-METHYLNAPH            8.21                1          49.32              1           12.77                         129.62
                 I-METHYLNAPH            4.51                1          49.84              1           9.27              1           75.07






                                                      Antarctic Palmer Fish Samples Aromatic Hydrocarbon Data


                 INVEST#:                 N. GIBBERIFRONS                 CORIICEPS                      CORIICEPS                      CORIICEPS
                 ID:                      DALLMAN BAY                     BAHIA PARAISO                  BAHIA PARAISO                  PALMER STATION
                 LABSAMNO:                J2017                           J2018                          J2019                          J2020
                 UNIT:                    ng/g                            ng/g                           ng/g                           ng/g
                 PNA Analyte              Conc                 DB QUAL Conc                  DB QUAL Conc                   DB QUAL Conc                  DB QUAL


                 2.6-DIME'n-INAPH         3.22                 1          39.37              1           5.23               1           29.35


                 2,3,5-TRIMETHNAPH        1.71                 1          19.81              1           1.70               1           13.82


                 I-METHYLPHEN             0.75                 1          9.77               1           0.47               1           7.75

                 Surrogate Recoveries
                 NAPHD8:                  57.3                            52.7                           47.1                           45.0
                 ACEND10:                 60.4                            54.5                           59.1                           48.2
                 PHENDIO:                 71.6                            57.6                           72.4                           52.9
                 CHRYD12:                 68.9                            56.3                           72.3                           53.6
                 PERYD12-                 49.0                            48.9                           45.7                           51.2



       CD
       )4-






                                                       Antarctic Palmer Fish Samples Aromatic Hydrocarbon Data


                  INVEST#:                 CORIICEPS                        CORIICEPS                     PROC BLANK                     COR11CEPS
                  ID:                      PALMER STATION                   LAB QA SAMPLE                 LAB QA SAMPLE                  LAB QA SAMPLE
                  LABSAMNO:                J2021                            Q4609                         Q4610                          Q4611
                  UNIT:                    ng/g                             ng/g                          ng/g                           %
                  ,PNA Analyte             Conc                 DB QUAL Conc                   D13 QUAL Conc                 DB QUAL % Recov                DB QUAL

                  INVEST#:                 CORIICEPS                        CORIICEPS                     PROC BLANK                     CORIICEPS
                  ID:                      PALMER STATION                   LAB QA SAMPLE                 LAB QA SAMPLE                  LAB QA SAMPLE
                  LABSAMNO:                J2021                            Q4609                         Q4610                          Q4611
                  SAMPLETYPE:              SAMP                             DUPE OF J2013                 PROC BLANK                     MS OF J2013
                  COLLECTION DATE:         03/29/92                         03/28/92                                                     03/28/92
                  RECEIPT DATE:
                  QCBATCH:                 M827                             M778                          M778                           M778
                  EXTRACTION DATE:         04/26/93
                  METHOD:                  GCFID                            GCFID                         GCFID                          GCFID
                  ANALYSIS DATE:
                  METHOD:                  GCMS                             GCMS                          GCMS                           GCMS
                  ANALYSIS DATE:           05/24/93                         03/03/93                      03/03/93                       03/03/93
                  METHOD:                  GCECD                            GCECD                         GCECD                          GCECD
        I-j       ANALYSIS DATE:           06/02/93                         03/15/93                      03/15/93                       03/15/93
        rD        MATRIX:                  TISSUE                           TISSUE                        TISSUE                         TISSUE
        (-n       SUBMAT.                  MUSCLE                           MUSCLE                                                       MUSCLE
                  SAMPLWT:
                  V&-INW.                  5.044                            0.668                                                        0.551
                  DRYWT:                   1.28                             0.18                          10.00                          0.13
                  WTUNITS:                 GRAMS                DRY         GRAMS              DRY        GRAMS              DRY         GRAMS              DRY
                  PCTSOLIDS:
                  VOL.
                  VOLUNrI7S:               LITERS                           LITERS                        LITERS                         LITERS


                  NAPHTHALENE              21.05                            69.00                         1.95                           82.30
                  CI-NAPHTHALENES          31.23                            116.02                        1.91                                              NA
                  C2-NAPHTHALENES          14.56                1           0                  ND         0                  ND                             NA
                  C3-NAPHTHALENES          0                    ND          0                  ND         0                  ND                             NA
                  C4-NAPHTHALENES          0                    ND          0                  ND         0                  ND                             NA
                  BIPHENYL                 0.00                 ND          55.73                         0.68               1           75.3
                  ACENAPHTHYLENE           0.44                 j           26.61              1          0.60               1           92.0
                  ACENAPHTHENE             0.94                 1           23.07              j          0.79               1           86.1
                  FLUORENE                 2.06                 1           24.57              1          0.42               1           83.6
                  CI-FLUORENES             0                    ND          0                  ND         0                  ND                             NA






                                                   Antarctic Palmer Fish Samples Aromatic Hydrocarbon Data


                INVEST#*                CORIICEPS                       CORIICEPS                    PROC BLANK                    CORIICEPS
                ID:                     PALMER STATION                  LAB QA SAMPLE                LAB QA SAMPLE                 LAB QA SAMPLE
                LABSAMNO:               J2021                           Q4609                        Q4610                         Q4611
                UNIT-                   ng/g                            ng/g                         ng/g                          %
                PNA Analyte             Conc                 DB QUAL Conc                 DB QUAL Conc                  DB QUAL % Recov               DB QUALI
                C2-FLUORENES            0                    ND         0                 ND         0                  ND                            NA
                C3-FLUORENES            0                    ND         0                 ND         0                  ND                            NA
                PHENANTHRENE            2.93                 1          29.21             1          0.60               1          81.7
                ANTHRACENE              0.68                 1          17.94             1          0.43               1          71.2
                CI-PHEN  -ANTHR         0                    ND         0                 ND         0                  ND                            NA
                C2-PHEN  -ANTUR         0                    ND         0                 ND         0                  ND                            NA
                C3-PHEN  -ANTHR         0                    ND         0                 ND         0                  ND                            NA
                C4-PHEN  -ANTHR         0                    ND         0                 ND         0                  ND                            NA
                DIBENZOTHIO             0.79                 1          23.41             1          0.36               1          60.9
                CI-DIBEN                0                    ND         0                 ND         0                  ND                            NA
                C2-DIBEN                0                    ND         0                 ND         0                  ND                            NA
                C3-DIBEN                0                    ND         0                 ND         0                  ND                            NA
                FLUORANTHENE            2.07                 1          26.46             1          0.33               1          95.5
                PYRENE                  2.04                 1          22.79             1          0.57               1          96.9
                CI-FLUORAN-PYR          0                    ND         0                 ND         0                  ND                            NA
                BENaANTHRACENE          0.81                 1          9.59              1          0.17               1          90.8
                CHRYSENE                1.06                 1          14.78             1          0.23               j          96.5
                CI-CHRYSENES            0                    ND         0                 ND         0                  ND                            NA
                C2-CHRYSENES            0                    ND         0                 ND         0                  ND                            NA
                C3-CHRYSENES            0                    ND         0                 ND         0                  ND                            NA
                C4-CHRYSENES            0                    ND         0                 ND         0                  ND                            NA
                BENbFLUORAN             0.42                 1          13.93             1          0.22               1          104.8
                BENkFLUORAN             0.42                 1          13.93             1          0.20               1          104.8
                BENePYRENE              0.52                 1          15.46             1          0.27               j          92.7
                BENaPYRENE              0.58                 1          10.49             1          0.25               1          97.7
                PERYLENE                0.39                 1          153.81                       3.94               1          84.5
                1123edPYRENE            0.49                 1          15.17             1          0.21               1          115.6
                DBahANTHRA              0.44                 j          15.44             1          0.26               1          114.5
                BghIPERYLENE            0.43                 1          22.71             1          0.31               1          i08.0

                TOTAL PAH's             84.0                            566.3                        10.8                                             NA
                   (W/O PERYLENE)
                2-MFMM.NAP14                                            71.A7                        n.ai
                I-METHYLNAPH            11.30                           44.15             1          1.10                          96.3



   M M M M M M M M M M M M M M M M M @ M

                                                  Antarctic Palmer Fish Samples Aromatic Hydrocarbon Data


                INVESTC                CORIICEPS                      CORIICEPS                    PROC BLANK                   CORUCEPS
                ID:                    PALMER STATION                 LAB QA SAMPLE                LAB QA SAMPLE                LAB QA SAMPLE
                LABSAMNO:              J2021                          Q4609                        Q4610                        Q4611
                UNIT:                  ng/g                           ng/g                         ng/g                         %
                PNA Analyte            Conc                 1313 QUAL Conc              DB QUAL Conc                 DB QUAL % Recov              DB QUAL


                2,6-DIMETHNAPH         4.45                 1         42.01             1          0.42              1          99.9


                2.3.5-IMMETHNAPH       2.30                 1         39.57             1          0.39              1          89.7


                I-METHYLPHEN           0.57                 1         16.02             1          0.19              1          70.0


                Sun,ogate Recovertes
                NAPHD8:                52.0                           48.0                         44.2                         57.2
                ACENDIO:               66.0                           45.9                         50.2                         56.5
                PHENDIO:               78.8                           51.4                         53.9                         66.4
                CHRYD12:               73.9                           36.6                         48.2                         55.3
                PERYD12-               48.7                           18.8              Q          3.6               Q          46.7


      ba
      W






                                                      Antarctic Palmer Fish Samples Aromatic Hydrocarbon Data


                    INVEST#:                NIST REF TISSUE                GERG REF OIL 11               CINDER CONES                CINDER CONES
                    ID:                     IAB QA SAMPLE                  LAB QA SAMPLE                 REPL. I                     REPL.2
                    LABSAMNO:               Q4612                          W8006                         J2022                       J2023
                    UNIT-                   ng/g                           ng/amp                        ng/g                        ng/g
                    PNA Analyte             Cone                DB QUAL Cone                 DB QUAL Cone                 DB QUAL Cone                DB QUALI

                    INVEST#:                NIST REF TISSUE                GERG REF OIL II               CINDER CONES                CINDER CONES
                    ID:                     LAB QA SAMPLE                  LAB QA SAMPLE                 REPL. I                     REPL.2
                    LABSAMNO:               Q4612                          W8006                         J2022                       J2023
                    SAMPLE TYPE:            REF NIST                       REF OIL                       SAMP                        SAMP
                    COLLECTION DATE:                                                                     12/05/91                    12/05/91
                    RECEIPT DATE:
                    QCBATCH:                M778                           M778                          M779                        M779
                    EXTRACTION DATE:
                    METHOD:                 GCFID                          GCFID                         GCFID                       GCFID
                    ANALYSIS DATE:
                    METHOD:                 GCMS                           GCMS                          GCMS                        GCMS
                    ANALYSIS DATE:          03/03/93                       03/03193                      03/06/93                    03/06/93
                    METHOD*                 GCECD                          GCECD                         GCECD                       GCECD
                    ANALYSIS DATE:          03/15/93                                                     03/15/93                    03/15/93
         w          MATRIX:                 TISSUE                         OIL                           TISSUE                      TISSUE
         0          SUBMAT:
         00         SAMPLWT:
                    WETWT:                  5.005                                                        10,151                      10.208
                    DRYWT:                  0.69                                                         1.35                        1.86
                    W17UNITS:               GRAMS               DRY        GRAMS                         GRAMS            DRY        GRAMS            DRY
                    PCTSOLIDS:
                    VOL.                                                   1.00
                    VOLUNITS:               LITERS                         AMPOULLE                      LITERS                      LITERS


                    NAPHTHALENE             19.32                          569.2                         14.90            1          31.42
                    CI-NAPHTHALENES         36.03                          2013.0                        12.20            1          47.23
                    C2-NAPHTHALENES,        75.69                          2017.6                        0                ND         43.88
                    C3-NAPHTHALENES         231                            1641.5                        0                ND         0                ND
                    C4-NAPHTHALENES         360.91                         1120.3                        0                ND         0                ND
                    BIPHENYL                21.80                          170.1                         14.49                       6.39
                    ACENAPHTHYLENE          5.07                1          0.9                           0.93             1          2.16
                    ACENAPHTHENE            15.41               j          15.3                          4.99             j          7.18
                    FLUORENE                9.19                1          72.3                          2.74             j          3.58
                    CI-FLUORENES            38.41                          196.1                         0                ND         0                ND






                                                      Antarctic Palmer Fish Samples Aromatic Hydrocarbon Data


                    INVEST#:                NIST REF TISSUE                GERG REF OIL II               CINDER CONES                CINDER CONES
                    ID:                     LAB QA SAMPLE                  LAB QA SAMPLE                 REPL. 1                     REPL.2
                    LABSAMNO:               Q4612                          W8006                         J2022                       J2023
                    UNIT:                   ng/g                           ng/amp                        ng/g                        ng/g
                    PNA Analyte             Conc                DB QUAL Conc                  DB QUAL Conc                DB QUAL Conc                 DB QUAL,

                    C2-FLUORENES            178.76                         290.4                         0                ND         0                 ND
                    C3-FLUORENES            358.54                         413.1                         0                ND         0                 ND
                    PHENANTHRENE            35.92                          191.9                         3.24             1          2.51
                    ANTHRACENE              11.69               1          5.5                           3.49             1          1.00
                    CI-PHEN-ANTHR           89.15                          476.7                         0                ND         0                 ND
                    C2-PHEN-ANTFiR          328.98                         663.2                         0                ND         0                 ND
                    C3-PHEN-ANTHR           574.53                         672.7                         0                ND         0                 ND
                    C4-PHEN-ANTHR           268.03                         365.5                         0                ND         0                 ND
                    DIBENZOTHIO             5.81                1          144.8                         2.00             1          1.47              1
                    CI-DIBEN                38.3                           300.5                         0                ND         0                 ND
                    C2-DIBEN                160.68                         488.9                         0                ND         0                 ND
                    C3-DIBEN                219.13                         514.1                         0                ND         0                 ND
                    FLUORANTHENE            226,28                         3.8                           3.03             1          0.63
                    PYRENE                  228.85                         10.0                          2.14             1          1.31
         to         CI-FLUORAN-PYR          180.02                         94.7                          0                ND         0                 ND
         (D         BENaANTHRACENE          31.86                          5.5                           0.65             j          1.27
                    CHRYSENE                111.53                         49.6                          2.77             j          0.98
                    CI-CHRYSENES            69.45                          85.9                          0                ND         0                 ND
                    C2-CHRYSENES            49.53                          146.4                         0                ND         0                 ND
                    C3-CHRYSENES            0                   ND         37.2                          0                ND         0                 ND
                    C4-CHRYSENES            0                   ND         27.9                          0                ND         0                 ND
                    BENbFLUORAN             38.70                          2.9                           0.67             1          0.15
                    BENkFLUORAN             38.70                          2.9                           0.67             1          0.15
                    BENePYRENE              79.18                          9.6                           1.50             j          0.53
                    BENaPYRENE              12.59               1          1.7                           1.89                        2.40              j
                    PERYLENE                9.38                j          2.1                           4.09                        0.49
                    1123cdPYRENE            16.40                          1.6                           0.63             1          0.61
                    DBahANTHRA              4.11                           3.1                           0.87             1          0.72
                    Bgh1PERYLENE,           23.26                          4.1                           0.77                        0.28

                    TOTAL PAH's             4192.8                         12830.3                       74.6                        155.9
                       (WIO PERYLENE)                                                                                                30.74
                    2-METHYLNAPH            16.39                          1078.7                        6.57
                    1-METHYLNAPH            19.64                          934.3                         5.63                        16.49






                                                    Antarctic Palmer Fish Samples Aromatic Hydrocarbon Data


                   INVEST#:                NIST REF TISSUE               GERG REF OIL II             CINDER CONES                CINDER CONES
                   ID:                     LAB QA SAMPLE                 LAB QA SAMPLE               REPL. 1                     REPL.2
                   LABSAMNO:               Q4612                         W8006                       J2022                       J2023
                   UNIT:                   ng/g                          ng/amp                      ng/9                        ng/g
                   PNA Analyte             Conc               DB QUAL Conc                 DB QUAL Conc               DB QUAL Conc                DB QUAL,


                   2,6-DIMETHNAPH          11.26              1          671.9                       8.44                        12.34


                   2,3,5-IMME'THNAPH       13.69              1          308.5                       4.02             1          2.26             j


                   I-METHYLPHEN            18.99                         141.5                       3.26             1          0.63


                   Surrogate Recoveries
                   NAPHD8:                 43.8                                            NA        60.2                        49.6
                   ACENDIO:                49.8                                            NA        46.5                        53.3
                   PHENDIO:                59.3                                            NA        51.0                        58.7
                   CHRYD12:                54.8                                            NA        51.7                        53.7
                   PERYD12:                47.5                                            NA        33.2                        48.2



        0






                                                    Antarctic Palmer Fish Samples Aromatic Hydrocarbon Data


                INVEST#:                CINDER CONES                BERNACCHI               BERNACCHI               OU17ALL               OL177ALL
                ID:                     REPL.3                      105'REPL. I             105'REPL.2              60'REPLI              60'REPL2
                LABSAMNO:               J2024                       J2025                   J2026                   J2027                 J2028
                UNIT:                   ng/g                        ng/g                    ng/g                    ng/g                  ng/g
                PNA Analyte             Conc             DB QUAL Conc            DB QUAL Conc            DB QUAL Conc          DB QUAL Conc          DB QUAL

                INVEST#:                CINDER CONES                BERNACCHI               BERNACCHI               OUTFALL               OUTFALL
                ID:                     REPL.3                      I05'REPL. I             105'REPL.2              60'REPLI              60'REPL2
                LABSAMNO:               J2024                       J2025                   J2026                   J2027                 J2028
                SAMPLE TYPE:            SAMP                        SAMP                    SAMP                    SAMP                  SAMP
                COLLECTION DATE:        12/05/91                    12/10/91                12/10/91                12/12/91              12/12/91
                RECEIPT DATE:
                QCBATCH:                M779                        M779                    M779                    M779                  M779
                EXTRACTION DATE:
                MEII-IOD:               GCFID                       GCFID                   GCFID                   GCFID,                GCFID
                ANALYSIS DATE:
                METHOD:                 GCMS                        GCMS                    GCMS                    GCMS                  GCMS
                ANALYSIS DATE:          03/06/93                    03/06/93                03/06/93                03/06/93              03/06/93
                METHOD:                 GCECD                       GCECD                   GCECD                   GCECD                 GCECD
                ANALYSIS DATE:          03/15/93                    03/15/93                03/15/93                03/15/93              03/15/93
                MATRIX:                 TISSUE                      TISSUE                  TISSUE                  TISSUE                TISSUE
        0
                SUBMAT:
                SAMPLWT:
                WETWT:                  10.405                      10.169                  10.467                  10.153                10.656
                DRYWT:                  1.28                        1.71                    1.69                    1.76                  1.84
                VMNrM:                  GRAMS            DRY        GRAMS        DRY        GRAMS        DRY        GRAMS      DRY        GRAMS      DRY
                PCTSOLIDS:
                VOL:
                VOLUNITS:               LITERS                      LITERS                  LITERS                  LITERS                LITERS

                NAPHTHALENE             14.60            j          6.85         j          18.63        1          9.50       1          17.53      1
                CI-NAPHTHALENES         18.15            1          9.73         1          15.95        1          26.82      1          27.61      j
                C2-NAPHTHALENES         0                ND         0            ND         0            ND         52.92      1          59.54      1
                C3-NAPHTHALENBS         0                ND         0            ND         0            ND         0          ND         0          ND
                C4-NAPHTUALENES         0                ND         0            ND         0            ND         0          ND         0          ND
                BIPHENYL                3.78             1          2.26         1          3.60         1          5.80       1          5.22       1
                ACENAPHTHYLENE          4.24             1          2.38         1          0.80         1          2.78       1          2.66       1
                ACENAPHTHENE            5.80             1          1.54         j          2.61         1          1.45       1          2.00       1
                FLUORENE                2.75             1          0.66         1          1.02         1          5.37       1          2.35       1
                CI-FLUORENES            0                ND         0            ND         0            ND         0          ND         0          ND






                                                     Antarctic Palmer Fish Samples Aromatic Hydrocarbon Data


                INVEST#:                CINDER CONES                 BERNACCHI                BERNACCHI                 OUTFALL                OUTFALL
                ID:                     REPL.3                       105'REPL. I              105'REPL.2                60'REPL1               60'REPL2
                LABSAMNO:               J2024                        J2025                    J2026                     J2027                  J2028
                UNIT-                   ng/g                         ng/g                     ng/g                      ng/g                   ng/g
                PNA Analyte             Conc              DB QUAL Conc              DB QUAL Conc             DB QUAL Conc          DB QUAL Conc           DB QUAL

                C2-FLUORENES,           0                 ND         0              ND        0              ND         0          ND          0          ND
                C3-FLUORENES            0                 ND         0              ND        0              ND         0          ND          0          ND
                PHENANTI-IRENE          1.67              1          0.82           1         4.12           1          5.25       1           3.53
                ANTHRACENE              1.99              1          0.81           1         0.65           j          1.49       1           1.81
                CI-PHEN  -ANTHR         0                 ND         0              ND        0              ND         0          ND          0          ND
                C2-PHEN  -ANTHR         0                 ND         0              ND        0              ND         0          ND          0          ND
                C3-PHEN  -ANTHR         0                 ND         0              ND        0              ND         0          ND          0          ND
                C4-PHEN  -ANTHR         0                 ND         0              ND        0              ND         0          ND          0          ND
                DIBENZOTHIO             4.81              1          1.58           1         1.96           1          2.41       1           1.85       1
                CI-DIBEN                0                 ND         0              ND        0              ND         0          ND          0          ND
                C2-DIBEN                0                 ND         0              ND        0              ND         0          ND          0          ND
                C3-DIBEN                0                 ND         0              ND        0              ND         0          ND          0          ND
                FLUORANTHENE            2.71              j          1.48           1         0.98           1          4.86       1           4.01       1
                PYRENE                  1.75              1          0.49           1         1.25           1          5.94       1           4.93       1
       ca       CI-FLUORAN-PYR          0                 ND         0              ND        0              ND         0          ND          0          ND
       0        BENaANTHRACENE          0.83              1          0.41           1         0.43           1          2.10       1           1.71       1
                CHRYSENE                0.65              1          0.27           1         0.67           1          3.56       1           2.86       1
                C I -CHRYSENES,         0                 ND         0              ND        0              ND         0          ND          0          ND
                C2-CHRYSENES            0                 ND         0              ND        0              ND         0          ND          0          ND
                C3-CHRYSENES,           0                 ND         0              ND        0              ND         0          ND          0          ND
                C4-CHRYSENES            0                 ND         0              ND        0              ND         0          ND          0          ND
                BENbFLUORAN             0.34              1          0.33           j         0.24           1          2.18       1           1.44       1
                BENkFLUORAN             0.34              1          0.28           j         0.31           1          2.18       1           1.44       1
                BENePYRENE              0.27              1          0.72           j         0.39           1          4.10       1           3.19       j
                BENaPYRENE              2.35              1          0.82           1         1.33           1          2.39       1           1.15       1
                PERYLENE                0.66              1          0.53           1         0.71           j          1.67       1           1.05       1
                1123cdPYRENE            0.67              1          0.56           j         0.23           1          0.89       j           0.82       1
                DBahANTTiRA             1.03              1          0.31           1         0.47           1          1.10       1           0.95       1
                BghIPERYLENE            0.43              j          0.32           1         0.54           1          2.16,      j           L69        -i

                TOTAL PAH's             69.2                         32.6                     56.2                      145.3                  148.3
                   CW/O PERYLENE)
                                                                                    T            on
                2 METIMNAPH             1. 0%. 2 -r-                 4.911 '17      u         v.vA,
                I-METHYLNAPH            7.90              1          4.76           1         9.13                      11.62                  11.90






                                                      Antarctic Palmer Fish Samples Aromatic Hydrocarbon Data


                 INVEST#:                CINDER CONES                 BERNACCHI                BERNACCHI                 OLn7ALL               OUTFALL
                 ID:                     REPL.3                       105' REPL. I             105'REPL.2                60'REPLI              60'REPL2
                 LABSAMNO:               J2024                        J2025                    J2026                     J2027                 J2028
                 UNrI%                   ng/g                         ng/g                     ng/g                      ng/g                  ng/g
                 PNA Analyte             Conc             DB QUAL Conc              DB QUAL Conc             DB QUAL Conc           DB QUAL Conc           DB QUAL


                 2.6-DIMETHNAPH          3.21             1           2.33          1          0.95          1           10.85                 12.72

                 2.3,5-TRIMEMNAPH        1.28             j           1.43          1          2.80          1           6.79                  6.54


                 I-METHYLPHEN            2.82             1           0.80          1          2.63          1           1.47       1          0.75        1


                 Surrogate Recoveries
                 NAPHD8:                 58.1                         54.2                     45.3                      55.0                  52.7
                 ACENDIO:                63.8                         50.8                     60.2                      52.3                  51.4
                 PHENDIO:                53.9                         63.3                     56.0                      59.7                  58.1
                 CHRYD12:                54.1                         51.3                     57.8                      61.4                  57.7
                 PERYD12:                46.5                         40.3                     48.2                      48.3                  40.5



        0






                                                       Antarctic Palmer Fish Samples Aromatic Hydrocarbon Data


                INVEST#:                 WINTER QUARTERS                   WINTER QUARTERS                    WINTER QUARTERS                   BAY OF SAILS
                ID:                      70' REPL. I                       70'REPL.2                          70'REPL.3                         REPLA
                LABSAMNO:                J2029                             J2030                              J2031                             J2032
                UNIT:                    ng/g                              ng/g                               ng/g                              ng/g
                PNA Analyte              Cone                   DB QUAL Cone                      DB QUAL Cone                      DB QUAL Cone                 DB QUALI

                INVEST#:                 WINTER QUARTERS                   WINTER QUARTERS                    WINTER QUARTERS                   BAY OF SAILS
                ID:                      70' REPL. I                       70'REPL.2                          70'REPL.3                         REPL. I
                IABSAMNO:                J2029                             J2030                              J2031                             J2032
                SAMPLE TYPE:             SAMP                              SAMP                               SAMP                              SAMP
                COLLECTION DATE:         12/09/91                          12/09/91                           12/09/91                          12/06/91
                RECEIPT DATE:
                QCBATCH:                 M779                              M779                               M779                              M780
                EXTRACTION DATE:
                METHOD:                  GCFID                             GCFID                              GCFID                             GCFID
                ANALYSIS DATE:
                METHOD:                  GCMS,                             GCMS                               GCMS                              GCMS,
                ANALYSIS DATE:           03/06/93                          03/07/93                           03/06/93                          03/07/93
                METHOD:                  GCECD                             GCECD                              GCECD                             GCECD
                ANALYSIS DATE:           03/15/93                          03/15/93                           03/15/93                          03/15/93
         w      MATRIX:                  TISSUE                            IISSUE                             TISSUE                            TISSUE
                SUBMAT:
                SAMPLWr:
                WETWT:                   10.641                            10.474                             10.224                            10.356
                DRYWT.                   1.78                              1.52                               2.17                              2.05
                WTUNITS:                 GRAMS                  DRY        GRAMS                  DRY         GRAMS                 DRY         GRAMS            DRY
                PCTSOLIDS:
                VOL:
                VOLUNITS:                LITERS                            LITERS                             LITERS                            LITERS


                NAPHTHALENE              16.46                  1          18.99                  j           34.23                             21.39            B
                CI-NAPHTHALENES          26.03                  1          34.56                  1           67.91                             20.37            B
                C2-NAPHTHALENES          68.79                  1          0                      ND          49.53                             0                ND
                C3-NAPHTHALENES          0                      ND         0                      ND          0                     ND          0                ND
                C4-NAPHTHALENES          0                      ND         0                      ND          0                     ND          0                ND
                BIPHENYL                 3.43                   1          11.10                              7.31                              6.86             1
                ACENAPHTHYLENE           1.74                   j          2.08                   1           2.83                  1           0.80             j
                ACENAPHTHENE             5.14                   1          7.37                   1           1.66                  1           2.02             j
                FLUORENE                 1.41                   -i         .549.                  j           1.00                  .1          .1 - 1.9;        j
                CI-FLUORENES             0                      ND         0                      ND          0                     ND          0                ND






                                                   Antarctic Palmer FIsh Samples Aromatic Hydrocarbon Data


             INVEST#:                WINTER QUAR77ERS                 WINTER QUARTERS                 WINTER QUARTERS                  BAY OF SAILS
             ID:                     70'REPL. I                       70'REPL.2                       70'REPL.3                        REPL. I
             LABSAMNO:               J2029                            J2030                           J2031                            J2032
             UNIT-                   ng/g                             ng/g                            ng/g                             ng/9
             PNA Analyte-            Cone                  DB QUAL Cone                    DB QUAL Cone                     DB QUAL Cone               DB QUAL,

             C2-FLUORENES            0                     ND         0                    ND         0                     ND         0               ND
             C3-FLUORENES            0                     ND         0                    ND         0                     ND         0               ND
             PHENANTHRENE            5.98                  1          5.56                 1          2.18                             2.42            1
             ANTHRACENE              1.72                  1          5.14                 1          1.07                             0.64            1
             CI-PHEN-ANTHR           0                     ND         0                    ND         0                     ND         0               ND
             C2-PHEN-ANTHR           0                     ND         0                    ND         0                     ND         0               ND
             C3-PHEN-ANTHR           0                     ND         0                    ND         0                     ND         0               ND
             C4-PHEN-ANTHR           0                     ND         0                    ND         0                     ND         0               ND
             DIBENZOTI-110           2.44                  1          6.82                 1          0.84                  1          0.92            1
             CI-DIBEN                0                     ND         0                    ND         0                     ND         0               ND
             C2-DIBEN                0                     ND         0                    ND         0                     ND         0               ND
             C3-DIBEN                0                     ND         0                    ND         0                     ND         0               ND
             FLUORANTRENE            4.21                  1          8.15                 1          5.85                             2.38            j
             FYRENE                  6.14                             15.15                           5.93                             2.01            1
             CI-FLUORAN-PYR          0                     ND         0                    ND         0                     ND         0               ND
             BENaANTHRACENE          1.20                  1          5.04                 1          0.95                  1          0.57            1
      Ln     CHRYSENE                3.14                  1          6.91                 1          1.50                  1          1.10            1
             CI-CHRYSENES            0                     ND         0                    ND         0                     ND         0               ND
             C2-CHRYSENES            0                     ND         0                    ND         0                     ND         0               ND
             C3-CHRYSENES            0                     ND         0                    ND         0                     ND         0               ND
             C4-CHRYSENES            0                     ND         0                    ND         0                     ND         0               ND
             BENbFLUORAN             1.87                  1          3.53                 1          1.30                             0.49            1
             BENkFLUORAN             1.87                  1          3.53                 1          1.30                             0.49            1
             BENcPYRENE              3.57                  1          7.91                 1          1.29                             0.87            j
             BENaPYRENE              0.81                  1          9.38                 1          0.46                             0.31            1
             PERYLENE                10.55                            5.44                 1          0.46                             0.72            1
             I 123cdPYRENE           0.86                  1          7.21                 1          0.73                             0.19            1
             DBahANTHRA              0.21                  1          7.22                 1          0.29                             0.12            1
             BghfPERYLENE            1.49                  1          5.96                 1          0.87                             0.24            1

             TOTAL PAH's             158.5                            177.0                           191.0                            67.3
                (W/O PERYLENE)
             2-METHYLNAPH            18.76                            24.55                           39.30                            11.59
             I-METHYLNAPH            7.27                             10.01                           28.61                            8.78






                                                      Antarctic Palmer Fish Samples Aromatic Hydrocarbon Data


                INVEST#:                WINTER QUARTERS                   WINTER QUARTERS                  WINTER QUARTERS                   BAY OF SAILS
                ID:                     70' REPL. I                       70'REPL.2                        70'REPL.3                         REPL. I
                LABSAMNO:               J2029                             J2030                            J2031                             J2032
                UNIT:                   ng/g                              ng/g                             ng/g                              ng/g
                PNA Analyte             Conc                  DB QUAL Conc                      DB QUAL Conc                      DB QUAL Conc                DB QUALI


                2.6-DIMETHNAPH          13.71                             18.04                            14.63                             6.79


                2.3.5-TRIMETHNAPH       8.51                              2.96                  1          3.07                   1          3.02


                1-ME'rHYLPHEN           0.92                  1           12.09                 M          1.17                   j          1.82


                Surrogate Recoveries
                NAPHD8:                 42.6                              60.5                             41.9                              52.1
                ACENDIO:                56.1                              82.2                             47.1                              50.7
                PHENDIO:                54.1                              59.7                             53.8                              57.6
                CHRYD12:                58.1                              73.7                             56.1                              57.6
                PERYD12:                12.8                              52.2                             50.1                              29.4



        0
        0)






                                                        Antarctic Palmer Fish Samples Aromatic Hydrocarbon Data


                 INVEST#:                 CINDER CONES                  WINTER QUARTERS                   WINTER QUARTERS                    PROC BLANK
                 ID:                      T BERNACCHII                  70'REPL.                          70'REPL.3                          LAB QA SAMPLE
                 LABS.AMNO:               J2033                         J2064                             Q4630                              Q4631
                 UNIT:                    ng/g                          ng/g                              ng/g                               ng/g
                 PNA Analyte              Conc              DB QUAL Conc                      DB, QUAL Conc                      DB QUAL Conc                   DB QUAL

                 INVEST#:                 CINDER CONES                  WINTER QUARTERS                   WINTER QUARTERS                    PROC BLANK
                 ID:                      T BERNACCHII                  70'REPL.                          70'REPL.3                          LAB QA SAMPLE
                 LABSAMNO:                J2033                         J2064                             Q4630                              Q4631
                 SAMPLE TYPE:             SAMP                          SAMP                              DUPE OF J2031                      PROC BLANK
                 COLLECTION DATE:         12/09/91                      12/09/91                          12/09/91
                 RECEIPT DATE:
                 QCBATCH:                 M780                          M827                              M779                               M779
                 EXTRAC71ON DATE:                                       04/26/93
                 METHOD:                  GCFID                         GCFID                             GCFID                              GCFID
                 ANALYSIS DATE:
                 METHOD-.                 GCMS                          GCMS                              GCMS                               GCMS
                 ANALYSIS DATE:           03/07/93                      05/24/93                          03/06/93                           03/06/93
                 METHOD:                  GCECD                         GCECD                             GCECD                              GCECD
                 ANALYSIS DATE:           03/15/93                      06/02/93                          03/15/93                           03/15/93
                 MATRIX:                  TISSUE                        TISSUE                            TISSUE                             TISSUE
        0        SUBMAT:
                 SAMPLArr:
                 WETWT*                   10.572                        10.039                            10.089
                 DRYWT:                   2.50                          1.43                              2.03                               10.00
                 WTUNITS:                 GRAMS             DRY         GRAMS                 DRY         GRAMS                  DRY         GRAMS              DRY
                 PCTSOLIDS:
                 VOL:
                 VOLUN`rJrS:              LITERS                        LITERS                            LITERS                             LITERS


                 NAPHTHALENE              55.52                         25.18                 1           41.07                              1.15
                 CI-NAPHTHALENES,         73.87                         45.14                 1           63.71                              1.98
                 C2-NAPHTHALENES,         53.61                         30.00                 1           69.44                              0                  ND
                 C3-NAPHTHALENES          55.49                         32.90                 j           0                      ND          0                  ND
                 C4-NAPHTHALENES          0                 ND          0                     ND          0                      ND          0                  ND
                 BIPHENYL                 8.88              j           7.52                              7.41                   1           0.61
                 ACENAPHTHYLENE           1.11              j           1.03                  1           3.56                   1           0.49
                 ACENAPHTHENE             1.40              j           2.76                  1           1.49                   1           0.70
                 FWORENE                  1.43              j           1.94                  1           3.18                   j           0.65
                 CI-FLUORENES             0                 ND          0                     ND          0                      ND          0                  ND






                                                      Antarctic Palmer Fish Samples Aromatic Hydrocarbon Data


                INVEST#:                CINDER CONES                  WINTER QUARTERS                  WINTER QUARTERS                    PROC BLANK
                ID:                     T BERNACCHII                  70'REPL.                         70'REPL.3                          1AB QA SAMPLE
                LABSAMNO:               J2033                         J2064                            Q4630                              Q4631
                UNIT-                   ng/g                          ng/g                             ng/g                               ng/g
                PNA Analyte             Conc              DB QUAL Conc                      DB QUAL Conc                      DB QUAL Conc                   DB QUAL
                C2-FLUORENES,           0                 ND          0                     ND         0                      ND          0                  ND
                C3-FLUORENES            0                 ND          0                     ND         0                      ND          0                  ND
                PHENANTHRENE            3.34              1           4.36                  j          4.33                   1           0.30               1
                ANTHRACENE              1.11              1           1.28                  1          4.00                   j           0.33               j
                CI-PHEN  -ANTHR         0                 ND          0                     ND         0                      ND          0                  ND
                C2-PHEN  -ANTHR         0                 ND          0                     ND         0                      ND          0                  ND
                C3-PHEN  -ANTHR         0                 ND          0                     ND         0                      ND          0                  ND
                C4-PHEN  -ANTHR         0                 ND          0                     ND         0                      ND          0                  ND
                DIBENZOTHIO             1.77              1           0.86                  1          2.84                   1           0.24               1
                CI-DIBEN                0                 ND          0                     ND         0                      ND          0                  ND
                C2-DIBEN                0                 ND          0                     ND         0                      ND          0                  ND
                C3-DIBEN                0                 ND          0                     ND         0                      ND          0                  ND
                FLUORANTHENE            0.94              1           3.76                  1          6.61                               0.35
       cc       PYRENE                  1.14              1           5.34                  1          6.84                               0.35
       0        CI-FLUORAN-PYR          0                 ND          0                     ND         0                      ND          0                  ND
       00       BENaANTHRACENE          0.30              1           1.18                  1          2.39                   1           0.04
                CHRYSENE                0.33              1           2.64                  1          2.75                   1           0.56
                CI-CHRYSENES,           0                 ND          0                     ND         0                      ND          0                  ND
                C2-CHRYSENES            0                 ND          0                     ND         0                      ND          0                  ND
                C3-CHRYSENES            0                 ND          0                     ND         0                      ND          0                  ND
                C4-CHRYSENES            0                 ND          0                     ND         0                      ND          0                  ND
                BENbFLUORAN             0.14              1           1.21                  1          2.76                   1           0.24
                BENkFLUORAN             0.14              1           1.21                  1          2.76                   1           0.22
                BENePYRENE              0.13              j           2.68                  1          3.75                   1           0.29               j
                BENaPYRENE              0.44              1           1.73                  1          2.64                   j           0.27
                PERYLENE                0.39              1           1.08                  1          2.38                   j           2.72
                1123cdPYRENE            0.09              1           0.73                  j          2.35                   1           0.23               1
                DBahANTHRA              0.14              1           0.34                  j          2.39                   1           0.26
                Bgh1PERYLENE            0.21              1           1.24                  1          2.49                   j           0.25

                TOTAL PAH's             261.5                         175.0                            238.8                              9.5
                  (W1O PERYLENE)
                2-METHYLNA.F1H          46.76
                                                                                                                                          0.89
                I-METHYLNAPH            27.11                         16.91                            24.54                              1.09






                                                   Antarctic Palmer Fish Samples Aromatic Hydrocarbon Data


               INVEST#:               CINDER CONES                WINTER QUARTERS                WINTER QUARTERS                 PROC BIANK
               ID:                    T BERNACCHII                70'REPL.                       70'REPL.3                       LAB QA SAMPLE
               LABSAMNO:              J2033                       J2064                          Q4630                           Q4631
               UNIT:                  ng/g                        ng/g                           ng/g                            ng/9
               PNA Analyte            Conc             DB QUAL Conc                   DB QUAL Conc                    DB QUAL Conc                 DB QUAL,


               2.6-DIMETHNAPH         14.09                       12.29                          19.49                           0.97


               2,3,5-TRIMETHNAPH      1.97             j          5.26                1          4.76                 1          0.56


               I-METHYLPHEN           1.50             1          0.90                j          4.70                 1          0.42              j


               Surrogate Recoveries
               NAPHD8:                63.2                        48.4                           47.0                            55.5
               ACENDIO:               62.2                        63.7                           48.5                            49.2
               PHENDIO.               65.4                        70.5                           54.2                            54.7
               CHRYD12:               66.6                        73.6                           50.4                            48.8
               PERYD12:               41.1                        40.4                           42.2                            7.1               Q


       0






                                                      Antarctic Palmer Fish Samples Aromatic Hydrocarbon Data


                  INVEST#:                WINTER QUARTERS                    NIST REFTISSUE                 CINDER CONES                 CINDER CONES
                  ID:                     70'REPL.3                          LAB QA SAMPLE                  T BERNACCHII                 T BERNACCHII
                  LABSAMNO:               Q4632                              Q4633                          Q4634                        Q4635
                  UNIT:                   %                                  ng/g                           ng/g                         %
                  PNA Analyte             % Recov                DB QUAL Conc                    DB QUAL Conc                DB QUAL % Recov               DB QUALJ

                  INVEST#:                WINTER QUARTERS                    NIST REF TISSUE                CINDER CONES                 CINDER CONES
                  ID:                     70'REPL.3                          LAB QA SAMPLE                  T BERNACCHII                 T BERNACCHII
                  LABSAMNO:               Q4632                              Q4633                          Q4634                        Q4635
                  SAMPLE TYPE:            MS OF J2031                        NIST FEF                       DUPE OF J2033                MS OF J2033
                  COLLECTION DATE:        12/09/91                           12/06/91                       12/09/91
                  RECEIPT DATE:
                  QCBATCH:                M779                               M779                           M780                         M780
                  EX17RACTION DATE:
                  METHOD:                 GCFID                              GCFID                          GCFID                        GCFID
                  ANALYSIS DATE:
                  METHOD:                 GCMS                               GCMS                           GCMS                         GCMS
                  ANALYSIS DATE:          03/06/93                           03/06/93                       03/07/93                     03/07/93
                  METHOD:                 GCECD                              GCECD                          GCECD                        GCECD
                  ANALYSIS DATE:          03/15/93                           03/15/93                       03/15/93                     03/15/93
                  MATRIX:                 TISSUE                             TISSUE                         TISSUE                       TISSUE
                  SUBMAT:
                  SAMPLWr:
                  WETWT:                  10.517                             5.013                          10.345                       10.22
                  DRYWT:                  2.25                               0.62                           2.36                         2.35
                  WTUNITS:                GRAMS                  DRY         GRAMS               DRY        GRAMS             DRY        GRAMS             DRY
                  PCT'SOLIDS:
                  VOL.
                  VOLUNITS:               LITERS                             LITERS                         LITERS                       LITERS


                  NAPHTHALENE             77.3                               29.03                          62.26                        84.4
                  CI-NAPHTHALENES                                NA          42.11                          80.77                                          NA
                  C2-NAPHTHALENES                                NA          95.43                          49.86                                          NA
                  C3-NAPHTHALENES                                NA          230.03                         43.48                                          NA
                  C4-NAPHTHALENES                                NA          329.44                         0                 ND                           NA
                  BIPHENYL                96.6                               7.09                j          11.41                        75.1
                  ACENAPHTHYLENE          90.1                               5.87                1          0.75              1          71.6
                  ACENAPHTHENE            86.4                               10.31               1          3.73              j          78.2
                                                                             12.42               i          2.                1          72.4
                  Cl-FLUORENES                                   NA          56.22                          0                 ND                           NA






                                                      Antarctic Palmer Fish Samples Aromatic Hydrocarbon Data


                   INVEST#:                WINTER QUARTERS                  NIST REF TISSUE                CINDER CONES                CINDER CONES
                   ID:                     70'REPL.3                        LAB QA SAMPLE                  T BERNACCHII                T BERNACCHII
                   LABSAMNO:               Q4632                            Q4633                          Q4634                       Q4635
                   UNIT:                   %                                ng/g                           ng/g                        %
                   PNA Analyte             % Recov               DB QUAL Conc                   DB QUAL Conc                DB QUAL % Recov              DB QUALI

                   C2-FLUORENES                                  NA         163.01                         0                ND                           NA
                   C3-FLUORENES                                  NA         397.8                          0                ND                           NA
                   PHENANTHRENE            87.5                             32.58                          3.73             1          68.1
                   ANTHRACENE              49.5                             13.44               1          2.05             1          44.3
                   CI-PHEN-ANMR                                  NA         101.12                         0                ND                           NA
                   C2-PHEN-ANTHR                                 NA         323.72                         0                ND                           NA
                   C3-PHEN-ANTHR                                 NA         473.3                          0                ND                           NA
                   C4-PHEN-ANTHR                                 NA         289.49                         0                ND                           NA
                   DIBENZOTHIO             67.1                             7.77                1          1.08             1          51.1
                   CI-DIBEN                                      NA         41.67                          0                ND                           NA
                   C2-DIBEN                                      NA         2210.43                        0                ND                           NA
                   C3-DIBEN                                      NA         264.18                         0                ND                           NA
                   FLUORAMMENE             105.8                            228.73                         1.31             1          86.5
                   PYRENE                  103.8                            231.95                         1.22             1          83.3
                   CI-FLUORAN-PYR                                NA         173.67                         0                ND                           NA
                   BENaANTHRACENE          90.6                             42.23                          0.82             1          75.4
                   CHRYSENE                87.3                             108.71                         0.70             1          86.6
                   CI-CHRYSENES                                  NA         69.59                          0                ND                           NA
                   C2-CHRYSENES                                  NA         51.88                          0                ND                           NA
                   C3-CHRYSENES                                  NA         0                   ND         0                ND                           NA
                   C4-CHRYSENES                                  NA         0                   ND         0                ND                           NA
                   BENbFLUORAN             110.6                            41.93                          0.68             1          108.6
                   BENkFLUORAN             8.4                              41.93                          0.79             1          111.2
                   BENePYRENE              99.2                             87.81                          0.76             1          99.8
                   BENaPYRENE              97.4                             17.06               1          0.38             1          84.1
                   PERYLENE                78.3                             8.48                1          0.63             1          92.2
                   1123cdPYRENE            123.1                            19.64               1          0.37             1          75.2
                   DBahANTHRA              141.6                            7.42                1          0.71             1          85.2
                   BghIPERYLENE            121.8                            24.35                          0.55             1          79.6

                   TOTAL PAH's                                   NA         6283.4                         270.0                                         NA
                     (W/O PERYLENE)
                   2-METHYLNAPH            169.3                            23.38                         .49.90                       140.1
                   I-METHYLNAPH            105.3                            18.73                          30.87                       113.7






                                                     Antarctic Palmer Fish Samples Aromatic Hydrocarbon Data


                  INVEST#:                WINTER QUARTERS                  NIST REF TISSUE                CINDER CONES                CINDER CONES
                  ID:                     70'REPL.3                        LAB QA SAMPLE                  T BERNACCHII                T BERNACCHII
                  LABSAMNO:               Q4632                            Q4633                          Q4634                       Q4635
                  UNIT:                   %                                ng/g                           ng/g                        %
                  PNA Analyte             % Recov               DB QUAL Conc                   DB QUAL Conc                DB QUAL % Recov              DB QUALI


                  2,6-DIMETHNAPH          100.9                            20.61                          15.82                       79.5


                  2.3,5-TRIMETHNAPH       98.0                             17.76                          3.13             1          78.8

                  I-ML-11MPHEN            82.7                             18.52                          2.01             1          60.7

                  Surrogate Recoveries
                  NAPHD8:                 41.4                             48.9                           50.8                        51.9
                  ACENDIO:                46.7                             51.4                           53.5                        66.6
                  PHENDIO:                38.5                             61.1                           58.7                        73.0
                  CHRYD12:                53.4                             50.4                           54.5                        61.0
                  PERYD12-                44.7                             42.3                           35.4                        35.3






                                                    Antarctic Palmer Fish Samples Aromatic Hydrocarbon Data


                   INVEST#:               PROC BLANK                  NIST REFTISSUE               GERG REF OIL 11             GERG REF OIL 11
                   ID:                    LAB QA SAMPLE               LAB QA SAMPLE                1AB QA SAMPLE               IAB QA SAMPLE
                   LABSAMNO:              Q4636                       Q4637                        W8022                       W8026
                   UNIT:                  ng/g                        %                            ng/amp                      ng/amp
                   PNA Analyte            Conc              DB QUAL % Recov             DB QUAL Conc                 DB QUAL Conc                DB QUAL

                   INVEST#:               PROC BLANK                  NIST REF TISSUE              GERG REF OIL 11             GERG REF OIL 11
                   ID:                    LAB QA SAMPLE               LAB QA SAMPLE                LAB QA SAMPLE               LAB QA SAMPLE
                   LABSAMNO:              Q4636                       Q4637                        W8022                       W8026
                   SAMPLE TYPE:           PROC BLANK                  NIST REF                     REF OIL                     REF OIL
                   COLLECTION DATE:
                   RECEIPT DATE:
                   QCBATCH:               M780                        M780                         M779                        M780
                   EXTRACTION DATE:
                   METHOD:                GCFID                       GCFID                        GCFID                       GCFID
                   ANALYSIS DATE:
                   METHOD:                GCMS                        GCMS                         GCMS                        GCMS
                   ANALYSIS DATE:         03/07/93                    03/07/93                     03/06/93                    03/06/93
                   METHOD:                GCECD                       GCECD                        GCECD                       GCECD
                   ANALYSIS DATE:         03/15/93                    03/15/93
                   MATRIX:                TISSUE                      TISSUE                       OIL                         OIL
                   SUBMAT:
                   SAMPLWT:
                   WETWT:                                             5.139
                   DRYWT-                 10.00                       0.62
                   MITUNITS:              GRAMS             DRY       GRAMS             DRY        GRAMS             DRY       GRAMS             DRY
                   PCTSOLIDS:
                   VOL:                                                                            1.00                        1.00
                   VOLUNITS:              LITERS                      LITERS                       AMPOULLE                    AMPOULLE

                   NAPHTHALENE            0.83                        25.28                        476.2                       574.2
                   CI-NAPHTHALENES,       1.39                        37.89                        2044.0                      2183.6
                   C2-NAPHTHALENES        0                 ND        70.85                        2067.9                      2278.5
                   C3-NAPHTHALENES        0                 ND        124.69                       1929.3                      1998.7
                   C4-NAPHTHALENES        0                 ND        236.75                       1157.5                      1241.8
                   BIPHENYL               0.58                        12.20             1          173.0                       177.3
                   ACENAPHTHYLENE         0.64                        10.50             1          2.2                         0.7
                   ACENAPHTHENE           0.54                        7.73              1          14.5                        16.1
                   FLUORENE               0.65                        8.04              1          70.6                        76.9
                   CI-FLUORENES           0                 ND        34.13                        190.6                       212.9






                                                   Antarctic Palmer Fish Samples Aromatic Hydrocarbon Data


                 INVESTC                PROC BLANK                   NIST REF TISSUE              GERG REF OIL 11              GERG REF OIL II
                 ID:                    LAB QA SAMPLE                LAB QA SAMPLE                LAB QA SAMPLE                LAB QA SAMPLE
                 LABSAMNO:              Q4636                        Q4637                        W8022                        W8026
                 UNIT:                  ng/g                         %                            ng/amp                       ng/amp
                 PNA Analyte            Conc              DB QUAL % Recov              DB QUAL Conc                 DB QUAL Conc                 DB QUAL

                 C2-FLUORENES           0                 ND         190.26                       306.8                        321.2
                 C3-FLUORENES           0                 ND         450.2                        410.7                        383.5
                 PHENANTHRENE           0.55              j          33.83                        214.9                        211.3
                 ANTHRACENE             0.32              1          13.89             1          5.0                          4.1
                 CI-PHEN-ANTHR          0                 ND         104.09                       569.9                        534.7
                 C2-PHEN   ANTHR        0                 ND         356.25                       770.2                        743.5
                 C3-PHEN   ANTI-IR      0                 ND         286.52                       761.1                        644.4
                 C4-PHEN-ANTHR          0                 ND         291.58                       441.2                        374.8
                 DIBENZOTHIO            0.54              1          4.12              1          160.4                        151.9
                 CI-DIBEN               0                 ND         37.68                        362.9                        330.8
                 C2-DIBEN               0                 ND         209.95                       551.5                        575.8
                 C3-DIBEN               0                 ND         295.56                       627.3                        574.0
                 FLUORANTFIENE          0.27              j          252.77                       5.3                          4.7
                 PYRENE                 0.32              j          252.16                       13.3                         18.7
                 Cl-FLUORAN-PYR         0                 ND         202.72                       107.1                        92.7
                 BENaANTHRACENE         0.17                         49.31                        5.0                          5.1
                 CHRYSENE               0.30                         101.52                       45.7                         40.9
                 Cl-CHRYSENES           0                 ND         75.23                        91.7                         88.2
                 C2-CHRYSENES           0                 ND         49.61                        145.1                        139.1
                 C3-CHRYSENES           0                 ND         0                 ND         39.1                         40.8
                 C4-CHRYSENES           0                 ND         0                 ND         27.7                         30.2
                 BENbFLUORAN            0.10                         46.46                        3.5                          3.9
                 BENkFLUORAN            0.10                         46.46                        3.5                          3.9
                 BENePYRENE             0.25              1          94.90                        11.4                         11.8
                 BENaPYRENE             0.24              1          15.19             1          1.9                          5.5
                 PERYLENE               9.13                         9.71              1          1.7                          4.3
                 I 123cdPYRENE          0.15                         14.20             1          0.6                          0.9
                 DBahANTHRA             0.05                         2.65              1          1.8                          2.2
                 BghIPERYLENE           0.13                         17.36             1          3.5                          4.1


                 TOTAL PAH's            8.1                          4062.5                       13813.5                      14103.3
                    (W/O PERYLENE)
                 2-METHnMkf)H           0.69              j          15.73                        !090.9                       1128.5
                 I-METHYLNAPH           0.70                         22.16                        953.1                        1055.2






                                                      Antarctic Palmer Fish Samples Aromatic Hydrocarbon Data


                    INVEST#:               PROC BLAW                    NIST REF TISSUE               GERG REF OIL II              GERG REF OIL 11
                    ID:                    LAB QA SAMPLE                LAB QA SAMPLE                 LAB QA SAMPLE                LAB QA SAMPLE
                    LABSAMNO:              Q4636                        Q4637                         W8022                        W8026
                    UNIT:                  ng/g                         %                             ng/arnp                      ng/amp
                    PNA Analyte            Cone              DB QUAL % Recov               1313 QUAL Cone               1313 QUAL Cone               1313 QUAL


                    2.6-DIMETF-INAPH       0.45              j          23.22                         693.4                        713.4


                    2,3.5-TRIMETHNAPH      0.44              j          18.13                         330.8                        330.1


                    I-METHYLPHEN           0.39              j          18.66                         149.3                        154.7


                    Surrogate Recoveries
                    NAPH138:               66.0                         65.0                                            NA                           NA
                    ACENDIO:               56.1                         54.9                                            NA                           NA
                    PHENDIO:               57.8                         67.3                                            NA                           NA
                    CHRYD12:               52.2                         64.5                                            NA                           NA
                    PERYD12,               3.0               Q          33.0                                            NA                           NA




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I
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I           Palmer Fish Pesticides and PCB Data
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                                                      ,Antarctic Palmer Fish Samples Pesticides and PCB Data


                    INVEST#:                  C.NEGLECTA                 CORIICEPS                  C. ACERATUS                N. GIBBERIFRONS
                    ID:                      LOWE ISLAND                 LOWE ISLAND                LOATE ISLAND               DALLMAN BAY
                    LABSAMNO:                J2013                       J2014                      J2015                      J2016
                    UNIT:                               ng/g                       ng/g                       ng/g                             ng/g
                    ,Analyte (Cont)                     Conc DB QUAL               Conc DB QUAL               Conc DB QUAL                     Conc DB QUAL

                    SAMPLE TYPE:                        SAMP                       SAMP                       SAMP                             SAMP
                    COLLECTION DATE:               03/28/92                    03/28/92                   03/28/92                        04/05/92
                    RECEIPT DATE:
                    QCBATCH:                       M827                            M778                       M778                             M778
                    EXTRACTION DATE:            04/26/93
                    METHOD:                            GCFID                       GCFID                      GCFID                            GCFID
                    ANALYSIS DATE:
                    METHOD:                            GCMS                        GCMS,                      GCMS                             GCMS
                    ANALYSIS DATE:              05/24/93                      03/03/93                    03/03/93                       03/03/93
                    METHOD:                          GCECD                      GCECD                      GCECD                           GCECD
                    ANALYSIS DATE:                 06/02/93                   03/15/93                    03/15/93                       03/15/93
                    MATRIX:                          TISSUE                     TISSUE                     TISSUE                          TISSUE
                    SUBMAT:                         MUSCLE                         LIVER                      LIVER                            LIVER
     Co             SAMPLWT:
                    WETWT:                              5.184                      0.727                      0.517                            0.657
                    DRYWT:                              1.26                       0.20                       0.14                             0.25
                    WUNITS:                          GRAMS DRY                  GRAMS DRY                  GRAMS DRY                       GRAMS DRY
                    PCTSOLIDS:
                    VOL:
                    VOLUNITS:                        LITERS                     LITERS                     LITERS                          LITERS

                    TOTAL BHC'S                         0.00 ND                    0.00 ND                    0.00                             0.00 ND
                    TOTAL CHLORDANES,                   0.21 J                     2.73                       0.00  ND                         2.82
                    TOTAL DDT'S                         0.75 J                     8.32                       43.67                            5.69
                    TOTAL PCB'S                         2.3  J                     20.2 J                     48.9  J                          7.7 J

                    ALPHA-BHC                           0.00 ND                    0.00 ND                    0.00  ND                         0.00 ND
                    HCB                                 0.64 J                     1.47                       2.39                             1.45
                    BETA-BHC                            0.00 ND                    0.00 ND                    0.00  ND                         0.00 ND
                    GAMMA-BHC                           0.00 ND                    0.00 ND                    0.00  ND                         0.00 ND
                    DELTA-BHC                           0.00 ND                    0.00 ND                    0.00  ND                         0.00 ND
                    HEPTACHLOR                          0.00 ND                    0.00 ND                    0.00  ND                         0.00 ND
                    HEPTA-EPOXIDE                       0.00 ND                    0.00 ND                    0.00  ND                         0.00 ND
                    OXYCHLORDANE                        0.21 J                     0.00 ND                    0.00  ND                         0.00 ND






                                                       Antarctic Palmer Fish Samples Pesticides and PCB Data


                     INVEST#:                   C.NEGLECTA                CORIICEPS                   C.ACERATUS                N. GIBBERIFRONS
                     ID:                       LOWE ISLAND                LOWE ISLAND                LOWE ISLAND                DALLMAN BAY
                     LABSAMNO:                 J2013                      J2014                      J2015                      J2016
                     UNIT:                               ng/g                       ng/g                       ng/g                            ng/g
                     ,Analyte (Cont)                     Conc DB QUAL               Cone DB QUAL               Conc DB QUAL                    Conc DB QUAL,

                     GAMMA-CHLORDANE                     0.00  ND                   0.00  ND                   0.00  ND                        0.00  ND
                     ALPHA-CHLORDANE                     0.00  ND                   0.00  ND                   5.19  M                         0.00  ND
                     TRANS-NONACHLOR                     0.00  ND                   2.73                       7.79  M                         2.82
                     CIS-NONACHLOR                       0.00  ND                   0.00  ND                   0.00  ND                        0.00  ND
                     ALDRIN                              0.00  ND                   0.00  ND                   0.00  ND                        0.00  ND
                     DIELDRIN                            0.00  ND                   0.00  ND                   0.00  ND                        0.00  ND
                     ENDRIN                              0.00  ND                   0.00  ND                   0.00  ND                        0.00  ND
                     MIREX                               0.00  ND                   0.00  ND                   4.71                            0.00  ND
                     2,4'DDE (0,P'DDE)                   0.00  ND                   0.00  ND                   0.00  ND                        0.00  ND
                     4,4'DDE (P,P'DDE)                   0.00  ND                   0.00  ND                  18.38                            0.00  ND
                     2,4'DDD (O.P'DDD)                   0.00  ND                   0.00  ND                   0.00  ND                        0.86  J
                     4,4'DDD (P,P'DDD)                   0.00  ND                   4.10                      12.95                            3.38
                     2,4'DDT (0,P'DD-n                   0.00  ND                   1.72                       0.00  ND                        0.00  ND
       Co            4,4'DDT (P,P'DDTI                   0.75  J                    2.49                      12.33                            1.45

       00            PCB # (CLORINATION)

                     8 (CL2)                             0.00  ND                   0.00  ND                   0.00  ND                        0.00  ND
                     18 (CL3)                            0.00  ND                   0.00  ND                   0.00  ND                        0.00  ND
                     28 (CL3)                            0.00  ND                   0.00  ND                   0.00  ND                        0.00  ND
                     44 (CIA)                            0.00  ND                   1.19  j                   12.41  J                         0.00  ND
                     52(CLA)                             0.00  ND                   0.00  ND                   0.00  ND                        0.00  ND
                     66 (CIA)                            0.00  ND                   0.00  ND                   0.00  ND                        0.00  ND
                     101 (CL5)                           0.00  ND                   0.00  ND                   0.00  ND                        0.00  ND
                     105 (CL5)                           0.00  ND                   0.00  ND                   0.00  ND                        0.00  ND
                     110/77 (CL5/4)                      0.00  ND                   0.00  ND                   2.62  J                         0.00  ND
                     118/108/149(CL5/5/6)                0.00  ND                   1.44  J                    3.11  J                         0.16  J
                     128 (CL6)                           0.00  ND                   1.67  J                    7.31  J                         0.28  J
                     138 (CL6)                           0.44  J                    0.00  ND                  108.65 M                         0.00  ND
                     126 (CL5)                                 NA                         NA                         NA                              NA
                     153(CL66)                           0.00  ND                   4.33  J                   13.78  J                         0.00  ND
                     170 (CL7)                           0.00  ND                   0.94  J                    0.00  ND                        0.00  ND
                     180 (CL7)                           0.00  ND                   2.57  J                    5.41  J                         2.63  J
                     187/182/159(CL7/7/6)                0.00  ND                   1.37  J                    6.27  J                         0.89  J






                                                       Antarctic Palmer Fish Samples Pesticides and PCB Data


                     INVEST#:                  C.NEGLECTA                 CORI]CEPS                   C.ACERATUS                N. GIBBERIFRONS
                     ID:                      LOWE ISLAND                 LOWE ISLAND                LOWE ISLAND                DALLMAN BAY
                     LABSAMNO:                J2013                       J2014                      J2015                      J2016
                     UNIT:                               ng/g                       ng/g                       ng/g                            ng/g
                     ,Analyte (Cont)                     Conc DB QUAL               Conc DB QUAL               Conc DB QUAL                    Conc DB QUAL.

                     195 (CL8)                           0.00 ND                    0.00 ND                    0.00 ND                         0.00 ND
                     206(CL9)                            0.00  ND                   0.00  ND                   0.00  ND                        0.00  ND
                     209 (CLIO)                          0.00  ND                   0.00  ND                   0.00  ND                        0.00  ND


                     Surrogate Recoveries
                     DBOFB%:                             66.3                       33.5                       28.7                            30.8
                     PCB#103%:                           69.3                       69.0                       53.6                            63.2
                     PCB#198%:                           79.2                       59.8                       43.4                            55.9


                     PCB #(CHLORINATION)

                     7 (CL2)                             0.00  ND                   0.00  ND                   0.00  ND                        0.00  ND
                     15 (CL2)                            0.00  ND                   0.00  ND                   0.00  ND                        0.00  ND
                     24 (CL3)                            0.00  ND                   0.00  ND                   0.00  ND                        0.00  ND
                     16/32 (CL3)                         0.00  ND                   0.00  ND                   0.00  ND                        0.00  ND
                     29 (CL3)                            0.00  ND                   0.00  ND                   0.00  ND                        0.52  J
                     26(CL3)                             0.00  ND                   0.00  ND                   0.00  ND                        0.00  ND
                     25 (CW)                             0.00  ND                   0.00  ND                   0.00  ND                        0.00  ND
                     50 (CIA)                            0.00  ND                   0.00  ND                   0.00  ND                        0.00  ND
                     3 1 (C L,3)                         0.00  ND                   0.00  ND                   0.00  ND                        0.00  ND
                     33 (CL3)                            0.00  ND                   0.00  ND                   0.00  ND                        0.00  ND
                     22 (CL3)                            0.00  ND                   0.00  ND                   0.00  ND                        0.00  ND
                     45 (CIA)                            0.00  ND                   0.00  ND                   0.00  ND                        0.00  ND
                     46 (CIA)                            0.44  J                    1.22  J                    5.72  J                         0.00  ND
                     49 (CIA)                            0.00  ND                   0.83  J                    0.00  ND                        0.52  J
                     47/48 (CIA)                         0.56  J                    0.00  ND                   0.00  ND                        0.00  ND
                     37/42 (CIA)                         0.00  ND                   0.00  ND                   0.00  ND                        0.00  ND
                     41/64 (CIA)                         0.00  ND                   0.00  ND                   0.00  ND                        0.00  ND
                     40 (CIA)                            0.00  ND                   0.00  ND                   0.00  ND                        0.00  ND
                     100 (CL5)                           0.00  ND                   0.00  ND                   0.00  ND                        0.00  ND
                     74 (CIA)                            0.00  ND                   0.00  ND                   0.00  ND                        0.00  ND
                     70 (CIA)                            0.00  ND                   0.00  ND                   0.00  ND                        0.00  ND
                     88 (CL5)                            0.00  ND                   0.00  ND                   0.00  ND                        0.00  ND
                     60/56 (CL5)                         0.00  ND                   0.00  ND                   0.00  ND                        0.00  ND






                                                            Antarctic Palmer Fish Samples Pesticides and PCB Data


                        INVEST#:                   C.NEGLECTA                   CORIICEPS                    C.ACERATUS                  N. GIBBERIFRONS
                        ID:                       LOWE ISLAND                   LOWE ISLAND                 LOWE ISLAND                  DALLMAN BAY
                        LABSAMNO:                 J2013                         J2014                       J2015                        J2016
                        UNIT:                                 ng/g                         ng/g                        ng/g                              ng/g
                       ,Analyte (Cont)                        Cone DB QUAL,                Conc DB QUAL                Conc DB QUAL,                     Conc DB QUAL

                        92? (CL5)                             0.00  ND                     0.00  ND                    0.00   ND                         0.00  ND
                        84? (CL5)                             0.00  ND                     0.00  ND                    0.00   ND                         0.00  ND
                        99 (CL5)                              0.00  ND                     1.15  1                     2.41   j                          0.00  ND
                        83 (CL5)                              0.00  ND                     0.00  ND                    0.00   ND                         0.00  ND
                        97 (CL5)                              0.00  ND                     0.00  ND                    0.00   ND                         0.00  ND
                        87 (CL5)                              0.00  ND                     0.00  ND                    8.97   J                          0.00  ND
                        85 (CL5)                              0.00  ND                     0.00  ND                    0.00   ND                         0.00  ND
                        136 (CL6)                             0.00  ND                     0.00  ND                    0.00   ND                         0.00  ND
                        82 (CL5)                              0.00  ND                     0.00  ND                    0.00   ND                         0.00  ND
                        151 (CL6)                             0.00  ND                     0.00  ND                    0.00   ND                         0.38  ND
                        107/108/144(CL5/5/6)                  0.00  ND                     1.06  J                     3.99   1                          0.88  J
                        149 (CL6)                             0.00  ND                     0.47  J                     2.34   J                          0.30  J
                        188 (CL7)                             0.00  ND                     0.00  ND                    0.00   ND                         0.00  ND
                        146 (CL6)                             0.00  ND                     0.00  ND                    0.00   ND                         1.27  J
         CO             141 (CL6)                             0.00  ND                     0.00  ND                    0.00   ND                         0.00  ND
         to             137 (CL6)                             0.00  ND                     0.00  ND                    0.00   ND                         0.00  ND
                        UNK (CL6)                             0.00  ND                     0.00  ND                    0.00   ND                         0.00  ND
                        158(CL7)                              0.00  ND                     0.00  ND                    0.00   ND                         0.00  ND
                        129 (CL6)                             0.00  ND                     0.00  ND                    0.00   ND                         0.00  ND
                        178(CL7)                              0.00  ND                     0.00  ND                    0.00   ND                         0.00  ND
                        183 (CL7)                             0.85  J                      1.79  J                     0.00   ND                         0.00  ND
                        167 (CL6)                             0.00  ND                     0.00  ND                    0.00   ND                         0.00  ND
                        185 (CL7)                             0.00  ND                     0.00  ND                    0.00   ND                         0.00  ND
                        174 (CL7)                             0.00  ND                     0.00  ND                    0.00   ND                         0.00  ND
                        177(CL7)                              0.00  ND                     0.00  ND                    0.00   ND                         0.00  ND
                        156/171/202(CL6/7/8)                  0.00  ND                     7.80  J                     0.00   ND                         2.20  J
                        200 (CL8)                             0.00  ND                     0.00  ND                    0.00   ND                         0.00  ND
                        172 (CL7)                             0.00  ND                     1.58  J                     0.00   ND                         1.17  J
                        191 (CL7)                             0.00  ND                     0.00  ND                    0.00   ND                         0.00  ND
                        201 (CL8)                             0.00  ND                     0.00  ND                    0.00   ND                         0.00  ND
                        196 (CL-8)                            0.00  ND                     0.00  ND                    0.00   ND                         0.00  ND
                        189 (CL7)                             0.00  ND                     0.00  ND                    0.00   ND                         0.00  ND
                        194 (CI,8)                            0.00  ND                     0.00  ND                    0.00   ND                         0.00  ND
                        205 (CL9)                             0.00  ND                     0.00  ND                    0.00   ND                         0.00  ND






                                                        Antarctic Palmer Fish Samples Pesticides and PCB Data


                 INVEST#:                 N. GIBBERIFRONS,                 CORIICEPS                     CORIICEPS                     CORIICEPS
                 ID:                      DALLMAN BAY                     BAHIA PARAISO                  BAHIA PARAISO                 PALMER STATION
                 IABSAMNO:                J2017                           J2018                         J2019                          J2020
                 UNIT:                                    ng/g                          ngfg                          ng/g                             ng/g
                 [Analyte (Cont)                          Conc DB QUAL                  Conc D13 QUAL                 Conc D13 QUAL                    Conc DB QUAL,

                 SAMPLE IWE:                             SAMP                           SAMP                          SAMP                             SAMP
                 COLLECTION DATE:                    04/05/92                      04/22/92                      04/22/92                         03/29/92
                 RECEIPT DATE:
                 QCBATCH:                         M827                                  M778                   M827                                    M778
                 EXTRACTION DATE:               04/26/93                                                     04/26/93
                 METHOD:                                GCFID                           GCFID                        GCFID                            GCFID
                 ANALYSIS DATE:
                 METHOD:                                 GCMS,                          GCMS                         GCMS                             GCMS
                 ANALYSIS DATE:                 05/24/93                           03/03/93                  05/24/93                             03/03/93
                 METHOD:                               GCECD                         GCECD                         GCECD                             GCECD
                 ANALYSIS DATE:                      06/02/93                      03/15/93                       06/02/93                        03/15/93
                 MATRIX:                               TISSUE                        TISSUE                        TISSUE                            TISSUE
                 SUBMAT:                              MUSCLE                            LIVER                      MUSCLE                             LIVER
                 SAMPLWT:
                 WETWT:                                  5.034                          0.514                         5.196                            0.501
                 DRYWT:                                   1.06                          0.17                          1.17                             0.18
                 VvTUNITS:                             GRAMS DRY                     GRAMS DRY                     GRAMS DRY                        GRAMS DRY
                 PCTSOLIDS:
                 VOL:
                 VOLUNITS:                             LITERS                        LITERS                        LrTERS,                           LITERS

                 TOTAL BHC'S                              0.00 ND                       0.00  ND                      0.00  ND                         0.00  ND
                 TOTAL CHLORDANES                         0.00 ND                       1.35                          0.00  ND                         0.00  ND
                 TOTAL DDT"S                              0.00 ND                       6.45                          0.00  ND                         0.00  ND
                 TOTAL PCB'S                              0.1  1                          9.3 J                         2.7 J                            0.0 ND

                 ALPHA-BHC                                0.00 ND                       0.00  ND                      0.00  ND                         0.00  ND
                 HCB                                      0.00 ND                       0.80  J                       0.27  J                          0.00  ND
                 BETA-BHC                                 0.00 ND                       0.00  ND                      0.00  ND                         0.00  ND
                 GAMMA-BHC                                0.00 ND                       0.00  ND                      0.00  ND                         0.00  ND
                 DELTA-BHC                                0.00 ND                       0.00  ND                      0.00  ND                         0.00  ND
                 HEPTACHLOR                               0.00 ND                       0.00  ND                      0.00  ND                         0.00  ND
                 HEPTA-EPOXIDE                            0.00 ND                       0.00  ND                      0.00  ND                         0.00  ND
                 OXYCHLORDANE                             0.00 ND                       0.00  ND                      0.00  ND                         0.00  ND






                                                       Antarctic Palmer Fish Samples Pesticides and PCB Data


                 INVEST#:                 N. GIBBERIFRONS                CORUCEPS                     CORUCEPS                      CORIICEPS
                 ID:                      DALLMAN BAY                    BAHIA PARAISO                BAHIA PARAISO                 PALMER STATION
                 LABSAMNO:                J2017                          J2018                        J2019                         J2020
                 UNIT:                                  ng/g                          ng/g                         ng/g                            ng/g
                 Analyte (Cont)                         Conc DB QUAL                  Conc 1313 QUAL               Conc DB QUAL                    Conc DB QUAL,

                 GAMMA-CHLORDANE                        0.00  ND                      0.00 ND                      0.00  ND                        0.00  ND
                 ALPHA-CHLORDANE                        0.00  ND                      0.00 ND                      0.00  ND                        0.00  ND
                 TRANS-NONACHLOR                        0.00  ND                      1.35                         0.00  ND                        0.00  ND
                 CIS-NONACHLOR                          0.00  ND                      0.00 ND                      0.00  ND                        0.00  ND
                 ALDRIN                                 0.00  ND                      0.00 ND                      0.08  1                         0.00  ND
                 DIELDRIN                               0.00  ND                      0.00 ND                      0.00  ND                        0.00  ND
                 ENDRIN                                 0.00  ND                      0.00 ND                      0.00  ND                        0.00  ND
                 MIREX                                  0.00  ND                      0.00 ND                      0.00  ND                        0.00  ND
                 2,4'DDE (0,P'DDE)                      0.00  ND                      0.00 ND                      0.00  ND                        0.00  ND
                 4.4'DDE (P,P'DDE)                      0.00  ND                      6.11                         0.00  ND                        0.00  ND
                 2,4'DDD (0,P'DDD)                      0.00  ND                      0.00 ND                      0.00  ND                        0.00  ND
                 4,4'DDD (P,P'DDD)                      0.00  ND                      0.00 ND                      0.00  ND                        0.00  ND
                 2,4'DDT (0,P'DErn                      0.00  ND                      0.34 J                       0.00  ND                        43.66 M
                 4.4'DDT (P,P'DErn                      0.00  ND                      0.00 ND                      0.00  ND                        0.00  ND


                 PCB # (CLORINATION)


                 8 (CL2)                                0.03  ND                      0.00 ND                      0.06  J                         0.00  ND
                 18 (CL3)                               0.00  ND                      0.00 ND                      0.00  ND                        0.00  ND
                 28 (CL3)                               0.11  1                       0.00 ND                      0.32  J                         0.00  ND
                 44 (CIA)                               0.00  ND                      2.95 J                       0.00  ND                        0.00  ND
                 52 (CIA)                               0.00  ND                      0.00 ND                      0.00  ND                        0.00  ND
                 66 (CIA)                               0.00  ND                      0.00 ND                      0.00  ND                        0.00  ND
                 101 (CL5)                              0.00  ND                      0.00 ND                      0.00  ND                        0.00  ND
                 105 (CL5)                              0.00  ND                      0.00 ND                      0.00  ND                        0.00  ND
                 110/77 (CL5/4)                         0.00  ND                      0.00 ND                      0.00  ND                        0.00  ND
                 118/108/149(CL5/5/6)                   0.00  ND                      0.00 ND                      0.00  ND                        0.00  ND
                 128 (CL6)                              0.00  ND                      0.00 ND                      0.00  ND                        0.00  ND
                 138 (CL6)                              0.00  ND                      0.00 ND                      0.84  J                         0.00  1
                 126 (CL5)                                    NA                           NA                            NA                              NA
                 153 (CL6)                              0.00  ND                      0.00 ND                      0.00  ND                        0.00  M
                 170 (CL7)                              0.00  ND                      0.00 ND                      0.00  ND                        0.00  ND
                 180 (CL71                              0.00  ND                      1.33 J                       0.00  ND                        0.00  ND
                 187/182/159(CL7/7/6)                   0.00  ND                      0.00 ND                      0.00  ND                        0.00  ND



   M M M M M M M M M M M M M M M M M M @

                                                            Antarctic Palmer Fish Samples Pesticides and PCB Data


                  INVEST#:                   N. GIBBERIFRONS                   CORIICEPS                       CORIICEPS                       CORIICEPS
                  ID:                        DALLMAN BAY                       BAHIA PARAISO                   BAHIA PARAISO                   PALMER STATION
                  LABSAMNO:                  J2017                            J2018                            J2019                           J2020
                  UNIT:                                      ng/g                            ng/g                            ng/g                               ng/g
                  [Analyte (Cont)                            Conc D13 QUAL                   Conc DB QUAL                    Conc 1313 QUAL                     Conc 1313 QUAL

                  195 (CL8)                                  0.00 ND                         0.00 ND                         0.00 ND                            0.00 ND
                  206 (CL9)                                  0.00  ND                        0.00  ND                        0.00  ND                           0.00  ND
                  209 (CLIO)                                 0.00  ND                        0.00  ND                        0.00  ND                           0.00  ND

                  Surrogate Recoverles
                  DBOFB%:                                    73.9                            33.0                            71.5                               35.2
                  PCB#103%:                                  79.3                            66.1                            76.8                              111.9
                  PCB#198%:                                  64.7                            58.2                            69.9                               87.4


                  PCB #(CHLORINATION)

                  7 (CL2)                                    0.00  ND                        0.00  ND                        0.00  ND                           0.00  ND
                  15 (CL2)                                   0.00  ND                        0.00  ND                        0.14  J                            0.00  ND
                  24 (CL3)                                   0.00  ND                        0.00  ND                        0.00  ND                           0.00  ND
                  16/32 (CL3)                                0.00  ND                        0.00  ND                        0.00  ND                           0.00  ND
        w         29 (CL3)                                   0.00  ND                        0.00  ND                        0.00  ND                           0.00  ND
                  26 (CL3)                                   0.00  ND                        0.00  ND                        0.00  ND                           0.00  ND
                  25 (CW)                                    0.00  ND                        0.00  ND                        0.00  ND                           0.00  ND
                  50 (CIA)                                   0.00  ND                        0.00  ND                        0.00  ND                           0.00  ND
                  31 (CL3)                                   0.00  ND                        0.00  ND                        0.00  ND                           0.00  ND
                  33 (CL,3)                                  0.00  ND                        0.00  ND                        0.00  ND                           0.00  ND
                  22 (CL3)                                   0.00  ND                        0.00  ND                        0.00  ND                           0.00  ND
                  45 (CL4)                                   0.00  ND                        0.00  ND                        0.00  ND                           0.00  M
                  46 (CIA)                                   0.00  ND                        0.00  ND                        0.00  ND                           0.00  M
                  49 (CIA)                                   0.00  ND                        0.00  ND                        0.00  ND                           0.00  ND
                  47/48 (CIA)                                0.00  ND                        0.00  ND                        0.05  J                            0.00  ND
                  37/42 (CIA)                                0.00  ND                        0.00  ND                        0.00  ND                           0.00  ND
                  41/64 (CIA)                                0.00  ND                        0.00  ND                        0.00  ND                           0.00  ND
                  40 (CIA)                                   0.00  ND                        0.00  ND                        0.00  ND                           0.00  ND
                  100 (CL5)                                  0.00  ND                        0.00  ND                        0.00  ND                           0.00  ND
                  74 (CIA)                                   0.00  ND                        0.00  ND                        0.00  ND                           0.00  ND
                  70 (CIA)                                   0.00  ND                        0.00  ND                        0.00  ND                           0.00  ND
                  88 (CL5)                                   0.00  ND                        0.00  ND                        0.15  J                            0.00  M
                  60/56 (CL5)                                0.00  ND                        0.00  ND                        0.00  ND                           0.00  ND






                                                         Antarctic Palmer Fish Samples Pesticides and PCB Data


                 INVEST#:                  N. GIBBERIFRONS                  CORIICEPS                     CORIICEPS                      CORIICEPS
                 ID:                       DALLMAN BAY                      BAHIA PARAISO                 BAHIA PARAISO                  PALMER STATION
                 LABSAMNO:                 J2017                           J2018                          J2019                          J2020
                 UNIT:                                    ng/g                           ng/g                           ng/g                             ng/g
                 Analyte (Cont)                           Conc DB QUAL                   Conc DB QUAL                   Conc DB QUAL                     Conc DB QUAL,

                 92? (CL5)                                0.00   ND                      0.00  ND                       0.00  ND                         0.00  ND
                 84? (CL5)                                0.00   ND                      0.00  ND                       0.00  ND                         0.00  ND
                 99 (CL5)                                 0.00   ND                      0.00  ND                       0.00  ND                         0.00  ND
                 83 (CL5)                                 0.00   ND                      0.00  ND                       0.00  ND                         0.00  ND
                 97 (CL5)                                 0.00   ND                      0.00  ND                       0.00  ND                         0.00  ND
                 87 (CI-5)                                0.00   ND                      0.00  ND                       0.00  ND                         0.00  ND
                 85 (CL5)                                 0.00   ND                      0.00  ND                       0.00  ND                         0.00  ND
                 136 (CL6)                                0.00   ND                      0.00  ND                       0.00  ND                         0.00  ND
                 82 (CL5)                                 0.00   ND                      0.00  ND                       0.00  ND                         0.00  ND
                 151 (CL6)                                0.00   ND                      0.00  ND                       0.00  ND                         0.00  ND
                 107/108/144(CL5/5/6)                     0.00   ND                      1.95  J                        0.00  ND                         0.00  M
                 149 (CL6)                                0.00   ND                      0.00  ND                       0.00  ND                         0.00  ND
                 188 (CL7)                                0.00   ND                      0.00  ND                       0.56  J                          0.00  ND
                 146 (CL6)                                0.00   ND                      0.00  ND                       0.00  ND                         0.00  ND
                 141 (CL6)                                0.00   ND                      0.00  ND                       0.00  ND                         0.00  ND
                 137 (CL6)                                0.00   ND                      0.00  ND                       0.00  ND                         0.00  ND
                 UNK (CL66)                               0.00   ND                      0.00  ND                       0.00  ND                         0.00  ND
                 158 (CL7)                                0.00   ND                      0.00  ND                       0.00  ND                         0.00  ND
                 129 (CL6)                                0.00   ND                      0.00  ND                       0.57  J                          0.00  ND
                 178 (CL7)                                0.00   ND                      0.00  ND                       0.00  ND                         0.00  ND
                 183 (CL7)                                0.00   ND                      0.00  ND                       0.00  ND                         0.00  M
                 167 (CL6)                                0.00   ND                      0.00  ND                       0.00  ND                         0.00  ND
                 185 (CL7)                                0.00   ND                      0.00  ND                       0.00  ND                         0.00  ND
                 174 (CL7)                                0.00   ND                      0.00  ND                       0.00  ND                         0.00  ND
                 177 (CL7)                                0.00   ND                      0.00  ND                       0.00  ND                         0.00  ND
                 156/171/202(CL6/7/8)                     0.00   ND                      4.42  J                        0.00  ND                         0.00  ND
                 200 (CL8)                                0.00   ND                      0.00  ND                       0.00  ND                         0.00  ND
                 172 (CL7)                                0.00   ND                      0.00  ND                       0.00  ND                         0.00  ND
                 191 (CL7)                                0.00   ND                      0.00  ND                       0.00  ND                         0.00  ND
                 201 (CL8)                                0.00   ND                      0.00  ND                       0.00  ND                         0.00  ND
                 196 (CL8)                                0.00   ND                      0.00  ND                       0.00  ND                         0.00  ND
                 189 (CL7)                                0.00   ND                      0.00  ND                       0.00  ND                         0.00  ND
                 194 (CL8)                                0.00   ND                      0.00  ND                       0.00  ND                         0.00  ND
                 205 ("CL9)                               0.00   ND                      0.00  ND                       0.00  ND                         0.00  ND






                                                          Antarctic Palmer Fish Samples Pesticides and PCB Data


                 INVEST#:                   CORIICEPS                       CORIICEPS                    PROC BLANK                     CORIICEPS
                 ID:                       PALMER STATION                  LAB QA SAMPLE                 LAB QA SAMPLE                 LAB QA SAMPLE
                 LABSAMNO:                 J2021                           Q4609                         Q4610                         Q4611
                 UNIT:                                    ng/g                          ng/g                          ng/g                              %
                 ,Analyte (Cont)                          Conc DB QUAL                  Conc DB QUAL                  Conc DB QUAL               % Recov DB QUAL,

                 SAMPLE TYPE:                             SAMP              DUPE OF J2013                    PROC BI.AM                    MS OF J2013
                 COLLECTION DATE:                     03/29/92                      03/28/92                                                    03/28/92
                 RECEIPT DATE:
                 QCBAT`CH:                         M827                                 M778                          M778                          M778
                 EXTRACTION DATE:                04/26/93
                 METHOD:                                  GCFID                         GCFID                         GCFID                         GCFID
                 ANALYSIS DATE:
                 METHOD:                                  GCMS                          GCMS                          GCMS                          GCMS
                 ANALYSIS DATE:                  05/24/93                           03/03/93                      03/03/93                      03/03/93
                 METHOD:                                  GCECD                      GCECD                         GCECD                          GCECD
                 ANALYSIS DATE:                       06/02/93                      03/15/93                      03/15/93                      03/15/93
                 MATRIX:                                  TISSUE                     TISSUE                        TISSUE                         TISSUE
                 SUBMAT:                               MUSCLE                        MUSCLE                                                      MUSCLE
                 SAMPLWT:
                 WETWT:                                   5.044                         0.668                                                       0.551
                 DRYWT:                                   1.28                          0.18                          10.00                         0.13
                 WTUNITS:                                 GRAMS DRY                  GRAMS DRY                     GRAMS DRY                     GRAMS DRY
                 PCTSOLIDS:
                 VOL:
                 VOLUNITS:                                LITERS                     LITERS                        LITERS                          LITERS


                 TOTAL BHC'S                              0.00  ND                      0.00  ND                      0.00  ND                            NA
                 TOTAL CHLORDANES                         0.44  J                       0.00  ND                      0.00  ND                            NA
                 TOTAL DDT"S                              1.22                          0.00  ND                      3.26                                NA
                 TOTAL PCB'S                              12.2                            9.1                           9.7                               NA


                 ALPHA-BHC                                0.00  ND                      0.00  ND                      0.00  ND                      41.0
                 HCB                                      0.34  J                       1.48                          0.00  ND                      15.0
                 BETA-BHC                                 0.00  ND                      0.00  ND                      0.00  ND                      12.0
                 GAMMA-BHC                                0.00  ND                      0.00  ND                      0.00  ND                      52.0
                 DELTA-BHC                                0.00  ND                      0.00  ND                      0.00  ND                      41.0
                 HEPTACHLOR                               0.10  1                       0.00  ND                      0.00  ND                      65.0
                 HEPTA-EPOXIDE                            0.00  ND                      0.00  ND                      0.00  ND                      66.0
                 OXYCHLORDANE                             0.14  J                       0.00  ND                      0.00  ND






                                                       Antarctic Palmer Fish Samples Pesticides and PCB Data


                 INVEST#:                 CORIICEPS                       CORIICEPS                    PROC BLANK                     CORIICEPS
                 ID:                      PALMER STATION                  LAB QA SAMPLE                LAB QA SAMPLE                 LAB QA SAMPLE
                 LABSAMNO:                J2021                           Q4609                        Q4610                         Q4611
                 UNIT:                                   ng/g                          ng/g                         ng/g                              %
                 Analyte (Cont)                          Conc DB QUAL                  Conc DB QUAL                 Conc 1313 QUAL             % Recov DB QUAL

                 GAMMA-CHLORDANE                         0.00  ND                      0.00  ND                     0.00   ND                     65.0
                 ALPHA-CHLORDANE                         0.00  ND                      0.00  ND                     0.00   ND                     66.0
                 TRANS-NONACHLOR                         0.20  J                       0.00  ND                     0.00   ND                     62.0
                 CIS-NONACHLOR                           0.00  ND                      0.00  ND                     0.00   ND
                 ALDRIN                                  0.14  J                       0.00  ND                     0.00   ND                     60.0
                 DIELDRIN                                0.00  ND                      0.00  ND                     0.00   ND                     61.0
                 ENDRIN                                  0.00  ND                      0.00  ND                     0.00   ND                     53.0
                 MIREX                                   0.00  ND                      0.00  ND                     0.00   ND                     87.0
                 2,4'DDE (O,P'DDE)                       0.00  ND                      0.00  ND                     0.00   ND                     52.0
                 4,4'DDE (P,P'DDE)                       0.00  ND                      0.00  ND                     3.26                          26.0
                 2,4'DDD (0,P'DDD)                       0.00  ND                      0.00  ND                     0.00   ND                     82.0
                 4,4'DDD (P,P'DDD)                       0.00  ND                      0.00  ND                     0.00   ND                     55.0
                 2,4'DDT (0,P'DM                         0.00  NDD                     0.00  ND                     0.00   ND                       5.0
                 4,4'DDT (P,P'DDD                        1.22                          0.00  ND                     0.00   ND                     51.0
        w
        t,D
        0)       PC13 # (CLORINATION)

                 8 (CL2)                                 0.00  ND                      0.00  ND                     0.00   ND                     76.0
                 18 (CL3)                                0.00  ND                      0.00  ND                     0.00   ND                     40.0
                 28 (CL3)                                0.14  J                       0.00  ND                     0.00   ND                     87.0
                 44 (CIA)                                0.34  J                       0.00  ND                     1.72                          92.0
                 52 (CIA)                                0.00  ND                      0.00  ND                     0.00   ND                     97.0
                 66 (CIA)                                0.00  ND                      0.00  ND                     0.00   ND                    142.0
                 101 (CL5)                               0.00  ND                      0.00  ND                     0.00   ND                     77.0
                 105 (CL5)                               0.46  J                       0.00  ND                     0.00   ND                    117.0
                 110/77 (CL,5/4)                         0.00  ND                      0.00  ND                     0.00   ND                     63.0
                 118/108/149(CL5/5/6)                    1.80                          0.00  ND                     0.00   ND                    114.0
                 128 (CL6)                               0.20  J                       0.00  ND                     0.00   ND                     96.0
                 138 (CL6)                               3.11                          0.00  ND                     0.00   ND                     87.0
                 126 (CL5)                                     NA                            NA                            NA                           NA
                 153 (CL6)                               3.14                          0.00  ND                     0.00   ND                     75.0
                 170 (CL7)                               0.00  ND                      0.00  ND                     0.00   ND                     77.0
                 180 (CL7)                               3.16                          0.79  J                      1.41                          76.0
                 187/182/159(CL7/7/6)                    2.53                          0.84  J                      0.00   ND                     73.0






                                                            Antarctic Palmer Fish Samples Pesticides and PCB Data


                   INVEST#:                   CORIICEPS,                         CORIICEPS                       PROC BLANK                       CORIICEPS
                   ID:                        PALMER STA71ON                     LAB QA SAMPLE                   LAB QA SAMPLE                    LAB QA SAMPLE
                   LABSAMNO:                  J2021                              Q4609                           Q4610                            Q4611
                   UNIT:                                       ng/g                            ng/g                             ng/g                                %
                  ,Analyte (Cont)                              Conc DB QUAL                    Conc DB QUAL                     Conc DB QUAL                % Recov DB QUAL,

                   195 (CL8)                                   0.00 ND                         0.00 ND                          0.00 ND                         77.0
                   206 (CL9)                                   0.00  ND                        0.00   ND                        0.26   J                        65.0
                   209 (CLIO)                                  0.00  ND                        0.00   ND                        0.00   ND                       67.0

                   Surrogate Recoveries
                   DBOFB%:                                     79.6                            27.1                             26.9                            31.0
                   PCB#103%:                                   83.8                            58.8                             61.1                            65.9
                   PCB#198%:                                   64.5                            50.3                             53.0                            50.8


                   PCB #(CHLORINA110N)

                   7 (CL2)                                     0.00  ND                        0.97   J                         0.00   ND                              NA
                   15 (CL2)                                    0.00  ND                        0.00   ND                        0.00   ND                              NA
                   24 (CL3)                                    0.00  ND                        0.00   ND                        0.00   ND                              NA
                   16/32 (CL3)                                 0.00  ND                        0.00   ND                        0.00   ND                              NA
                   29 (CL3)                                    0.12  J                         0.00   ND                        0.00   ND                              NA
                   26 (CL3)                                    0.00  ND                        0.00   ND                        0.00   ND                              NA
                   25 (CI.3)                                   0.00  ND                        0.00   ND                        0.00   ND                              NA
                   50 (CIA)                                    0.00  ND                        0.00   ND                        0.00   ND                              NA
                   31 (CI.3)                                   0.00  ND                        0.00   ND                        0.00   ND                              NA
                   33 (CL3)                                    0.00  ND                        0.00   ND                        0.00   ND                              NA
                   22 (CL3)                                    0.00  ND                        0.00   ND                        0.00   ND                              NA
                   45 (CIA)                                    0.00  ND                        0.00   ND                        0.00   ND                              NA
                   46 (CIA)                                    0.00  ND                        0.00   ND                        0.00   ND                              NA
                   49 (CIA)                                    0.31  J                         0.69   J                         0.00   ND                              NA
                   47/48 (CL4)                                 0.25  J                         0.00   ND                        0.00   ND                              NA
                   37/42 (CIA)                                 0.00  ND                        0.00   ND                        0.00   ND                              NA
                   41/64 (CIA)                                 0.00  ND                        0.00   ND                        0.00   ND                              NA
                   40 (CIA)                                    0.00  ND                        0.00   ND                        0.00   ND                              NA
                   100 (CL5)                                   0.00  ND                        0.00   ND                        0.00   ND                              NA
                   74 (CIA)                                    0.31  J                         0.00   ND                        0.00   ND                              NA
                   70 (CIA)                                    0.00  ND                        0.00   ND                        0.00   ND                              NA
                   88 (CL5)                                    0.17  J                         0.00   ND                        0.00   ND                              NA
                   60/56 (CL5)                                 0.00  ND                        0.00   ND                        0.00   ND                              NA






                                                        Antarctic Palmer Fish Samples Pesticides and PCB Data


                 INVEST#:                  CORIICEPS                       CORIICEPS                     PROC BI-AM                    CORIICEPS
                 ID:                       PALMER STATION                  LAB QA SAMPLE                 LAB QA SAMPLE                 LAB QA SAMPLE
                 LABSAMNO:                J2021                            Q4609                         Q4610                         Q4611
                 UNIT:                                    ng/g                          ng/g                          ng/g                             %
                 ,Analyte (Cont)                          Conc DB QUAL                  Conc DB QUAL                  Conc DB QUAL               % Recov DB QUAL

                 92? (CL5)                                0.00  ND                      0.00  ND                      0.00  ND                            NA
                 84? (CL5)                                0.00  ND                      0.00  ND                      0.00  ND                            NA
                 99 (CL5)                                 1.00  1                       0.00  ND                      0.00  ND                            NA
                 83 (CL5)                                 0.00  ND                      0.00  ND                      0.00  ND                            NA
                 97 (CL5)                                 0.00  ND                      0.00  ND                      0.00  ND                            NA
                 87 (CL5)                                 0.00  ND                      0.00  ND                      0.00  ND                     105.0
                 85 (CL5)                                 0.00  ND                      0.00  ND                      0.00  ND                            NA
                 136 (CL6)                                0.00  ND                      0.00  ND                      0.00  ND                            NA
                 82 (CL5)                                 0.00  ND                      0.00  ND                      0.00  ND                            NA
                 151 (CL6)                                0.23  J                       0.00  ND                      0.00  ND                            NA
                 107/108/144(CL5/5/6)                     0.00  ND                      1.75                          0.00  ND                            NA
                 149 (CL6)                                1.03  J                       0.00  ND                      0.00  ND                            NA
                 188 (CL7)                                0.00  ND                      0.00  ND                      0.00  ND                            NA
                 146 (CL6)                                0.00  ND                      0.00  ND                      0.00  ND                            NA
                 141 (CL6)                                0.00  ND                      0.00  ND                      0.00  ND                            NA
       00        137 (CL6)                                0.00  ND                      1.78                          0.00  ND                            NA
                 UNK (CL6)                                0.00  ND                      0.00  ND                      0.00  ND                            NA
                 158 (CL7)                                0.21  J                       0.00  ND                      0.00  ND                            NA
                 129 (CL6)                                0.00  ND                      0.00  ND                      0.00  ND                            NA
                 178 (CL7)                                0.00  ND                      0.00  ND                      0.00  ND                            NA
                 183 (CL7)                                0.77  J                       0.00  ND                      0.00  ND                            NA
                 167 (CL6)                                0.00  ND                      0.00  ND                      0.00  ND                            NA
                 185 (CL7)                                0.00  ND                      0.00  ND                      0.00  ND                            NA
                 174 (CL7)                                0.45  J                       0.00  ND                      0.00  ND                            NA
                 177 (CL7)                                0.33  J                       0.00  ND                      0.00  ND                            NA
                 156/171/202(CL6/7/8)                     0.00  ND                      2.28                          6.20                                NA
                 200 (CLB)                                0.00  ND                      0.00  ND                      0.00  ND                            NA
                 172 (CL7)                                0.00  ND                      1.60                          1.78                                NA
                 191 (CL7)                                0.00  ND                      0.00  ND                      0.00  ND                            NA
                 201 (CL8)                                0.34  J                       0.00  ND                      0.00  ND                            NA
                 196 (CL8)                                0.61  J                       0.00  ND                      0.00  ND                            NA
                 189 (CL7)                                0.00  ND                      0.00  ND                      0.00  ND                            NA
                 194 (CL8)                                0.00  ND                      0.00  ND                      0.00  ND                            NA
                 205 (CL9)                                0.00  ND                      0.00  ND                      0.00  ND                            NA





                                                       Antarctic Palmer Fish Samples Pesticides and PCB Data


                           INVEST#:                 NIST REF TISSUE                              CINDER CONES                 CINDER CONES
                           ID:                      LAB QA SAMPLE                                REPL. I                      REPL.2
                           LABSAMNO:                Q4612                                        J2022                        J2023
                           UNIT:                                   ng/g                                      ng/g                         ng/g
                           Analyte (Cont)                          Conc DB QUAL                              Conc DB QUAL                 Conc DB QUAL

                           SAMPLE TYPE:                       REF NIST                  REF OIL              SAMP,                        SAMP
                           COLLECTION DATE:                                                              12/05/91                     12/05/91
                           RECEIPT DATE:
                           QCBATCH:                                M778                     M778        M779                         M779
                           EXTRACTION DATE:
                           METHOD:                                 GCFID                  GCFID              GCFID                        GCFID
                           ANALYSIS DATE:
                           METHOD:                                 GCMS                    GCMS              GCMS                         GCMS
                           ANALYSIS DATE-                      03/03/93               03/03/93 03/06/93                       03/06/93
                           METHOD:                              GCECD                     GCECD           GCECD                        GCECD
                           ANALYSIS DATE:                      03/15/93                                  03/15/93                     03/15/93
                           MATRIX:                              TISSUE                        OIL         TISSUE                       TISSUE
                           SUBMAT:
                           SAMPLWT:
                           WETWT:                                  5.005                                     10.151                       10.208
                           DRYV4T*.                                0.69                                      1.35                         1.86
                           WTUNITS:                             GRAMS DRY                 GRAMS           GRAMS DRY                    GRAMS DRY
                           PCTSOLIDS:
                           VOL:                                                             1.00
                           VOLUNITS:                            LITERS               AMPOULLE             LITERS                       LITERS


                           TOTAL BHC'S                             6.75                                      0.00  ND                     0.00  ND
                           TOTAL CHLORDANES                        60.10                                     0.00  ND                     0.59  J
                           TOTAL DDT'S                             80.13                                     1.89  1                      2.38
                           TOTAL PCB'S                          2603.4                                       18.1                         16.5


                           ALPHA-BHC                               2.11  J                                   0.00  ND                     0.00  ND
                           HCB                                     0.00  ND                                  0.40  J                      0.27  J
                           BETA-BHC                                0.19  1                                   0.00  ND                     0.00  ND
                           GAMMA-BHC                               0.56  J                                   0.00  ND                     0.00  ND
                           DELTA-BHC                               3.89                                      0.00  ND                     0.00  ND
                           HEPTACHLOR                              2.00  J                                   0.00  ND                     0.00  ND
                           HEPTA-EPOXIDE                           0.00  ND                                  0.00  ND                     0.00  ND
                           OXYCHLORDANE                            8.38                                      0.00  ND                     0.00  ND






                                                            Antarctic Palmer Fish Samples Pesticides and PCB Data


                             INVEST#:                    NIST REF TISSUE                                 CINDER CONES                    CINDER CONES
                             ID:                         LAB QA SAMPLE                                   REPL. 1                         REPL.2
                             LABSAMNO:                   Q4612                                           J2022                           J2023
                             UNIT:                                      ng/g                                          ng/g                            ng/g
                             ,Analyte (Cont)                            Cone DB QUAL                                  Conc DB QUAL                    Conc DB QUAL

                             GAMMA-CHLORDANE                           13.14                                          0.00   ND                       0.00  ND
                             ALPHA-CHLORDANE                           14.83                                          0.00   ND                       0.36  J
                             TRANS-NONACHLOR                           13.78                                          0.00   ND                       0.24  J
                             CIS-NONACHLOR                              7.97                                          0.00   ND                       0.00  ND
                             ALDRIN                                     0.00   ND                                     2.74                            2.15
                             DIELDRIN                                   9.71                                          0.77   J                        0.71  J
                             ENDRIN                                     0.00   ND                                     0.00   ND                       1.03  J
                             MIREX                                      1.63   J                                      0.00   ND                       0.00  ND
                             2.4'DDE (0,P'DDE)                          0.00   ND                                     0.00   ND                       0.00  ND
                             4.4'DDE (P,P'DDE)                         29.46                                          0.57   J                        1.11
                             2,4'DDD (0,P'DDD)                          5.58                                          0.00   ND                       0.00  ND
                             4.4'DDD (P,P'DDD)                         35.67                                          0.00   ND                       0.00  ND
                             2,4'DDT (O.P'DDTj                          5.62                                          0.65   J                        0.42  J
                             4,4'DDrr (P,P'DDTI                         3.81                                          0.67   J                        0.86  J
        Co
                             PCB # (CLORINATION)


                             8 (CL2)                                    2.67   J                                      0.00   ND                       0.00  ND
                             18 (CL.3)                                  7.81                                          0.00   ND                       0.10  1
                             28 (CL3)                                  75.22                                          0.00   ND                       0.00  ND
                             44 (CIA)                                  69.89                                          0.22   J                        0.00  ND
                             52 (CIA)                                  97.13                                          0.00   ND                       0.18  J
                             66 (CIA)                                 150.71                                          0.00   ND                       0.19  1
                             101 (CL5)                                105.11                                          0.00   ND                       0.57  J
                             105 (CL5)                                 47.94                                          0.00   ND                       0.00  ND
                             110/77(CL5/4)                            129.65                                          0.00   ND                       0.00  ND
                             118/108/149(CL5/5/6)                     139.40                                          0.22   J                        0.25  J
                             128 (CL6)                                 13.30                                          0.16   J                        0.07  J
                             138 (CL66)                               115.23                                          1.01   1                        1.17
                             126 (CL5)                                         NA                                            NA                             NA
                             153 (CL6)                                128.58                                          2.08                            1.70
                             170 (CL7)                                  3.59                                          0.00   ND                       0.00  ND
                             180 (CL7)                                 11.99                                          0.95   J                        0.00  ND
                             187/182/159(CL7/7/6)                      21.92                                          0.81   J                        0.84  J






                                                       Antarctic Palmer Fish Samples Pesticides and PCB Data


                           INVEST#:                 NIST REF TISSUE                              CINDER CONES                 CINDER CONES
                           ID:                      LAB QA SAMPLE                                REPL. I                      REPL.2
                           LA13SAMNO:               Q4612                                        J2022                        J2023
                           UNIT:                                   ng/g                                      ng/g                         ng/g
                           ,Analyte (Cont)                         Conc DB QUAL                              Conc DB QUAL                 Cone DB QUAL

                           195 (CL8)                               0.76 J                                    0.25 J                       0. 17 J
                           206 (CL9)                               0.84  J                                   0.00  ND                     0.00  ND
                           209 (CLIO)                              0.83  J                                   0.00  ND                     0.00  ND

                           Surrogate Recoveries
                           DBOFB%:                                 29.7                                      27.0                         34.3
                           PCB#103%:                               64.2                                      42.8                         51.8
                           PCB#198%:                               51.4                                      30.4                         42.1


                           PCB #(CHLORINATION)


                           7 (CL2)                                 0.00  ND                                  0.00  ND                     0.00  ND
                           15 (CL2)                               29.50                                      0.00  ND                     0.10  1
                           24 (CL3)                                2.76  J                                   0.00  ND                     0.00  ND
                           16/32 (CL3)                            15.79                                      0.00  ND                     0.00  ND
                           29 (CL-3)                               0.00  ND                                  0.00  ND                     0.00  ND
                           26 (CL3)                                9.03                                      0.00  ND                     0.00  ND
                           25 (CL3)                                9.51                                      0.00  ND                     0.00  ND
                           50 (CIA)                               37.48                                      0.00  ND                     0.00  ND
                           31 (CL3)                                0.00  ND                                  0.00  ND                     0.00  ND
                           33 (CL3)                                7.56                                      0.00  ND                     0.00  ND
                           22 (CL3)                                7.08                                      0.49  J                      0.37  J
                           45 (CIA)                                7.82                                      0.34  J                      0.28  J
                           46 (CIA)                                5.91                                      0.00  ND                     0.00  ND
                           49 (CIA)                               94.59                                      1.20  J                      0.78  J
                           47/48 (CIA)                            86.26                                      0.00  ND                     0.00  ND
                           37/42 (CIA)                            42.26                                      0.00  ND                     0.00  ND
                           41/64 (CIA)                           560.87                                      0.00  ND                     0.00  ND
                           40 (CIA)                               10.58                                      0.00  ND                     0.00  ND
                           100 (CLS)                               0.00  ND                                  0.00  ND                     0.00  ND
                           74 (CIA)                               89.51                                      0.00  ND                     1.84
                           70 (CIA)                              140.77                                      0.00  ND                     0.00  ND
                           88 (CL5)                               16.18                                      0.00  ND                     0.00  ND
                           60/56 (CL5)                            87.68                                      0.00  ND                     0.00  ND






                                                      Antarctic Palmer Fish Samples Pesticides and PCB Data


                           INVEST#:                NIST REF TISSUE                             CINDER CONES                CINDER CONES
                           ID:                     LAB QA SAMPLE                               REPL. 1                     REPL.2
                           LABSAMNO:               Q4612                                       J2022                       J2023
                           UNIT:                                 nglg                                     ng/g                        ng/g
                           Analyte (Cont)                        Conc DB QUAL                             Cone DB QUAL                Conc DB QUAL

                           92? (CL5)                            25.05                                     0.00  ND                    0.00  ND
                           84? (CL5)                            25.65                                     0.00  ND                    0.00  ND
                           99 (CL5)                             56.04                                     0.00  ND                    0.15  J
                           83 (CL5)                              8.80                                     0.00  ND                    0.00  ND
                           97 (CL5)                             33.22                                     0.00  ND                    0.00  ND
                           87 (CL5)                             49.26                                     0.09  j                     0.00  ND
                           85 (CL5)                             22.17                                     0.16  J                     0.00  ND
                           136 (CL6)                             7.18                                     0.10  j                     0.00  ND
                           82 (CL5)                             14.51                                     0.00  ND                    0.00  ND
                           151 (CL6)                            13.68                                     4.01                        2.90
                           107/108/144(CL5/5/6)                 14.59                                     0.00  ND                    0.00  ND
                           149 (CL6)                            50.31                                     0.43  J                     0.51  J
                           188 (CL7)                             0.00  ND                                 1.38  J                     0.67  J
                           146 (CL6)                            11.67                                     6.07                        4.17
                           141 (CL6)                             0.00  ND                                 0.00  ND                    0.00  ND
                           137 (CL6)                             0.71  J                                  0.00  ND                    0.00  ND
                           UNK (CL6)                             3.37                                     0.00  ND                    0.00  ND
                           158 (CL7)                             9.06                                     0.00  ND                    0.00  ND
                           129 (CL6)                             0.00  ND                                 0.00  ND                    0.00  ND
                           178 (CL7)                             3.44                                     0.27  J                     0.27  J
                           183 (CL7)                            11.07                                     0.20  J                     0.29  J
                           167 (CL6)                             3.53                                     0.00  ND                    0.00  ND
                           185 (CL7)                             0.00  ND                                 0.00  ND                    0.00  ND
                           174 (CL7)                             0.00  ND                                 0.37  J                     0.39  J
                           177 (CL7)                             8.89                                     0.32  J                     0.26  J
                           156/171/202(CL6/7/8)                  9.77                                     0.18  J                     0.13  J
                           200 (CL8)                             2.92                                     0.00  ND                    0.00  ND
                           172 (CL7)                             0.00  ND                                 0.35  J                     0.28  J
                           191 (CL7)                             0.73  J                                  0.00  ND                    0.00  ND
                           201 (CL8)                             0.40  J                                  0.00  ND                    0.00  ND
                           196 (CL8)                             1.33  J                                  0.29  J                     0.33  J
                           189 (CL7)                             0.00  ND                                 0.00  ND                    0.00  ND
                           194 (CL8)                             0.82  J                                  0.30  J                     0.29  J
                           205 (CL9)                             0.00  ND                                 0.00  ND                    0.00  ND






                                                         Antarctic Palmer Fish Samples Pesticides and PCB Data


                INVEST#:                  CINDER CONES                  BERNACCHI                 BERNACCHI                 OUTFALL                OUTFALL
                ID:                       REPL.3                        105' REPL. 1              105'REPL.2                60'REPLI.              60'REPL2
                LABSAMNO:                 J2024                         J2025                     J2026                     J2027                  J2028
                UNIT:                                  ng/g                     ng/g                      ng/g                    ng/g                   ng/g
                ,Analyte (Cont)                        Conc DB QUAL             Conc DB QUAL              Conc DB QUAL            Conc DB QUAL           Conc DB QUAL,

                SAMPLE TYPE:                           SAMP                     SAMP                      SAMP                   SAMP                   SAMP
                COLLECTION DATE:                  12/05/91                  12/10/91                  12/10/91              12/12/91               12/12/91
                RECEIPT DATE:
                QCBATCH:                         M779                       M779                     M779                     M779                   M779
                EXTRACTION DATE:
                METHOD:                                GCFID                   GCFID                     GCFID                  GCFID                  GCFID
                ANALYSIS DATE:
                METHOD:                                GCMS,                    GCMS                     GCMS                   GCMS                   GCMS
                ANALYSIS DATE:            03/06/93                      03/06/93                  03/06/93                  03/06/93               03/06/93
                METHOD:                             GCECD                     GCECD                     GCECD                  GCECD                 GCECD
                ANALYSIS DATE:                    03/15/93                  03/15/93                  03/15/93              03/15/93               03/15/93
                MATRIX:                             TISSUE                    TISSUE                    TISSUE                 TISSUE                71SSUE
                SUBMAT:
                SAMPLVv7:
                WETWT:                                 10.405                  10.169                    10.467                 10.153                 10.656
                DRYWT:                                 1.28                     1.71                      1.69                    1.76                   1.84
                V.TUNITS:                           GRAMS DRY                GRAMS DRY                 GRAMS DRY              GRAMS DRY              GRAMS DRY
                PCTSOLIDS:
                VOL:
                VOLUNITS:                           LITERS                     LITERS                   LITERS                 LITERS                LITERS


                TOTAL BHC'S                            0.00 ND                  0.38  J                   0.37  J                 0.61 J                 2.83
                TOTAL CHLORDANES                       0.45 J                   0.43  J                   0.41  J                 1.53                   1.61
                TOTAL DDT"S                            2.88 J                   4.10                      5.22                    8.77                   8.88
                TOTAL PCB'S                            13.9                     15.6                      17.9                  235.1                  262.8


                ALPHA-BHC                              0.00 ND                  0.00  ND                  2.09  M                 0.00 ND                2.19
                HCB                                    0.41 J                   0.34  J                   0.31  J                 0.43 J                 0.34 J
                BETA-BHC                               0.00 ND                  0.00  ND                  0.00  ND                0.00 ND                0.00 ND
                GAMMA-BHC                              0.00 ND                  0.38  J                   0.37  J                 0.61 J                 0.64 J
                DELTA-BHC                              0.00 ND                  0.00  ND                  0.00  ND                0.00 ND                0.00 ND
                HEPTACHLOR                             0.00 ND                  0.00  ND                  0.10  1                 0.00 ND                0.00 ND
                HEPTA-EPOXIDE                          0.00 ND                  0.00  ND                  0.00  ND                0.00 ND                0.00 ND
                OXYCHLORDANE                           0.00 ND                  0.00  ND                  0.00  ND                0.00 ND                0.00 ND






                                                         Antarctic Palmer Fish Samples Pesticides and PCB Data


                INVEST#:                  CINDER CONES                  BERNACCHI                 BERNACCHI                 OUTFALL                OUTFALL
                ID:                       REPL.3                        105' REPL. 1              105'REPL.2                60'REPL1               60'REPL2
                LABSAMNO:                 J2024                        J2025                     J2026                      J2027                  J2028
                UNIT:                                 ng/g                      ng/g                      ng/g                   ng/g                    ng/g
                Analyte (Cont)                        Conc DB QUAL              Conc DB QUAL              Conc DB QUAL           Conc DB QUAL            Conc DB QUAL,

                GAMMA-CHLORDANE                       0.00  ND                  0.00  ND                  0.00  ND               0.00  ND                0.00 ND
                ALPHA-CHLORDANE                       0.25  J                   0.00  ND                  0.00  ND               0.00  ND                0.00 ND
                TRANS-NONACHLOR                       0.20  J                   0.19  1                   0.31  J                0.00  ND                0.00 ND
                CIS-NONACHLOR                         0.00  ND                  0.24  J                   0.00  ND               1.53                    1.61
                ALDRIN                                2.66                      1.83                      1.91                   0.00  ND                1.66
                DIELDRIN                              0.79  J                   0.66  J                   0.00  ND               0.00  ND                0.00 ND
                ENDRIN                                1.07  J                   0.00  ND                  0.41  J                0.00  ND                0.00 ND
                MIREX                                 0.00  ND                  0.00  ND                  0.00  ND               0.00  ND                0.00 ND
                2,4'DDE (0,P'DDE)                     0.00  ND                  0.00  ND                  0.00  ND               0.00  ND                0.00 ND
                4,4'DDE (P.P'DDE)                     0.94  J                   0.61  J                   1.62                   1.63                    1.72
                2,4'DDD (O.P'DDD)                     0.18  1                   0.00  ND                  0.00  ND               0.40  J                 0.34 J
                4,4'DDD (P,P'DDD)                     0.00  ND                  0.80  1                   0.36  J                1.75                    1.89
                2,4'DDT (0,P'DDT)                     0.85  J                   1.58                      2.11                   3.19                    3.03
                4,4'DDT (P,P'DEM                      0.92  J                   1.11  1                   1.11  1                1.81                    1.90


                PCB # (CLORINATION)


                8 (CL2)                               0.00  ND                  0.00  ND                  0.37  J                0.00  ND                0.47 J
                18 (CW)                               0.00  ND                  0.17  J                   0.24  J                0.00  ND                0.38 J
                28 (CL3)                              0.00  ND                  0.00  ND                  0.00  ND               0.00  ND                0.00 ND
                44 (CIA)                              0.00  ND                  0.17  J                   0.15  J                0.35  J                 0.38 J
                52 (CL4)                              0.00  ND                  0.00  ND                  0.00  ND               0.72  J                 0.75 J
                66 (CIA)                              0.13  J                   0.19  1                   0.20  J                0.00  ND                0.00 ND
                101 (CL5)                             0.48  J                   0.00  ND                  0.00  ND               7.65                    7.95
                105 (CL5)                             0.00  ND                  0.23  J                   0.00  ND               0.00  ND                3.96
                110/77(CL5/4)                         0.00  ND                  0.00  ND                  0.12  J                0.00  ND                0.00 ND
                118/108/149(CL5/5/6)                  0.00  ND                  0.00  ND                  0.06  J                0.00  ND                5.10
                128 (CL6)                             0.08  J                   0.26  J                   0.00  ND               2.15                    2.34
                138 (CL6)                             1.31  J                   0.70  J                   0.80  J              39.45                  42.83
                126 (CL5)                                   NA                        NA                        NA                     NA                     NA
                153 (CL6)                             1.74                      0.94  J                   0.62  J              51.22                  49.71
                170 (CL7)                             0.00  ND                  0.00  ND                  0.00  ND             19.69                  21.58
                180 (CL7)                             0.89  J                   0.50  J                   0.31  J              42.29                  44.22
                187/182/159(CL7/7/6)                  0.81  J                   0.29  J                   0.27  J              27.92                  28.90






                                                       Antarctic Palmer Fish Samples Pesticides and PCB Data


                INVEST#:                 CINDER CONES                  BERNACCHI                BERNACCHI                OUTFALL                OUTFALL
                ID:                      REPL.3                       105'REPL. I               105'REPL.2               60'REPLI               60'REPL2
                LABS"NO-                 J2024                       J2025                     J2026                     J2027                  J2028
                UNIT:                                ng/g                     ng/g                     ng/g                    ng/g                  ng/g
               ,Analyte (Cont)                       Conc DB QUAL             Conc DB QUAL             Conc DB QUAL            Conc DB QUAL          Conc DB QUAL,

                195 (CL8)                            0.10 1                   0.34 J                   0.00 ND                 4.43                  4.43
                206(CL9)                             0.00  ND                 0.63  J                  0.00  ND                2.21                  2.22
                209 (CL10)                           0.00  ND                 0.62  J                  0.00  ND                0.00 ND               0.00  ND

                Surrogate Recoveries
                DBOFB%:                              32.7                     33.7                     34.5                    34.0                  36.1
                PCB#103%:                            51.8                     50.8                     53.0                    52.3                  55.8
                PCB#198%:                            41.5                     44.1                     44.9                    43.9                  47.2


                PCB #(CHLORINATION)

                7 (CL2)                              0.00  ND                 0.00  ND                 0.00  ND                0.00 ND               0.00  ND
                15 (CL2)                             0.15  J                  0.05  J                  0.07  J                 0.00 ND               0.00  ND
                24 (CL3)                             0.00  ND                 0.00  ND                 0.00  ND                0.00 ND               0.00  ND
       co       16/32 (CL3)                          0.00  ND                 0.00  ND                 0.00  ND                0.00 ND               0.00  ND
       co       29 (CL3)                             0.00  ND                 0.00  ND                 0.00  ND                0.00 ND               0.00  ND
        01      26 (CW)                              0.00  ND                 0.00  ND                 0.00  ND                0.00 ND               0.00  ND
                25(CL3)                              0.00  ND                 0.00  ND                 0.00  ND                0.00 ND               0.00  ND
                50 (CIA)                             0.00  ND                 0.00  ND                 0.00  ND                0.00 ND               0.00  ND
                31 (CL3)                             0.00  ND                 0.00  ND                 0.00  ND                0.00 ND               0.00  ND
                33 (CL3)                             0.78  J                  0.51  J                  0.00  ND                0.00 ND               0.49  J
                22 (CL3)                             0.00  ND                 0.46  J                  0.43  J                 0.00 ND               0.57  J
                45 (CIA)                             0.00  ND                 0.00  ND                 0.00  ND                0.00 ND               0.00  ND
                46 (CIA)                             0.00  ND                 0.00  ND                 0.00  ND                0.00 ND               0.00  ND
                49 (CIA)                             0.00  ND                 0.00  ND                 0.54  J                 0.00 ND               0.47  J
                47/48 (CIA)                          0.00  ND                 0.00  ND                 0.00  ND                0.00 ND               0.00  ND
                37/42 (CIA)                          0.00  ND                 0.62  J                  0.00  ND                0.00 ND               0.00  ND
                41/64 (CL4)                          0.00  ND                 0.00  ND                 0.00  ND                0.00 ND               0.00  ND
                40 (CIA)                             0.00  ND                 0.00  ND                 0.00  ND                0.00 ND               0.00  ND
                100 (CL5)                            0.00  ND                 0.00  ND                 0.00  ND                0.00 ND               0.00  ND
                74 (CIA)                             1.17  J                  1.00  1                  0.64  J                 0.00 ND               0.00  ND
                70 (CIA)                             0.00  ND                 0.00  ND                 0.00  ND                0.00 ND               0.00  ND
                88 (CL5)                             0.00  ND                 0.00  ND                 0.00  ND                0.00 ND               0.00  ND
                60/56 (CL5)                          0.00  ND                 0.00  ND                 0.00  ND                0.00 ND               0.00  ND






                                                        Antarctic Palmer Fish Samples Pesticides and PCB Data


                INVEST#:                  CINDER CONES                  BERNACCHI                BERNACCHI                 OUTFALL                OUTFALL
                ID:                       REPL.3                       105' REPL. I              105'REPL.2                60'REPLI               60'REPL2
                LABSAMNO:                J2024                        J2025                     J2026                      J2027                 J2028
                UNIT:                                 ng/g                     ng/g                      ng/g                   ng/g                   ng/g
                Analyte (Cont)                        Conc DB QUAL             Conc DB QUAL              Conc DB QUAL           Conc DB QUAL           Conc DB QUAL

                92? (CL5)                             0.00  ND                 0.00  ND                  0.00  ND               1.07 J                 1.23
                84? (CL5)                             0.00  ND                 0.00  ND                  0.00  ND               0.00 ND                0.00 ND
                99 (CL5)                              0.04  J                  0.00  ND                  0.29  J                1.23                   1.20
                83 (CL5)                              0.00  ND                 0.00  ND                  0.00  ND               0.12 J                 0.16 J
                97 (CL5)                              0.00  ND                 0.00  ND                  0.00  ND               0.47 J                 0.57 J
                87(CL5)                               0.00  ND                 0.00  ND                  0.00  ND               1.01 j                 1.30
                85(CL5)                               0.00  ND                 0.00  ND                  0.00  ND               0.34 J                 0.29 J
                136 (CL6)                             0.00  ND                 0.00  ND                  0.00  ND               4.04                   4.93
                82 (CL5)                              0.00  ND                 0.00  ND                  0.00  ND               0.08 J                 0.14 J
                151 (CL6)                             1.81                     1.85                      1.87                 13.46                  14.54
                107/108/144(CL5/5/6)                  0.00  ND                 0.00  ND                  0.00  ND               8.37                   9.93
                149 (CL6)                             0.25  J                  0.00  ND                  0.14  J              34.10                  32.71
                188 (CL7)                             1.75                     3.25                      6.26                   0.00 ND                1.54
                146 (CL6)                             4.08                     6.01                      5.44                   6.25                   9.03
        W       141 (CL6)                             0.12  J                  0.00  ND                  0.00  ND               9.34                   9.50
                137 (CL6)                             0.00  ND                 0.00  ND                  0.00  ND               0.24 J                 0.26 J
                UNK (CL6)                             0.00  ND                 0.00  ND                  0.00  ND               0.00 ND                0.00 ND
                158 (CL7)                             0.00  ND                 0.00  ND                  0.00  ND               4.15                   4.25
                129 (CL6)                             0.00  ND                 0.00  ND                  0.00  ND               0.35 J                 0.00 ND
                178 (CL7)                             0.11  1                  0.00  ND                  0.00  ND               5.34                   5.87
                183 (CL7)                             0.31  J                  0.00  ND                  0.00  ND             12.11                  12.49
                167(CL66)                             0.00  ND                 0.00  ND                  0.00  ND               1.03 J                 1.07 J
                185 (CL7)                             0.00  ND                 0.00  ND                  0.00  ND               2.51                   2.37
                174 (CL7)                             0.31  J                  0.00  ND                  0.00  ND             20.80                  22.07
                177 (CL7)                             0.16  J                  0.00  ND                  0.00  ND             11.63                  12.22
                156/171/202(CL6/7/8)                  0.00  ND                 0.00  ND                  0.00  ND               8.24                 10.32
                200 (CL8)                             0.00  ND                 0.00  ND                  0.00  ND               1.96                   2.28
                172 (CL7)                             0.36  J                  0.19  1                   0.26  J                3.66                   3.78
                191 (CL7)                             0.00  ND                 0.00  ND                  0.00  ND               1.05 1                 1.03 J
                201 (CL8)                             0.00  ND                 0.00  ND                  0.00  ND             12.34                  12.66
                196 (CL8)                             0.35  J                  0.00  ND                  0.00  ND             10.56                  10.00
                189 (CL7)                             0.00  ND                 0.00  ND                  0.00  ND               0.56 J                 0.66 J
                194 (CL8)                             0.17  J                  0.00  ND                  0.00  ND               7.43                   7.77
                205(CL9)                              0.00  ND                 0.00  ND                  0.00  ND               0.92 J                 0.93 J






                                                         Antarctic Palmer Fish Samples Pesticides and PCB Data


              INVEST#:                  WINTER QUARTERS                   WINTER QUARTERS                   WINTER QUARTERS                   BAY OF SAILS
              ID:                       70' REPL. 1                       70'REPL.2                         70'REPL.3                         REPL. I
              LABSAMNO:                 J2029                             J2030                             J2031                             J2032
              UNIT:                                      ng/g                              ng/g                              ng/g                       ng/g
              Analyte (Cont)                             Cone DB QUAL,                     Conc DB QUAL                      Conc DB QUAL               Conc DB QUAL

              SAMPLE TYPE:                               SAMP                              SAMP                             SAMP                        SAMP
              COLLECTION DATE:                       12/09/91                          12/09/91                         12/09/91                    12/06/91
              RECEIPT DATE:
              QCBATCH:                           M779                              M779                             M779                           M780
              EXTRACTION DATE:
              METHOD:                                    GCFID                            GCFID                            GCFID                       GCFID
              ANALYSIS DATE:
              METHOD:                                    GCMS                             GCMS                              GCMS                       GCMS
              ANALYSIS DATE:            03/06/93                          03/07/93                          03/06/93                          03/07/93
              METHOD:                                 GCECD                             GCECD                             GCECD                      GCECD
              ANALYSIS DATE:                        03/15/93                          03/15/93                          03/15/93                    03/15/93
              MATRUC                                  TISSUE                            TISSUE                            TISSUE                     TISSUE
              SUBMAT:
              SAMPLWr:
              WETWT.                                     10.641                           10.474                           10.224                      10.356
              DRywr:                                     1.78                              1.52                              2.17                       2.05
              VvTUNITS:                               GRAMS DRY                         GRAMS DRY                        GRAMS DRY                   GRAMS DRY
              PCTSOLIDS:
              VOL:
              VOLUNrIS:                               LITERS                            LITERS                             LITERS                    LITERS


              TOTAL BHC'S                                2.39                              2.66                              0.35 J                     0.42  J
              TOTALCHLORDANES                            2.27                              1.88                             32.68                       0.15  J
              TOTAL DDT'S                                9.61                              8.64                            105.90                       1.87
              TOTAL PCB'S                                286.5                            263.9                            6250.1                         4.8 JJ


              ALPHA-BHC                                  1.96                              2.25                              0.00 ND                    0.00  ND
              HCB                                        4.75                              8.43                             15.03                       0.32  J
              BETA-BHC                                   0.00  ND                          0.00 ND                           0.00 ND                    0.00  ND
              GAMMA-BHC                                  0.43  J                           0.41 J                            0.35 J                     0.42  J
              DELTA-BHC                                  0.00  ND                          0.00 ND                           0.00 ND                    0.00  ND
              HEPTACHLOR                                 0.00  ND                          0.00 ND                           0.00 ND                    0.03  J
              HEPTA-EPO)aDE                              0.00  ND                          0.00 ND                           0.00 ND                    0.00  ND
              OXYCHLORDANE                               0.00  ND                          0.00 ND                           1.93                       0.00  ND






                                                       Antarctic Palmer Fish Samples Pesticides and PCB Data


               INVEST#:                WINTER QUARTERS                   WINTER QUARTERS                  WINTER QUARTERS                  13AY OF SAILS
               ID:                      70' REPL. 1                      70'REPL.2                        70'REPL.3                        REPL. 1
               IABSAMNO:               J2029                             J2030                            J2031                            J2032
               UNIT:                                     ng/g                            ng/g                              ng/g                      ng/g
               Analyte (Cont)                            Conc DB QUAL                    Conc DB QUAL                      Conc DB QUAL              Conc DB QUAL

               GAMMA-CHLORDANE                           0.00 ND                         0.00  ND                          0.13 J                    0.00  ND
               ALPHA-CHLORDANE                           0.39 J                          0.00  ND                          0.00 ND                   0.00  ND
               TRANS-NONACHLOR                           0.00 ND                         0.14  J                           2.73                      0.12  J
               CIS-NONACHLOR                             1.88                            1.75                            27.88                       0.00  ND
               ALDRIN                                    1.64                            1.88                              0.00 ND                   0.00  ND
               DIELDRIN                                  0.00 ND                         0.00  ND                          0.00 ND                   0.88  ND
               ENDRIN                                    0.32 J                          0.00  ND                          0.00 ND                   0.00  ND
               MIREX                                     0.00 ND                         0.00  ND                          0.00 ND                   0.00  ND
               2,4'DDE (0,P'DDE)                         0.00 ND                         0.00  ND                          0.00 ND                   0.00  ND
               4.4'DDE (P,P'DDE)                         1.69                            1.67                            31.65                       0.17  J
               2,4'DDD (0,P'DDD)                         0.36 J                          0.24  J                           4.15                      0.00  ND
               4,4'DDD (P.P'DDD)                         1.83                            1.79                            13.75                       0.00  ND
               2.4'DDT (O,P'DD11                         3.65                            3.00                            48.59                       1.09
        w      4,4'DDT- (13,13131]rn                     2.07                            1.94                              7.77                      0.60  J
        Co
        00     PCB # (CLORINAMON)

               8 (CL2)                                   0.00 ND                         0.00  ND                          0.81 J                    0.00  ND
               18 (CL3)                                  0.31 J                          0.32  J                           0.00 ND                   0.00  ND
               28 (CL3)                                  0.00 ND                         0.00  ND                          1.44                      0.00  ND
               44 (CIA)                                  0.61 J                          0.50  J                           3.15                      0.10  j
               52 (CIA)                                  1.39                            1.38                            21.07                       0.00  ND
               66 (CIA)                                  0.00 ND                         0.00  ND                       160.81                       0.00  ND
               101 (CL5)                               10.46                             9.78                           223.75                       0.00  ND
               105 (CL5)                                 7.94                            6.76                           222.65                       0.00  ND
               110/77 (CL5/4)                            0.00 ND                         0.00  ND                       108.86                       0.07  J
               118/108/149(CL5/5/6)                      4.12                            0.00  ND                       193.10                       0.00  ND
               128 (CL6)                                 2.57                            2.42                           128.15                       0.00  ND
               138 (CL6)                               45.75                            42.32                           432.60                       0.82  J
               126 (CL5)                                      NA                               NA                               NA                         NA
               153 (CL6)                               48.72                            47.03                           685.10                       0.00  ND
               170 (CL7)                               22.09                            19.97                           183.80                       0.00  ND
               180 (CL7)                               40.93                            40.33                           533.80                       0.28  J
               187/182/159(CL7/7/6)                    28.84                            26.97                           479.40                       0.00  ND






                                                             Antarctic Palmer Fish Samples Pesticides and PCB Data


               INVEST#:                    WINTER QUARTERS                     WT,4TER QUARTERS                    WINTER QUARTERS                      BAY OF SAILS
               ID:                         70'REPL. I                          70'REPL.2                            70'REPL.3                           REPL.1
               IABSAMNO:                   J2029                               J2030                               J2031                                J2032
               UNIT.-                                        ng/g                                ng/g                                 ng/g                         ng/g
               ,Analyte (Cont)                               Conc DB QUAL                        Conc DB QUAL                         Conc 1313 QUAL               Conc DB QUAL

               195 (CLB)                                     3.79                                3.97                               121.15                         0.00 ND
               206 (CL9)                                     2.07                                1.98                                45.25                         0.00   ND
               209 (CLIO)                                    0.00  ND                            0.00   ND                            1.55                         0.00   ND

               Surrogate Recoveries
               DBOFB0/6:                                     30.3                                33.6                                 33.5                         34.5
               PCB#103%:                                     50.8                                53.0                                 52.4                         53.4
               PCB# 1980h:                                   42.4                                44.5                                 62.6                         49.4

               PCB #(CHLORINATION)


               7 (CL2)                                       0.00  ND                            0.00   ND                            0.00  ND                     0.00   ND
               15 (CL2)                                      0.00  ND                            0.00   ND                            0.14  J                      0.00   ND
               24 (M)                                        0.00  ND                            0.00   ND                            0.00  ND                     0.02   J
               16/32 (CL3)                                   0.00  ND                            0.00   ND                            0.00  ND                     0.00   ND
               29 (CL3)                                      0.00  ND                            0.00   ND                            0.00  ND                     0.00   ND
               26 (CL3)                                      0.00  ND                            0.00   ND                            0.00  ND                     0.00   ND
               25 (CL3)                                      0.00  ND                            0.00   ND                            0.00  ND                     0.00   ND
               50 (CIA)                                      0.00  ND                            0.00   ND                            0.00  ND                     0.00   ND
               31 (CL3)                                      0.00  ND                            0.00   ND                            0.00  ND                     0.00   ND
               33 (CL3)                                      0.50  J                             0.56   J                             0.00  ND                     0.00   ND
               22 (CL3)                                      0.67  J                             0.64   J                             0.00  ND                     0.38   J
               45 (CIA)                                      0.00  ND                            0.00   ND                            0.00  ND                     0.00   ND
               46 (CIA)                                      0.00  ND                            0.00   ND                            0.00  ND                     0.00   ND
               49 (CIA)                                      0.42  J                             0.42   J                             5.56                         0.00   ND
               47/48 (CIA)                                   0.00  ND                            0.00   ND                            0.00  ND                     0.00   ND
               37/42 (CIA)                                   0.00  ND                            0.00   ND                            2.02                         0.00   ND
               41/64 (CIA)                                   0.00  ND                            0.00   ND                            5.78                         0.00   ND
               40 (CIA)                                      0.00  ND                            0.00   ND                            0.00  ND                     0.00   ND
               100 (CL,5)                                    0.00  ND                            0.00   ND                            0.00  ND                     0.00   ND
               74 (CL4)                                      0.00  ND                            0.00   ND                           11.76                         0.00   ND
               70 (CIA)                                      0.84  J                             1.01   1                             2.28                         0.00   ND
               88 (CL5)                                      0.15  J                             0.11   1                             6.91                         0.00   ND
               60/56 (CL5)                                   0.00  ND                            0.00   ND                            2.02                         0.00   ND






                                                     Antarctic Palmer Fish Samples Pesticides and PCB Data


             INVEST#:                 WINTER QUARTERS                 WINTER QUARTERS                 WINTER QUARTERS                  BAY OF SAILS
             ID:                      70'REPL. I                      70'REPL.2                       70'REPL.3                        REPL. I
             LABSAMNO:                J2029                           J2030                           J2031                           J2032
             UNIT:                                    ng/g                            ng/g                             ng/g                      ng/g
             Analyte (Cont)                           Conc DB QUAL                    Conc DB QUAL                     Conc DB QUAL              Conc DB QUALI

             92? (CL5)                                1.52                            1.44                           34.74                       0.00 ND
             84? (CL5)                                0.00  ND                        0.00  ND                         0.00 ND                   0.00 ND
             99 (CL5)                                 2.23                            1.66                           68.64                       0.00 ND
             83 (CL5)                                 0.28  J                         0.28  J                          4.87                      0.00 ND
             97 (CL5)                                 0.86  J                         0.90  1                        17.75                       0.00 ND
             87 (CL5)                                 1.85                            1.52                           47.32                       0.00 ND
             85 (CL5)                                 0.40  J                         0.29  J                        12.04                       0.00 ND
             136 (CL6)                                5.48                            5.16                           57.74                       0.00 ND
             82 (CL5)                                 0.19  1                         0.22  J                          3.21                      0.00 ND
             151 (CL6)                               16.01                           14.74                          427.35                       0.00 ND
             107/108/144(CL5/5/6)                    11.10                            9.80                          190.92                       0.15 ND
             149 (CL6)                               37.82                           38.89                          651.16                       0.00 ND
             188 (CL7)                                3.27                            1.34                             0.00 ND                   1.60 ND
             146 (CL6)                                9.38                            8.05                          283.59                       1.45 ND
             141 (CL6)                               11.54                           10.45                          429.37                       0.00 ND
       0     137 (CL6)                                0.34  J                         0.31  J                        22.50                       0.00 ND
             UNK (CL6)                                0.00  ND                        0.00  ND                         0.00 ND                   0.00 ND
             158 (CL7)                                4.54                            4.49                          116.71                       0.00 ND
             129 (CL6)                                0.00  ND                        0.00  ND                       10.64                       0.00 ND
             178 (CL7)                                5.73                            5.46                          142.85                       0.00 ND
             183 (CL7)                               12.66                           11.71                          301.11                       0.00 ND
             167 (CL6)                                1.15                            1.03  J                        27.26                       0.00 ND
             185 (CL7)                                2.56                            2.55                           85.59                       0.00 ND
             174 (CL7)                               22.18                           21.06                          268.32                       0.00 ND
             177 (CL7)                               12.26                           11.93                          191.44                       0.00 ND
             156/171/202(CL6/7/8)                    10.30                            8.81                          259.27                       0.00 ND
             200 (CL8)                                2.17                            1.84                           30.24                       0.00 ND
             172 (CL7)                                3.87                            3.59                          125.69                       0.22 J
             191 (CL7)                                0.77  J                         0.62  J                        32.87                       0.00 ND
             201 (CL8)                               12.26                           11.97                          244.60                       0.00 ND
             196 (CLS)                               10.11                            9.92                          307.59                       0.00 ND
             189 (CL7)                                0.53  J                         0.48  J                        27.09                       0.00 ND
             194 (CL8)                                6.80                            6.53                          272.90                       0.00 ND
             205 (CL9)                                0.62  J                         0.60  J                        21.91                       0.00 ND




   M M M M M M M M M M M M M M M M M M M






                                                       Antarctic Palmer Fish Samples Pesticides and PCB Data


               INVEST#:                 CINDER CONES                 WINTER QUARTERS                   WINTER QUARTERS                   PROC BLANK
               ID:                      T BERNACCHII                 70'REPL.                          70'REPL.3                         LAB QA SAMPLE
               LABSAMNO:                J2033                        J2064                             Q4630                             Q4631
               UNIT:                                ng/g                              ng/g                              ng/g                          ng/g
               ,Analyte (Cont)                      Conc D13 QUAL                     Conc DB QUAL                      Conc DB QUAL                  Conc DB QUAL,

               SAMPLE TYPE:                         SAMP                              SAMP             DUPE OF J2031                     PROC BLANK
               COLLECTION DATE:                 12/09/91                          12/09/91                          12/09/91
               RECEIPT DATE-
               QCBATCH:                        M780                           M827                              M779                            M779
               EXTRACTION DATE:                                             04/26/93
               METHOD:                              GCFID                             GCFID                           GCFID                          GCFID
               ANALYSIS DATE:
               METHOD:                              GCMS                              GCMS                            GCMS                           GCMS
               ANALYSIS DATE:           03/07/93                            05/24/93                   03/06/93                          03/06/93
               METEOD:                            GCECD                            GCECD                              GCECD                        GCECD
               ANALYSIS DATE:                   03/15/93                          06/02/93                         03/15/93                       03/15/93
               MATRIX:                            TISSUE                           TISSUE                             TISSUE                       TISSUE
               SUBMAT:
               SAMPLWT:
               WETWT:                               10.572                            10.039                          10.089
               DRYWT:                               2.50                              1.43                              2.03                         10.00
               Wl'UNITS:                          GRAMS DRY                        GRAMS DRY                          GRAMS DRY                    GRAMS DRY
               PCTSOLIDS:
               VOL:
               VOLUNITS:                          LITERS                           LITERS                             LITERS                       LITERS


               TOTAL BHC'S                          0.74  J                           0.00  ND                          0.48 J                        0.00  ND
               TOTALCHLORDANES                      4.58                              1.84                            35.53                           0.93  J
               TOTAL DDT"S                          3.93                              8.01                            117.48                          2.96
               TOTAL PCB'S                          143.7                             233.8                           6375.1                         184.2


               ALPHA-BHC                            0.00  ND                          0.00  ND                          0.00 ND                       0.00  ND
               HCB                                  1.82                              0.48  J                           7.39                          0.10  1
               BETA-BHC                             0.00  ND                          0.00  ND                          0.00 ND                       0.00  ND
               GAMMA-BHC                            0.74  J                           0.00  ND                          0.48 J                        0.00  ND
               DELTA-BHC                            0.00  ND                          0.00  ND                          0.00 ND                       0.00  ND
               HEPTACHLOR                           0.98                              0.28  J                           0.00 ND                       0.00  ND
               HEPTA-EPOXIDE                        0.00  ND                          0.00  ND                          0.00 ND                       0.00  ND
               OXYCHLORDANE                         0.99                              0.00  ND                          1.51                          0.00  ND






                                                         Antarctic Palmer Fish Samples Pesticides and PCB Data


                 INVEST#:                 CINDER CONES                 WINTER QUARTERS                  WINTER QUARTERS                   PROC BIANK
                 ID:                      T BERNACCHII                 70'REPL.                          70'REPL.3                        I.AB QA SAMPLE
                 LABSAMNO:                J2033                        J2064                             Q4630                            Q4631
                 UNIT:                                ng/g                              ng/g                             ng/g                           ng/g
                 ,Analyte (Cont)                      Conc DB QUAL                      Conc DB QUAL                     Conc DB QUAL                   Conc DB QUAL

                 GAMMA-CHLORDANE                      0.00  ND                          0.00  ND                         0.22  J                        0.00  ND
                 ALPHA-CHLORDANE                      0.00  ND                          0.00  ND                         0.00  ND                       0.00  ND
                 TRANS-NONACHLOR                      0.53  J                           0.00  ND                         2.34                           0.00  ND
                 CIS-NONACHLOR                        2.07                              1.56                            31.46                           0.93  J
                 ALDRIN                               0.00  ND                          0.00  ND                         0.00  ND                       1.09
                 DIELDRIN                             0.90                              0.00  ND                         0.00  ND                       0.00  ND
                 ENDRIN                               0.00  ND                          0.00  ND                         0.00  ND                       0.00  ND
                 MIREX                                0.00  ND                          0.00  ND                         0.00  ND                       0.00  ND
                 2,4'DDE (0,P'DDE)                    0.00  ND                          0.00  ND                         0.00  ND                       0.00  ND
                 4,4'DDE (P,P'DDE)                    1.11                              1.45  R                         32.75                           1.25
                 2.4'DDD (0,P'DDD)                    0.00  ND                          0.00  ND                         4.56                           0.00  ND
                 4,4'DDD (P,P'DDD)                    1.00                              0.33  J                         15.70                           0.00  ND
                 2,4'DDT fO,P'DDT)                    0.00  ND                          0.42  J                         55.81                           1.71
                 4,4'DDT (P,P'DDTI                    1.82                              5.81                             8.66                           0.00  ND


                 PCB # (CLORINATION)


                 8 (CL2)                              0.00  ND                          1.38  J                          1.38                           0.00  ND
                 18 (CL3)                             0.00  ND                          0.73  J                          0.00  ND                       0.00  ND
                 28 (CL3)                             0.00  ND                          0.30  J                          1.46                           0.00  ND
                 44 (CIA)                             1.27                              0.00  ND                         3.50                           0.20  J
                 52 (CIA)                             0.52  J                           1.39  J                         21.15                           0.33  J
                 66 (CIA)                             1.45                              0.00  ND                       176.75                           0.00  ND
                 101 (CL5)                            3.54                              9.98                           225.45                           5.08
                 105 (CL5)                            0.00  ND                          0.00  ND                       181.64                           0.00  ND
                 110/77 (CL5/4)                       1.83                              4.06                             0.00  ND                       0.00  ND
                 118/108/149(CL5/5/6)                 2.77                              4.60                           195.51                           2.91
                 128 (CL6)                            0.48  J                           1.32  J                        128.35                           1.72
                 138 (CL6)                           12.19                             37.29                           461.60                         34.43
                 126 (CL5)                                  NA                                NA                               NA                             NA
                 153 (CL6)                           18.46                             50.89                           695.20                         45.65
                 170 (CL7)                            5.80                             15.15                           197.80                         14.67
                 180 (CL7)                           14.00                             37.76                           596.00                         36.37
                 187/182/159(CL7/7/6)                12.27                             36.77                           519.10                         24.64






                                                        Antarctic Palmer Fish Samples Pesticides and PCB Data


                INVEST#:                 CINDER CONES                 WINTER QUARTERS                   WINTER QUARTERS                   PROC BLANK
                ID:                      T BERNACCHII                  70'REPL.                         70'REPL.3                         LAB QA SAMPLE
                LABSAMNO:                J2033                        J2064                             Q4630                             Q4631
                UNIT:                                ng/g                              ng/g                              ng/g                          ng/g
                ,Analyte (Cont)                      Cone DB QUAL                      Conc DB QUAL                      Conc DB QUAL                  Conc DB QUAL,

                195 (CL8)                            1.23                              2.73                            124.38                          2.59
                206 (CL9)                            0.66  J                           0.70  J                          47.62                          1.11
                209 (CLIO)                           0.00  ND                          0.00  ND                          0.97  J                       0.00  ND

                Surrogate Recoveries
                DBOFBO/6:                            37.2                              68.2                              28.0                          33.7
                PCB#103%:                            58.8                              72.6                              47.7                          54.2
                PCB#198%:                            54.8                              56.3                              55.4                          46.5


                PCB #(CHLORINA'nON)


                7 (CL2)                              0.00  ND                          0.00  ND                          0.00  ND                      0.00  ND
                15 (CL2)                             0.00  ND                          0.00  ND                          0.16  J                       0.00  ND
                24 (CL3)                             0.00  ND                          0.00  ND                          0.00  ND                      0.00  ND
        W       16/32 (CL3)                          0.00  ND                          0.00  ND                          0.00  ND                      0.00  ND
        0,      29 (CL3)                             0.00  ND                          0.00  ND                          0.00  ND                      0.00  ND
                26 (CL3)                             0.00  ND                          0.00  ND                          0.00  ND                      0.00  ND
                25 (CL3)                             0.00  ND                          0.00  ND                          0.00  ND                      0.00  ND
                50 (CIA)                             0.00  ND                          0.00  ND                          0.00  ND                      0.00  ND
                31 (CL3)                             0.00  ND                          0.00  ND                          0.00  ND                      0.00  ND
                33 (CL3)                             0.00  ND                          0.00  ND                          0.00  ND                      0.00  ND
                22 (CL3)                             0.81                              0.00  ND                          0.00  ND                      0.00  ND
                45 (CIA)                             0.00  ND                          0.00  ND                          0.00  ND                      0.00  ND
                46 (CIA)                             0.00  ND                          0.00  ND                          0.00  ND                      0.00  ND
                49 (CIA)                             0.15  J                           0.00  ND                          5.51                          0.19  1
                47/48 (CIA)                          0.00  ND                          0.00  ND                          0.00  ND                      0.00  ND
                37/42 (CIA)                          0.00  ND                          0.30  J                           2.18                          0.00  ND
                41/64 (CIA)                          5.13                              0.00  ND                          5.83                          0.00  ND
                40 (CIA)                             0.00  ND                          0.00  ND                          0.00  ND                      0.00  ND
                100 (CL5)                            0.00  ND                          0.00  ND                          0.00  ND                      0.00  ND
                74 (CIA)                             0.17  J                           0.00  ND                          11.43                         0.00  ND
                70 (CIA)                             1.07  J                           0.00  ND                          2.28                          0.00  ND
                88 (CL5)                             0.00  ND                          0.00  ND                          7.19                          0.00  ND
                60/56 (CL5)                          0.00  ND                          0.00  ND                          1.42                          0.00  ND






                                                         Antarctic Palmer Fish Samples Pesticides7@knd PCB Data


                 INVEST#:                 CINDER CONES                 WINTER QUARTERS                   WINTER QUARTERS                  PROC BLANK
                 ID:                      T BERNACCHII                 70'REPL.                          70'REPL.3                        LAB QA SAMPLE
                 LABSAMNO:                J2033                        J2064                             Q4630                            Q4631
                 UNIT:                                 ng/g                             ng/g                              ng/g                          ng/g
                ,Analyte (Cont)                        Conc DB QUAL                     Conc DB QUAL                      Conc DB QUAL                  Conc DB QUAL

                 92? (CL5)                             0.00 ND                          0.59  J                         34.97                           0.55  J
                 84? (CL5)                             0.00 ND                          0.00  ND                          0.00 ND                       0.00  ND
                 99 (CL5)                              0.72 J                           1.75                            69.49                           1.11
                 83 (CL5)                              0.00 ND                          0.00  ND                          5.18                          0.00  ND
                 97 (CL5)                              0.00 ND                          0.73  J                         18.16                           0.24  J
                 87 (CL5)                              0.70 J                           1.13  J                         47.48                           0.49  J
                 85 (CL5)                              0.00 ND                          0.00  ND                        11.85                           0.19  1
                 136 (CL6)                             o.bo ND                          2.22                            59.97                           0.00  ND
                 82 (CL5)                              0.00 ND                          0.00  ND                          2.89                          0.00  ND
                 151 (CL6)                             2.44                             7.68                           443.65                           9.91
                 107/108/144(CL5/5/6)                  1.81                             0.00  ND                       205.45                           3.46
                 149 (CL6)                             7.75                            32.13                           687.41                          17.83
                 188 (CL7)                            41.73                             0.00  ND                          0.00 ND                       0.00  ND
          w      146 (CL6)                            22.82                            15.33                           295.72                           6.39
                 141 (CL6)                             2.53                            23.05                           449.91                           6.27
                 137 (CL6)                             1.93                             0.00  ND                        24.92                           0.33  J
                 UNK (CL6)                             0.00 ND                          0.00  ND                          0.00 ND                       0.00  ND
                 158 (CL7)                             0.77 J                           6.23                           114.70                           3.65
                 129 (CL6)                             0.00 ND                          0.62  J                         10.64                           0.00  ND
                 178 (CL7)                             2.29                             5.70                           149.87                           4.83
                 183 (CL7)                             4.74                            14.63                           315.70                           9.71
                 167 (CL6)                             0.48 J                           0.73  J                         28.69                           0.40  J
                 185 (CL7)                             0.61 J                           2.35                            88.24                           1.99
                 174 (CL7)                             4.39                            21.55                           280.80                           8.37
                 177 (CL7)                             2.34                            11.18                           199.68                           5.89
                 156/171/202(CL6/7/8)                  2.16                             0.00  ND                       304.47                           4.48
                 200 (CL8)                             0.00 ND                          2.20                            33.31                           0.73  J
                 172 (CL7)                             0.00 ND                          2.13                           128.40                           3.32
                 191 (CL7)                             0.18 1                           0.52  J                         32.80                           0.71  J
                 201 (CL8)                             4.33                             8.90                           255.43                           8.55
                 196 (CL8)                             4.31                             7.57                           318.93                           7.75
                 189 (CL7)                             0.00 ND                          0.00  ND                        25.75                          25.75
                 194 (CL8)                             2.82                             3.55                           279.22                           6.05
                 205 (CL9)                             0.44 J                           0.00  ND                        18.62                           0.40  J






                                                         Antarctic Palmer Fish Samples Pesticides and PCB Data


                 INVEST#:                  WINTER QUARTERS                   NIST REF TISSUE                CINDER CONES                 CINDER CONES
                 ID:                       70'REPL.3                         LAB QA SAMPLE                  T BERNACCHII                 T BERNACCHII
                 LARSAMNO:                 Q4632                             Q4633                          Q4634                        Q4635
                 UNIT:                                          %                          ng/g                         ng/g                             %
                 Analyte (Cont)                          % Recov DB QUAL                   Conc DB QUAL                 Conc DB QUAL             % Recov DB QUALI

                 SAMPLE'IYPE:              MS OF J2031                       NIST REF                       DUPE OF J2033                MS OF J2033
                 COLLECTION DATE:                       12/09/91                       12/06/91                     12/09/91
                 RECEIPT DATE:
                 QCBATCH:                           M779                             M779                         M780                         M780
                 EXTRACTION DATE:
                 METHOD:                                   GCFID                           GCFID                      GCFID                        GCFID
                 ANALYSIS DATE:
                 METHOD:                                   GCMS                            GCMS                       GCMS                         GCMS
                 ANALYSIS DATE:            03/06/93                          03/06/93                       03/07/93                     03/07/93
                 METHOD:                                 GCECD                          GCECD                        GCECD                         GCECD
                 ANALYSIS DATE:                        03/15/93                        03/15/93                    03/15/93                     03/15/93
                 MATRIX:                                 TISSUE                         IISSUE                       TISSUE                        TISSUE
                 SUBMAT:
                 SAMPLWT:
                 WETWT:                                    10.517                          5.013                      10.345                        10.22
                 DRYWT:                                    2.25                            0.62                         2.36                        2.35
                 MITUNITS:                               GRAMS DRY                      GRAMS DRY                    GRAMS DRY                    GRAMS DRY
                 PCTSOLIDS:
                 VOL:
                 VOLUNITS:                               LITERS                         LITERS                       LITERS                        LITERS


                 TOTAL BHC'S                                      NA                       0.00  ND                     0.45  J                            NA
                 TOTAL CHLORDANES                                 NA                    108.76                          5.54                               NA
                 TOTAL DDTS                                       NA                    112.11                          5.23                               NA
                 TOTAL PCB'S                                      NA                    2696.9                        183.2                                NA


                 ALPHA-BHC                                 73.0                            0.00  ND                     0.00  ND                    82.0
                 HCB                                       30.0                            0.00  ND                     0.82  J                     45.0
                 BETA-BHC                                  21.0                            0.00  ND                     0.00  ND                    25.0
                 GAMMA-BHC                                 88.0                            0.00  ND                     0.45  J                     98.0
                 DELTA-BHC                                 64.0                            0.00  ND                     0.00  ND                    75.0
                 HEPTACHLOR                                80.0                            16.64                        1.61                       114.0
                 HEPTA-EPOXIDE                             74.0                            0.00  ND                     0.00  ND                    79.0
                 OXYCHLORDANE                                     NA                       12.52                        1.35                               NA






                                                        Antarctic Palmer Fish Samples Pesticides and PCB Data


                  INVEST#:                 WINTER QUARTERS                   NIST REF TISSUE                CINDER CONES                CINDER CONES
                  ID:                      70'REPL.3                         IAB QA SAMPLE                  T BERNACCHII                T BERNACCHII
                  LABSAMNO:                Q4632                             Q4633                          Q4634                       Q4635
                  UNIT:                                         %                          ng/g                         nglg                             %
                  ,Analyte (Cont)                        % Recov DB QUAL                   Conc DB QUAL                 Conc DB QUAL             % Recov DB QUAL

                  GAMMA-CHLORDANE                           84.0                          21.20                         0.00 ND                     88.0
                  ALPHA-CHLORDANE                           91.0                          23.65                         0.00 ND                     81.0
                  TRANS-NONACHLOR                           82.0                          20.92                         0.82 J                      95.0
                  CIS-NONACHLOR                                   NA                      13.83                         1.76                              NA
                  ALDRIN                                    82.0                           0.00  ND                     0.00 ND                     91.0
                  DIELDRIN                                 119.0                          13.40                         1.57                        90.0
                  ENDRIN                                    83.0                           0.00  ND                     0.00 ND                     111.0
                  MIREX                                     95.0                           0.00  ND                     0.00 ND                     99.0
                  2.4'DDE (O.P'DDE)                         59.0                           0.00  ND                     0.00 ND                     65.0
                  4,4'DDE (P,P'DDE)                        121.0                          41.11                         2.39                        94.0
                  2,4*DDD (0,P'DDD)                        100.0                           9.32                         0.00 ND                     112.0
                  4,4'DDD (P,P'DDD)                        106.0                          43.23                         0.73 J                      114.0
                  2,4'DDT fO,P'DDD                          80.0                          15.55                         0.00 ND                     81.0
                  4,4'DDT (P,P'DErn                        115.0                           2.89  J                      2.11                        83.0
         W
                  PCB # (CLORINATION)


                  8 (CL2)                                  104.0                           8.26                         0.00 ND                     109.0
                  18 (CL3)                                  63.0                          15.23                         0.00 ND                     77.0
                  28 (CL3)                                 114.0                        143.29                          0.00 ND                     125.0
                  44 (CIA)                                 108.0                          86.30                         1.29                        114.0
                  52 (CIA)                                  92.0                        113.45                          0.47 J                      117.0
                  66 (CIA)                                 102.0                        140.61                          1.63                        130.0
                  101 (CL5)                                   0.0                       126.12                          3.07                        82.0
                  105 (CL5)                                -297.0                         80.43                         0.00 ND                     114.0
                  110/77(CL5/4)                             82.0                           0.00                         0.00 ND                     78.0
                  118/108/149(CL5/5/6)                     -35.0                        135.61                          2.90                        120,0
                  128(CL6)                                  96.0                          22.70                         0.91                        118.0
                  138 (CL6)                                 33.0                        205.45                        14.50                         119.0
                  126 (CL5)                                       NA                             NA                          NA                           TVA
                  153 (CL6)                                238.0                        221.83                        20.14                         81.0
                  170 (CL7)                                 19.0                          43.65                         6.70                        116.0
                  180 fCL7)                                 74.0                        107.96                        15.20                         97.0
                  187/182/159(CL7/7/6)                      52.0                          84.40                       14.60                         84.0






                                                             Antarctic Palmer Fish Samples Pesticides and PCB Data


                   INVEST#:                    WINTER QUARTERS                     NIST REF TISSUE                   CINDER CONES                    CINDER CONES
                   ID:                         70'REPL.3                           LAB QA SAMPLE                     T BERNACCHIT                    T BERNACCHII
                   LABSAMNO:                   Q4632                               Q4633                             Q4634                           Q4635
                   UNIT:                                             %                             ng/g                           ng/g                               %
                  ,Analyte (Cont)                            % Recov DB QUAL                       Conc DB QUAL                   Conc DB QUAL.               % Recov DB QUAL,

                   195 (CL8)                                       0.0                             8.67                           1.46                           120.0
                   206 (CL9)                                     86.0                              4.15                           0.94                           116.0
                   209 (CLIO)                                    98.0                              0.00                           0.00   ND                      110.0

                   Surrogate Recoveries
                   DBOFB%:                                       33.7                              30.5                           37.6                             38.2
                   PCB#103%:                                     52.6                              48.2                           55.0                             55.1
                   PCB# 1980/6:                                  66.6                              42.9                           55.2                             57.8


                   PCB #(CHLORINATION)


                   7 (CL2)                                              NA                         0.00                           0.00   ND                             NA
                   15 (CL2)                                             NA                        47.28                           0.00   ND                             NA
                   24 (CL3)                                             NA                         3.27                           0.00   ND                             NA
                   16/32 (CL3)                                          NA                        23.70                           0.00   ND                             NA
                   29 (CI-3)                                            NA                         0.00                           0.00   ND                             NA
          4        26 (CL3)                                             NA                        14.53                           0.00   ND                             NA
                   25 (CL3)                                             NA                        15.62                           0.00   ND                             NA
                   50 (CIA)                                             NA                        26.81                           0.00   ND                             NA
                   31 (CL3)                                             NA                         0.00                           0.00   ND                             NA
                   33 (CL3)                                             NA                        11.95                           0.00   ND                             NA
                   22 (CL3)                                             NA                        14.35                           1.75                                  NA
                   45 (CIA)                                             NA                         9.71                           0.00   ND                             NA
                   46 (CIA)                                             NA                         4.58                           0.00   ND                             NA
                   49 (CIA)                                             NA                       119.85                           0.17   J                              NA
                   47/48 (CL4)                                          NA                       113.54                           0.00   ND                             NA
                   37/42 (CIA)                                          NA                        57.52                           0.00   ND                             NA
                   41/64 (CIA)                                          NA                        89.81                           6.55                                  NA
                   40 (CIA)                                             NA                        12.67                           0.00   ND                             NA
                   100 (CL5)                                            NA                         0.00                           0.00   ND                             NA
                   74 (CIA)                                             NA                        87.49                           0.18   j                              NA
                   70 (CIA)                                             NA                       136.04                           1.12                                  NA
                   88 (CL5)                                             NA                        22.40                           0.00   ND                             NA
                   60/56 (CL5)                                          NA                        80.31                           0.00   ND                             NA






                                                            Antarctic Palmer Fish Samples Pesticides and PCB Data


                   INVEST#:                   WINTER QUARTERS                    NISr REF TISSUE                 CINDER CONES                   CINDER CONES
                   ID:                        70'REPL.3                          LAB QA SAMPLE                   T BERNACCHII                   T BERNACCHII
                   LABSAMNO:                  Q4632                              Q4633                            Q4634                         Q4635
                   UNIT.                                           %                            nglg                          ng/g                              %
                  ,Analyte (Cont)                           % Recov DB QUAL                     Conc DB QUAL                  Conc DB QUAL               % Recov DB QUAL

                   92? (CL5)                                          NA                       32.79                          0.00  ND                             NA
                   84? (CL5)                                          NA                       28.83                          0.00  ND                             NA
                   99 (CL5)                                           NA                       71.20                          0.80  1                              NA
                   83 (CL5)                                           NA                        9.74                          0.00  ND                             NA
                   97 (CL5)                                           NA                       39.96                          1.03                                 NA
                   87 (CL5)                                   125.0                            60.30                          0.89  J                      124.0
                   85 (CL5)                                           NA                       27.02                          0.00  ND                             NA
                   136 (CL66)                                         NA                       12.76                          0.00  ND                             NA
                   82 (CL5)                                           NA                       14.90                          0.00  ND                             NA
                   151 (CL6)                                          NA                       43.24                          2.53                                 NA
                   107/108/144(CL5/5/6)                               NA                       29.60                          1.80                                 NA
                   149 (CL6)                                          NA                       92.58                          8.75                                 NA
                   188 (CL7)                                          NA                        2.88  J                      57.88                                 NA
                   146 (CL6)                                          NA                       35.28                         32.20                                 NA
                   141 (CL6)                                          NA                        0.00  ND                      2.90                                 NA
          04       137 (CL6)                                          NA                        1.51  J                       3.38                                 NA
          00       UNK (CL6)                                          NA                        0.00  ND                      0.00  ND                             NA
                   158 (CL7)                                          NA                       18.88                          0.82  J                              NA
                   129 (CL6b)                                         NA                        0.00  ND                      0.00  ND                             NA
                   178 (CL7)                                          NA                       16.46                          2.51                                 NA
                   183 (CL7)                                          NA                       38.19                          6.10                                 NA
                   167 (CL6)                                          NA                        6.82                          1.31                                 NA
                   185 (CL7)                                          NA                        5.84                          0.70  J                              NA
                   174 (CL7)                                          NA                       22.64                          4.70                                 NA
                   177 (CL7)                                          NA                       26.11                          2.71                                 NA
                   156/171/202(CLro/7/8)                              NA                       13.19                          3.67                                 NA
                   200 (CL8)                                          NA                        0.00  ND                      0.00  ND                             NAL
                   172 (CL7)                                          NA                       12.36                          0.00  ND                             NA
                   191 (CL7)                                          NA                        0.00  ND                      0.15  J                              NA
                   201 (CL8)                                          NA                       23.04                          4.99                                 NA
                   196 (CL8)                                          NA                       24.70                          4.94                                 NA
                   189 (CL7)                                          NA                        0.00  ND                      0.00  ND                             NA
                   194 (CL8)                                          NA                       17.15                          3.28                                 NA
                   205 (CL9)                                          NA                        0.00  ND                      0.61  J                              NA






                                                        Antarctic Palmer Fish Samples Pesticides and PCB Data


                             INVEST#:                 PROC BLANK                    NIST REF TISSUE
                             ID:                      LAB QA SAMPLE                 LAB QA SAMPLE
                             L&BSAMNO:                Q4636                         Q4637
                             UNIT:                                 ng/g                           ng/g
                             ,Analyte (Cont)                       Conc DB QUAL                   Conc DB QUAL

                             SAMPLE TYPE:             PROC BLANK                    NIST REF                       REF OIL            REF OIL
                             COLLECTION DATE:
                             RECEIPT DATE:
                             QCBATCH:                       M780                            M780                      M779                M780
                             EXTRACTION DATE:
                             METHOD:                              GCFID                           GCFID                  GCFID              GCFID
                             ANALYSIS DATE:
                             METHOD:                               GCMS                           GCMS                   GCMS               GCMS
                             ANALYSIS DATE:           03/07/93                      03/07/93                       03/06/93           03/06/93
                             METHOD:                             GCECD                         GCECD                   GCECD               GCECD
                             ANALYSIS DATE:                    03/15/93                       03/15/93
                             MATRIX:                             TISSUE                        TISSUE              OIL                OIL
                             SUBMAT:
                             SAMPLVJT:
                             WETWT:                                                               5.139
                             DRYWT:                                10.00                          0.62
         (o
                             WI`UNITS:                           GRAMS DRY                     GRAMS DRY                GRAMS DRY          GRAMS DRY
                             PCTSOLIDS:
                             VOL.-                                                                                        1.00                1.00
                             VOLUNITS:                           LITERS                        LITERS              AMPOULLE           AMPOULLE


                             TOTAL BHC'S                           0.30  J                        0.00  ND
                             TOTAL CHLORDANES                      0.80  J                     102.72
                             TOTAL DDT'S                           1.55  J                     104.94
                             TOTAL PCB'S                             4.0                       2394.1


                             ALPHA-BFIC                            0.00  ND                       0.00  ND
                             HCB                                   0.05  J                        0.00  ND
                             BETA-BHC                              0.00  ND                       0.00  ND
                             GAMMA-BHC                             0.30  J                        0.00  ND
                             DELTA-BHC                             0.00  ND                       0.00  ND
                             HEPTACHLOR,                           0.23  J                        15.58
                             HEPTA-EPOXIDE                         0.18  J                        0.00  ND
                             OXYCHLORDANE                          0.00  ND                       14.40






                                                         Antarctic Palmer Fish Samples Pesticides and PCB Data


                             INVEST#:                  PROC BLANK                   NIST REF TISSUE
                             ID:                       LAB QA SAMPLE                LAB QA SAMPLE
                             LABSAMNO:                 Q4636                        Q4637
                             UNIT:                                  ng/g                          ng/g
                             ,Analyte (Cont)                        Conc DB QUAL                  Cone DB QUAL

                             GAMMA-CHLORDANE                        0.00  ND                     19.30
                             ALPHA-CHLORDANE                        0.17  J                      22.63
                             TRANS-NONACHLOR                        0.22  J                      18.33
                             CIS-NONACHL)OR                         0.00  ND                     12.48
                             ALDRIN                                 0.00  ND                      0.00  ND
                             DIELDRIN                               0.00  ND                     10.85
                             ENDRIN                                 0.19  j                       0.00  ND
                             MIREX                                  0.00  ND                      0.78  J
                             2,4'DDE (0,PDDE)                       0.00  ND                      0.00  ND
                             4XI)DE (P,P'DDE)                       0.36  J                      37.31
                             2,4'DDD (0,P'DDD)                      0.11  1                       6.55
                             4.4'DDD (P.P'DDD)                      0.35  J                      46.27
                             2.4'DEYr (0,P'DEM                      0.27  J                      11.73
                             4,4'DI)T (P,PDDT)                      0.44  J                       3,08  J


                             PCB # (CLORINATION)


                             8 (CL2)                                0.24  ND                      8.62
                             18 (CL3)                               0.20  ND                     15.64
                             28 (CL3)                               0.00  ND                    148.07
                             44 (CIA)                               0.34  ND                     91.44
                             52 (CIA)                               0.13  ND                    112.78
                             66 (CL4)                               0.11  j                     155.22
                             101 (CL5)                              0.00  ND                    122.20
                             105 (CL5)                              0.10  j                      79.60
                             110/77 (CL5/4)                         0.00  ND                      0.00  ND
                             118/108/149(CL5/5/6)                   0.11  1                     141.81
                             128 (CL6)                              0.00  ND                     17.85
                             138 (CL6)                              1.30                        127.38
                             126 (CL5)                                    NA                            NA
                             153 (CL6)                              0.65  J                     121.20
                             170 (CL7)                              0.00  ND                      0.00  ND
                             180 (CL7)                              0.56  J                      14.83
                             187/182/159(CL7/7/6)                   0.41  J                      27.29






                                                            Antarctic Palmer Fish Samples Pesticides and PCB Data


                               INVEST#:                   PROC BLANK                     NIST REFTISSUE
                               ID:                       LAB QA SAMPLE                   LAB QA SAMPLE
                               IABSAMNO:                  Q4636                          Q4637
                               UN11%                                    ng/g                            ng/g
                              lAnalyte (Cont)                           Conc DB QUAL                    Cone DB QUAL

                               195 (CLS)                                0. 19 1                         0.00 ND
                               206 (CL9)                                0.21  J                         0.00  ND
                               209 (CLIO)                               0.22  J                         0.00  ND

                               Surrogate Recoveries
                               DBOFB%:                                  34.7                            33.3
                               PCB#103%-                                56.7                            53.2
                               PCB#198%:                                53.7                            49.6


                               PCB #(CHLORINATION)

                               7 (CL2)                                  0.00  ND                        0.00
                               15 (CL2)                                 0.00  ND                       50.54
                               24 (C1.3)                                0.00  ND                        5.77
                               16/32 (CL3)                              0.00  ND                       26.82
          Ln                   29 (CL3)                                 0.04  J                         0.00  ND
                               26 (C1.3)                                0.00  ND                       15.83
                               25 (CL3)                                 0.00  ND                       15.70
                               50 (CIA)                                 0.00  ND                       32.19
                               31 (CL3)                                 0.00  ND                        0.00  ND
                               33 (CL3)                                 0.00  ND                       12.41
                               22 (CL3)                                 0.00  ND                       13.77
                               45 (CIA)                                 0.00  ND                       10.92
                               46 (CIA)                                 0.00  ND                        4.69
                               49 (CIA)                                 0.14  J                        124.60
                               47/48 (CIA)                              0.00  ND                       93.80
                               37/42 (CL4)                              0.00  ND                       67.63
                               41/64 (CIA)                              0.00  ND                       73.35
                               40 (CIA)                                 0.00  ND                       13.19
                               100 (CL5)                                0.00  ND                        0.00  ND
                               74 (CIA)                                 0.00  ND                       93.84
                               70 (CIA)                                 0.00  ND                       145.06
                               88 (CL5)                                 0.00  ND                       23.70
                               60/56 (CL5)                              0.00  ND                       88.26






                                                         Antarctic Palmer Fish Samples Pesticides and PCB Data


                             ffqvFzr#:                 PROC BIANK                    NIST REF TISSUE
                             ID:                       IAB QA SAMPLE                 LAB QA SAMPLE
                             LABSAMNO:                 Q4636                         Q4637
                             Uw.                                    ng/g                           ng/g
                            ,Analyte (Cont)                         Conc DB QUAL                   Conc DB QUAL

                             92? (CL5)                              0.00   ND                    30.75
                             84? (CL5)                              0.00   ND                      0.00   ND
                             99 (CL5)                               0.00   ND                    70.32
                             83 (CL5)                               0.00   ND                      6.47
                             97 (CL5)                               0.00   ND                    38.54
                             87 (CL5)                               0.11   1                     59.16
                             85 (CL5)                               0.00   ND                    28.29
                             136 (CL6)                              0.00   ND                      7.76
                             82 (CL5)                               0.00   ND                    17.44
                             151 (CL6)                              0.00   ND                    21.88
                             107/108/144(CL5/5/6)                   0.00   ND                    22.67
                             149 (CL6)                              0.12   J                     56.22
                             188 (CL7)                              0.47   J                       2.00   J
         cc                  146 (CL6)                              0.11   j                     23.62
         (n                  141 (CL6)                              0.09   j                       0.00   ND
         w                   137 (CL6)                              0.00   ND                      1.48   J
                             UNK (CL6)                              0.00   ND                      6.53
                             158 (CL7)                              0.00   ND                    12.76
                             129 (CL6)                              0.00   ND                      0.00   ND
                             178 (CL7)                              0.00   ND                      4.41
                             183 (CL7)                              0.00   ND                    14.64
                             167 (CL6)                              0.00   ND                      5.06
                             185 (CL7)                              0.00   ND                      0.00   ND
                             174 (CL7)                              0.00   ND                      0.36   J
                             177 (CL7)                              0.00   ND                    11.13
                             156/171/202(CL6/7/8)                   0.00   ND                      9.60
                             200 (CLS)                              0.00   NID                     0.00   ND
                             172 (CL7)                              0.26   J                       4.27
                             191 (CL7)                              0.00   ND                      0.00   ND
                             201 (CL8)                              0.00   ND                      0.00   ND
                             196 (CL8)                              0.00   ND                      2.89   J
                             189 (CL7)                              0.00   ND                      0.83   J
                             IQ& WT.R)                              n.iA   T                       I.AA   T
                                   ---1                             - - -  -                       - --   -
                             205 (CL9)                              0.00   ND                      0.91   j




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                                                                   Antarctic Palmer Fish Samples Metal Data


           INVESr#:               C. NEGLECrA              CORIICEPS         CACERATUS            N. GIBBERIFRONS           N. GIBBERIFIRONS                 CORIICEPS
           ID:                    LOWE ISLAND          LOWE ISLAND           LOWE ISLAND              DALLMAN BAY               DALLMAN BAY            BAHIA PARAISO
           LABSAMNO:                      J2013                  J2014                 J2015                    J2016                     J2017                   J2018

           SAMPLE rfPE-                    SAMP                  SAMP                  SAMP                     SAMP                      SAMP                    SAMP
           COLLECIION DATE:            03/28/92              03/28/92             03/28/92                  04/05/92                  04/05/92                04/22/92
           MATRIX                        TISSUE                TISSUE                TISSUE                   TISSUE                    TISSUE                  TISSUE
           ADGDAT                 10/13/92              10/13/92             10/13/92             10/13/92                  10/13/92                   10/13/92
           HGDGDAT                10/09/92              10/09/92             10/09/92             10/09/92                  10/09/92                   10/09/92
           SAMPTYPE                   SAMP                 SAMP                   SAMP                    SAMP                     SAMP                      SAMP
           Acid Digest Wt:                0.211                  0.203                 0.195                    0.202                     0.207                   0.034
           Hg Digest Wt                   0.204                  0.192                 0.204                    0.192                     0.190                   0.185
           WrUNrrS:                     GRAMS DRY             GRAMS DRY             GRAMS DRY                GRAMS DRY                 GRAMS DRY                GRAMS DRY

           War                             (pptn)                (PPM)                 (PPM)                    (pprn)                    (PPM)                   (PPM)

           Ag                             0.000  ND              0.113J                0.000 ND                 0.244                     0.000 ND                0.672 J
           As                                2.5                   4.9                 12.9                       5.9                       5.5                    0.6  J
           Cd                              0.04  J               2.05                  1.63                     5.12                      0.02  J                 4.76
                                             2.2                   0.3J                 2.5                       2.2                       1.4                    0.4  J
           @ru                             1.08  1               3.03                  3.22                     4.66                      0.48  J                 8.05
           4Fe                             36.3  J                126                    85                     317                       13.6  J                  147  J
           Hg                             0.226                  0.182                 0.517                    0.124 J                   0.218                   0.146 J
           N1                              1.14                  0.29 J                3.66                     2.07                      0.98                    1.58  J
           Pb                              0.06  J               0.02 J                0.03 J                   0.13  J                   0.05  J                 0.25  J
           Se                              2.17  J               6.39                  5.72                     7.91                      3.21                    6.05  J
           Sn                              0.00  ND              0.04 J                0.00 ND                  0.00  ND                  0.01  1                 0.00  ND
           Zn                                 38                   84                    89                        81                        21                    102






                                                                 Antarctic Palmer Fish Samples Metal Data


                 INVEST#:                     COR11CEPS                   CORIICEPS                  CORIICEPS        CINDER CONES            CINDER CONES
                 ID:                    BAHIA PARAISO             PALMER STATION             PALMER STATION                     REPL. I                  REPL.2
                 LABSAMNO-                          J2019                      J2020                       J2021                   J2022                   J2023


                 SAMPLE TYPE:                       SAMP                       SAMP                        SAMP                    SAMP                    SAMP
                 COLLECTION DATE:               04/22/92                   03/29/92                   03/29/92                12/05/91                12/05/91
                 MATRIX:                         TISSUE                       TISSUE                     TISSUE                 TISSUE                  TISSUE
                 ADGDAT                 10/13/92                 10/13/92                   10/13/92                    10/13/92                10/13/92
                 HGDGDAT                10/09/92                 10/09/92                   10/09/92                    10/09/92                10/09/92
                 SAMPTYPE                     SAMP                      SAMP                        SAMP                     SAMP                    SAMP
                 Acid Digest Wt:                    0.193                      0.195                       0.203                   0.200                   0.182
                 Hg Digest Wt                       0.203                      0.188                       0.193                   0.187                   0.214
                 VnUNITS:                        GRAMS DRY                   GRAMS DRY                  GRAMS DRY               GRAMS DRY               GRAMS DRY


                 UNIT:                              (PPM)                       (PPM)                      (PPM)                   (PPM)                   (PPM)

                 Ag                                 0.000 ND                   0.094  J                    0.000 ND                1.917                   3.014
                 As                                    1.8                        4.5                        0.7 J                 19.9                    24.2
                 Cd                                  0.03 J                      1.23                      0.02  J                 23.14                   24.57
                 Cr                                    1.9                        1.1                        1.1                   27.6                    91.0
       to        Cu                                  1.46                       6.08                       1.18  j                 15.14                   16.67
        ul
                 Fe                                  26.3 J                      377                       28.5  J                 9578                    7119
                 Hg                                 0.165 J                    0.170  J                    0.372                   0.026J                  0.037J
                 N1                                  1.14                       0.68  J                    0.76  J                 20.7                    59.4
                 Pb                                  0.12 J                     0.32  J                    0.14  J                 0.95                    1.07
                 Se                                  0.87 J                     6.46                       0.60  J                 16.3                    19.1
                 Sn                                  0.01 1                     0.00  ND                   0.00  ND                0.00 ND                 0.02 J
                 Zn                                     29                         79                         36                    186                       70






                                                                   Antarctic Palmer Fish Samples Metal Data


                   INVEST#:              CINDER CONES              BERNACCHI           BERNACCHI           OUTFALL           OUTFALL          WINTER QUARTERS
                   ID:                              REPL.3         105'REPL.1           105'REPL.2         60'REPLI          60'REPL2                    70'REPL.I
                   LABSAMNO:                         J2024                J2025               J2026             J2027            J2028                        J2029

                   SAMPLE TYPE:                      SAMP                 SAMP                SAMP              SAMP             SAMP                         SAMP
                   COLLEC71ON DATE:              12/05/91             12/10/91            12/10/91         12/12/91         .12/12/91                     12/09/91
                   MATRIX:                         TISSUE               77SSUE              TISSUE            TISSUE           TISSUE                       TISSUE
                   ADGDAT                 10/13/92               10/13/92             10/13/92             10/13/92          10/13/92         10/13/92
                   HGDGDAT                10/09/92               10/09/92             10/09/92             10/09/92          10/09/92         10/09/92
                   SAMPTYPE                     SAMP                 SAMP                SAMP               SAMP              SAMP                   SAMP
                   Acid Digest Wt:                   0.196                0.207               0.201             0.200            0.205                        0.208
                   Hg Digest Wt                      0.190                0.212               0.213             0.198            0.190                        0.204
                   WTUNITS:                       GRAMS DRY            GRAMS DRY           GRAMS DRY GRAMS DRY GRAMS DRY                                   GRAMS DRY

                   UNr1%                             (PPM)                (PPM)               (PPM)             (PPM)            (PPM)                        (PPM)

                   Ag                                2.653                1.916               1.783             1.004            0.961                        0.823
                   As                                21.4                 19.2                18.7              23.8             22.9                         35.5
                   Cd                                22.31                11.79               11.23             10.36            10.54                        11.01
                   Cr                                17.6                 20.7                33.5              47.7             73.7                         36.8
                                                                                                                                                              26.26
           Ln      Cu                                14.31                9.21                9.07              20.07            19.05
           0)      Fe                                7920                 8923                8197              22778            20500                        20985
                   Hg                                0.033 J              0.023 J             0.000 ND          0.048 J          0.042 J                      0.070 J
                   Ni                                13.3                 24.4                30.2              38.4             53.7                         29.2
                   Pb                                0.87                 1.11                1.10              12.3             11.8                         13.5
                   Se                                14.9                 8.77                8.80              8.59             8.61                         9.19
                   Sn                                0.53  J              0.00  ND            0.05  J           0.00  ND         0.04  J                      0.19  1
                   Zn                                  173                  168                 151               160              162                          174






                                                                Antarctic Palmer Fish Samples Metal Data


               INVEST#:              WINTER QUARTERS             WINTER QUARTERS             BAY OF SAILS         CINDER CONES           WINTER QUARTERS
               ID:                              70'REPL.2                   70'REPL.3               REPL. I        T BERNACCHII                      70'REPL.
               LABSAMNO:                             J2030                       J2031                 J2032                 J2033                        J2064


               SAMPLETYPE:                           SAMP                        SAMP                  SAMP                  SAMP                         SAMP
               COLLECTION DATE:                  12/09/91                    12/09/91             12/06/91               12/09/91                    12/09/91
               MATRIK                              TISSUE                      TISSUE               TISSUE                 TISSUE                      TISSUE
               ADGDAT                10/13/92                    10/13/92                    10/13/92             10/13/92               11/17/93
               HGDGDAT               10/09/92                    10/09/92                    10/09/92             10/09/92
               SAMPrYPE                     SAMP                        SAMP                      SAMP                  SAMP                     SAMP
               Acid Digest Wt,                       0.197                       0.201                 0.204                 0.209                        0.146
               Hg Digest Wt                          0.201                       0.191                 0.224                 0.198
               WI'UNII'S:                         GRAMS DRY                   GRAMS DRY            GRAMS DRY               GRAMS DRY                  GRAMS DRY

               UNM.                                  (PPM)                       (PPM)                 (PPM)                 (PPM)                        (PPM)

               Ag                                    0.724                       0.049J                2.286                 0.047 J                      0.307
               As                                    35.0                        35.2                  25.3                  23.9                         16.2
               Cd                                    10.29                       0.36                  16.75                 0.63                         17.8
               Cr                                    28.1                        11.7                  85.9                  36.3                         48.0
               Cu                                    25.33                       4.05                  12.40                 3.04                         13.01
         01    Fe                                    31848                       276                   7695                    775                        1464
               Hg                                    0.028 J                     0.316                 0.007J                0.129 J                      0.1091
               Ni                                    21.7                        3.26                  62.8                  8.86                         32.2
               Pb                                    16.5                        0.89                  1.17                  0.31  J                      4.08
               Se                                    8.74                        3.85                  16.3                  4.52                         10.77
               Sn                                    0.37  J                     2.02                  0.00 ND               0.10  1                      1.11 1
               Zn                                      174                         75                  163                      79                        210




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                                            Method Detection IAmits - Aromatics




                            Sediments                                              Tissues

                              Compound                 May '94                     Compound                May'94
                        Sample Dry Weight (g)             15                 Sample Dry Weight (10
                          FInal Volume (ml)               I                    Mal Volume (ml)
                                Units                 ng/g Dry                       Units                ng/g Dry



                           NAPHTHAIENE                    1.1                   NAPH711ALENE                  6.2
                         Cl-NAPHTHALENES                  2.3                 Cl-NAPETHALENES                 19.6
                         C2-NAPH7MAIENES                  1.2                 C2-NAPH71HALENES                17.3
                                                                          C3- & C4-NAPHrHALENES               24.8
                              BEPHENYL                    0.4                      BEPHENYL                   9.2
                                                          `3


                         ACENAPHTHYIENE                   0.5                 ACENAPHTHYLENE                  7.3
                          ACENAPHTHENE                    0.6                  ACENAPHIMENE                   8.5
                              FLUORENE                    0.6                      FLUORENE                   9.3
                        C I - to C3-FLUORENES             1.2                CI- to C3-FLUORENES              18.6
                          PHENANTHRENE                    0.6                  PHENANTHRENE                   3.5
                           ANTHRACENE                     0.5                   ANTHRACENE                    2.3
                    C I - to C4-PHENANTFMNES                             Cl- to C4-PHENANTHRENES
                             &ANTHRACENES                 1.1                     &ANTHRACENES                29.9
                        DIBENZOTMOPHENE                   0.5                DIBEN7.01MOPHENE                 2.2
                 Cl- tO C3-DIBENZ07MOPHENES                I          CI- tO C3-DI13ENZOTMOPHENES             4.4
                          FLUORANnMNE                     0.3                  FLUORk@MMNE                    4.2
                               PYRENE                     0.4                       PYRENE                    4.4
                      CI-FLUORANnHEENES &                                  Cl-FLUORANTHENES &
                                & PYRENES                 0.7                        & PYRENES                8.7
                         BENaANTHRACENE                   0.4                 BENaANTHRACENE                  5.1
                              CHRYSENE                    0.3                      CHRYSENE                   11.1
                        C I - to C4-CHMENES               0.7                C I - to C4-CHRYSENES            22.1
                        BENMAJORANTHENE                   0.3                BENbFLUORANTHENE                  4
                        BENkFLUORANTHENE                  0.3                BENkFLUORANTHENE                  4
                            BENePYRENE                    0.2                     BENePYRENE                  2.5
                            BENaPYRENE                    0.3                     BENaPYRENE                  4.9
                              PERYLENE                    2.7                      PERY1ENE                   4.8
                           1123cdPYRENE                   0.3                   1123cdPYRENE                  5.6
                         DBahANTHRACENE                   0.4                 DBahANTHRACENE                  2.8
                           BghIPERYLENE                   0.3                   B"ERYLENE                      3

                      2-ACrfHYLNAPHTHALENE                1.2              2-hflrrHYLNAPlfrHALENE             10.5
                      I-ACrrHYLN"HTHAIZNE                 1.1              I-bEgrHMNAPHTHALENE                 9
                     2.6-DDdETHNAPFrrHALENE               0.6             2.6-DIMMHNAPHTHALENE                8.7
                         1.6,74YUKEIHNAPH                 0.7                 1.6,74MMETHNAPH                 12.4
                     I-bCUrHYLPHENANTHRENE                0.5             I-METRYLPHENANTHRENE                14.9


                  bmus based an authentic standards;
                  other compounds estimated from
                 dosest Mated compound.


                                                                 360








                                          NDL Determinations

               Sediment Matrix

                     Sediment was acquired from GERG's Geochemical Prospecting
               archives. Oven dried sediment from the Gulf of Mexico was pre-extracted by
               Soxhlet extraction for four hours with methylene chloride three times. The
               WiLtz - ted sediment was thoroughly homogenized and seven aliquots of 15. 0
               grams were taken. Since this sediment was dry, 15 mL of HPLC grade water
               was added to each and thoroughly homogenized to simulate wet sediment.
               These aliquots were then fortified with the spike solution to yield final
               extract concentrations of -3 ppb for PHC's and -6 ppb for PAH's on a dry
               weight basis. These values are selected to be between I and 5 times the
               MDL based on historical data. Samples were extracted and purified
               according to the GERG SOP-8902. The final volume of extmct was reduced
               to 1.0 111L.

                     The MDL's for all peaks in the spiking solution were calculated
               according to the procedures outlined in the Federal Registry (Vol. 41), No
               209). The MDL for an analyte is the standard deviation of the seven
               replicates times the student's t value (2.681) for a one-tailed test at the 99%
               confidence level with n-1(6) degrees of freedom. For compounds not in the
               spiking solution and not found in the actual matrix at required levels, IdDLs
               were estimated. Dibenzothiophene (DBTj was not available. Therefore the
               MDL levels for phenanthrene was used. For alkylated PAH homologues,
               MDL's were estimated as twice that of a similar authentic compound.
               Homologue clusters can contain a number of isomers complicating the
               determination of the MDL. The MDL for C2-naphthalenes Is assumed be
               twice the MDL for 2.6-dimethylnaphthalene (0.6*2=1.2). If no standard was
               available for a given alkylation, the nearest alkylated homologue or parent
               was used. For example, the MDL for alkylated dibenzothiophenes, was
               assumed to be twice that for DBT. Since both Isomers of the C 1 -
               naphthalenes are present in the spike solution. the MDL for these data was
               assumed to be two times the average of the MDL's for 1-methyl and 2-
               methylnaphthalene. For Cl-fluoranthenes and pyrenes, the MDL was
               assumed to be 2 times the average MDL for fluoranthene and pyrene.

               Tissue Matrix

                     Fresh oyster tissue was purchased from a local market. The tissue was
               thoroughly homogenized and seven aliquots of 10.0 gram wet weight were
               taken. These aliquots were fortified with the spike solution to yield final
               extract concentrations of -3 ppb for PHC's and -6 ppb for PAH's on a wet
               weight basis. These values are selected to be between I and 5 times the
               estimated MDL based on historical data. Analyte levels greater than 10
               times the MDL were not used to calculate to the MDLs by definition.
               Samples were extracted and purified according to the GERG SOP-13903.
               Percent moisture vras determined for the tissue as outlined in GERG SOP-
               8903. The extracts were then sent to the analytical lab for analysis. -using


                                                    361






              GERG SOP-8904 for PHC's and GERG SOP-8905 for PAH's.                    Analyte
              concentrations were calculated on a dry weight basis.
                    The MDL's (Tables 3 & 4) for all target analytes were calculated
              according to the procedures outlined in the Federal Registry (Vol. 49. No
              209). The MDL for an analyte is the standard deviation of the seven
              replicates times the student's t value (2.681) for a one-tailed test at the 99%
              vonfidence level with n- 1(6) degrees of freedom. For compounds not in the
              spiking solution and not found in the actual matrix, MDLs, were estimated.
              Dibenzothlophene was not available. Therefore the MDL levels for
              phenanthrene was used. For alkylated PAH homologues, MDL's were
              estimated as twice that of a similar authentic compound. Homologue
              clusters can contain a number of isomers complicating the determination of
              the MDL. The MDL for C2-naphthalenes is assumed be twice the MDL for
              2.6-dimethylnaphthalene (8.3*2=16.5). If no standard was available for a
              given alliylation, the nearest alkylated homologue or parent was used. For
              example, the MDL for alkylated dibenzothiophenes, was assumed to be twice
              that for DBT. Since both isomers of the CI-naphthalenes are present in the
              spike solution, the MDL for these data was assumed to be two times the
              average of the MDL's for I-methyl and 2-methylnaphthalene. For Cj-
              fluoranthenes and pyrenes, the MDL was estimated as 2 times the average
              MDL for fluoranthene and pyrene.


























                                                   362




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                                                         Mussel Watch Year 8 - Bivalve Pesticide and PCB Method Detection Limits



                   RAW         DESIGNATOR           DBOF'B          PCB # 103        PCB #198            HCB           UNDANE               HEFrA-         ALDRIN             HEFrA
                  FILE                            % RECOV           % RECOV          % RECOV                                                CHLOR                          EPOXIDE
                                                                                                         (ppb)            (ppb)             (ppb)            (ppb)


                 91249P            MDL 2            67.6%             66.7%            68.7%             0.71             2.99              1.87             2.19             0.71
                 Q1250P            MDL 3            67.4%             65.5%            68.6%             0.87             3.10              1.95             2.01             0.71
                 91251P            MDL 4            68.8%             68.6%            71.9%             0.82             2.99              2.10             2.13             0.61
                 Q1252P            MDL 5            64.0%             66.0%            67.0%             1.13             2.84              2.12             1.89             1.11
                 91253P            MDL6             67.9%             70.0%            72.2%             0.74             2.84              1.88             2.26             0.52
                 91254P            MDL 7            70.9%             72.0%            72.7%             0.49             2.92              1.76             1.87             0.91
                 Q1255P            MDL 8            64.3%             65.1%            67.2%             0.73             2.75              1.59             1.80             0.91

                 Average                                                                                 0.783            2.919             1.898            2.022            0.781
                 Variance                                                                                0.032            0.012             0.030            0.027            0.037
              Std Deviation                                                                              0.179            0.111             0.172            0.164            0.191
             Coer of Variation                                                                           22.9%            3.8%              9.1%             8.1%             24.5%
                   NDL                                                                                   0.537            0.331             0.515            0.491            0.573
                   LCL                                                                                   0.344            0.212             0.330            0.315            0.367
                   UCL                                                                                   1.182            0.729             1.134            1.081            1.262







                                                          Mussel Watch Year 8 - Bivalve Pesticide and PCB Method Detection uxnits



                  RAW         DESIGNATOR           ALPHA-            TRANS-        DIELDRIN            MIREX          2.4'DDE          4.4'DDE          2.4'DOD          ENDM
                 FILE 0                        CHLORDANE NONACHLOR                                                   (O.F DDE)        RF DDE)          (O.P DDD)
                                                     (ppb)           (ppb)            (ppb)            (ppb)            fppb)            (ppb)            (ppb)            (ppb)


                91249P            MDL2               1.15            21.51            4.16             2.21             1.83             11.49            2.30             2.89
                Q125OF            MDL 3              1.34            22.92            4.51             2,29             1.58             11.98            2@10             2.89
                91251P            MDL 4              1.19            22.41            4.61             2.00             1.61             11.82            2.01             2.86
                91252P            MDL 5              1.74            20.93            4.24             2,37             1.65             11.43            2.02             2.66
                91253P            MDL6               1.10            21.77            4.31             2.54             1.62             11.36            1,78             2.68
                91254P            MDL 7              1.45            21.38            4.03             2.30             1.49             11.98            1.79             2.69
                91255P            MDL 8              1.74            22.10            3.96             2.00             1.72             11.95            1.62             2.40

                Averap                               1.387           21.860           4.259            2.2"             1.644            11.720           1.945            2-n2
                Variance                             0.063           0.384            0,049            0.033            0.010            0.064            0.046            0.027
             Std De-Aaffon                           0.251           &620             0,221            0.181            0.098            0.252            0,214            0.163
            Coef of Variation                        18.1%           2.8%             5.2%             8.1%             6.0%             2.2%             11.096           610%
                  MDL                                0.752           1.858            01663            0.543            0.295            0.756            0.642            0.488
                  LCL                                0.481           1.189            0.424            0,347            0.189            O@484            0.411            0.313
                  UCL                                1.653           4.MS             1.458            1.194            0.650            1.662            1.413            1.074



























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                                                            Mussel Watch Year 8 - Btvalve Pesticide and PCB Method Detection Limits


                    RAW         DESIGNATOR            4.4@ DDD          2X DtYr            4.4'DEYr           PCB #8            PCB 018           PCB #29            PCO #44            PCB #62
                  FIIZ                               (P.V DDD)          10,P D"           (P,F DDII              (CL2)              (CL3)             (CL3)             JCL4)              ICIA)
                                                         (ppb)             (ppb)              (ppb)              (ppb)              (ppb)             (ppb)             (ppb)              Jppb)

                  91249P             MDL2                3.68              1.12               2.96               1.9                0.9               2.2               2.4                2.7
                  91250P             MDL3                3.59              1.01               2.98               1.6                0.9               2,2               2.5                3.4
                  91251P             MDL4                3.77              0.94               2.92               1.5                1.0               1.9               2.5                3.4
                  91252P             MDL 5               3.93              1.39               2.93               2,1                1.4               2-0               2.5                3.7
                  91253P             MDL6                3.62              0.91               2.77               1.8                1.1               2.0               2.5                3.1
                  91254P             MDL 7               3.56              1.17               2.78               1.5                1.1               2.1               2.5                3.2
                  91255P             MDL 8               3.58              1.20               2.61               1.2                1.1               1.8               2.3                3.4
                  Averap                                 3-SW              1.108              2."S               1.640              1.076             2.039             2.456              3.253
                  Variance                               0.016             0.024              0.016              0.078              0.030             0.014             0.006              0.094
               Std Dwe-viation                           0.128             0.166              0.126              0.280              0.174             0.118             0.080              0.3ve
             Coef of Variation                           3.5%              14.1%              4.4%               17.1%              16.2%             5.8%              3.34b              9.4%
                    UDL                                  o.384             0.488              0.979              0.8"               0.522             0.354             0.241              0.917
                     LCL                                 0.246             0.299              0.242              0.537              0,334             0.227             0.154              0.587
                     UCL                                 0.845             1,029              0.833              1.847              1.148             0.779             0.530              2.017








                                                            Mussel Watch Year 8 - Bivalve Pesticide and PCB Method Detection Lhnits



                       RAW        DESIGNATOR          PCB #66          PCB#101          PCB #105       PCB# 110/77        PCB # 118        PCB #128         PCB #138         PCB#126
                     FILE                               (CIA)            (CLS)            (CL5)            (CL5/4)          (CL5)            (CL6)              (CLS)           (CL5)
                                                        (ppb)            (ppb)            (ppb)            (ppb)            (ppb)            (ppb)              (ppb)           (ppb)


                     91249P           MDL2               2.9              2.7              3.0              3.0              3.5              2.9               8.1              1.9
                     91250P           MDL3               2.5              2.9              3.2              3.6              3.5              3.0               7.8              115
                     91251P           MDL4               2.6              2.8              3.1              3.7              3.3              2.8               13.6             2.0
                     91252P           MDL 5              2.5              3.1              4.0              2.7              3.6              3.0               7.7              2.3
                     91253P           MDL 6              2.6              2.6              3.0              2.9              3.2              3.0               911              1.8
                     91254P           MDL 7              2.6              2.9              3.6              2.8              3.5              3.2               8.1              2.0
                     91255P           MDL 8              2.5              3.1              3.6              3.4              3.2              2.7               7.9              L7

                     Average                            2.597            2.876            3.347            3.156            &397             2.957              8.887           1.911
                     Variance                           0.017            0.029            0.128            0.138            0.024            0.018              3.871           0.058
                 Std Devlatlon                          0.129            0.171            0.358            0.371            0.156            0.133              1.967           0.241
                Coef of Variation                       5.0%             5.9%             10.7%            11.8%            4.6%             4.5%               22.1%           12.6%
                       NDL                              0.386            0.512            1.074            1.113            0.467            0.400              5.898           0.722
                       LCL                              0,247            0.328            0.688            0.712            0,299            0.256              3.775           0.462
                       UCL                              0.850            1.127            2.363            2.449            1.028            0,880              12.976          1.589








                                                            Muswl Watch Year 8 - BNake Pesticide and PCD Metbod Deteeftn tlvdto



                      RAW         DMMONATOR          PCO #153          PCs #170         PCO #ISO         PCB #187         PCs 0195         PCO #206         PCO OM
                     FILE                               (eta)             (CL7)           (CL7)            (CL71            (CLS)              (Cla)           ICLIO)
                                                        (Ppb)             (Ppb)           (ppb)            Ippb)            (ppb)              (ppb)           (ppb)


                     01249P           MDL2               5.3              wr               4.2              6.1              2.6               1.2             10.0
                     91250P           MOL 3              516              Mr               4.3              6.0              2.7               '1.7            10.5
                     01251P           MDL4               5.5              Mr               4.1              &4               2.3               1.7             10.5
                     91252P           MDL 5              6.8              wr               4.4              5.8              2.8               1.5             10.5
                     91263P           MDL6               515              lNr              4.4              6.0              1.9               1.4             10.4
                     91254P           MDL 7              6.3              Imr              4.4              5.6              2.5               1.4             10.0
                     9 12rasp         MDL 8              6.2              Mr               4.4              5.8              2.8               1.1             10,6

                     Averap                             5."s                              4.312            5IMS             2.516              1.436           10.327
                     varunce                            0.275                             0.014            0.056            M087               0.039           O.Ow
                 Std Deviatift                          0.524                             0.119            0,238            0.296              0.197           0.196
                Cftf Of Vatuflork                       &9%                               Z8%              4.1%             11.7%              13.7%           1.9%
                      MM                                1.872                             0.3"             0.712            OAM                0.501           01587
                      LCL                               1,006                             0.229            0.456            0.567              0,378           0.376
                      UCL                               3,458                             0.789            1.567            1.949              1.301           1.292





             0)
             OD




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                                          Mussel Watch Project Year 8 - Trace Metal Method Detection Limits


                                   Ag       Al      As     Cd       Cr    CU      Fe      Hg     Mn NI           Pb    Sb       Se      Sn      Zn
                                  PPM      PpIn PpIn       ppm PpIn PPM PPM               PpIn ppm      ppm PPM        PPM     PpIn    ppm PPM


                  Sediments


                  T-1                0.128    3476   4.17   0.275    2.03    4.23    378  0.113     126     4.9  *3.81  0.325   0.429   0.333    41.2
                  T-2                0.129    3414   4.18   0.273    2.01    4.24    379  0.113     127   4.63    3.71  0.378   0.347   0.325    41.7
                  T-3                0.128    3430   4.11   0.259        2   4.33    387  0.108     125   5.03    3.67  0.317   0.427     0.33   40.8
                  T-4                0.122    3416   4.02   0.265    2.02    4.04    387  0.109     126   4.95    3.71  0.313   0.412   0.297    40.8
                  T-5                0.125    3469   4.02   0.273        2   4.24    384  0.111     124   4.94    3.77  0.288   0.354   0.293    42.1
                  T-6                0.116    3551   4.17   0.273    2.02    3.89    382     0.11   124   5.01      3.8 0.327   0.376   0.311    40.9
                  T-7                0.123    3571   4.23   0.264        2   4.31    379  0.109     126   5.04    3.71  0.404   0.379   0.295    40.7
                  T-8                0.124    3559   4.06   0.273    2.05      4.2   384  0.112     124   4.77    3.73  0.366   0.398   0.276      41
                  Standard Dev.      0.004    65.9   0.08   0.006   0.018   0.148    3.59 0.002    1.16   0.142  0.049  0.039   0.031   0.021    0.499
                  MDL                0.013     198   0.24   0.018    0.05   0.044      11 0.006     3.5     0.4   0.15      0.1     0.1     0.1    1.5


                  Tissues


         CA       S-1                0.281    3.54   0.73   0.201   0.494    3.22    178  0.127           1.22   0.745            2.16  0.819      14
         4        S-2                0.274    3.64  0.637   0.196   0.499    3.22    176  0.123           1.19   0.878              2.2 0.753    14.5
         0        S-3                  0.27    3.2  0.703     0.19  0.446    3.27    170  0.125           1.22   0.715            2.08  0.787    14.4
                  S-4                0.267    3.21  0.695      0.2  0.537    3.15    174  0.121           1.31   0.691              2.1 0.848    14.7
                  S-5                  0.26    3.2  0.786   0.192    3535    3.24    174  0.135           1.31   0.738            2.04  0.753    14.5
                  S-6                0.253     3.8  0.834   0.191   0.437    3.12    172  0.124           1.16    0.75            2.15  0.803    14.1
                  S-7                0.266    3.62  0.843   0.194   0.498    3.19    175  0.134           1.06   0.699            2.16    0.85   13.7
                  S-8                0.249    3.46  0.771   0.195      0.4     3.1   170  0.122           1.21   0.767            2.13  0.846    13.7
                  Standard Dev. 0.0152       0.232  0.072   0.004   0.049    0.06   2.825 0.005           0.081  0.032          0.051     0.04   0.382
                  MDL                0.035     0.7     0.2  0.012    0.15    0.18    8.5  0.016           0.24      0.1           0.15    0.12     1.2























                                                                                                                                                      DATE, DUE















                                                                                                                          GAYL(DRDINo. 2333                                                        1 PRI;@"D 1:: 0 5 A



















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