[From the U.S. Government Printing Office, www.gpo.gov]



                                                                 NOAA STATUS AND TRENDS
                                                                                            Mussel Watch Project
                                                                                                                         Analytical Data
                                                                                                                                               Year VI
                                                                                                                                        WO-
                                                                                                                               ?M.K:M '17
                                                                                                                                                                                              M.-FIEFF.-.3
                                                                                                                        . . . . . . . . . . . . . . . . ..................                                                                  ........        ........             . .......................
                                                                                                                                     ............                                                                                                                       ... .....................
                                                                                                                                                                                                                                                           . ..... ...... ....................
                                                                                                                                                                                                                                            .......... ..
                                                                                                                               The Geochemical and
                                                                                                                               Environmental Research Group
                                                                                                                               Texas A&M Research Foundation







                                                                                                                                                                                                                                                                                               ............
                                                                                                                                                                                                                                                                                          ...................
                                                                                                                                                                                                                                                                   .......................................

                                                                                                                                                                                                                                                                                          . ...............
                                                                                                                                                                                                                          ... ..                                                             .........
                                                                                                                                                                                                                          ......                                                                            .......
                                                                                                                                                                                                                                                                                                   d        E,a:
                                                                                                                                                                                                                          N"

                                                                                                                                                                                                                                                                                             . ..........
                                                                                                                                                                                                                                                                                               .. .........
                                                                                                                                                                                                                          ..........
                                                                                                                                                                                                                                                                               ...........
                                                                                                                                                                                                                                                                                          X-3.2
                                                                                                                                                                                                                                                              ...                 ..........
                                                                                                                                                                                                                                            C
                                                                                                                                                                                                                                                   I    04i al'Y' I
                                                                                                                                                                                                                                                                         ....................................
                                                                                                                                                                                                                                                                                          ..............    ...
                                                                                                                                                                                                                                                                                                   ...........
                                                                                                                                                                                                                                                               .............................................
                                                                                                                                                                                                                                   .... .................................
                                                                                                                                                                                                                                . ..... .......
                                                                                                                                                                                                                                               . . . . . . . . . . . . . . . . . . ...... .. . . . . . . . . . . . . . . . . . . . . . . . . . .
                                                                                         7N






                                                        IOD-00T                                                                                                                                          woww                                                  3V 0019


                                                                                                                            At





                                                                                                                                                               Miss                   Alabama

                                                                                   Texas
                                                                                                                                  Louisiana                                                                               Florida                                      3VOCM







                                                                                                                                        GULF                      OF                 ME)WO




                                Q H
                                541.5
                                                                                                                                                                                                                                                                               Be cow
                     L31:IKU






                                    C65
                                A63
                                year 6
                                (1992)                                                                                                    April 1992











                                                              NOAA STATUS AND TRENDS
                                                                     Mussel Watch Project
                                                                            Analytical Data

                                                                         Table of Contents



                  Field Site Data              .................................................................................................................. 1


                  Field Station Data                ............................................................................................................ 4


                  131VALVES         .......................................................................................................................... 10


                             Aromatics Data               ..................................................................................................... 11
                             Aromatics QA/QC Data.                 ......................................................................................   42
                                        Aromatics Blanks, Spikes and QC Data                             ...........................................        43
                             Pesticides and PCBs Data                       ................................................................................. 80
                             Pesticides and PCBs QA/QC Data                               .................................................................. 105
                                        Duplicate Pesticide/PCBs                 ...........................................................  .........  106
                                        Pesticides and PCBs Blanks                          ................................................................ Ill.
                                        Pesticides and PCBs Spikes                          ................................................................ 116
                                        Pesticides and PCBs - NIST Data                              ...................................................... 125
                             Trace Metals Data                  ............................................................................................... 130
                                        Trace Metal Certified Reference Materials                                      .................................. 137
                             Trace Metal QA/QC Data.                  .................................................................................. 139
                                        Trace Metal Duplicates                      ......................................................................... 140
                                        Trace Metal Matrix Spikes and Blanks                                    .......................................... 144
                                        Mercury Duplicates, Spikes, Reference
                                        Material and Blanks              ................................................................................ 148
                             Method Detection Limits                        ................................................................................. 152
                                        Aromatics Method Detection Limits                                  ............................................... 153
                                        Pesticides and PCBs Method Detection Limits                                           ........................... 157
                                        Trace Metals Method Detection Limits                                     ......................................... 164
                                        Organotin TBT18 Method Detection Limits                                          ................................ 166
                             Percent Upids and Dry Weight Data                           .............................................................   168
                                        Percent Lipids - Duplicates and Spikes                                   ......................................... 173
                             Butyltin Concentrations                     ...........................w ........................................................ 175
                             Eafection, Condition and Gonadal Data                                  ....................................................... 179




                                                                                                        U - S - DEPARTMENT OF COMMERCE NOAA
                                                                                                        COASTAL SERVICES CENTER
                                                                                                        2234 SOUTH HOBSON AVENUE
                                                                                                        CHARLESTON , SC 29405-24 13


                                                                                                                 Property of CSC                   Library




I
I
I
I
.1
I
I
I
I
II                 Field Site Data
I
I
I
I
I
I
I
I
I                       I






                                                                                  MUSSEL WATCH PROJECT YEAR V1 - Field Site Data




                         Number                                                                                Deg Min       Deg Min M/D/Y                                                  (m)       oc        0/00
                              Site    Si Ite I)rpe                            Name                             Latitude      Longitude        Date         Scientist        Species         Depth    Temp    Salinity NIST

                              1       LMSB      B    SOUTH BAY LOWER LAGUNA MADRE                              26002.58'     97'10.49-       12/18/90       R. Fay        C. virginica      0.10     21.0       39.7
                              2       CCNB      NS   NEUCES BAY CORPUS CHRISTI                                 27'51.17'     97121.55'       12/17/90    D. Wilkinson     C. vtrgintca               22.0
                              3       CCIC      B    INGLESIDE COVE CORPUS CHRISTI                             27050-22'     97014.24'       12/17/90    D. Wilkinson     C. virginica      REEF     20.0       35.0
                              4       ABIR      B    LONG REEF ARANSAS BAY                                     28002.96'     96056.77'       12/18/90    D. Wilkinson     C. virginica      0.30     18.0       31.0        Y
                              5       CBCR      B    COPANO REEF COPANO BAY                                    28008.50'     97007.68'       12/18/90    D. Wilkinson     C. virginica      0.20     21.0       26.0
                              6       MBAR      B    AYRES REEF MESQUITE BAY                                   280 10. 10'   96049.90'       12/17/90    D. Wilkinson     C. virgintca      0.13     22.6       29.0        Y
                              7       SAPP      B    PANTHER PT. REEF SAN ANT)DNIO BAY                         28014. 10'    96042.50'       12/17/90    D. Wilkinson     C. virginica      0.50     19.0       26.0
                              8       SAMP      B    MOSQUITO PT., SAN ANTONIO BAY                             28020.57'     96042.69'       12/18/90    D. Wilkinson     C. virginica      0.20     19.0       25.0
                              9       ESSP      B    SOUTH PASS REEF ESPIRITU SANTO                            28017.83'     96037.50'       12/17/90    D. Wilkinson     C. vtrgtnfca      0.30     21.5       30.0
                              10      ESBD      NS   BILL DAYS REEF ESPIRITU SANTO                             28024.66'     96026.65'       12/19/90    D. Wilkinson     C. virgin(ca      0.25     18.0
                              12      MBGP      B    GALLINIPPER PT., MATAGORDA BAY                            28035.00'     96034.00'       12/18/90    D. Wilkinson     C. vtrgtntca      1.66     19.0       31.0
                              11      MBLR      B    LAVACA RIVER MOUTH MATAGORDA BAY                          29039.62'     96034.72'       12/18/90    D. Wilkinson     C. virgtnica      0.12     20.0
                              13      MBTP      B    TRES PALACIOS BAY MATAGORDA BAY                           28139.43'     96013.25'       12/16/90    D. Wilkinson     C. virginica      0.17     22.3       30.3
                              14      MBEM      B    EAST MATAGORDA MATAGORDA BAY                              28042.64'     95052.96'       12/16/90    D. Wilkinson     C. virginica      0.25     22.0       30.0
                              72      BRCL      B    BRAZOS RIVER CEDAR LAKE                                   28051,46'     95027.75'       12/5/90     D. Wilkinson     C. virgintca      0.20     12.7       30.0
                              57      BRFS      B    FREEPORT SURFSIDE BRAZOS RIVER                            28055.3 1 '   95020.56'       12/5/90     D. Wilkinson     C. virginica      0.43     13.8       28.7        Y
                              18      GBCR      B    CONFEDERATE REEF GALVESTON BAY                            29015.71'     94054.76'       12/6/90     D. Wilkinson     C. virginica      0.20     13.0       26.0
                              58      GBOB      B    OFFATS BAYOU GALVESTON BAY                                29016.96'     94050.08'       12/6/90     D. Wilkinson     C. vtrgintca      0.27     15.7       27.7
                              16      GBTD      B    TODD'S DUMP GALVESTON BAY                                 29029.70'     94053.82'       12/7/90     D. Wilkinson     C. virginica      1.23     13.3       22.0        Y
           N)                 15      GBYC      B    YACHT CLUB GALVESTON BAY                                  .29037.00'    94059.50'       12/6/90     D. Wilkinson     C. virginica      3.50     14.0       24.0
                              59      GBSC      B    SHIP CHANNEL GALVESTON BAY                                29041.97'     94059.37'       2/6/91      D. Wilkinson     C. virginica      1.50     16.0       10.0
                              17      GBHR      B    HANNA REEF GALVESTON BAY                                  29028.58'     94043.22'       12/6/90     D. Wilkinson     C. virgintca      2.00     12.0       23.0
                              19      SLBB      B    BLUE BUCK POINT SABINE LAKE                               29048.00'     93054.42'       12/8/90     D. Wilkinson     C. vtrgintca      1.50     13.0       15.0        Y
                              20      CL.SJ     B    ST. JOHNS ISLAND CALCASIEU LAKE                           29050.00'     93023.00'       12/7/90     D. Wilkinson     C. virgintca      1.75     13.3       27.7
                              60      CLLC      B    LAKE CHARLES CALCASIEU LAKE                               30003.42'     93018.42'       12/8/90     D. Wilkinson     C. virgintca      0.10     15.0       23.0        Y
                              21      JHJH      B    JOSEPH HARBOR BAYOU J. HARBOR BAYOU                       29037.75'     92145.75'       12/7/90     D. Wilkinson     C. virgintca      0.00     13.0       25.0
                              22      VBSP      B    SOUTHWEST PASS VERMILLION BAY                             29034.89'     '92003.14'      1/8/91      D. Wilkinson     C. v"tntca        1.50     12.0       10.0
                              24      ABOB      B    OYSTER BAYOU ATCHAFALAYA BAY                              29014.43'     91008.13'       1/9/91      D. Wilkinson     C. virginica      1.07     14.2       18.7
                              25      CLCL      B    CAILLOU LAKE CAILLOU LAKE                                 29015.42'     90055.9 1'      1/9/91      D. Wilkinson     C. v"tntca        2.00     14.0       14.0
                              26      TBLB      B    LAKE BARRE TERREBONNE BAY                                 29015.60'     90035.70'       1/8/91      D. Wilkinson     C. virginfca      0.17     14.7       19.0        Y
                              27      TBLF      B    LAKE FELICITY TERREBONNE BAY                              29016.17'     90024.43'       1/9/91      D. Wilkinson     C. virgintca      0.10     14.0       26.0
                              28      BBSD      B    BAYOU ST. DENIS BARATARIA BAY                             29024.15'     89059.85'       1/8/91      D. Wilkinson     C. virgintca      2.00     15.0       7.7
                              29      BBMB      B    MIDDLE BANK BARATARIA BAY                                 29016.55'     89056.54'       1/8/91      D. Wilkinson     C. virginica      1.50     16.0       23.0
                              65      MRTP      B    71GER PASS MISSISSIPPI RIVER                              29008.64'     89025.66'       1/11/91     D. Wilkinson     C. virginica      0.10     14.0       10.0
                              31      BSS1      B    SABLE ISLAND BRETON SOUND                                 29024.20'     89029.04'       1/11/91     D. Wilkinson     C. virgintca      1.33     12.7       4.3
                              30      BSBG      B    BAY GARDERNE BRETON SOUND                                 29035.99'     89037.67'       1/10/91     D. Wilkinson     C. vLrgfntca      0.35     17.0       24.0        Y
                              32      LBMP      B    MALHEUREUX POINT LAKE BORGNE                              29052.05'     89040.79'       1/10/91     D. Wilkinson     C. v"inica        0.30     16.0       16.0
                              63      LPGO      BS   GULF OUTLET, LAKE PONCHARTRAIN, LA                        30002.44'     90002.57'       1/25/91     D. Wilkinson     C. vtrgtntca      4.50     11.0       5.0
                              33      MSPC      B    PASS CHRISTIAN MISSISSIPPI SOUND                          30018.13'     89019.70'       1/12/91     D. Wilkinson     C. v"tnLm         0.20     11.0       17.3
                              34      MSBB      B    BILO)a BAY MISSISSIPPI SOUND                              30023.57'     88051.50'       1/12/90     D. Wilkinson     C. virginica      0.10     13.8       3.0
                              35      MSP13     B    PASCAGOULA BAY MISSISSIPPI SOUND                          30020.55'     88035.46        1/13/91     D. Wilkinson     C. virginica      1.00     10.8       6.0
                              36      MBCP      B    CEDAR POINT REEF MOBILE BAY                               30018.62'     88008.24'       1/12/91     D. Wilkinson     C. v(rgintca      0.15     13.0       8.0
                              66      MBHI      B    HOLLINGERS ISLE CHA MOBILE BAY                            30033.88'     88004.58'       1/12/91     D. Wilkinson     C. v(rginica      2.50     15.0       5.0




                                                                                     SAMPLE TYPE B=BIVALVE,S=SEDIMENT,NS=NO SAMPLE






                                                                            MUSSEL WATCH PROJECT YEAR VI - Field Site Data




                        Number                                                                          Deg Min     Deg Min       M/D/Y                                         (m)     0C       0/00
                           site     Site   Type                         Name                            Latitude    Longitude       Date        Scientist       Species      Depth     Temp    Salinity NIST


                           67       PBPH     B    PUBLIC HARBOR PENSACOLA BAY                           30024,53'   87011.48'     1/26/91     D. Wilkinson    C. virginica    6.00     12.0      21.0
                           37       PBIB     B    INDIAN BAYOU, PENSACOLA BAY, FLORIDA                  30028.82'   87007.43'     1/26/91     D. Wilkinson    C. virgtnica    2.00     12.0      25.0
                           73       CBJB     B    CHOCTAWATCHEE BAY JOES BAYOU                          30024.63'   86029.43'     1/27/91     D. Wilkinson    C. virgintca    0.30     12.0      15.0
                           38       CBSR     B    OFF SANTA ROSA CHOCTAWHATCHEE BAY                     30024.79'   86-12.23'     1/27/91     D. Wilkinson    C. virginica    2.83     10.7      12.0       Y
                           39       CBSP     B    SHIRK POINT CHOCTAWHATCHEE BAY                        30028.86'   86028.62'     1/27/91     D. Wilkinson    C. virgintca    0.17     13.7      17.3
                           74       PCLO     B    PANAMA CITY LITTLE OYSTER                             30015.18'   85040.84'     1/28/91     D. Wilkinson    C. vtrginica    0.23     13.2      18.3
                           40       SAWB     B    WATSON BAYOU ST. ANDREW BAY                           30008.53'   85037.93'     1/28/91     D. Wilkinson    C. virginica    0.10     14.0      14.0
                           41       APDB     B    DRY BAR APALACHICOLA BAY                              29040.40'   85004.5 1'    1/28/91     D. Wilkinson    C. virgtnica    0.30     13.0      10.0
                           42       APCP     B    CAT PT. BAR APALACHICOLA BAY                          29043.4 1'  84053.2 1'    1/28/91     D. Wilkinson    C. virgintca    0.35     14.0      22.3
                           75       AESP     B    APPALACHEE BAY SPRING CREEK                           30004.19'   84019.07'     1/29/91     D. Wilkinson    C. virginica    0.10               1.0
                           43       CKBP     B    BLACK POINT CEDAR KEY                                 29110.25'   83003.00'     1/29/91     D. Wilkinson    C. virgin(ca    0.50     16.0      23.0
                           76       TBNP     B    TAMPA BAY NAVAREZ PARK                                27048.30'   82045.28'     1/31/91     D. Wilkinson    C. uirginica    0.01     19.5      34.0       Y
                           47       TBMK     B    MULLET KEY BAYOU TAMPA BAY                            27037.24'   82043.59'     1/30/91     D. Wilkinson    C. virginica    0.25     22.0      35.0
                           44       TBPB     B    PAPYS BAYOU TAMPA BAY                                 27150.72'   82036.75'     1/31/91     D. Wilkinson    C. virginica    0.01     19.0      30.0
                           70       TBOT     B    OLD TAMPA BAY TAMPA BAY                               28001.48'   82037.95'     1/30/91     D. Wilkinson    C. virgtntca    0.20               7.3        Y
                           77       TBKA     B    TAMPA BAY PETER 0. KNIGHT AIRPORT                     27054.53'   82027.26'     1/29/91     D. Wilkinson    C. virgintca    0.30     22.0      27.0
                           46       TBCB     B    COCKROACH BAY TAMPA BAY                               27040,52'   82030.60'     1/30/91     D. Wilkinson    C. virgintca    0.30     27.0      30.0       Y
                           48       CBBI     B    BIRD ISLAND CHARLOTTE HARBOR                          26030.79'   82002.02'     1/31/91     D. Wilkinson    C. virginka     0.40     26.0      30.0
                           71       CBFM     B    FORT MEYERS CHARLOTTE HARBOR                          26033,42'   8 1055.40'    1/31/91     D. Wilkinson    C. virgin(ca    0.30     25.0      19.0
                           49       NBNB     B    NAPLES BAY NAPLES BAY                                 261106.85'  81047.20'     2/1/91      D. Wilkinson    C. utrgifta     0.20     25.0      32.0
                           50       RBHC     B    HENDERSON CREEK ROOKERY BAY                           26001.52'   81044.22'     2/2/91      D. Wilkinson    C. vtrgin(ca    0.25     25.0      34.0
                           51       EVFU     B    FAKA UNION BAY EVERGLADES                             24054.00'   81030.81'     2/2/91      D. Wilkinson    C. virginica    0.15     24.0      15.0
                           81       BHKF     BS   BAHIA HONDA KEY, FLORIDA                              24039.74'   81016.43'     1/22/91     D. Wilkinson CtL stnuosa        0.50     25.0      40.3



























                                                                               SAMPLE TYPE B=BIVALVE,S=SEDIMENT.NS=NO SAMPLE




                                             I
I
I
I
I
I
I
I
I                                          I
I
I                Field Station Data
I
I
I
I
I
I
I
I
                        4
I






                                                                       MUSSEL WATCH PROJECT YEAR VI - Field Station Data




                                       Site      site       Latitude        Longitude     Sample       Date       Collection Bottom Local Time LocalTime                Tidal       Tidal
                                 Number                     Deg Min         Deg Min        Type       M/D/Y         Method         Type   Low Water High Water       Reference    Horizon
                                                                                                                                                                                     (m)


                                       I       LMSB         26002-77'       97010.48'        B        12/18/90         H           N         10:37        19:15      Galveston      0.49
                                       1       LMSB         26002-77'       97010.48'        B        12/18/90         H           N         10:37        19:15      Galveston      0.49
                                       1       LMSB         26002-77'       97010.48'        B        12/18/90         H           N         10:37        19:15      Galveston      0.49
                                       3       CCIC         27050.28'       97114.28'        B        12/17/90         H           SNG       10:02        18:39      Galveston      0.52
                                       3       ccic         27050.28'       97014.28'        B        12/17/90         H           SNG       10:02        18:39      Galveston      0.52
                                       3       ccic         27'50-28'       97114.28'        B        12/17/90         H           SNG       10:02        18:39      Galveston      0.52
                                       4       ABLR         28003-88'       96157.80'        B        12/18/90         H           MNSG      10:37        19:15      Galveston      0.49
                                       4       ABLR         28003.88'       96057.80'        B        12/18/90         H           MNSG      10:37        19:15      Galveston      0.49
                                       4       ABLR         28003.88'       96057.80'        B        12/18/90         H           MNSG      10:37        19:15      Galveston      0.49
                                       5       CBCR         28008-47'       97007.67'        B        12/18/90         H           SM        10:37        19:15      Galveston      0.49
                                       5       CBCR         28'08.47'       97*07.67'        B        12/18/90         H           SM        10:37        19:15      Galveston      0.49
                                       5       CBCR         28'08.47'       97007.67'        B        12/18/90         H           SM        10:37        19:15      Galveston      0.49
                                       6       MBAR         28010.13'       96049.90'        B        12/17/90         H           SM        10:02        18:39      Galveston      0.52
                                       6       MBAR         28010-13'       96049.90'        B        12/17/90         H           SM        10:02        18:39      Galveston      0.52
                                       6       MBAR         28010-13'       96049-90'        B        12/17/90         1-1         SM        10:02        18:39      Galveston      0.52
                                       7       SAPP         28014.22'       96042.57'        B        12/17/90         H           S         10:02        18:39      Galveston      0.52
                                       7       SAPP         28014.22'       96042.57'        B        12/17/90         H           S         10:02        18:39      Galveston      0.52
                                       7       SAPP         28014.221       96042.57'        B        12/17J90         H           S         10:02        18-39      Galveston      0.52
         C.n                           8       SAMP         28120-57'       96042.69'        B        12/18/90         H           SR        10:37        19:15      Galveston      0.49
                                       8       SAMP         28120-57'       96042.69'        B        12/18/90         H           SR        10:37        19:15      Galveston      0.49
                                       8       SAMP         28120.57'       96042.69'        B        12/18/90         H           SR        10:37        19.15      Galveston      0.49
                                       9       ESSP         28ol7.85'       96037. 1 P       B        12/17/90         H           SH        10:02        18:39      Galveston      0.52
                                       9       ESSP         28017-85'       96037. 1 l'      B        12/17/90         H           SH        10:02        18:39      Galveston      0.52
                                       9       ESSP         28017,85'       96037. 11'       B        12/17/90         H           SH        10:02        18:39      Galveston      0.52
                                       12      MBGP         28035-25'       96034.17'        B        12/18/90         D           SR        10:37        19:15      Galveston      0.49
                                       12      MBGP         28035-25'       96'34.17'        B        12/18/90         D           SR.       10:37        19:15      Galveston      0.49
                                       12      MBGP         28035.25'       96034.17'        B        12/18/90         D           S         10:37        19:15      Galveston      0.49
                                       11      MBLR         29039.80'       96034.83'        B        12/18/90         H           S         10:37        19:15      Galveston      0.49
                                       11      MBLR         29039.80'       96034.83'        B        12/18/90         H           S         10:37        19:15      Galveston      0.49
                                       11      MBLR         29039.80'       96034.83'        B        12/18/90         H           S         10:37        19:15      Galveston      0.49
                                       13      MBTP         28039.50'       96013.45'        B        12/16/90         H           SRA       09:28        18:03      Galveston      0.52
                                       13      MBTP         28039.50,       96* 13.45'       B        12/16/90         H           SRA       09:28        18:03      Galveston      0.52
                                       13      MBTP         28039.50'       96013.45'        B        12/16/90         H           SRA       09:28        18:03      Galveston      0.52
                                       14      MBEM         28042.67'       95153.00'        B        12/16/90         H           Sc        09:28        18:03      Galveston      0.52
                                       14      MBEM         28042.67'       95153.00'        B        12/16/90         H           SHM       09:28        18:03      Galveston      0.52
                                       14      MBEM         28042-67'       95053.00'        B        12/16/90         H           SHM       09:28        18:03      Galveston      0.52
                                       72      BRCL         28051.5U        95027.83'        B        12/5/90          H           RM        12:18        20:51      Galveston      0.64
                                       72      BRCL         28051.50,       95027.83'        B        12/5/90          H           RS        12:18        20:51      Galveston      0.64
                                       72      BRCL         28051,50'       95027.83'        B,       12/5/90          H           SM        12:18        20:51      Galveston      0.64
                                       57      BRFS         28055.25'       95020,33'        B,       12/5/90          H           B         12:18        20:51      Galveston      0.64
                                       57      BRFS         28*55-25'       95120.33'        B        12/5/90          H           BM        12:18        20:51      Galveston      0.64



                     BOTTOM: S--SHELL,M=MUD,N=SAND,G=GRASS,H=HASH,C=CLAY.R=REEF.B=RUBBLE,K--KELP,A--ALGAET--ROOTS OYSTER: H=HANDT--TONGS,D=DREDGE SAMPLE TYPE : B=BIVALVE,S=SBDIMENT



                                                                      MM M mmm =
                                                                         MUSSEL WATCH PROJECT YEAR VI - Field Station Data




                                     Site         Site        Latitude        Longitude      Sample        Date       Collection Bottom Local TIme Local Time                'ndal       'ndal
                                  Number                      Deg Min         Deg Min         Type        M/D/Y        Method         Type    Low Water High Water        Reference    Horizon
                                                                                                                                                                                           (m)

                                     57          BRFS         28'55.25'       95020.33'         B         12/5/90          H           B         12:18         20:51      Galveston      0.64
                                     18          GBCR         29115.75'       94054.88,         B         12/6/90          H           SR        13:15         21:30      Galveston      0.55
                                     18          GBCR         29'15.75'       94154.88,         B         12/6/90          H           SR        13:15         21:30      Galveston      0.55
                                     18          GBCR         29'15.75'       94054.88'         B         12/6/90          H           SR        13:15         21:30      Galveston      0.55
                                     58          GBOB         29'17.08'       94050.15,         B         12/6/90          H           B         13:15         21:30      Galveston      0.55
                                     58          GBOB         29017.081       94050.15'         B         12/6/90          H           B         13:15         21:30      Galveston      0.55
                                     58          GBOB         29017.08'       94050.15'         B         12/6/90          H           B         13:15         21:30      Galveston      0.55
                                     16          GBTD         29'30.06'       94053.92'         B         12/7/90          H           SR        14:11         22:03      Galveston      0.40
                                     16          GBTD         29030.06'       94053.92'         B         12/7/90          T          SHC        14:11         22:03      Galveston      0.40
                                     16          GBTD         29030.06'       94,53.92,         B         12/7/90          H          SMH        14:11         22:03      Galveston      0.40
                                     15          GBYC         29036.30,       29036.50'         B         12/6/90          T           S         13:15         21:30      Galveston      0.55
                                     15          GBYC         29036.30,       29036.50,         B         12/6/90          T           S         13:15         21:30      Galveston      0.55
                                     15          GBYC         29036.30'       29036.50'         B         12/6/90          T           S         13:15         21:30      Galveston      0.55
                                     59          GBSC         29042.27'       94059.58,         B         12/6/90          T           SM        13:15         21:30      Galveston      0.55
                                     59          GBSC         29'42.27'       94059.58,         B         12/6/90          T           SM        13:15         21:30      Galveston      0.55
                                     59          GBSC         29042.27'       941,59.58,        B         12/6/90          T           SM        13:15         21:30      Galveston      0.55
                                     17          GBHR         29028.83'       94043.67'         B         12/6/90          D           SH        13:15         21:30      Galveston      0.55
                                     17          GBRR.        2GO28.8a        c34043.67'        B         1121161%         D           SH        13-.15        21*.30     Galveston      0.55
          0)                         17          GBHR         29'28.83'       94'43.67'         B         12/6/90          D           SH        13:15         21:30      Galveston      0.55
                                     19          SLBB         29147,50'       93054,42'         B         12/8/90          T           NIS       15:14         22:26      Galveston      0.28
                                     19          SLBB         29047.50'       93054.42'         B         12/8/90          T           MS        15-14         22:26      Galveston      0.28
                                     19          SLBB         29047.50'       93054.42'         B         12/8/90          T           MS        15:14         22:26      Galveston      0.28
                                     20          CLSJ         29049.83'       93023.00'         B         12/7/90        H/T           S         14:11         22:03      Galveston      0.40
                                     20          CLSJ         29'49.83'       93023.00'         B         12/7/90        H/T           S         14:11         22:03      Galveston      0.40
                                     20          ClIsi        29049.83,       93023.00'         B         12/7/90        H/T           S         14:11         22:03      Galveston      0.40
                                     60          CLLC         30'03.42'       93018.42'         B         12/8/90          H           SM        15:14         22:26      Galveston      0.40
                                     60          CLLC         30oO3.42'       93018.42'         B         12/8/90          H           SM        15:14         22:26      Galveston      0.40
                                     60          CLLC         30003.42'       93018.42,         B         12/8/90          H           SM        15:14         22:26      Galveston      0.40
                                     21          JHJH         29*37.75'       92'45.75'         B         12/7/90          H           R         14:11         22:03      Galveston      0.40
                                     21          JHJH         29037.75'       92045.75'         B         12/7/90          H           S         14:11         22:03      Galveston      0.40
                                     21          JHJH         29037.75'       92045.75'         B         12/7/90          H           S         14:11         22:03      Galveston      0.40
                                     22          VBSP         29034.50'       92002.50'         B         1/8/91           D           S         05:10         13:20      Galveston      0.30
                                     22          VBSP         29'34.50'       92002.50,         B         1/8/91           D           S         05:10         13:20      Galveston      0@30
                                     22          VBSP         29034.50'       92002.50'         B         1/8/91           D           S         05:10         13:20      Galveston      0.30
                                     24          ABOB         29013.00'       91008.00,         B         1/9/91           D           SM        05:55         14:57      Galveston      0.39
                                     24          ABOB         29'13.00'       91008.00,         B         1/9/91           H           Sm        05:55         14:57      Galveston      0.39
                                     24          ABOB         29013.00'       91008.00,         B         1/9/91           D           SM        05:55         14:57      Galveston      0.39
                                     25          CLCL         29015.42'       90055.83'         B         1/9/91           D           M         05:55         14:57      Galveston      0.39
                                     25          CLCL         29'15.42'       90'55.83'         B         1/9/91           D           M         05:55         14:57      Galveston      0.39
                                     25          CLCL         29015.42'       90055.83'         B         1/9/91           D           M         05:55         14:57      Galveston      0.39
                                     26          TBLB         29015.60'       90035.70,         B         1/8/91           H           SM        05:10         13:20      Galveston      0.30



                      BOTTOM   S--SHELL,M=MUD,N=SAND,G=GRASS,H=HASH,C=CIAYR--RFEF.B=RUBBLF,,K=KELP,A--ALCAE,T--ROOTS OYSTER: H=HANDT--TONGS,D=DREDGE SAMPLE TYPE : B--BfVALVE,S=SEDIMENT





                                                                         MUSSEL WATCH PROJECT YEAR VI - Field Station Data




                                     site        site         Latitude        Longitude     sarnple       Date        Collectlon Bottom LocalTime Local Time                Tidal        Tidal
                                  Number                      Deg Min         Deg Min         I)rpe      M/D/Y         Method         TYpe    Low Water High Water        Reference    Horizon
                                                                                                                                                                                           (m)

                                     26          TBLB         29015.60,       90035.70'         B        1/8/91           H           SM         05:10         13:20      Galveston      0.30
                                     26          TBLB         29015.60'       90035.70'         B        1/8/91           H           SM         05:10         13:20      Galveston      0.30
                                     27          TBLF         29,16,20,       90'24.40'         B        1/9/91           H           SM         05:55         14:57      Galveston      0.39
                                     27          TBLF         29016.201       90024.40'         B        1/9/91           H           M          05:55         14:57      Galveston      0.39
                                     27          TBLF         29016.20'       90'24.40'         B        1/9/91           H           MG         05:55         14:57      Galveston      0.39
                                     28          BBSD         29024,30'       89059.50'         B        1/8/91           D           M          05:10         13:20      Galveston      0.30
                                     28          BBSD         29024.39        8959.50'          B        1/8/91           D           M          05:10         13:20      Galveston      0.30
                                     28          BBSD         29024.30'       89059.50'         B        1/8/91           D           M          05:10         13:20      Galveston      0.30
                                     29          BBMB         29016.62'       89056.53'         B        1/8/91           H           MG         05:10         13:20      Galveston      0.30
                                     29          BBMB         29016.62'       89056,53'         B        1/8/91           H           MG         05:10         13:20      Galveston      0.30
                                     29          BBMB         29* 16.62'      89056.53'         B        1/8/91           H           MG         05:10         13:20      Galveston      0.30
                                     65          MRTP         29008,68'       89*25.67'         B        1/11/91          H           G          08:24         20:44        Mobile       0.62
                                     65          MRTP         29008.68'       89025.67'         B        1/11/91          H           G          08:24         20:44        Mobile       0.62
                                     65          MRTP         29008.68,       89025.67'         B        1/11/91          H           G          08:24         20:44        Mobile       0.62
                                     31          BSSI         29*24.701       89128.70'         B        1/11/91          D           SM         08:24         20:44        Mobile       0.62
                                     31          BSSI         29024.70,       89028.70'         B        1/11/91          D           SM         08:24         20:44        Mobile       0.62
                                     31          BSSI         29024.70'       89028.70'         B        1/11/91          D           SM         08:24         20:44        Mobile       0.62
                                     30          BSBG         29035.90,       89037,25!         B        1/10/91                      Ms         07:48         20:00        Mobile       0.57
                                     30          BSBG         29035.90,       89'37.25'         B        1/10/91          H           Ms         07:48         20:00        Mobile       0.57
                                     30          BSBG         29,35.90,       89*37.25!         B        1/10/91          H           NIS        07:48         20:00        Mobile       0.57
                                     32          LBMP         29052.25'       89040.62'         B        1/10/91          H           Ms         07:48         20:00        Mobile       0.57
                                     32          LBMP         29,52.25'       89040.62'         B        1/10/91          H           Ms         07:48         20:00        Mobile       0.57
                                     32          LBMP         29052.25'       89*40.62'         B        1/10/91          H           NIS        07:48         20:00        Mobile       0.57
                                     62          LPGO         30102.44'       90'02.57'         BS       1/25/91          D           MN         07:08         19:29        Mobile       0.75
                                     62          LPGO         30002.44'       90002.57'         BS       1/25/91          D           MN         07:08         19:29        Mobile       0.75
                                     62          LPGO         30002.44'       90*02.57'         BS       1/25/91          D           MN         07:08         19:29        Mobile       0.75
                                     33          MSPC         30018.17'       89019.62'         B        1/12/91          H           SNR        09:02         21:34        Mobile       0.65
                                     33          MSPC         30018.17'       89019.62'         B        1/12/91          H           SNR        09:02         21:34        Mobile       0.65
                                     33          MSPC         30018.17'       89019.62'         B        1/12/91          H           SNR        09:02         21:34        Mobile       0.65
                                     34          MSBB         30023.55,       88'51.45'         B        1/12/90          H           B          11:24         00:11        Mobile       0.70
                                     34          MSBB         30123.55'       88151.45'         B        1/12/90          H           R          11:24         00:11        Mobile       0.70
                                     34          MSBB         30123.55'       88051.45'         B        1/12/90          H           B          11:24         00:11        Mobile       0.70
                                     35          MSpB         30020.17'       88036.06'         B        1/13/91          D           SR         09:39         22:26        Mobile       0.65
                                     35          MSPB         30020.17'       88036.06'         B        1/13/91          D           SR         09:39         22:26        Mobile       0.65
                                     35          MSPB         30020.17'       88036.06'         B        1/13/91          D           SR         09:39         22:26        Mobile       0.65
                                     36          MBCp         30019.50,       88007.50'         B        1/12/91          H           NS         09:02         21:34        Mobile       0.65
                                     36          MBCP         30019.50,       88007,5U          B        1/12/91          H           NS         09,02         21:34        Mobile       0.65
                                     36          MBCP         30019.50,       88007.50'         B        1/12/91          H           NS         09:02         21:34        Mobile       0.65
                                     66          MBHI         30033.89        87004.50'         B        1/12/91          T           MSN        09:02         21:34        Mobile       0.65
                                     66          MBHl         30033.80,       87004.50'         B        1/12/91          T           MSN        09:02         21:34        Mobile       0.65
                                     66          MBHl         30*33.80'       87004.50'         B        1/12/91          T           MSN        09:02         21:34        Mobile       0.65


                      BOTrOM: S--SHELLM=MUD.N=SAND,G--GRASS.H=HASH.C--CLAY,R--REEF,B=RUBBLE,K--KELP.A--ALOAEI'-ROO'M OYSWR: H=HANDJ--TONGS.D=DREDGE SAMPLE TYPE : B=BrVALVES=SF-DIMENIT





                                                                        MUSSEL WATCH PROJECT YEAR VI - Field Station Data




                                     Site        Site        Latitude        Longitude     Sample        Date       Collection Bottom Local 71me Local Time               'ndal       'ndal
                                  Number                     Deg Min         Deg Min        Type        M/D/Y        Method          Type   Low Water High Water        Reference   Horizon
                                                                                                                                                                                        (m)

                                     67          PBPH        30024.63'       87011.42'        B         1/26/91          H           N        06:00         19:31       Pensacola     0.74
                                     67          PBPH        30024.63'       87'11.42'        B         1/26/91          H           N        06:00         19:31       Pensacola     0.74
                                     67          PBPH        30024.63'       87011-42'        B         1/26/91          H           N        06:00         19:31       Pensacola     0.74
                                     37          PBIB        30028.86'       87007.47         B         1/26/91          D           Sm       06:00         19:31       Pensacola     0.74
                                     37          PBIB        30028.86'       87007.47'        B         1/26/91          D           SM       06:00         19:31       Pensacola     0.74
                                     37          PBIB        30028.86'       87007.47'        B         1/26/91          D           SM       06:00         19:31       Pensacola     0.74
                                     73          CBJB        30024.62'       86129-45'        B         1/27/91          H       SBRMN        06:57         20:31       Pensacola     0.77
                                     73          CBJB        30024.62'       86*29-45'        B         1/27/91          H       SBRMN        06:57         20:31       Pensacola     0.77
                                     73          CBJB        30024.62'       86029-45'        B         1/27/91          H       SBRMN        06:57         20:31       Pensacola     0.77
                                     38          CBSR        30024.78'       86012-25'.       B         1/27/91          D           SM       06:57         20:31       Pensacola     0.77
                                     38          CBSR        30024.78'       86012-25'        B         1/27/91          D           SM       06:57         20:31       Pensacola     0.77
                                     38          CBSR        30024.78'       86012.25'        B         1/27/91          D           SM       06:57         20:31       Pensacola     0.77
                                     39          CBSP        30028.85'       86028.73'        B         1/27/91          H           B        06:57         20:31       Pensacola     0.77
                                     39          CBSP        30028.85'       86028.73'        B         1/27/91          H           B        06:57         20:31       Pensacola     0.77
                                     39          CBSP        30'28.85'       86028.73'        B         1/27/91          H           B        06:57         20:31       Pensacola     0.77
                                     74          PCLO        30015.00'       85'40.87'        B         1/28/91          H           BG       07:52         21:29       Pensacola     0.73
                                     74          PCLO        30015.00'       85040.87'        B         1/28/91          H           BG       07:52         21:29       Pensacola     0.73
          00                         74          PCLO        30015.00,       85040.87'        B         1/28/91          H           BG       07:52         21:29       Pensacola     0.73
                                     40          SAVvrB      30'08.53'       85'37.92'        B         1/28/91          H           B        07:52         21:29       Pensacola     0.73
                                     40          SAVVB       30008.53'       85037.92'        B         1/28/91          H           B        07:52         21:29       Pensacola     0.73
                                     40          SAWB        30008.53'       85037-92'        B         1/28/91          H           B        07:52         2i:29       Pensacola     0.73
                                     41          APDB        29040.50'       85004.22'        B         1/28/91          H           SNK      07:52         21:29       Pensacola     0.73
                                     41          APDB        29'40.50'       85004.22'        B         1/28/91          H           SNK      07:52         21:29       Pensacola     0.73
                                     41          APDB        29040.50'       85004-22'        B         1/28/91          H           SNK      07:52         21:29       Pensacola     0.73
                                     42          APCP        29043.50'       84052.83'        B         1/28/91          H           SNK      07:52         21:29       Pensacola     0.73
                                     42          APCP        29043,50'       84052-83'        B         1/28/91          H           SNK      07:52         21:29       Pensacola     0.73
                                     42          APCP        29043.50'       84052.83'        B         1/28/91          H           SNK      07:52         21:29       Pensacola     0.73
                                     75          AESP        30003.90'       84019-27'        B         1/29/91          H           SR       08:43         22:24       Pensacola     0.65
                                     75          AESP        30003.90'       84119.27'        B         1/29/91          H           SR       08:43         22:24       Pensacola     0.65
                                     75          AESP        30003,90'       84019-27'        B         1/29/91          H           SR       08:43         22:24       Pensacola     0.65
                                     43          CKBP        29011.60'       83004.40'        B         1/29/91          T           SM       08:43         22:24       Pensacola     0.65
                                     43          CKBP        29011.60'       83004.40'        B         1/29/91          T           Sm       08:43         22:24       Pensacola     0.65
                                     43          CKBP        29011.60'       83004.40'        B         1/29/91          T           SM       08:43         22:24       Pensacola     0.65
                                     76          TBNP        27*47.28'       82045.28'        B         1/31/91          H           B        09:22         01:52       St.Petrsbg    0.84
                                     76          TBNP        27047.28'       82145.28'        B         1/31/91          H           B,       09:22         01:52       St.Petrsbg    0.84
                                     76          TBNP        27o47.28'       82045-28'        B         1/31/91          H           B        09:22         01:52       St.Petrsbg    0.84
                                     47          TBMK        27037,75'       82043.50'        B         1/30/91          H           S        08:52         00:58       St.Petrsbg    0.96
                                     47          TBMK        27037.75'       82143-50'        B         1/30/91          H           S        08:52         00:58       St.Petrsbg    0.96
                                     47          TBMK        27037.75'       82143.50'        B         1/30/91          H           S        08:52         00:58       St.Petrsbg    0.96
                                     44          TBPB        27050.53'       82036.62'        B         1/31/91          H           NONE     09:22         01:52       St-Petrsbg    0.84
                                     44          TBPB        27050.53'       82036-62'        B         1/31/91          H           NONE     09:22         01:52       St-Petrsbg    0.84


                      BoTrOM: [email protected]=MUD,N=SAND.G=GRASS,H=HASH.C=CIAY.R@-PEEF,B--RUBBLE,K--lKELP,A=ALGAFT--ROOTS OYSMR: [email protected]=DREDGE SAMPLE TYPE : B=BIVALVE.S=SEDIMENT





                                                                       MUSSEL WATCH PROJECT YEAR Vi - Field Station Data




                                    site         site        Latitude        Longitude     Sample        Date       Collection Bottom Local'nme LocalTime                 Tidal        Tidal
                                 Number                      Deg Min         Deg Min        Type       M/D/Y         Method        Type    Low Water High Water        Reference    Horizon
                                                                                                                                                                                       (m)

                                    44           TBPB        27050.53'       82036.62'        B        1/31/91          H          NONE       09:22         01:52      St.Petrsbg      0.84
                                    70           TBOT        28'01,48'       82037.95'        B        1/30/91          H           NS        08:52         00:58      St.Petrsbg      0.96
                                    70           TBOT        28001.48'       82037.95'        B        1/30/91          H           NS        08:52         00:58      St.Petrsbg      0.96
                                    70           TBOT        28001.4&        82*37.95!        B        1/30/91          H           NS        08:52         00:58      St.Petrsbg      0.96
                                    77           TBKA        27054.47'       87027.28'        B        1/29/91          H          NBH        08:16         00:01      St.Petrsbg      1.03
                                    77           TBKA        27054.47'       87127.28'        B        1/29/91          H          NBH        08:16         00:01      St.Petrsbg      1.03
                                    77           TBKA        27054.47'       87027.28'        B        1/29/91          H          NBH        08:16         00:01      St.Petrsbg      1.03
                                    46           TBCB        27*40.55'       82130.57'        B        1/30/91          H           NS        08:52         00:58      St.Petrsbg      0.96
                                    46           TBCB        27140.55'       82030.57'        B        1/30/91          H           NS        08:52         00:58      St.Petrsbg      0.96
                                    46           TBCB        27040.55'       82130.57'        B        1/30/91          H           NS        08:52         00:58      St.Petrsbg      0.96
                                    48           CBBI        26131.00'       82102.19         B        1/31/91          H           SR.       09:22         01:52      St.Petrsbg      0.84
                                    48           CBBI        26131.00'       82102.18'        B        1/31/91          H           SR        09:22         01:52      St.Petrsbg      0.84
                                    48           CBBI        26031.00'       82*02.18'        B        1/31/91          H           SR        09:22         01:52      St.Petrsbg      0.84
                                    71           CBFM        26133.50,       81,55.37'        B        1/31/91          H          HBN        09:22         01:52      St.Petrsbg      0.84
                                    71           CBFM        26033.50,       81055.37'        B        1/31/91          H           HN        09:22         01:52      St.Petrsbg      0.84
                                    71           CBF`M       26133.50,       81055.37'        B        1/31/91          H            H        09:22         01:52      St.Petrsbg      0.84
                                    49           NBNB        26106.85'       81047.20'        B        2/1/91           H          CHMK       09:47         02:42      St.Petrsbg      0.70
                                    49           NBNB        26006.85'       81147.20'        B        2/l/91           H          SRNM       09:47         02:42      StPetrsbg       0.70
                                    49           NBNB        26006.85'       81047.20'        B        2/1/91           H          SRNM       09:47         02:42      St.Petrsbg      0.70
                                    50           RBHC        26001.50,       81044.20'        B        2/2/91           H           SN        10:08         03:33      St.Petrsbg      0.54
                                    50           RBHC        26001.50'       81044.20'        B        2/2/91           H           SN        10:08         03:33      St.Petrsbg      0.54
                                    50           RBHC        26001.50'       81044.20'        B        2/2/91           H           SN        10:08         03:33      St.Petrsbg      0.54
                                    51           EVFU        24055.08'       8 1030.78'       B        2/2/91           H           sm        10:08         03:33      St.Petrsbg      0.54
                                    51           EVFU        24055.08'       81030.78'        B        2/2/91           H           sm        10:08         03:33      St.Petrsbg      0.54
                                    51           EVFU        24055-08'       81030.78'        B        2/2/91           H           SM.       10*08         03:33      St.Petrsbg      0.54
                                    81           BHKF        24039.74'       81016.43'        BS       1/22/91          H           NG        00:22         18:10      St.Petrsbg      0.55
                                    81           BHKF        24039.74'       81016.43'        BS       1/22/91          H           NG        00:22         18:10      St.Petrsbg      0.55
                                    81           BHKF        24039.74'       81016.43'        BS       1/22/91          H           NG        00:22         18:10      St.Petrsbg      0.55















                      BoTIOM   S--SHELL,M=MUD,N=SAND.G=GRASS,H=HASH,C--ClAY.R--REEF,B=RUBBLE,K=KELP,A@-ALGAEX--ROOI@S OYSTER: H=HANDT--TONGS,D=DRFDGE S"PLE IWE : B=BrVALVE,S=SEDIM ENT




I
 1
I
I
I
I
I
I
I
I             BIVALVES
I
I
i
I
I
I
I
 I
                 10




I
I
I
I
I
I
I
I
I
I                 Aromatics Data
I
I
I
I
I
I
I


                        11
Il- - -






                                                                                MUSSEL WATCH YEAR VI - Bivalve Aromatics Data





                                                                                               Ci-       C2-        C3-        C4-                                                                      CI- C2-
                  FILE          SITE      REP LOCATION SAMPLE                    NAPH       NAPH       NAPH       NAPH       NAPH     BIPHENYL       ACENAPH-        ACENAPH-      FLUORENE FLUOR             FLUOR
                                                      # AND        WEIGHT                                                                             THYLENE            THENE
                                                      STATE          (g dry)     (ppb)+      (ppb)       (ppb)      (ppb)      (ppb)       (ppb)+           (ppb)          (ppb)+          (ppb)+      (ppb)   (ppb)


                  K5135         LMSB          I       TX-1               1.6        7.6        12.7      0.0        0.0        0.0            3.2             2.0             0.9             1.7       0.0        0.0
                  K5136         LMSB          2       Tx- 1              2.5        4.5        8.4       14.2       0.0        0.0            2.6             2.0             1.7             1.4       8.1        0.0
                  K5137         LMSB          3       TX-i               2.2        5.6        4.5       0.0        0.0        0.0            2.7             1.1             1.9             019       7.7        0.0
                  K5087         CCIC          I       TX-3               2.5        5.4        7.0       10.4       16.3       19.3           2.0             0.6             2.2             3.1       6.1        0.0
                  K5088         CCIC          2       TX-3               2.7        5.7        12.7      17.7       23.1       26.2           2.4             0.7             1.9             2.5       4.9       27.0
                  K5089         CCIC          3       TX-3               2.6        7.6        7.2       15.5       26.8       24.7           4.5             1.2             5.3             2.8       3.5       26.1
                  K5147         ABLR          I       TX-4               3.7        5.4        6.9       6.9        6.5        7.2            1.8             0.3             0.5             1.1       0.0        0.0
                  K5148         ABLR          2       TX-4               3.4        3.5        5.0       6.5        8.3        10.8           0.7             1.8             0.3             0.8       0.0        0.0
                  K5149         ABLR          3       TX-4               2.3        7.0        6.2       6.4        2.7        10.7           2.2             4.7             0.9             1.6       0.0        0.0
                  K5141         CI3CR         1       TX-5               2.4        5.9        5.6       9.7        0.0        0.0            1.9             0.1             0.3             0.5       0.0        0.0
                  K5142         CI3CR         2       TX-5               2.9        3.8        5.1       6.7        0.0        0.0            1.3             0.5             2.1             0.9       0.0        0.0
                  K5143         CBCR          3       TX-5               2.0        8.2        6.4       6.2        0.0        0.0            4.0             0.5             1.1             0.9       8.6       22.9
                  K5099         MBAR          I       TX-6               3.1        3.4        3.9       0.0        0.0        0.0            2.2             0.3             0.9             1.0       0.0        0.0
                  K5100         MBAR          2       TX-6               3.5        4.0        3.7       0.0        0.0        0.0            1.2             0.7             0.3             1.2       0.0        0.0
                  K5101         MBAR          3       TX-6               3.4        4.5        2.5       0.0        0.0        0.0            2.3             0.7             0.3             1.0       0.0        0.0
                  K5111         SAPP          I       TX-7               2.5        7.2        9.2       11.1       8.3        10.6           2.7             0.2             1.0             1.4       0.0        0.0
                  K5112         SAPP          2       TX-7               2.9        5.8        8.3       11.2       13.8       0.0            1.7             0.3             1.3             2.3       0.0        0.0
                  K5113         SAPP          3       TX-7               2.7        5.4        6.1       8.7        0.0        0.0            2.9             0.4             0.7             1.8       4.7        0.0
                  K5117         SAMP          1       TX-8               3.6        5.1        6.0       4.4        5.9        6.2            2.5             0.9             110             1.3       0.0        0.0
                  K5118         SAMP          2       TX-8               3.4        4.9        8.2       7.9        8.2        0.0            2.0             1.9             1.7             1.8       0.0        0.0
                  K5119         SAMP          3       TX-8               3.9        3.2        4.4       0.0        0.0        9.2            1.7             1.7             0.4             1.7       0.0        0.0
                  K5105         ESSP          1       TX-9               2.8        5.2        8.0       14.9       20.3       20.0           2.9             0.4             1.5             1.9       4.7       33.3
                  K5106         ESSP          2       TX-9               2.7        8.0        13.5      16.4       26.6       19.8           2.4             1.1             0.6             2.0       7.1       27.2
                  K5107         ESSP          3       TX-9               2.7        5.0        6.8       13.9       21.2       19.9           3.5             1.2             1.6             2.5       7.8       21.2
                  K5129         MBGP          1       IX-12              3.2        6.2        7.1       8.6        13.8       12.9           2.4             1.3             1.3             2.3       0.0        0.0
                  K5130         MBGP          2       TX- 12             3.0        3.6        6.2       9.1        16.5       20.9           2.6             1.3             1.2             1.7       0.0        0.0
                  K5131         MBGP          3       'fX- 12            3.5        3.4        4.8       8.4        17.4       21.0           2.8             1.6             1.7             1.4       0.0        0.0
                  K5123         MBLR          1       TX-11              2.5        5.2        5.2       5.0        8.2        5.7            2.2             1.1             1.0             2.0       0.0        0.0
                  K5124         MBLR          2       TX-11              1.9       13.4        12.2      33.5       41.4       0.0            4.6             2.2             2.9             3.5       0.0        0.0
                  K5125         MBLR          3       Irx- 11            2.2        7.0        6.1       9.3        16.6       17.7           3.0             1.5             1.3             2,9       0.0        0.0
                  K5081         MBTP          1       TX-13              2.7        4.3        3.7       0.0        0.0        0.0            3.1             0.5             0.2             1.0       0.0        0.0
                  K5082         MBTP          2       TX- 13             2.8        3.8        5.9       0.0        0.0        0.0            1.8             0.5             0.7             1.2       0.0        0.0
                  K5083         MBTP          3       TX-13              2.9        4.4        4.9       0.0        0.0        0.0            2.4             0.4             0.3             1.3       0.0        0.0
                  K5075         MBEM          I       TX-14              2.2        6.3        7.5       0.0        0.0        22.1           2.4             2.4             0.7             2.8       0.0       23.0
                  K5076         MBEM          2       TX-14              2.2        6.4        8.5       0.0        0.0        0.0            2.4             0.6             1.1             2.0       0.0       22.9
                  K5077         MBEM          3       TX-14              2.5        6.4        5.1       6.8        14.8       22.7           2.9             0.6             1.6             2.1       0.0       18.8
                  K5015         BRCL          1       TX-72              2.5       10.1        10.1      0.0        0.0        0.0            6.7             9.4             1.9             3.2       0.0       29.5
                  K5016         BRCL          2       TX-72              2.0        5.2        9.6       0.0        0.0        0.0            3.4             7.8             2.9             2.1       0.0        0.0






                                                                               MUSSEL WATCH YEAR VI - Bivalve Aromatics Data




                                                                                            Ci-        C2-        d3-       C4-                                                                    Cl- C2-
                  FILE          SITE      REP LOCATION SAMPLE                  NAPH       NAPH       NAPH       NAPH        NAPH   BIPHENYL      ACENAPH-        ACENAPH-      FLUORENE FLUOR             FLUOR
                                                    # AND         WEIGHT                                                                           THYLENE           THENE
                                                    SrATE          (g dry)     (ppb)+       (ppb)      (ppb)      (ppb)     (ppb)       (ppb)+          (ppb)          (ppb)+         (ppb)+       (ppb)  (ppb)



                  K5017       BRCL           3      TX-72              2.3        6.8       7.6        7.8        17.2      19.6           2.9            9.3             2.1            2.8       6.4       34.0
                  K5021       BRFS           1      TX-57              2.3        6.9       11.8       24.1       43.2      59.6           5.0          33.9             17.9           14.9       12.3      64.6
                  K5022       BRFS           2      TX-57              2.0      11.7        14.3       22.0       55.3      56.4           3.3          15.0             11.5            6.0       18.5      60.8
                  K5023       BRFS           3      TX-57              1.4        1.2       10.2       0.0        38.4      33.1           6.1          15.2              8.2            6.7       12.8      50.6
                  K5009       GBCR           1      TX-18              2.4        6.4       9.4        16.0       28.2      25.4           4.6            4.2             7.5            6.6       11.7      39.9
                  K5010       GBCR           2      'rX-18             2.4      10.5        15.8       25.0       32.2      31.4           2.5            6.9             7.4            7.9       14.0      33.0
                  K5011       GBCR           3      TX-18              2.4        6.6       17.6       21.3       34.4      41.0           2.3            9.1             8.8            6.5       10.6      39.3
                  K5003       GBOB           I      TX-58              2.5        5.4       7.5        0.0        0.0       0.0            1.6            4.8             6.6            4.5       0.0       31.7
                  K5004       GBOB           2      TX-58              2.4        6.1       9.4        0.0        0.0       0.0            2.5            3.9             3.1            2.7       7.5       33.0
                  K5005       GBOB           3      TX-58              2.4        3.7       5.4        0.0        12.0      18.2           2.5            5.0             2.7            1.4       0.0       23.3
                  K5057       GBTD           I      TX-16              3.2        5.1       10.4       18.4       42.1      53.3           3.0            2.8             1.5            2.6       13.3      57.4
                  K5058       GBT`D          2      TX-16              3.8        6.5       20.1       33.6       64.6      58.3           2.9            4.0             1.5            4.3       18.5      71.1
                  K5059       GBT`D          3      TX-16              3.4      26.3        57.1       42.9       89.3      106.6          3.0            4.2             2.6            7.0       35.0     135.5
                  K5063       GBYC           1      TX-15              3.0        3.9       4.2        8.6        15.9      21.6           3.6            5.3             2.6            2.5       6.9       34.0
                  K5064       GBYC           2      TX-15              2.7        6.0       8.0        9.0        24.7      16.3           2.0            2.6             2.6            1.5       8.4       28.2
                  K5065       GBYC           3      TX-15              3.0        6.3       6.9        8.6        17.3      25.9           3.1            2.8             2.6            1.9       7.3       29.0
                  K5384       GBSC           I      TX-59              2.3      74.5     1979.4     6077.5    8112.0     6954.1         374.7           31.4           728.3           605.9    1676.9    3138.4
                  K5385       GBSC           2      TX-59              2.3     157.2     2189.9     5158.6    6260.3     5024.5         484.8           55.8           914.5           733.9    1735.0    3417.7
                  K5386       GBSC           3      TX-59              2.1     147.1     2297.6     5626.9    7213.3     7067.2         590.4           68.1          1078.7          1074.9    2365.1    5092.8
                  K5039       G13HR          1      TX-17              3.1        4.2       6.8        5.7        7.9       18.1           3.2            6.0             3.3            4.3       6.5         0.0
                  K5040       GBHR           2      TX-17              3.3        4.8       9.9        15.0       31.7      32.7           3.8            3.5             3.1            4.9       7.9       26.7
                  K5041       GBHR           3      TX-17              2.9        7.2       7.4        13.6       37.7      25.6           4.6            2.2             4.5            2.5       4.3       31.1
                  K5027       SLBB           I      TX-19              1.0      10.1        9.6        22.2       33.7      54.8           4.9          10.7              4.2            4.4       10.0      52.8
                  K5028       SLBB           2      TX-19              2.0      12.3        21.2       8.4        18.3      23.8           3.9          11.4              3.5            5.9       18.4      63.3
                  K5029       SLBB           3      TX-19              2.0        5.4       11.3       12.2       22.7      55.2           4.4            5.0             1.7            2.6       10.6      42.6
                  K5033       CLSIJ          1      IA-20              3.2        5.8       11.6       14.9       61.9      92.7           1.6            1.1             2.8            7.5       17.8      117.2
                  K5034       CLSj           2      IA-20              2.3      11.8        19.6       33.8       91.7      178.0          2.9            1.0             4.4            5.5       32.7      120.4
                  K5035       CLSj           3      LA-20              2.5        6.5       9.6        17.0       57.9      134.1          3.0            1.0             1.0            4.5       12.2      93.5
                  K5045       CLLC           I      IA-60              3.5        6.6       11.5       17.0       40.6      52.7        111.4             6.7             5.8            6.8       17.4      99.6
                  K5046       CLL(-1         2      IA-60              3.3        4.8       6.3        15.2       24.1      39.2          40.6            2.9             3.4            3.8       12.6      77.7
                  K5047       CLLC           3      LA-60              3.4      57.5        91.3       40.1       51.2      71.5        106.4             6.3             5.0            5.7       16.4      61.0
                  K5069       JHJH           I      LA-21              3.0        7.3       9.0        10.2       15.8      13.0           4.0            1.9             5.3            7.9       6.4         0.0
                  K5070       JHJH           2      LA-21              2.7        8.0       9.2        0.0        17.4      25.4           4.3            1.5             3.3            5.1       8.3       35.8
                  K5071       JHJH           3      IA-21              2.6        9.4       7.6        6.8        16.4      17.4           4.3            2.0             2.0            4.2       3.4       13.4
                  K5159       VBSP           1      LA-22              2.7        6.4       7.1        10.6       22.9      21.2           3.9            1.1             1.1            2.4       7.6       51.5
                  K5160       VBSP           2      LA-22              2.6        3.8       6.5        11.3       27.8      24.0           2.7            1.9             1.3            1.6       9.5         0.0
                  K5161       VBSP           3      IA-22              2.8        4.0       7.5        9.3        21.1      24.4           2.7            1.1             1.2            2.6       13.2      53.6
                  K5189       ABOB           1      IA-24              2.7        7.1       10.5       0.0        0.0       0.0            5.5            2.2             0.8            2.4       0.0         0.0






                                                                                  MUSSEL WATCH YEAR VI - Bivalve Aromatics Data





                                                                                                 ci-        C2-        C3-        C4-                                                                        Cl- C2-
                  FILE          SITE        REP LOCATION SAMPLE                    NAPH          NAPH       NAPH       NAPH       NAPH   BIPHENYL       ACENAPH-         ACENAPH-      FLUORENE FLUOR              FLUOR
                                                       # AND         WEIGHT                                                                              THYLENE             THENE
                                                       STATE           (g dxy)     (ppb)+        (ppb)      (ppb)      (ppb)      (ppb)       (ppb)+            (ppb)          (ppb)+          (ppb)+        (ppb)  (ppb)


                  K5190         ABOB           2       LA-24              2.5        4.6         6.2        8.6        12.5       13.5           2.5             1.2              1.5             1.7        5.8       12.9
                  K5191         ABOB           3       LA-24              3.2        3.8         4.2        0.0        8.2        6.2            1.0             0.9              0.8             1.5        2.5        0.0
                  K5195         CLCL           1       LA-25              2.9        8.4         8.4        17.4       26.0       22.4           3.6             2.0              1.3             4.3        11.2      30.2
                  K5196         CLCL           2       IA-25              3.1        4.6         5.5        6.5        16.3       6.2            2.4             1.6              0.8             1.9        7.0       14.5
                  K5197         CLCL           3       LA-25              3.2        4.4         5.9        5.9        10.3       12.7           2.5             0.8              0.9             2.0        2.4       14.6
                  K5165         TBL13          1       LA-26              2.5        6.1         7.3        11.1       21.7       18.8           2.6             1.0              0.7             3.2        9.7       27.6
                  K5166         TBLB           2       LA-26              2.2        9.4         11.6       0.0        0.0        0.0            2.9             1.5              1.3             2.3        0.0        0.0
                  K5167         TBLB           3       LA-26              2.4        7.3         9.7        0.0        0.0        0.0            3.3             0.9              2.5             1.6        0.0        0.0
                  K5183         TBLF           1       LA-27              3.4        6.5         10.3       7.2        11.8       15.9           2.5             0.8              1.2             2.9        5.5       29.5
                  K5184         TBLF           2       IA-27              3.5        6.4         9.3        8.8        15.8       10.5           2.0             1.0              1.4             2.6        7.7       21.2
                  K5185         TBLF           3       LA-27              3.6        5.7         8.1        0.0        0.0        12.7           2.0             1.1              1.4             1.9        6.6       26.8
                  K5168         BBSD           I       LA-28              2.4        5.1         9.2        15.0       26.3       39.5           3.8             1.2              1.2             4.3        7.0       56.0
                  K5169         BBSD           2       LA-28                         6.1         9.6        16.0       25.3       27.4           2.0             1.3              0.7             2.6        7.8        0.0
                  K5170         BBSD           3       LA-28              2.9        4.7         5.8        10.4       17.9       25.7           3.1             0.5              1.3             2.7        7.5       36.3
                  K5174         BBM13          I       LA-29              2.7       12.3         16.9       18.6       35.7       36.2           4.7            14.0            14.8            15.8         15.3      47.0
                  K5175         BBM13          2       LA-29              2.2        7.4         13.5       13.7       21.3       18.2           1.7             4.7            10.7              9.0        13.9      30.6
                  K5176         BBMB           3       IA-29              2.4        7.9         16.4       14.1       26.5       35.5           3.4             6.8            13.7            11.4         12.7      28.9
                  K5210         MRIP           1       IA-65              2.5       21.2         12.9       37.6       88.7       158.5          4.4             4.7              5.0             9.2        23.9    104.1
                  K5211         h=             2       LA-65              3.0        9.7         .9.7       18.6       52.1       83.5           2.3             3.2              2.8             5.8        11.7      77.4
                  K5212         MRIP           3       LA-65              1.4       13.0         11.5       14.8       31.0       42.1           5.1             2.7              2.9             4.0        14.7      57.2
                  K5216         BSSI           1       LA-31              2.4        7.8         16.3       43.1       120.5      224.1          6.4             2.6              3.4             8.9        54.5    214.4
                  K5217         BSSI           2       IA-31              2.3        6.8         13.4       21.6       61.6       117.0          4.2             2.9              4.1             6.3        18.1      95.8
                  K5218         BSSI           3       LA-31              2.8        4.7         10.5       19.3       47.5       71.1           3.6             1.9              2.6             5.4        19.4      90.3
                  K5201         BSBG           1       LA-30              2.8       12.2         9.8        17.0       0.0        0.0            5.8             0.8              2.2             6.4        8.0       35.4
                  K5202         BSBG           2       LA-30              2.7       11.3         8.7        8.3        0.0        13.9           3.9             0.9              2.2             2.8        4.7       16.4
                  K5203         BSBG           3       LA-30              2.6        5.8         6.1        0.0        8.6        9.9            1.4             0.7              1.1             1.7        5.0       13.8
                  K5207         LBMP           1       LA-32              2.1       28.5         17.2       20.1       33.7       44.2           4.6             1.7              2.3             3.6        10.8      37.0
                  K5208         LBMP           2       LA-32              1.9       22.1         13.2       12.6       12.9       21.6           2.1             2.3              2.0             2.7        6.7       30.4
                  K5209         LBMP           3       LA-32              2.4       16.4         7.8        7.5        9.8        15.7           1.5             1.2              2.8             2.3        5.2       30.3
                  K5249         LPGO           1       LA-63              2.0       27.3         498.7   1819.0     4806.6     5336.1           57.8            27.4            67.3           176.8      892.6     3176.1
                  K5250         LPGO           2       LA-63              1.9       22.7         416.6   1545.5     3945.3     4322.3           58.8            37.8            70.0           190.2     1033.0     3302.7
                  K5251         LPGO           3       LA-63              2.0       34.4         653.2  3437.9      6181.5     6576.7           87.8            43.7            90.4           271.4     1547.0     4717.2
                  K5222         MSPC           1       MS-33              2.1        8.1         9.6        22.7       57.5       77.8           4.9             4.9              7.1           11.5         21.5    119.4
                  K5223         MSPC           2       MS-33              2.7        5.8         7.0        15.3       35.6       36.7           2.9             3.4              5.2             6.9        10.3      59.2
                  K5224         MSPC           3       MS-33              2.7        2.9         4.1        7.7        19.6       27.3           2.2             1.4              3.0             3.8        7.8       37.3
                  K5228         MSBB           I       MS-34              2.3       23.1         93.1       297.3      552.9      546.3         26.7             4.8            33.4            68.6       195.4     701.0
                  K5229         MSBB           2       MS-34              2.1       20.7         151.3      342.5      734.9      582.5         35.8            10.4            59.5           103.5      287.9      856.2
                  K5230         MSBB           3       MS-34              2.0        7.3         38.9       104.4      222.1      178.1         13.4             0.9            15.7            28.9         92.9    274.5





                                                                                  MUSSEL WATCH YEAR VI - Bivalve Aromatics Data





                                                                                                Cl-        C2-        C3-        C4-                                                                      Cl- C2-
                  FILE          SITE       REP LOCATION SAMPLE                    NAPH          NAPH       NAPH       NAPH       NAPH   BIPHENYL       ACENAPH-        ACENAPH-      FLUORENE FLUOR              FLUOR
                                                      #AND          WEIGHT                                                                              THYLENE            THENE
                                                      STATE           (g dry)     (ppb)+        (ppb)      (ppb)      (ppb)      (ppb)       (ppb)+           (ppb)          (ppb)+         (ppb)+        (ppb)  (ppb)



                  K5246         MSP13         1       MS-35               2.1        9.1        14.2       15.9       39.6       55.8           3.3            1.9              2.7            2.7        13.4      66.6
                  K5247         MSPB          2       MS-35               2.1        7.0        9.2        17.6       37.6       67.8           0.7            2.6              3.1            3.5        9.1       65.5
                  K5248         MSP13         3       MS-35               2.1        3.3        6.7        9.0        28.6       31.9           2.8            0.9              1.2            2.4        6.8       35.3
                  K5234         M13CP         1       AL-36               3.1        6.4        9.1        15.4       23.1       27.3           2.4            3.3              2.5            6.3        6.5       57.9
                  K5235         MBCP          2       AL-36               3.5        4.7        6.2        9.9        14.4       22.6           1.8            3.5              2.4            4.1        5.6       28.3
                  K5236         MBCP          3       AL-36               3.1        3.5        4.9        6.1        13.8       22.0           2.5            0.6              2.2            2.5        4.1       27.1
                  K5240         MBHI          I       AL-66               1.6      10.3         13.0       19.7       63.5       94.5           4.1            8.3              7.1            8.2        20.0      82.3
                  K5241         MBHI          2       AL-66               2.0        7.6        8.5        16.7       50.6       82.1           2.1            6.6              5.1            4.5        15.7      87.9
                  K5242         MBH1          3       AL-66               1.4        5.4        8.6        12.5       24.4       63.1           4.4            2.7              4.1            4.6        15.4      76,2
                  K5261         PBPH          1       FL-67               3.1      81.6         71.5       62.5       64.7       50.9         19.7             9.1           117.9          131.4         52.2      77.1
                  K5262         PBPH          2       FL-67               2.1     175.7         135.5      100.1      94.0       85.9         35.3            15.7           201.0          218.6         81.0     123.5
                  K5263         PBPH          3       FL-67               2.1     123.4         94.8       72.5       76.2       55.7         27.6            11.8           155.4          166.9         59.5      97.0
                  K5255         PBIB          I       FL-37               3.7        4.8        5.7        10.7       118.5      22.9           2.1            2.5              5.9            7.3        7.5       17.6
                  K5256         PBIB          2       FL-37               2.9      11.4         11.6       13.4       22.5       25.4           5.3            4.1              8.9            9.8        9.1       28.6
                  K5257         PBIB          3       FL-37               2.8        5.0        5.8        13.3       19.9       25.4           4.7            5.1              8.0            8.9        9.9       27.3
                  K5267         CI3,JI3       I       FL-73               2.0      52.0         158.3      131.3      128.9      142.3          &7             8.0            46.7            46.4        39.1     101.3
                  K5268         CBJ13         2       FL-73               2.1      59.1         155.4      120.6      114.9      144.6          9.5            8.3            54.7            49.5        44.2     100.1
                  K5269         CI3JI3        3       FL-73               1.9      64.3         173.3      148.3      130.2      130.0        11.7             9.4            86.6            74.5        51.6     132.7
                  K5273         CBSR          I       FL-38               2.3        4.8        5.6        13.7       24.5       22.2           2.7            1.6              2.6            3.5        6.7       19.4
                  K5274         CBSR          2       FL-38               2.1      10.3         7.4        8.2        15.7       5.6            4.6            2.0              2.4            3.9        8.7       26.0
                  K5275         CBSR          3       FL-38               2.2        8.0        7.5        14.5       11.8       27.8           2.9            1.5              3.9            4.7        11.2      25.2
                  K5279         CBSP          I       FL-39               1.9      15.7         37.0       36.8       41.51      36.8           4.2            2.8              6.6            7.9        10.2      28.2
                  K5280         CBSP          2       FL-39               2.3        7.3        23.4       22.3       23.7       31.4           4.3            2.3              319            5.3        8.7       33.2
                  K5281         CBSP          3       FL-39               1.9      17.9         56.5       57.9       67.7       46.6           5.1            3.0              8.1            9.0        15.8      45.5
                  K5303         PCLO          I       FL-74               2.2        7.7        14.1       19.7       37.2       42.6           2.4            2.5              2.3            5.2        11.9      27.8
                  K5304         PCI)O         2       FL-74               1.6      24.6         48.8       52.1       57.7       85.3           8.1            7.1            13.4            19.8        37.2     125.9
                  K5305         PCL0          3       FL-74               2.2      13.2         31.4       28.6       45.3       46.1           5.2            3.0              7.9            6.8        23.4      49.3
                  K5297         SAWB          I       FL-40               2.5      14.3         65.6       242.9   1075.0    2390.6           16.6             9.6            27.8            50.4      350.5    1172.6
                  K5298         SAWB          2       FL-40               1.7      31.9         107.8      401.6   1432.3    3668.5           30.8            14.8            42.3            99.0      660.1    2618.4
                  K5299         SAM713        3       FL-40               1.8      24.5         104.4      353.7   1465.3    3333.0           23.8            15.3            40.3            76.9      517.8    2735.1
                  K5291         APD13         1       FL-41               1.6      11.9         16.0       19.4       35.9       31.8           2.8            1.6              1.9            2.5        10.1      35.5
                  K5292         APD13         2       FL-41               1.7      18.7         24.4       18.7       25.3       0.0            2.9            1.8              1.9            3.1        15.7      40.2
                  K5293         APD13         3       FL-41               1.6      11.1         17.0       18.8       26.2       18.5           5.0            1.3              2.2            4.1        10.2      26.2
                  K5285         APCP          I       FL-42               2.1        8.0        41.0       64.5       92.1       105.0          2.8            2.4              4.7            5.7        23.0     103.3
                  K5286         APCP          2       FL-42               2.1      16.4         65.8       96.8       115.4      118.9          4.6            2.0              4.6            5.7        23.7     114.5
                  K5287         APCP          3       FL-42               2.5      11.5         63.2       99.1       130.0      140.9          5.6            2.7              6.6            7.2        26.3     146.5
                  K5321         AESP          1       FL-75               1.5      10.4         11.8       0.0        0.0        0.0            2.7            3.2              2.2            4.2        0.0         0.0
                  K5322         AESP          2       FL-75               1.7      16.8         14.3       0.0        0.0        0.0            3.0            0.6              310            2.9        0.0         0.0






                                                                          MUSSEL WATCH YEAR VI - Bivalve Aromatics Data





                                                                                        Ci-       C2-       C3-        C4-                                                                Cl- C2-
                 FILE        SITE       REP LOCATION SAMPLE                 NAPH      NAPH      NAPH      NAPH         NAPH  BIPHENYL      ACENAPH-       ACENAPH-     FLUORENE FLUOR           FLUOR
                                                  #AND        WEIGHT                                                                        THYLENE           THENE
                                                  STATE         (g dry)    (ppb)+       (ppb)     (ppb)     (ppb)      (ppb)      (ppb)+         (ppb)         (ppb)+         (ppb)+      (ppb)  (ppb)



                 K5323       AESP          3      FL-75             1.5       8.1       14.0      0.0       0.0        0.0          3.9            2.4            1.8           3.6       0.0        0.0
                 K5315       CKBP          I      FL-43             1.8       5.3       7.7       0.0       0.0        0.0          2.5            1.1            3.7           1.6       0.0        0.0
                 K5316       CKBP          2      FL-43             2.0     11.9        11.0      10.0      0.0        0.0          3.2            0.8            0.6           1.9       6.2        0.0
                 K5317       CKBP          3      FL-43             2.2       8.7       8.6       0.0       0.0        0.0          1.9            0.8            110           1.8       0.0        0.0
                 K5353       TBNP          I      FL-76             2.7     10.5        39.6      44.7      59.6       75.3         4.7            3.7            6.2           6.3       15.7     67.1
                 K5351       TBNP          2      FL-76             2.9       9.7       49.7      45.1      63.4       67.9         3.4            2.4            5.4           7.6       15.9     72.1
                 K5352       TBNP          3      FL-76             2.8     14.4        65.8      63.4      85.3       101.7        2.9            3.0            4.2           910       25.0     81.5
                 K5333       TBMK          1      FL-47             3.2       6.6       14.3      11.8      14.9       18.4         2.6            0.8            3.2           5.2       4.8      15.4
                 K5334       TBMK          2      FL-47             1.6     19.5        31.5      31.8      32.6       39.5         4.6            1.4            7.3           10.9      15.0     35.9
                 K5335       TBMK          3      FL-47             1.8     14.3        27.0      30.5      44.0       45.0         7.0            3.6            8.5           12.1      12.2     49.3
                 K5327       TBPB          1      FL-44             2.3       6.6       6.3       0.0       13.2       26.7         2.2            1.0            1.7           1.5       0.0      13.8
                 K5328       TBPB          2      FL-44             1.8     12.4        13.2      13.0      18.2       25.7         4.2            2.1            3.8           2.8       0.0        0.0
                 K5329       TBPB          3      FL-44             2.6       6.5       7.1       0.0       0.0        0.0          5.7            2.3            2.3           3.3       0.0      18.4
                 K5339       TBOT          I      FL-70             1.4     12.3        11.7      0.0       0.0        0.0          2.1            2.2            3.7           2.5       10.8     20.7
                 K5340       TBOT          2      FL-70             1.4     14.5        16.7      14.8      28.0       30.3         2.1            3.1            7.5           3.2       12.8     32.9
                 K5341       TBOT          3      FL-70             1.4     13.7        23.1      20.9      39.6       0.0          5.0            1.6            5.0           5.1       0.0        0.0
                 K5309       TBKA          I      FL-77             2.0       6.8       8.3       10.1      27.1       32.6         1.3            4.1            3.5           2.7       7.1      37.7
                 K5310       TBKA          2      FL-77             1.4     10.5        10.2      12.8      31.1       45.6         2.6            3.8            4.6           4.3       10.4     58.2
                 K5311       TBKA          3      FL-77             1.5     16.5        18.0      25.9      55.1       149.8        4.6           17.7            5.7           7.4       27.5    118.7
                 K5345       TBC13         I      FL-46             2.5     23.3        36.1      21.7      20.9       23.1         3.5            1.9            1.4           2.7       0.0      18.0
                 K5347       TI3CB         2      FL-46             2.5     16.2        42.2      25.5      33.8       25.9         4.6            2.1            1.7           4.1       9.8      18.3
                 K5346       TBC13         3      FL-46             1.6     29.6        57.9      37.2      36.0       30.5         6.0            2.6            2.1           5.3       16.8     26.4
                 K5369       CBBI          I      FL-48             2.3     10.7        15.6      10.9      19.7       23.3         1.6            1.9            1.2           2.0       4.0      29.0
                 K5370       CBBI          2      FL-48             2.1     14.3        14.9      29.0      36.1       0.0          3.8            0.8            1.4           1.7       7.3      29.4
                 K5371       CBBI          3      FL-48             2.5       9.4       12.@      11.0      22.7       21.1         4.4            0.8            1.8           1.6       8.3      18.7
                 K5363       CBFM          1      FL-71             2.3     37.5        64.9      30.8      25.9       26.2         2.6            2.9            1.6           3.7       5.7      33.3
                 K5364       CBFM          2      FL-71             1.8     57.7        88.3      45.2      31.0       34.6         3.8            4.7            2.5           4.4       12.4     42.7
                 K5365       CBFM          3      FL-71             1.8     14.8        17.8      28.6      38.2       40.3         5.7            4.3            2.6           1.7       15.3     49.0
                 K5357       NBNB          I      FL-49             2.2       7.8       15.8      17.6      35.6       71.0         3.7            1.8            1.5           2.0       19.8    105.3
                 K5358       NBNB          2      FL-49             2.4     10.1        17.7      16.6      34.1       69.8         2.0            1.9            1.3           4.0       16.3    101.9
                 K5359       NBNB          3      FL-49             2.4     10.7        20.6      18.9      36.9       60.7         3.7            2.4            1.9           3.6       19.9    117.5
                 K5381       RBHC          1      FL-50             2.4       9.1       13.8      13.0      26.8       21.0         2.2            0.8            1.5           1.2       7.6      30.2
                 K5382       RBHC          2      FL-50             2.4     10.8        23.9      17.8      24.3       22.8         3.7            0.8            0.7           1.8       10.5     39.9
                 K5383       RBHC:         3      FL-50             2.4     10.6        18.8      18.2      32.7       36.3         3.4            0.7            1.2           2.6       9.5      50.6
                 K5375       EVFU          I      FL-51             1.4     13.5        11.5      0.0       0.0        0.0          2.3            0.8            1.4           2.2       0.0        0.0
                 K5376       EVFU          2      FL-51             2.4     13.6        12.1      0.0       0.0        0.0          2.8            0.6            1.5           1.3       0.0        0.0
                 K5377       EVFU          3      FL-51             2.3       8.0       10.7      16.6      19.0       27.9         4.8            0.6            2.0           2.6       7.8      17.9
                 K5396       BHKF          I      FL-81             2.9     10.8        18.3      16.3      20.3       21.8         2.9            0.8            0.6           2.6       4.0      14.9



                                                                             MM MM M M M M M
                                                                                 MUSSEL WATCH YEAR VI - Bivalve Aromatics Data





                                                                                                Cl-        C2-        C3-         C4-                                                                     Cl- C2-
                  FILE          SITE       REP LOCATION SAMPLE                    NAPH NAPH              NAPH       NAPH       NAPH    BIPHENYL ACENAPH-              ACENAPH- FLUORENE FLUOR FLUOR
                                                       # AND        WEIGHT                                                                              THYLENE             THENE
                                                       STATE          (g dry)    (ppb)+        (ppb)      (ppb)      (ppb)      (ppb)       (ppb)+            (ppb)          (ppb)+         (ppb)+      (ppb) (ppb)


                   K5397       BHKF          2         FL-81               2.7       6.6        19.6       14.7      20.7        18.2           1.5              1.4             1.2           0.9         3.2      16.3
                   K5398       BHKF          3         FL-81               2.5      12.1       30.0        17.6      21.8        24.2          3.0              0.9              1.3           0.9         2.2      14.7





                                                                           MUSSEL WATCH YEAR VI - Bivalve Aromatics Data




                                                                   P3-                                 CI-        C2-         C3-         C4-      DBT      Cl-     C2-      C3-
                 FILE         SITE      REP LOCAMON FLUOR               PHENAN ANTHRAC PHEN + PHEN + PHEN + PHEN +                                         DBT      DBT      DBT   FLUORANTH
                                                   #AND                                           ANTHRA     ANTHRA      ANTHRA      ANTHRA
                                                   STATE          (ppb)     (ppb)+       (ppb)+        (ppb)      (ppb)       (ppb)       (ppb)   (ppb)    (ppb)    (ppb)    (ppb)     (ppb)+


                 K5135        LMSB         I       Tx- 1           0.0       10.1          1.4         0.0        0.0         0.0         0.0      0.8      0.0     0.0      0.0             16.3
                 K5136        LMSB         2       TX-1            0.0         4.3         1.3         10.5       0.0         0.0         0.0      0.4      0.0     5.5      0.0             13.0
                 K5137        LMSB         3       TX-i            0.0         3.1         1.2         6.1        0.0         0.0         0.0      0.5      0.0     0.0      0.0             8.7
                 K5087        ccic         1       TX-3            0.0       14.1          4.4         21.6       27.8        14.1        11.0     1.4      6.6     12.5     9.7             51.2
                 K5088        ccic         2       TX-3            0.0       12.8          4.9         20.6       26.9        18.4        14.9     2.1      5.2     14.6     10.7            43.4
                 K5089        CCIC         3       TX-3            0.0       19.1          4.6         22.0       34.0        22.8        20.4     2.4      4.2     8.8      9.8             51.3
                 K5147        ABLR         1       TX-4            0.0         2.4         1.2         16.8       8.3         0.0         0.0      0.4      0.0     0.0      0.0             0.7
                 K5148        ABLR         2       TX-4            0.0         2.6         1.1         12.6       9.5         0.0         0.0      0.4      0.0     0.0      0.0             0.7
                 K5149        ABLR         3       TX-4            0.0         3.6         2.0         34.5       11.7        0.0         0.0      0.5      0.0     0.0      0.0             0.7
                 K5141        CBCR         1       TX-5            0.0         1.8         0.6         0.0        0.0         0.0         0.0      0.3      0.0     0.0      0.0             0.9
                 K5142        CBCR         2       TX-5            0.0         2.1         0.5         0.0        0.0         0.0         0.0      0.5      0.0     0.0      0.0             0.7
                 K5143        CBCR         3       TX-5           23.1         2.7         0.3         0.0        0.0         0.0         0.0      0.7      0.0     0.0      0.0             0.9
                 K5099        MBAR         1       TX-6            0.0         2.0         0.6         0.0        0.0         0.0         0.0      0.4      0.0     0.0      0.0             0.6
                 K5100        MBAR         2       TX-6            0.0         2.5         1.4         0.0        0.0         0.0         0.0      0.9      0.0     0.0      0.0             0.7
                 K5101        MBAR         3       TX-6            0.0         2.7         1.0         0.0        0.0         0.0         0.0      0.3      0.0     0.0      0.0             0.7
                 K51 11       SAPP         1       TX-7            0.0         2.7         0.8         0.0        0.0         0.0         0.0      0.5      0.0     0.0      0.0             0.5
         00      K5112        SAPP         2       TX-7            0.0         3.0         0.9         0.0        0.0         0.0         0.0      0.6      0.0     0.0      0.0             0.6
                 K5113        SAPP         3       TX-7            0.0         2.5         1.2         0.0        0.0         0.0         0.0      0.3      0.0     0.0      0.0             0.6
                 K5117        SAMP         1       TX-8            0.0         3.5         2.2         7.4        12.9        14.4        18.1     0.5      0.0     5.8      7.4             1.7
                 K5118        SAMP         2       TX-8            0.0         3.6         2.7         15.5       22.8        19.2        24.7     0.7      0.0     9.4      14.3            0.9
                 K5119        SAMP         3       TX-8            0.0         3.6         3.2         7.2        12.2        9.7         8.5      0.3      0.0     4.6      5.8             0.8
                 K5105        ESSP         1       TX-9            0.0         7.6         1.8         14.4       21.3        14.4        14.4     1.5      4.6     12.4     9.6             2.7
                 K5106        ESSP         2       TX-9            0.0         8.5         2.4         18.7       19.7        10.8        20.4     1.3      4.5     13.0     8.7             4.4
                 K5107        ESSP         3       TX-9            0.0       10.5          2.5         18.7       27.8        14.9        0.0      2.5      3.5     7.3      8.2             4.4
                 K5129        MBGP         I       TX- 12          0.0         8.1         4.9         50.3       31.5        18.5        19.8     0.8      0.0     9.4      12.4            9.4
                 K5130        MBGP         2       TX- 12          0.0         8.0         4.3         29.4       31.7        17.7        0.0      1.7      0.0     13.4     13.1            8.8
                 K5131        MBGP         3       TX-12           0.0         7.0         5.8         24.6       39.2        33.7        23.1     1.2      0.0     10.7     13.4            8.8
                 K5123        MBLR         1       TX-11           0.0         8.5         4.7         8.5        12.1        9.8         8.8      0.9      0.0     6.8      7.4             23.3
                 K5124        MBLR         2       TX-11           0.0       14.7          4.7         15.0       26.9        0.0         0.0      2.0      0.0     21.7     20.2            30.8
                 K5125        MBLR         3       7X-11           0.0         8.8         4.4         11.5       21.6        0.0         14.6     1.5      0.0     5.9      0.0             18.3
                 K5081        MBTP         1       TX-13           0.0         2.0         2.1         7.1        5.2         0.0         0.0      0.4      0.0     0.0      0.0             0.8
                 K5082        MBTP         2       TX-13           0.0         3.1         2.1         7.3        8.4         0.0         0.0      1.7      0.0     0.0      0.0             0.6
                 K5083        MBTP         3       TX-13           0.0         2.9         1.4         6.9        10.0        010         0.0      0.7      0.0     0.0      0.0             0.9
                 K5075        MBEM         1       TX-14           0.0         4.2         3.5         13.8       20.2        31.8        14.4     1.2      010     9.3      15.1            2.5
                 K5076        MBEM         2       TX- 14         22.2         3.9         2.3         9.9        20.0        24.8        15.9     1.5      2.3     13.0     15.1            1.7
                 K5077        MBEM         3       TX- 14          6.6         3.4         3.0         6.6        21.4        15.8        010      0.5      0.0     6.7      8.8             1.9
                 K5015        BRCL         1       TX-72           0.0         5.9         3.8         11.8       24.0        27.6        0.0      1.1      4.8     11.5     14.2            11.7
                 K5016        BRCL         2       TX-72           0.0         6.6         5.0         11.3       35.8        27.2        0.0      1.2      0.0     13.1     14.3            14.1





                                                                                 MUSSEL WATCH YEAR VI - Bivalve Aromatics Data





                                                                       C3-                                    Ci-          C2-         C3-          C4-      DBT       Ci-       C2-      C3-
                  FILE           SITE      REP LOCATION FLUOR                 PHENAN ANTHRAC PHEN + PHEN + PHEN + PHEN +                                               DBT       DBT      DBT FLUORANTH
                                                      #AND                                               ANMRA        ANTHRA      ANTHRA       ANTHRA
                                                      STATE           (ppb)      (ppb)+        (ppb)+         (ppb)        (ppb)       (ppb)        (ppb)    (ppb)     (ppb)     (ppb)    (ppb)      (ppb)+


                  K5017        BRCL           3       TX-72           61.4          7.7           3.1         9.2          30.2        42.8         37.6      0.8      0.0       14.4     19.3             14.2
                  K5021        BRFS           1       TX-57           185.2        98.0          45.9         81.4         142.9       97.9         56.9      5.5      10.5      34.5     72.8           479.1
                  K5022        BRFS           2       TX-57           149.6        38.1          18.8         38.6         86.2        78.8         34.8      3.0      11.0      36.0     37.6           150.4
                  K5023        BRFS           3       TX-57           72.1         36.3           6.5         23.8         87.8        57.6         35.5      4.5      8.3       33.3     39.8           159.7
                  K5009        GBCR           1       TX-18           73.8         18.4           7.4         23.9         52.7        48.1         27.9      1.8      3.5       15.3     16.2           114.7
                  K5010        GBCR           2       TX-18           63.7         17.0          15.4         73.3         54.9        54.0         20.9      1.7      8.0       24.6     20.6             92.4
                  K5011        GBCR           3       TX-18           100.6        20.4          15.5         29.0         48.4        27.6         17.5      1.6      4.1       13.9     12.7           119.4
                  K5003        GBOB           1       TX-58           37.0         22.3          11.9         22.9         47.1        45.5         33.8      1.4      4.5       14.5     16.9           138.9
                  K5004        GBOB           2       TX-58           62.4         14.1          12.9         21.2         46.2        72.4         52.0      1.9      5.3       19.7     21.6             87.4
                  K5005        GBOB           3       TX-58           49.8          6.5          12.6         12.6         33.8        29.1         18.9      0.8      2.0       10.5     15.6             63.8
                  K5057        GI3TD          I       TX- 16          116.1        10.0           9.4         40.4         102.0       126.0        214.7     3.4      11.4      52.6     141.2            9.7
                  K5058        GI3TD          2       TX-16           156.5        11.4           9.9         44.9         115.3       224.8        307.0     3.0      10.7      60.5     186.5            9.7
                  K5059        GBTD           3       TX-16           360.0        13.5          13.0         89.8         287.9       645.1    1079.5        3.9      27.4      184.2    707.4            12.3
                  K5063        GBYC           1       TX-15           35.5          7.4          21.0         0.0          44.7        52.5         33.0      2.0      4.4       11.4     18.3             9.6
                  K5064        GBYC           2       TX-15            0.0          7.2          12.7         26.3         25.7        46.9         44.6      3.8      0.0       26.1     27.5             12.0
                  K5065        GBYC           3       TX-15           28.3          .6.4          9.3         20.0         42.0        34@O         29.8      2.6      6.0       14.6     24.5             1012
                  K5384        GBSC           1       TX-59         6205.8       1471.3        273.2       2754.7       5225.2     13187.0      8866.7      103.2    567.2    1901.8   5212.8            673.6
                  K5385        GBSC           2       TX-59         5782.4       1366.3        307.1       2489.8       4459.8      8495.4      6167.1      115.0    507.7   1642.1    4172.1            629.8
                  K5386        GBSC           3       TX-59         7659.2       1699.8        263.7       3266.0       6289.1     12037.5      8399.3      129.6    552.5   1788.5    4805.0            841.7
                  K5039        GBHR           I       TX-17           50.8          6.8           9.0         27.6         31.9        32.8         23.1      0.9      010       9.6      12.3             7.3
                  K5040        GBHR           2       TX-17           71.3          7.2           5.9         21.3         36.2        34.2         27.3      0.9      4.5       11.5     16.6             7.1
                  K5041        GBHR           3       TX-17           52.0          8.2           4.9         16.1         27.3        24.0         21.2      1.4      7.1       12.3     18.2             7.4
                  K5027        SLBB           I       TX-19           95.5         12.2          17.0         71.0         85.7        142.5        75.8      2.0      11.5      27.3     29.4             25.3
                  K5028        SLBB           2       TX-19           178.5        22.1          18.8         60.6         120.9       139.6        156.0     5.7      17.8      65.3     80.0             38.6
                  K5029        SLBB           3       TX-19           122.7         8.4           4.7         19.5         44.7        68.3         65.8      3.6      5.3       21.8     22.5             15.0
                  K5033        CLSJ           1       IA-20           253.6        16.8           3.5         97.4         221.7       127.5        58.0      2.1      12.0      46.1     50.3             10.3
                  K5034        CLSIJ          2       IA-20           337.8        19.2           2.4         79.5         239.1       194.5        96.3      3.9      12.5      74.4     92.5             10.1
                  K5035        CL-1:0         3       LA-20           197.2        11.6           2.1         65.5         201.3       140.3        64.7      1.8      9.9       49.9     64.5             8.6
                  K5045        CLLC           1       LA-60           216.3        19.0          32.6         82.1         144.6       177.4        112.4     3.6      10.6      34.0     45.5             71.0
                  K5046        CLLC           2       LA-60           102.9        12.0          17.1         43.4         84.0        111.8        98.8      3.5      10.9      40.4     54.3             52.0
                  K5047        CLLC           3       LA-60           114.2        18.7          18.1         65.5         133.5       117.7        78.9      5.4      15.9      49.3     71.5             69.9
                  K5069        JHJH           I       I-A-21           0.0         23.6           5.6         23.3         27.6        23.3         16.6      1.3      2.3       4.4      10.1             18.9
                  K5070        JHJH           2       IA-21           52.6         15.8           3.4         13.7         22.1        16.0         16.2      2.5      4.2       15.2     13.1             16.0
                  K5071        JHJH           3       IA-21            0.0         15.1           2.8         8.2          15.7        10.6         7.8       2.0      1.6       6.8      7.7              11.4
                  K5159        VBSP           I       LA-22           27.8          7.2           2.0         19.0         26.9        16.8         16.5      0.7      4.5       12.0     12.6             5.0
                  K5160        VBSP           2       IA-22            0.0          6.9           1.8         17.7         27.1        17.6         21.0      0.7      9.9       15.6     10.3             4.8
                  K5161        VBSP           3       IA-22           43.0          7.2           2.8         13.5         28.7        23.5         17.7      0.7      2.1       6.2      8.6              5.2
                  K5189        ABOB           1       IA-24            0.0          5.6           1.8         13.1         17.2        16.3         0.0       1.1      0.0       0.0      0.0              2.2





                                                                              MUSSEL WATCH YEAR VI - Bivalve Aromatics Data





                                                                      C3-                                   Ci-         C2-         C3-          C4-     DBT       Cl-      C2-      C3-
                  FILE         SITE       REP LOCATION FLUOR                PHENAN ANTHRAC PHEN + PHEN + PHEN + PHEN +                                             DBT      DBT      DBT FLUORANTH
                                                     # AND                                            ANTHRA       ANTI-IRA    ANTHRA      ANTHRA
                                                     STATE          (ppb)       (ppb)+       (ppb)+         (ppb)       (ppb)       (ppb)        (ppb)   (ppb)     (ppb)    (ppb)    (ppb)     (ppb)+


                  K5190        ABOB          2       LA-24            0.0         4.7           2.2         8.8         12.5        22.5         0.0      0.8      4.6      8.1      6.7              2.5
                  K5191        ABOB          3       IA-24            0.0         4.1           1.9         5.5         11.2        10.1         0.0      0.4      0.0      0.0      0.0              2.0
                  K5195        CLCL          1       IA-25            0.0         7.0           1.5         13.6        23.6        0.0          0.0      0.9      0.0      14.7     10.8             4.2
                  K5196        CLCL          2       LA-25            0.0         6.5           1.2         11.4        16.1        0.0          0.0      1.3      3.1      10.3     8.0              3.4
                  K5197        CLCL          3       IA-25            0.0         5.7           1.3         8.1         13.9        11.0         10.6     0.7      0.0      0.0      0.0              3.5
                  K5165        TBLI3         I       LA-26            0.0         4.1           1.8         10.5        16.4        18.9         14.5     0.8      0.0      10.5     8.1              4.7
                  K5166        TBLB          2       IA-26            0.0         9.0           3.4         15.8        19.6        15.4         19.3     1.3      0.0      14.9     9.9              8.3
                  K5167        TBLB          3       LA-26            0.0         5.6           1.7         9.1         19.3        33.8         26.8     0.6      0.0      7.1      9.5              5.0
                  K5183        TBLF          1       IA-27          54.6          6.4           1.4         9.5         17.0        33.7         25.9     1.0      2.4      11.1     10.8             4.0
                  K5184        TBLF          2       LA-27          52.0          5.7           2.0         15.9        23.6        18.3         30.9     1.2      6.2      10.8     11.2             4.3
                  K5185        TBLF          3       IA-27            0.0         5.1           1.7         11.4        15.5        26.0         26.7     0.8      2.5      6.9      8.6              3.0
                  K5168        BBSD          1       IA-28            0.0         8.4           4.5         36.7        44.5        40.4         0.0      1.4      4.7      14.6     15.7             4.0
                  K5169        BBSD          2       IA-28            0.0         5.7           2.3         0.0         24.8        18.1         30.2     1.6      9.7      13.1     12.5             4.2
                  K5170        BBSD          3       LA-28          59.9          6.7           1.7         15.6        29.4        39.5         30.5     1.0      5.0      14.8     12.6             4.9
                  K5174        B13MB         1       IA-29          110.3        69.7         42.6          52.0        109.5       112.2        48.9     4.3      12.2     37.4     42.6          202.5
                  K5175        BBMB          2       IA-29          37.5         50.3         20.9          38.3        87A         91.4         54.8     3.5      9.6      27.8     34.3          235.4
          0       K5176        BBMB          3       LA-29          49.7         61.3         28.3          42.3        92.6        96.7         6.1      3.1      4.5      17.6     21.8          273.8
                  K5210        MRIP          I       LA-65          240.4        31.0         10.1          100.5       300.3       300Z         159,4    6.8      24.3     110.2    130.5           31.1
                  K5211        MRTP          2       LA-65          213.2        18.3           8.0         58.0        151.3       143.8        73.1     3.1      11.5     45.2     64.2            16.0
                  K5212        MRT?          3       LA-65          124.7        16.8           3.6         43.0        135.2       137.5        76.2     3.1      11.1     38.7     50.4            17.7
                  K5216        BSSI          I       LA-31          414.2        23.7           7.5         85.1        254.6       232.9        122.6    5.8      17.4     85.5     85.8            33.9
                  K5217        BSSI          2       LA-31          186.8        15.2           5.7         57.6        164.3       104.5        59.5     4.2      12.8     40.7     38.4            29.0
                  K5218        BSSI          3       IA-31          128.5        17.7           5.6         77.5        173.1       142.8        81.0     3.6      12.2     37.0     36.6            28.9
                  K5201        BSBG          1       LA-30            0.0         7.9           1.6         30.9        0.0         0.0          0.0      1.0      0.0      15.7     11.7             3.6
                  K5202        BSBG          2       IA-30            0.0         6.5           0.8         14.4        20.5        13.7         15.7     1.1      0.0      0.0      5.3              3.3
                  K5203        BSBG          3       IA-30            0.0         4.4           0.6         6.4         13.4        11.2         7.8      0.4      0.0      0.0      0.0              3.0
                  K5207        LBMP          I       LA-32          68.6          8.9           2.3         14.5        41.1        23.1         18.8     1.0      6.8      16.5     11.7            10.7
                  K5208        LBMP          2       LA-32            0.0         8.6           2.2         i4.7        26.9        12.2         0.0      1.0      0.0      11.0     6.0             10.0
                  K5209        LBMP          3       LA-3@          39.8          6.8           1.3         9.3         27.1        11.9         0.0      0.7      0.0      5.2      0.0              8.6
                  K5249        LPGO          1       IA-63        4261.3        632.8         94.3      3078.6      5959.9       4895.8      2250.2     122.3      884.9  2293.1 2412.2            430.4
                  K5250        LPGO          2       IA-63        3869.0        558.8         83.6      3038.1      5237.4       3362.8       1440.9    108.1      740.2  1850.2 1821.7            359.2
                  K5251        LPGO          3       LA-63        5511.5       1154.8         92.7      6032.9      9982.5       5615.4      2347.2     229.3   1367.3   3246.5  3098.9            589.5
                  K5222        MSPC          1       MS-33          250.9        36.19        11.2          62.5        133.6       130.8        78.3     5.2      30.4     146.9    156.4           78.8
                  K5223        MSPC          2       MS-33            0.0        24.2           9.9         34.1        71.1        47.5         32.6     2.6      11.3     47.5     51.3            55.7
                  K5224        MSPC          3       MS-33          66.7         19.9           3.6         29.4        62.4        44.8         29.2     2.3      9.8      46.3     53.5            42.7
                  K5228        MSB13         1       MS-34        1244.2         124.4        33.6          417.0   1008.3          928.7        493.3   31.0      197.0    876.9 1039.3           129.8
                  K5229        MSBB          2       MS-34        1234.3         185.1        49.2          714.3   1580.8          972.7        460.5   34.0      187.4    747.6    838.5         235.5
                  K5230        MSBB          3       MS-34          390.3        64.5           7.1         252.3       565.6       297.3        151.5    15.7     88.2     303.8    353.0           94.7





                                                                            MUSSEL WATCH YEAR VI - Bivalve Aromatics Data





                                                                   C3-                                Ci-         C2-          C3-        C4-     DBT       Ci-      C2-     C3-
                 FILE         SITE      REP LOCATION FLUOR              PHENAN ANTHRAC PHEN + PHEN + PHEN + PHEN +                                          DBT DBT DErr           FLUORANTH
                                                  #AND                                            ANTHRA     ANTHRA      ANTHRA      ANTHRA
                                                  STATE          (ppb)      (ppb)+       (ppb)+       (ppb)       (ppb)      (ppb)        (ppb)   (ppb)     (ppb)    (ppb)   (ppb)     (ppb)+


                 K5246        MSP13        I      MS-35          177.4       14.4         11.1        50.2        127.3      117.3        106.9     2.3     17.6     103.1   111.4          43.8
                 K5247        MSPB         2      MS-35          130.0       12.1         11.4        47.9        99.8       87.1         48.6      1.3     11.0     56.6    57.1           36.7
                 K5248        MSP13        3      MS-35          63.7        11.4           3.2       29.9        97.4       70.8         60.8      1.2     8.4      41.4    57.8           36.6
                 K5234        M13CP        1      AL-36          104.6       34.5         17.0        46.7        85.2       70.3         53.7      2.4     11.8     56.9    46.6           69.9
                 K5235        MBCP         2      AL-36            0.0       19.5         10.1        27.1        53.4       30.4         21.4      0.8     4.2      16.1    16.4           41.9
                 K5236        MBCP         3      AL-36          45.8        13.5           2.0       17.4        38.3       22.3         22.9      1.2     4.7      15.5    17.4           33.7
                 K5240        MBHI         I      AL-66          229.1       25.8         22.4        62.5        179.0      148.4        41.8      2.9     23.6     115.8   123.7         135.0
                 K5241        MBHI         2      AL-66          259.5       19.2         23.9        59.6        128.5      87.4         56.2      2.1     14.1     54.9    61.3          124.0
                 K5242        MBHI         3      AL-66          136.1       16.0           8.2       41.1        104.0      64.5         50.5      2.3     11.8     52.7    53.0          106.0
                 K5261        PI3PH        I      FL-67          110.0      425.4         64.5        179.2       150.7      108.6        53.6    21.7      23.4     58.4    52.8          538.7
                 K5262        PBPH         2      FL-67          178.5      724.5         92.2        264.7       226.4      157.5        68.1    36.5      34.9     91.4    78.6          829.0
                 K5263        P13PH        3      FL-67          171.8      536.2         33.5        189.8       186.3      162.9        74.0    22.4      23.7     74.7    74.1          597.4
                 K5255        PBIB         I      FL-37          31.5        19.9         13.3        25.3        24.9       53.4         28.0      1.7     4.5      10.8    9.9            30.3
                 K5256        PBIB         2      FL-37          52.5        33.8         19.7        32.1        39.5       53.1         31.4      3.0     5.7      19.3    15.3           50.3
                 K5257        PBIB         3      FL-37            0.0       26.3         15.0        24.3        36.3       63.2         42.5      2.4     7.4      20.8    15.2           37.6
                 K5267        CBJ13        1      FL-73          208.8       96.4         20.7        147.2       289.0      276.6        119.7     8.2     33.8     159.9   164.3         270.1
                 K5268        CBJB         2      FL-73          200.0      140.4         21.7        161.2       329.5      283.8        153.1   11.0      38.2     165.8   176.5         317.3
                 K5269        CBJB         3      FL-73          230.4      164.9         12.8        155.0       282.4      217.9        126.9   12.5      31.7     142.3   136.1         325.0
                 K5273        CBSR         1      FL-38          43.5        11.8           2.7       15.0        23.2       31.3         16.2      1.3     4.5      11.6    10.7           12.1
                 K5274        CBSR         2      FL-38          51.8        13.8           2.0       14.3        20.8       28.2         22.6      1.3     4.0      10.5    10.3           12.7
                 K5275        CBSR         3      FL-38          53.0        12.0           2.1       12.6        21.8       29.5         14.1      1.1     3.0      12.3    13.7           10.6
                 K5279        CBSP         1      FL-39          35.6        38.3           8.2       54.7        98.4       83.6         88.3      3.2     11.5     36.7    45.1           74.6
                 K5280        CBSP         2      FL-39            0.0       27.3           6.0       45.5        78.3       80.3         84.5      2.2     11.8     38.9    47.5           47.3
                 K5281        CBSP         3      FL-39          51.8        45.3           5.4       52.3        89.8       77.3         64.4      3.0     9.2      35.0    33.5           94.6
                 K5303        PCLO         1      FL-74          75.9        22.2         11.9        51.0        80.0       99.7         63.7      1.9     11.4     39.0    42.2           40.3
                 K5304        PCLO         2      FL-74          235.3       84.8         19.3        124.0       202.5      272.1        120.4     5.0     20.4     75.9    88.0          152.7
                 K5305        PCLO         3      FL-74          104.4       34.9           8.8       50.5        93.1       118.3        50.0      2.0     8.1      30.3    34.4           44.9
                 K5297        SAWB         I      FL-40         3206.8      294.6         74.7      1979.8     4004.1      2968.4       1134.8    46.7      514.2  1895.3  1708.2          521.9
                 K5298        SAWB         2      FL-40         4707.5      462.4         70.3        322.8    6721.2      4081.9       1453.0    78.0      759.4  2727.1  2511.6          895.8
                 K5299        SAWB         3      FL-40         4651.4      465.3         56.0      3057.7     6682.4      3792.3       1454.8    69.1      680.8  2352.5  2005.9          885.9
                 K5291        APD13        I      FL-41          74.7          8.7          3.2       22.9        38.8       50.4         51.1      1.0     5.8      19.2    23.6           12.6
                 K5292        APDB         2      FL-41          74.6        10.4           3.0       20.5        29.6       64.6         38.4      1.5     5.0      17.2    18.7           11.8
                 K5293        APDB         3      FL-41          52.4        13.0           2.2       17.5        36.5       60.9         42.4      1.1     5.1      12.6    15.2           12.9
                 K5285        APCP         I      FL-42          200.6       26.9         12.6        89.6        200.8      187.8        174.5     2.9     16.5     71.9    90.2           54.4
                 K5286        APCP         2      FL-42          196.5       38.3         11.2        117.6       238.3      202.2        164.5     4.6     22.8     92.9    97.2           67.5
                 K5287        APCP         3      FL-42          296.8       49.7           7.5       130.3       287.8      262.3        273.8     4.8     27.1     97.4    111.5          80.2
                 K5321        AESP         I      FL-75            0.0       10.8           2.4       10.3        15.3          0.0       0.0       1.1     0.0      0.0     0.0              9.7
                 K5322        AESP         2      FL-75            0.0       12.1           1.3       11.2        15.6          0.0       0.0       1.1     0.0      0.0     0.0              9.9





                                                                          MUSSEL WATCH YEAR VI - Bivalve Aromatics Data





                                                                  C3-                                 Ci-        C2-         C3-        C4-      DBT      Ci-     C2-      C3-
                 FILE        SITE      REP LOCATION FLUOR              PHENAN ANTHRAC PHEN + PHEN + PHEN + PHEN +                                         DErr    DBT      DBT   FLUORANTH
                                                 #AND                                            ANTHRA     ANTHRA      ANTHRA     ANTHRA
                                                 SrATE          (ppb)      (ppb)+       (ppb)+        (ppb)      (ppb)     (ppb)        (ppb)   (ppb)     (ppb)   (ppb)    (ppb)     (ppb)+


                 K5323       AESP         3      FL-75            0.0       14.3          1.1         15.1       18.2        0.0        0.0      1.1      0.0     0.0      0.0             11.3
                 K5315       CKBP         1      FL-43            0.0         5.1         0.6         0.0        0.0         0.0        0.0      0.8      0.0     0.0      0.0             3.2
                 K5316       CKBP         2      FL-43            0.0         6.7         0.8         0.0        0.0         0.0        0.0      0.9      0.0     0.0      0.0             3.8
                 K5317       CKBP         3      FL-43            0.0         5.9         0.8         0.0        0.0         0.0        0.0      1.3      0.0     0.0      0.0             3.0
                 K5353       TBNP         I      FL-76          105.7       27.8          6.8         56.2       130.2     124.5        74.8     3.1      5.0     27.5     43.0         168.0
                 K5351       TBNP         2      FL-76          116.2       27.4          8.2         51.0       101.3     115.0        52.8     2.1      6.9     26.6     31.5         167.5
                 K5352       TBNP         3      FL-76          131.4       35.2          8.9         51.6       117.9     125.4        55.6     2.1      6.8     22.5     26.4         185.8
                 K5333       TBMIK        I      FL-47            0.0       23.7          1.7         20.5       17.2      39.3         0.0      1.7      0.0     8.7      5.9             22.7
                 K5334       TBMK         2      FL-47          119.9       51.0          4.3         46.9       89.6      90.9         0.0      3.2      6.5     15.7     11.2            65.3
                 K5335       TBMK         3      FL-47          97.0        65.5          5.0         32.5       29.0      43.4         33.3     4.6      0.0     17.9     14.6            73.1
                 K5327       TBPB         1      FL-44          41.9          7.2         2.5         11.2       22.1        0.0        0.0      1.3      0.0     8.3      7.4             39.9
                 K5328       TBPB         2      FL-44            0.0       12.5          3.9         20.4       29.8        0.0        0.0      1.5      0.0     12.7     12.7            69.8
                 K5329       TBPB         3      FL,44          38.8          7.5         2.5         11.9       20.4        0.0        0.0      0.6      0.0     12.3     0.0             40.2
                 K5339       TBOT         1      FL-70            0.0         7.0         1.3         12.6       23.8        0.0        0.0      0.8      0.0     10.8     0.0             24.7
                 K5340       TBOT         2      FL-70          30.3        11.6          3.1         19.3       31.7      34.1         0.0      1.5      0.0     10.7     10.0            42.5
                 K5341       TBOT         3      FL-70            0.0       12.2          3.1         16.2       33.7        0.0        0.0      2.0      0.0     0.0      0.0             36.5
                 K5309       TBKA         1      FL-77          111.7       14.7          16.3        38.9       137.0     252.1        178.3    1.8      8.1     49.7     114.4        122.7
                 K5310       TBKA         2      FL-77          146.8       22.3          12.2        47.0       137.5     224.7        130.4    2.5      8.3     56.4     86.6         122.1
                 K5311       TBKA         3      FL-77          324.4       42.4          28.8        83.9       229.9     321.2        167.4    6.8      17.0    81.7     117.9        258.6
                 K5345       7BCB         I      FL-46            0.0       11.8          1.3         22.3       15.8      44.8         0.0      1.0      0.0     6.2      0.0             11.7
                 K5347       TBCB         2      FL-46          32.3        17.2          1.0         14.3       19.6      32.5         12.1     1.0      0.0     0.0      0.0             15.7
                 K5346       TBCB         3      FL-46          86.2        27.3          2.1         27.6       30.5      77.8         0.0      3.0      0.0     11.4     0.0             23.7
                 K5369       CBBI         I      FL-48          47.5          3.6         1.3         18.6       29.1      34.9         14.7     0.5      0.0     10.0     8.9             17.1
                 K5370       CBBI         2      FL-48          45.9          3.1         2.3         11.0       24.0      30.3         16.4     0.4      0.0     10.2     8.2             14.0
                 K5371       CBBI         3      FL-48          23.6          4.0         1.6         9.7        19.7      22.8         9.4      0.6      0.0     7.7      6.1             11.1
                 K5363       CBFM         1      FL-71          63.6          7.1         3.0         12.4       30.7      38.1         22.5     0.6      2.3     12.3     13.3            26.6
                 K5364       CBFM         2      FL-71          82.6          8.6         4.1         19.6       33.7      45.2         25.4     1.1      2.3     12.8     14.2            31.2
                 K5365       CBFM         3      FL-71          138.2         7.0         4.0         18.8       45.6      57.1         42.4     0.8      6.0     17.5     24.1            39.0
                 K5357       NBNB         I      FL-49          163.6         6.8         6.9         28.6       125.2     149.7        69.4     0.9      5.4     29.7     37.1            67.7
                 K5358       NBNB         2      FL-49          187.3         6.2         6.2         29.1       115.7     142.0        63.0     1.7      4.2     26.8     37.3            55.7
                 K5359       NBNB         3      FL-49          210.4       12.1          8.9         26.1       134.1     133.4        53.6     1.5      5.8     22.8     27.0            67.5
                 K5381       RBHC         I      FL-50          44.2          2.2         1.7         7.5        28.0      33.9         20.3     1.1      0.0     6.6      8.6             10.6
                 K5382       RBHC         2      FL-50          65.4          3.6         1.5         13.2       32.7      41.2         19.0     0.5      0.0     8.2      8.6             14.9
                 K5383       RBHC         3      FL-50          81.9          4.6         2.8         12.0       33.6      32.9         20.8     0.4      0.0     0.0      0.0             15.7
                 K5375       EVFU         1      FL-51            0.0         2.0         0.6         6.3        12.9      25.4         14.9     1.0      0.0     0.0      0.0             4.2
                 K5376       EVFU         2      FL-51            0.0         1.7         0.9         0.0        0.0         0.0        0.0      0.3      0.0     0.0      0.0             4.1
                 K5377       EVFU         3      FL-51          30.1          2.5         0.9         7.2        16.0        0.0        0.0      0.2      0.0     0.0      0.0             4.3
                 K5396       BHKF         1      FL-81          24.6          4.3         1.4         13.3       28.2      25.5         0.0      1.4      0.0     7.1      8.8             6.9





                                                                         MUSSEL WATCH YEAR VI - Bivalve Aromatics Data





                                                                  C3-                                Ci-         C2-        C3-         C4-     DBT      Cl-     C2-      C3-
                 FILE        SITE      REP LOCATION FLUOR              PHENAN ANTHRAC PHEN + PHEN + PHEN + PHEN +                                       DBT      DBT    DBT FLUORANTH
                                                 # AND                                          ANTHRA     ANTHRA      ANTHRA     ANTHRA
                                                 STATE          (ppb)     (ppb)+      (ppb)+        (ppb)      (ppb)       (ppb)      (ppb)    (ppb)   (ppb)    (ppb)   (ppb)     (ppb)+


                 K5397      BHKF         2       FL-81           32.3        4.6         0.8        15.7        30.3       25.6        12.5      0.9     0.0      0.0     7.8            8.3
                 K5398      BHKF         3       FL-81           34.2        4.2          1.2        11.8       31.3       23.1        14.6      1.2     0.0      5.6     7.9            7.4

















         ND





                                                                           MUSSEL WATCH YEAR VI - Bivalve Aromatics Data





                                                                                    Ci-                                 Ci-      C2-       C3-      C4-
                 FILE         SITE      REP LOCATION PYRENE                FLUORANTH         BENZ(a)  CHRYSENE CHRYS CHRYS CHRYS CHRYS                       BENZO(b)       BENZO(k)     BENZO(e)
                                                   # AND                    +PYRENES       ANTHRAC                                                       FLUORANTH       FLUORANTH        PYRENE
                                                   STATE          (ppb)+            (ppb)      (ppb)+        (ppb)+     (ppb)    (ppb)    (ppb)    (ppb)          (ppb)           (ppb)    (ppb)+


                 K5135        LMSB         I       Tx- 1             7.3            14.9          1.0           4.3     0.0      0.0       0.0      0.0            0.8             1.4           0.7
                 K5136        LMSB         2       Tx- 1             5.5            4.7           0.7           3.8     0.0      0.0       0.0      0.0            1.6             0.7           0.7
                 K5137        LMSB         3       Tx- 1             3.7            6.3           0.4           2.4     0.0      0.0       0.0      0.0            0.7             0.3           1.2
                 K5087        CCIC         I       TX-3            29.6             14.5          5.3         23.1      0.0      0.0       0.0      0.0            6.4             4.5           6.8
                 K5088        CCIC         2       TX-3            25.6             14.5          3.6         22.5      0.0      0.0       0.0      0.0            5.0             3.5           6.7
                 K5089        CCIC         3       TX-3            27.9             15.2          3.9         24.1      5.1      0.0       0.0      0.0            8.4             2.3           5.5
                 K5147        ABLR         I       TX-4              0.8            0.0           0.6           0.6     0.0      0.0       0.0      0.0            0.5             0.2           0.4
                 K5148        ABLR         2       TX-4              0.8            0.0           0.2           0.7     0.0      0.0       0.0      0.0            0.6             0.3           0.2
                 K5149        ABLR         3       TX-4              1.3            0.0           0.6           0.4     0.0      0.0       0.0      0.0            0.3             0.1           0.4
                 K5141        CBCR         1       TX-5              0.9            0.0           0.7           0.5     0.0      0.0       0.0      0.0            0.6             0.4           0.5
                 K5142        CBCR         2       TX-5              1.0            0.0           0.4           0.5     0.0      0.0       0.0      0.0            0.5             0.1           0.4
                 K5143        CBCR         3       TX-5              1.6            0.0           0.3           0.7     0.0      0.0       0.0      0.0            0.5             0.2           0.2
                 K5099        MBAR         I       TX-6              0.8            0.0           0.4           0.7     0.0      0.0       0.0      0.0            0.4             0.3           0.4
                 K5100        MBAR         2       TX-6              1.2            0.0           0.5           0.7     0.0      0.0       0.0      0.0            0.8             0.4           0.4
                 K5101        MBAR         3       TX-6              1.1            0.0           0.6           1.0     0.0      0.0       0.0      0.0            0.7             0.2           0.6
         b D     K5111        SAPP         I       TX-7              0.6            0.0           0.6           0.r.    0.0      0.0       0.0      0.0            0.2             0.1           0.5
         hL,     K5112        SAPP         2       TX-7              0.8            0.0           0.3           0.6     0.0      0.0       0.0      0.0            0.4             0.1           0.5
                 K5113        SAPP         3       TX-7              0.9            0.0           0.3           0.6     0.0      0.0       0.0      0.0            0.2             0.2           0.3
                 K5117        SAMP         1       TX-8              1.6            0.0           1.3           2.0     2.8      0.0       0.0      0.0            1.0             0.8           1.0
                 K5118        SAMP         2       TX-8              1.8            7.2           1.1           2.9     3.8      0.0       0.0      0.0            1.4             0.4           0.8
                 K5119        SAMP         3       TX-8              1.7            0.0           1.0           1.2     0.0      0.0       0.0      0.0            0.4             0.3           0.4
                 K5105        ESSP         1       TX-9              3.2            0.0           1.3           1.6     0.0      0.0       0.0      0.0            1.3             0.4           1.0
                 K5106        ESSP         2       TX-9              3.4            0.0           0.8           2.1     0.0      0.0       0.0      0.0            1.9             0.8           1.1
                 K5107        ESSP         3       TX-9              5.0            0.0           0.8           2.2     0.0      0.0       0.0      0.0            1.1             0.6           0.6
                 K5129        MBGP         I       TX-12             7.0            12.4          4.7           8.5     0.0      0.0       0.0      0.0            4.4             5.3           4.1
                 K5130        MBGP         2       TX-12             7.0            13.7          4.2           7.0     0.0      0.0       0.0      0.0            6.1             3.6           3.5
                 K5131        MBGP         3       TX-12             6.7            16.1          2.7           5.2     0.0      0.0       0.0      0.0            6.3             2.6           2.5
                 K5123        MBLR         1       7,X- 11         19.3             1011          6.3         13.0      5.7      0.0       0.0      0.0            9.8             12.1         10.1
                 K5124        MBLR         2       TX-11           25.3             mi            7.6         15.0      8.5      0.0       0.0      0.0            14.0            10.6          9.8
                 K5125        MBLR         3       TX-11           15.4             16.0          4.7         10.2      5.3      0.0       0.0      0.0            17.5            10.1          6.6
                 K5081        MBTP         1       TX-13             0.9            0.0           0.5           0.8     0.0      0.0       0.0      0.0            0.6             0.6           0.4
                 K5082        MBTP         2       TX-13             0.7            0.0           0.6           0.7     0.0      0.0       0.0      0.0            0.6             0.3           0.5
                 K5083        MBTP         3       TX- 13            1.4            0.0           0.4           1.2     0.0      0.0       0.0      0.0            0.4             0.2           0.3
                 K5075        MBEM         I       TX-14             2.9            8.7           1.4           3.6     0.0      010       0.0      0.0            1.6             0.4           2.3
                 K5076        MBEM         2       TX-14             2.6            0.0           0.8           1.6     0.0      0.0       0.0      0.0            0.7             0.2           0.8
                 K5077        MBEM         3       TX-14             2.8            0.0           0.4           2.4     0.0      0.0       0.0      0.0            0.9             0.5           0.4
                 K5015        BRCL         1       TX-72           13.9             17.3          2.3           7.8     0.0      0.0       0.0      0.0            3.3             2.1           3.2
                 K5016        BRCL         2       TX-72           18.1             14.0         17.4         13.7      0.0      0.0       0.0      0.0            4.5             3.0           2.7





                                                                          MUSSEL WATCH YEAR VI - Bivalve Aromatics Data





                                                                                   Ci-                                 Cl-      C2-      C3-      C4-
                 171LE        SITE      REP LOCATION PYRENE FLUORANTH                       BENZ(a)  CHRYSENE CHRYS CHRYS CHRYS CHRYS                      BENZO(b)        BENZON      BENZO(e)
                                                  # AND                    +PYRENES       ANTHRAC                                                       FLUORANTH      FLUORANTH        PYRENE
                                                  STATE          (Ppb)+            (ppb)      (ppb)+        (ppb)+     (ppb)    (ppb)    (ppb)    (ppb)         (ppb)           (ppb)    (ppb)+



                 K5017       BRCL         3       TX-72           16.1             23.7          4.0          9.3      5.1      5.7      4.1      12.7            3.6            2.8          2.6
                 K5021       BRFS         1       TX-57          378.0             168.3      151.2          187.4     0.0      10.9     0.0      0.0           86.6            52.1         57.2
                 K5022       BRFS         2       TX-57          127.7             52.8        27.3          68.0      0.0      0.0      0.0      0.0           11.3             7.2          9.7
                 K5023       BRFS         3       TX-57          133.0             69.8        29.2          59.5      11.7     6.6      0.0      0.0           18.9            14.7         14.4
                 K5009       GBCR         1       TX-18           63.2             46.0        10.6          25.9      5.0      7.2      0.0      0.0             6.8            6.6          4.9
                 K5010       GBCR         2       TX-18           61.7             35.3        13.4          38.3      9.9      7.4      0.0      0.0             8.9            3.6          5.7
                 K5011       GBCR         3       Tx- 18          71.5             43.0        14.2          38.9      0.0      0.0      0.0      0.0             6.4           15.6          9.0
                 K5003       GBOB         I       TX-58          106.7             65.6        26.2          66.5      12.5     11.3     0.0      0.0           38.2            14.3         28.3
                 K5004       GBOB         2       TX-58           61.1             45.3        16.8          54.4      22.3     15.3     0.0      0.0           24.0            13.7         20.4
                 K5005       GBOB         3       TX-58           43.8             37.2          9.8         39.8      10.0     0.0      0.0      0.0           12.1            20.7         16.2
                 K5057       GI3TD        I       TX-16           15.4             37.5          2.4         13.8      27.1     42.1     19.8     10.4            4.4            3.5          4.8
                 K5058       GI3TD        2       TX-16           13.6             52.1          3.1         11.9      31.9     52.3     29.3     17.0            3.4            4.1          4.8
                 K5059       GBTD         3       TX- 16          28.6             144.0         6.2         23.9      96.9     173.7    121.2    44.1            7.4           10.2         12.3
                 K5063       GBYC         1       TX-15           16.5             27.7          3.5         14.8      16.3     22.9     0.0      39.5            7.1            1.0          8.7
                 K5064       GBYC         2       TX-15           17.8             32.0          2.8         14.4      13.7     20.2     0.0      0.0             4.7            3.1          8.0
         t-0     K5065       GBYC         3       Tx- 15          20.6             17.6          32          15.6      13.8     14.1     0.0      0.0             3.3            3.6          7.4
         r-n     K5384       GBSC         1       TX-59          1672.4         6716.5        269.9         729.5   2265.2   2071.0      540.9    168.4         134.4           130.2       263A
                 K5385       GBSC         2       TX-59          1367.0         5527.4        416.5        1090.0   2916.6   2668.8      701.5    211.4         383.3           103.8       446.3
                 K5386       GBSC         3       TX-59          1803.3         7070.1        395.5         933.8   2737.8   2798.2   1118.5      246.0         266.3           160.9       512.6
                 K5039       G13HR        I       TX-17            7.9             9.8           1.7          4.5      5.2      10.5     0.0      0.0             2.4            0.7          2.2
                 K5040       GBHR         2       TX-17            6.8             9.0           9.3          7.6      7.8      11.7     0.0      0.0             1.9            0.9          2.8
                 K5041       GBHR         3       TX-17            7.8             13.1          1.6          4.6      6.1      6.6      0.0      0.0             2.5            1.6          2.1
                 K5027       SLBB         1       Tx- 19          31.6             48.4          5.7         16.5      20.3     22.0     0.0      51.9            5.9            1.6          8.4
                 K5028       SLBB         2       TX-19           57.8             76.7          7.5         24.2      37.8     38.9     0.0      0.0             6.2            3.4         13.3
                 K5029       SLBB         3       TX-19           18.8             38.6          3.0         11.9      14.7     19.0     9.7      8.9             3.0            2.0          4.4
                 K5033       CLSIJ        1       IA-20           16.4             29.7          1.9          6.8      4.5      5.5      0.0      34.1            1.6            0.6          1.6
                 K5034       CL&I         2       LA-20           18.2             22.5          3.1         11.3      3.1      4.0      0.0      0.0             3.1            0.4          1.9
                 K5035       CL&J         3       LA-20           14.3             29.7          1.9          4.5      3.2      5.2      0.0      0.0             2.0            0.8          1.4
                 K5045       CLLC         1       IA-60           95.4             88.2        10.5          36.3      32.5     28.3     10.6     0.0             8.8            2.2         12.7
                 K5046       CLLC         2       LA-60           59.3             50.2          5.8         22.8      19.7     24.5     11.9     0.0             4.2            3.0          7.2
                 K5047       CLLC         3       LA-60           96.4             94.2          9.0         31.1      30.3     16.6     8.0      0.0             8.3            2.7          9.7
                 K5069       JHJH         1       LA-21           13.5             13.9          2.6          5.4      3.6      8.4      0.0      0.0             1.9            0.5          2.0
                 K5070       JHJH         2       IA-21           11.4             15.1          1.7          4.0      3.6      8.1      0.0      0.0             2.0            0.9          1.3
                 K5071       JHJH         3       LA-21            8.9             6.9           1.4          3.3      3.0      0.0      0.0      8.3             1.7            0.6          0.9
                 K5159       VBSP         I       LA-22            7.7             7.1           1.2          2.7      0.0      0.0      0.0      0.0             0.6            0.6          1.5
                 K5160       VBSP         2       LA-22            6.8             11.6          0.9          2.9      0.0      0.b      0.0      0.0             2.1            0.9          1.5
                 K5161       VBSP         3       LA-22            7.3             1.7           0.8          2.4      2.6      9.0      3.6      0.0             0.9            0.7          1.3
                 K5189       ABOB         1       LA-24            3.0             0.0           0.7          2.2      0.0      0.0      0.0      0.0             1.3            0.2          0.9





                                                                           MUSSEL WATCH YEAR VI - Bivalve Aromatics Data





                                                                                    ci-                                 Ci-      C2-       C3-      C4-
                 FILE        S17B       REP LOCATION PYRENE                FLUORANTH         BENZ(a)  CHRYSENE CHRYS CHRYS CHRYS CHRYS                       BENZO(b)        BENZO(k)    BENZO(e)
                                                  # AND                     +PYRENES       ANTHRAC                                                       FLUORANTH       FLUORANTH        PYRENE
                                                  STATE           (ppb)+            (ppb)      (ppb)+        (ppb)+     (ppb)    (ppb)   (ppb)    (ppb)           (ppb)           (ppb)    (ppb)+


                 K5190       ABOB         2       LA-24             2.6             3.6           0.5           1.3     0.0      0.0       0.0      0.0            0.7             0.3           0.8
                 K5191       ABOB         3       LA-24             2.5             3.5           0.5           1.3     0.0      0.0       0.0      0.0            0.4             0.3           0.5
                 K5195       CLCL         1       LA-25             3.5             0.0           1.1           3.2     0.0      0.0       0.0      0.0            2.1             0.8           019
                 K5196       CLCL         2       LA-25             3.6             0.0           0.5           1.5     0.0      0.0       0.0      0.0            1.3             0.6           0.7
                 K5197       CLCL         3       IA-25             3.5             0.0           0.6           1.6     0.0      0.0       0.0      0.0            0.6             0.5           0.7
                 K5165       TBLB         I       IA-26             3.7             5.7           1.2           2.4     0.0      0.0       0.0      0.0            1.4             018           0.7
                 K5166       TBLB         2       LA-26             8.3             13.0          2.2           3.1     0.0      0.0       0.0      0.0            2.9             1.3           1.1
                 K5167       TBLI3        3       LA-26             4.5             9.7           1.7           4.0     0.0      0.0       0.0      0.0            2.5             1.2           1.5
                 K5183       TBLF         I       LA-27             3.9             7.8           018           2.1     4.1      5.8       5.0      3.5            0.5             0.5           0.7
                 K5184       TBLF         2       LA-27             3.7             9.7           0.7           2.4     7.0      0.0       0.0      0.0            1.3             0.3           1.1
                 K5185       TBLF         3       LA-27             3.2             7.7           0.6           1.6     4.8      4.8       0.0      0.0            0.3             0.4           0.7
                 K5168       BBSD         I       LA-28             4.5             0.0           0.6           3.0     0.0      0.0       0.0      0.0            0.9             0.5           0.5
                 K5169       BBSD         2       LA-28             3.5             11.5          1.1           2.2     0.0      0.0       0.0      0.0            1.9             0.8           0.8
                 K5170       BBSD         3       LA-28             4.9             11.6          1.4           2.6     2.4      7.5       5.9      6.8            1.6             0.9           1.0
                 K5174       BBMB         1       LA-29           132.0             118.1       91.1         129.2      35.6     16.8      0.0      0.0           41.5            20.5         23.6
                 K5175       BBMB         2       LA-29           138.9             134.7       63.2         100.4      23.9     9.0       0.0      0.0           26.0            14.7         16.5
                 K5176       BBMB         3       LA-29           151.8             130.7       56.3          90.2      23.2     10.1      0.0      0.0           25.1            16.5         15.7
                 K5210       MRTP         I       LA-65            51.8             57.7          8.2         17.7      13.5     15.4      0.0      0.0            3.9             4.5           6.4
                 K5211       MRTP         2       LA-65            22.8             34.6          5.8         15.2      12.1     14.9      0.0      0.0            3.9             3.5           5.5
                 K5212       MRTP         3       LA-65            27.7             32.1          5.7         13.1      12.4     10.2      4.1      0.0            3.7             2.5           5.3
                 K5216       BSSI         1       LA-31            50.5             55.7          7.7         21.3      17.0     16.8      0.0      0.0            5.8             3.2           6.0
                 K5217       BSSI         2       LA-31            34.7             42.4          6.3         22.2      16.6     16.5      0.0      0.0            5.6             1.7           6.6
                 K5218       BSSI         3       LA-31            37.8             49.0          5.6         13.0      17.7     13.5      0.0      0.0            3.4             3.7           5.2
                 K5201       BSBG         1       IA-30             3.1             13.6          0.8           2.4     6.0      0.0       0.0      0.0            1.8             0.5           0.8
                 K5202       BSBG         2       LA-30             3.2             0.0           0.9           3.7     5.8      0.0       0.0      0.0            1.0             1.0           0.9
                 K5203       BSBG         3       LA-30             2.4             3.9           0.4           2.1     3.3      0.0       0.0      0.0            0.5             0.6           0.7
                 K5207       LBMP         I       LA-32            11.9             10.5          2.8           4.5     2.8      0.0       0.0      0.0            4.8             1.4           1.5
                 K5208       LBMP         2       LA-32             8.8             9.0           2.2           5.0     4.5      0.0       0.0      0.0            2.5             1.0           2.3
                 K5209       LBMP         3       LA-32             8.2             7.1           1.8           3.5     2.4      0.0       0.0      0.0            1.3             1.4           1.1
                 K5249       LPGO         1       LA-63          1333.2          1457.2        395.9         552.6     250.4     186.0   58.1     44.4           226.8           232.1        206.5
                 K5250       LPGO         2       LA-63          1311.2          1118.8        457.9         698.4     357.3     192.2   56.3     41.8           377.5           243.5        263.8
                 K5251       LPGO         3       LA-63          1930.0          1922.5        443.6         780.3     358.6     178.7   27.9     42.9           430.6           202.8        345.9
                 K5222       MSPC         1       MS-33            67.5             57.3        23.5          46.7      17.8     11.9      0.0      0.0           15.2             8.1         13.9
                 K5223       MSPC         2       MS-33            41.9             35.0        12.7          31.2      8.3      0.0       0.0      0.0            6.9             7.3           8.4
                 K5224       mspc         3       MS-33            33.4             28.6        10.9          24.7      8.5      5.7       0.0      0.0            4.8             6.1           6.7
                 K5228       MSBB         1       MS-34           139.1             150.4       30.9          57.1      33.8     25.4      0.0      0.0           16.7             9.1         18.0
                 K5229       MSBB         2       MS-34           203.5             280.8       49.9         110.9      74.9     39.6      0.0      0.0           25.5            20.7         37.0
                 K5230       MSBB         3       MS-34            85.1             104.5       18.4          42.0      28.4     13.7      0.0      0.0           17.3            26.7         11.9






                                                                         MUSSEL WATCH YEAR VI - Bivalve Aromatics Data





                                                                                   ci-                                ci-      C2-      C3-      C4-
                 FILE        SITE      REP LOCA71ON PYRENE FLUORANTH                       BENZ(a)  CHRYSENE CHRYS CHRYS CHRYS CHRYS                      BENZO(b)       BENZO(k)    BENZO(e)
                                                 # AND                     +PYRENES      ANTHRAC                                                      FLUORANTH       FLUORANTH      PYRENE
                                                 STATE          (ppb)+             (ppb)     (ppb)+        (ppb)+     (ppb)    (ppb)    (ppb)    (ppb)         (ppb)          (ppb)     (ppb)+


                 K5246       MSPB         I      MS-35            39.3             37.2         8.6         30.7      0.0      0.0      0.0      0.0            5.7             2.7          6.2
                 K5247       MSPB         2      MS-35            30.4             21.7         9.7         23.9      12.4     0.0      0.0      0.0            5.0             7.2          6.8
                 K5248       NISPB        3      MS-35            29.2             27.9         6.7         18.0      10.9     7.7      0.0      0.0            4.2             3.6          4.3
                 K5234       NIBCP        1      AL-36            74.8             43.0       13.2          23.7      0.0      0.0      0.0      0.0            6.2             3.1          7.9
                 K5235       MBCP         2      AL-36            43.4             23.9         8..3        20.1      0.0      8.3      0.0      0.0            2.7             6.5          5.3
                 K5236       MBCP         3      AL-36            34.0             21.1         5.8         16.6      0.0      5.0      0.0      0.0            2.4             2.9          4.0
                 K5240       MBHI         1      AL-66          164.4              86.2       69.5          56.6      36.7     21.6     0.0      0.0           19.8             5.1          19.3
                 K5241       MBHI         2      AL-66          146.0              81.8       24.3          56.2      17.9     16.4     0.0      0.0            9.5           18.9           20.1
                 K5242       MBHI         3      AL-66          119.3              64.5       18.1          42.4      14.8     7.8      0.0      0.0            9.5             8.7          13.3
                 K5261       PBPH         I      FL-67          317.0              183.7      68.7          92.6      20.4     18.0     0.0      0.0           23.1           24.5           18.7
                 K5262  ,    PBPH         2      FL-67          468.2              276.5      120.4        180.5      32.4     17.6     0.0      0.0           63.3           34.3           38.4
                 K5263       PBPH         3      FL-67          368.7              213.6      64.8         129.2      25.3     18.4     0.0      0.0           35.5           10.7           24.7
                 K5255       PBIB         1      FL-37            17.0             18.4         4.5          8.3      4.9      36.9     0.0      0.0            2.4             3.7          2.4
                 K5256       PBIB         2      FL-37            28.4             25.5         9.0         14.1      8.2      10.9     0.0      0.0            9.9             4.1          4.4
                 K5257       PBIB         3      FL-37            22.7             26.4         5.5          9.5      7.4      22.1     0.0      0.0            3.4             5.5          4.0
                 K52657      CBJB         I      FL-73          172.8              128.3      53.0         105.4      26.7     11.7     010      0.0           34.1           38.1           25.8
                 K5268       CBJB         2      FL-73          198.1              160.0      70.6         143.3      30.1     16.1     0.0      0.0           83.6           37.1           38.6
                 K5269       CEkJB        3      FL-73          206.3              143.6      47.9         134.7      28.5     13.7     6.5      0.0           72.7           19.3           32.0
                 K5273       CBSR         I      FL-38             7.6             11.2         1.6          4.9      3.1      10.8     0.0      0.0            1.0             1.7          1.2
                 K5274       CBSR         2      FL-38             8.0             12.7         1.7          6.0      4.7      7.8      0.0      0.0            2.1             1.3          1.4
                 K5275       CBSR         3      FL-38             7.2             10.0         1.5          6.1      4.3      4.5      0.0      0.0            1.8             1.5          1.7
                 K5279       CBSP         I      FL-39            66.7             91.0       30.2          67.4      89.8     86.1     31.0     18.2          15.2           33.4           29.7
                 K5280       CBSP         2      FL-39            40.3             71.2       19.2          44.2      82.4     82.1     40.8     15.9          14.5           10.4           24.3
                 K5281       CBSP         3      FL-39            74.6             95.8       26.7          72.0      87.3     86.6     36.2     16.7          26.5           20.2           33.7
                 K5303       PCLO         I      FL-74            23.9             24.5         4.4         19.2      6.6      16.3     010      0.0            5.9             6.3          6.3
                 K5304       PCLO         2      FL-74            80.0             75.4       15.5          40.8      12.9     11.9     0.0      0.0            4.1           24.1           11.0
                 K5305       PCLO         3      FL,74            22.3             19.7         3.9         14.0      4.7      8.8      010      0.0            4.5             0.9          3.5
                 K5297       SAWB         1      FL-40          408.5              551.8      93.9         202.9      79.0     49.3     14.6     9.1           47.7           58.2           43.2
                 K5298       SAVVB        2      FL-40          641.5              833.9      156.4        368.4      143.3    70.5     30.4     25.3          145.2          29.7           69.9
                 K5299       SAVYrB       3      FL-40          651.7              749.6      113.3        319.4      107.7    63.2     25.2     0.0           126.0          28.3           62.5
                 K5291       APDB         1      FL-41            11.4             19.4         2.1          6.0      4.2      16.3     0.0      0.0            1.1             2.0          1.8
                 K5292       APDB         2      FL-41            11.9             14.8         1.6          6.9      4.1      7.1      0.0      0.0            2.5             0.7          1.7
                 K5293       APDB         3      FL-41            11.4             12.0         1.6          7.2      4.0      7.8      0.0      0.0            2.2             0.9          1.8
                 K5285       APCP         I      FL-42            53.9             70.6       11.4          24.4      15.3     10.2     0.0      0.0            9.1             9.9          8.0
                 K5286       APCP         2      FL-42            68.6             M.7        13.3          28.2      18.0     10.2     0@0      0.0            5.2             5.4          8.7
                 K5287       APCP         3      FL-42            86.2             101.0      11.9          28.3      14.0     9.1      010      0.0           14.9             7.0          9.8
                 K5321       AESP         I      FL-75             6.9             14.0         1.1          3.5      0.0      0.0      0.0      0.0            1.1             0.4          0.7
                 K5322       AESP         2      FL-75             6.6             9.0          1.2          3.8      0.0      0.0      0.0      0.0            4.3             1.6          0.8





                                                                          MUSSEL WATCH YEAR VI - Bivalve Aromatics Data





                                                                                   Ci-                                 Ci-      C2-      C3-      C4-
                 FILE         ME        REP LOCAMON PYRENE FLUORANTH                        BEN4a)   CHRYSENE CHRYS CHRYS CHRYS CHRYS                      BENZO(b)        BENZO(k)    BENZO(e)
                                                  # AND                    +PYRENES       ANTHRAC                                                       FLUORANTH      FLUORANTH        PYRENE
                                                  SrATE          (ppb)+            (ppb)      (ppb)+        (ppb)+     (ppb)    (ppb)   (ppb)     (ppb)         (ppb)           (ppb)    (ppb)+



                 K5323        AESP        3       FL-75            8.8             12.7          1.2          4.1      0.0      0.0      0.0      0.0             1.6            1.3          0.9
                 K5315        CKBP        1       FL-43            2.5             0.0           0.3          1.2      0.0      0.0      0.0      0.0             0.6            0.4          0.2
                 K5316        CKBP        2       FL-43            2.2             0.0           0.6          1.6      0.0      0.0      0.0      0.0             0.4            0.5          0.5
                 K5317        CKBP        3       FL-43            3.1             0.0           0.5          1.6      0.0      0.0      0.0      0.0             0.7            0.4          0.6
                 K5353        TBNP        1       FL-76           95.1             69.1          9.9         46.6      15.0     12.9     7.3      10.4          15.2            10.6         15.4
                 K5351        TBNP        2       FL-76           91.7             57.7          9.7         42.4      11.9     11.8     0.0      0.0           10.2             8.4         11.8
                 K5352        TBNP        3       FL-76           97.6             65.2        11.7          44.1      10.1     11.8     4.7      9.9           14.0             6.0         12.1
                 K5333        TBMK        1       FL-47            9.7             9.2           1.8          7.3      3.4      7.8      0.0      0.0             2.0            1.6          1.4
                 K5334        TBMK        2       FL-47           29.1             24.4          5.5         19.7      7.1      16.7     0.0      0.0             7.0            2.4          5.0
                 K5335        TBMK        3       FL-47           34.9             24.0          7.0         21.4      4.9      12.6     0.0      0.0             6.4            4.2          5.3
                 K5327        TBPB        1       FL-44           20.5             14.8          2.7         18.6      5.2      9.4      0.0      0.0             5.5            4.4          4.7
                 K5328        TBPB        2       FL-44           34.4             24.3          4.6         29.4      6.0      7.5      0.0      0.0           13.7             3.4          7.2
                 K5329        TBPB        3       FL-44           23.8             17.9          3.6         19.7      3.8      6.8      4.9      0.0             6.5            7.4          5,3
                 K5339        TBOT        1       FL,70           18.7             19.9          3.5         10.4      5.3      7.8      0.0      0.0             4.4            6.0          4.3
                 K5340        TBOT        2       FL-70           32.0             24.3          7.1         16.0      9.7      7.8      0.0      0.0             5.8           11.4          6.5
                 K5341        TBOT        3       FL-70           28.9             22.7          6.4         17.1      9.8      11.4     0.0      0.0           11.1             9.9          8.4
         00      K5309        TBKA        I       FL-77          130.1             97.5        14.4          43.9      18.9     20.4     7.0      23.2          17.3            16.8         19.3
                 K5310        TBKA        2       FL-77          128.0             93.3        19.9          46.0      21.4     21.0     8.6      19.0          15.9            21.9         18.6
                 K5311        TBKA        3       FL-77          275.0             178.7       36.5          105.4     33.3     40.9     22.0     32.3          50.0            40.0         47.1
                 K5345        TBCB        1       FL-46            7.7             010           1.1          3.9      2.4      0.0      0.0      0.0             1.0            1.5          1.1
                 K5347        TBCB        2       FL-46            9.4             9.9           1.9          5.8      2.6      6.7      0.0      0.0             1.8            1.0          1.5
                 K5346        TBCB        3       FL-46           13.6             13.1          1.3          6.5      4.7      10.5     0.0      0.0             1.6            0.7          1.6
                 K5369        CBBI        1       FL-48           10.6             13.9          1.2          4.5      0.0      0.0      0.0      0.0             1.3            1.2          1.4
                 K5370        CBBI        2       FL-48            9.4             9.2           1.0          4.5      0.0      0.0      0.0      0.0             1.2            1.3          1.1
                 K5371        CBBI        3       FL-48            8.3             9.4           1.0          3.5      2.2      6.0      0.0      0.0             1.1            0.7          1.2
                 K5363        CBFM        1       FL-71           23.3             19.0          4.4         14.8      4.7      9.3      0.0      0.0           12.9            13.3          5.7
                 K5364        CBFM        2       FL-71           27.2             22.1          3.5         15.4      5.5      9.9      0.0      0.0             6.4            7.7          6.0
                 K5365        CBFM        3       FL-71           31.8             29.1          5.0         17.6      7.7      10.8     0.0      0.0             7.1           12.1          8.2
                 K5357        NBNB        I       FL-49           85.4             86.9        14.6          40.0      16.0     10.4     0.0      0.0           12.9            11.1         16.7
                 K5358        NBNB        2       FL-49           74.6             86.9        15.2          39.5      19.6     12.5     2.7      9.5           22.7             5.4         15.5
                 K5359        NBNB        3       FL-49           85.6             92.4        17.6          43.4      12.2     10.0     5.0      10.3          14.1            14.5         18.9
                 K5381        RBHC        1       FL-50            9.0             13.3          1.6          3.9      2.7      6.8      0.0      0.0             1.1            1.4          1.4
                 K5382        RBHC        2       FL-50           14.2             18.2          2.1          5.2      3.1      14.2     0.0      0.0             2.4            1.4          2.2
                 K5383        RBHC        3       FL-50           13.2             18.7          2.4          5.5      3.1      12.0     0.0      0.0             1.9            1.6          2.2
                 K5375        EVFU        1       FL-51            5.2             9.2           1.2          2.2      2.4      11.8     0.0      0.0             0.6            0.7          1.1
                 K5376        EVFU        2       FL-51            5.0             8.3           1.0          2.1      4.8      4.9      0.0      0.0             0.7            0.7          0.9
                 K5377        EVFU        3       FL-51            5.7             10.3          1.1          1.8      1.7      5.8      0io      0.0             1.1            0.5          0.9
                 K5396        BHKF        1       FL-81            7.8             15.7          2.4          5.4      0.0      0.0      0.0      0.0             1.6            1.4          3.1





                                                                         MUSSEL WATCH YEAR VI - Bivalve Aromatics Data





                                                                                  ci-                                 Ci-      C2-      C3-     C4-
                FILE         SITE      REP LOCATION PYRENE FLUORANTH                     BENZ(a) CHRYSENE CHRYS CHRYS CHRYS CHRYS                        BENZO(b)      BENZO(k) BENZO(e)
                                                 # AND                    +PYRENES      ANTHRAC                                                     FLUORANTH FLUORANTH PYRENE
                                                 STATE         (ppb)+            (ppb)       (ppb)+      (ppb)+     (ppb)    (ppb)    (ppb)    (ppb)          (ppb)          (ppb)    (ppb)+


                K5397       BHKF        2        FL-81            8.3             14.1          2.4         5.6       0.0      0.0      0.0      0.0            1.6            1.9          2.3
                K5398       BHKF        3        FL-81            8.2             14.1          2.5          4.7      0.0      0.0      0.0      0.0            1.4            1.1          2.1





                                                                                MUSSEL WATCH YEAR V1 - Bivalve Aromatics Data





                                                                                                                                                                                                        2,3,4-TRI
                  FILE          SITE      REP LOCATION BENZO(a)                    PERYLENE            INDENO-           DIBENZ        BENZO(ghl)         2-METHYL        1-METHYL        2,6 DIME      METHYL-
                                                      # AND          PYRENE                             PYRENE         ANTHRAC         PERYLENE                NAPH            NAPH            NAPH        NAPH
                                                      STATE             (ppb)+           (ppb)+             (ppb)           (ppb)+             (ppb)           (ppb)+          (ppb)+          (ppb)+      (ppb)


                  K5135         LMSB          1       TX-1                 0.9              0.9               0.5              0.4              0.5               7.4             5.3            3.1             1.5
                  K5136         LMSB          2       TX-i                 0.4              0.6               0.2              0.3              0.3               4.0             4.4            3.9             1.5
                  K5137         LMSB          3       TX-1                 0.5              1.1               0.9              0.7              0.3               2.7             1.8            1.8             1.1
                  K5087         CCIC          1       TX-3                 0.7              0.5               1.3              0.4              1.1               3.7             3.3            3.5             4.4
                  K5088         CCIC          2       TX-3                 1.4              0.6               0.7              0.2              0.8               6.9             5.7            5.6             5.9
                  K5089         CCIC          3       TX-3                 0.7              0.4               1.5              0.6              1.7               4.7             2.5            4.0             4.5
                  K5147         ABLR          1       TX-4                 0.1              0.3               0.1              0.1              0.1               4.4             2.5            2.2             0.3
                  K5148         A13LR         2       TX-4                 0.2              0.4               0.2              0.1              0.2               3.2             1.9            2.1             1.5
                  K5149         ABLR          3       TX-4                 0.2              0.7               0.6              0.2              0.7               3.0             3.2            3.9             0.8
                  K5141         CBCR          1       TX-5                 0.2              0.4               0.5              0.2              0,6               3.2             2.4            2.3             0.8
                  K5142         CBCR          2       TX-5                 0.4              0.3               0.3              0.2              0.1               3.3             1.8            2.2             1.1
                  K5143         C13CR         3       TX-5                 0.3              0.7               0.2              0.3              0.4               3.8             2.6            3.5             1.8
                  K5099         M13AR         I       TX-6                 0.2              0.3               0.4              0.4              0.5               1.9             2.0            1.5             1.1
                  K5100         MOAR          2       TX-6                 0.5              0.7               0.2              0.1              0.4               1.6             2.1            1.8             1.5
                  K5101         MBAR          3       TX-6                 0.2              0.5               0.6              0.5              0.2               1.6             1.0            3.6             0.8
                  K5111         SAPP          I       TX-7                 0.3              0.2               0.3              0.2              0.2               6.1             3.1            3.6             1.0
                  K5112         SAPP          2       TX-7                 0.3              0.6               0.2              0.2              0.3               5.7             2.6            2.5             3.1
                  K5113         SAPP          3       TX-7                 0.4              0.2               0.3              0.2              0.1               3.5             2.7            3.4             1.0
                  K5117         SAMP          1       TX-8                 0.5              1.5               0.6              0.2              0.7               3.4             2.6            2.3             2.0
                  K5118         SAMP          2       TX-8                 0.6              1.3               0.2              0.2              0.4               4.3             3.9            2.6             1.8
                  K5119         SAMP          3       TX-8                 0.2              0.6               0.5              0.3              0.5               2.9             1.5            2.0             3.1
                  K5105         ESSP          1       TX-9                 0.4              0.9               0.4              0.2              0.9               4.2             3.8            5.1             4.7
                  K5106         ESSP          2       TX-9                 0.6              1.1               0.5              0.3              0.5               8.1             5.4            5.1             5.8
                  K5107         ESSP          3       TX-9                 0.2              -0.7              0.5              0.6              0.9               3.6             3.2            7.6             7.9
                  K5129         MBGP          1       TX-12                2.0              7.7               2.7              1.2              2.6               4.0             3.1            2.6             2.8
                  K5130         MBGP          2       TX-12                2.2              7.9               1.8              0.3              1.2               [email protected]            2.8            2.2             2.6
                  K5131         MBGP          3       'IX- 12              1.7              10.1              2.1              0.6              2.1               1.9             2.9            1.9             2.5
                  K5123         MBLR          I       TX-11                2.9              5.4               4.2              1.2              3.9               2.7             2.5            2.1             2.3
                  K5124         MBLR          2       TX-11                6.6              5.9               6.4              1.0              4.5               8.4             3.8            7.5             7.4
                  K5125         MBLR          3       IX-11                2.5              3.6               3.5              0.8              3.6               4.2             119            4.5             o.5
                  K5081         MBTP          I       TX-13                0.4              0.5               0.2              0.2              0.2               2.2             1.6            2.8             1.1
                  K5082         M13TP         2       TX-13                0.3              0.4               0.4              0.3              0.2               2.3             3.7            3.1             3.9
                  K5083         MBTP          3       TX-13                0.1              0.4               0.2              0.2              0.2               2.6             2.3            2.2             1.4
                  K5075         MBEM          1       TX-14                0.3              0.5               0.8              0.6              1.0               3.2             4.3            3.9             2.2
                  K5076         MBEM          2       TX-14                0.9              0.6               0.6              0.6              0.4               3.7             4.8            3.2             1.1
                  K5077         MBEM          3       TX-14                0.3              0.5               0.5              0.4              0.5               3.1             2.0            3.0             2.3
                  K5015         BRCL          1       TX-72                1.6              2.4               1.8              0.4              1.5               6.3             3.7            6.6             7.7
                  K5016         BRCL          2       TX-72                2.7              0.8               0.3              0.2              0.6               5.0             4.7            3.3             2.5





                                                                             MUSSEL WATCH YEAR VI - Bivalve Aromatics Data





                                                                                                                                                                                                2,3,4-TRI
                  FILE          SITE     REP LOCATION BENZO(a)                  PERYLENE           INDENO-           DIBENZ       BENZOW)           2-METHYL        1-METHYL       2,6 DIME     METHYL-
                                                   # AND           PYRENE                           PYRENE         ANTHRAC         PERYLENE             NAPH             NAPH           NAPH       NAPH
                                                   STATE             (ppb)+           (ppb)+            (ppb)          (ppb)+             (ppb)         (ppb)+          (ppb)+          (ppb)+      (ppb)


                  K5017       BRCL          3      'IX-72               0.6              2.1             0.9              0.3              1.7             4.6             3.0            2.7            4.4
                  K5021       BRFS          1      TX-57               19.4              6.8             7.7              4.3              8.5             7.8             4.0            9.4            12.0
                  K5022       BRFS          2      TX-57                3.3              1.0             0.4              0.3              0.7             8.3             6.0            4.6            10.2
                  K5023       BRFS          3      TX-57                3.9              5.4             2.0              1.6              2.5             5.8             4.4            5.2            6.6
                  K5009       GBCR          1      TX-18                1.2              1.6             1.7              0.7              1.7             5.5             3.9            7.5            5.7
                  K5010       G13CR         2      TX-18                2.3              1.1             0.4              0.3              0.8             9.5             6.3            7.2            4.7
                  K5011       GBCR          3      TX-18                1.0              3.5             3.5              1.6              2.7            11.4             6.2            7.3            7.4
                  K5003       GBOB          1      TX-58                9.9              2.7            13.7              6.5             19.4             3.4             3.9            3.3            3.8
                  K5004       GBOB          2      TX-58                4.0              2.2             3.3              1.0              4.5             5.6             3.8            2.9            1.6
                  K5005       GBOB          3      TX-58                1.1              1.8             4.1              1.6              5.6             2.9             2.5            3.7            3.2
                  K5057       GBT`D         I      TX-16                1.3              5.2             1.1              1.5              1.8             7.5             2.9            9.0            10.3
                  K5058       GBTD          2      TX-16                1.4              7.5             0.6              1.1              1.9            13.2             6.9           17.2            16.6
                  K5059       GBTD          3      TX-16                3.6             20.3             2.0              1.8              4.0            39.2             18.0          22.3            24.0
                  K5063       GBYC          I      TX-15                1.7              3.9             1.0              1.1              4.2             2.6             1.6            5.4            6.7
                  K5064       GBYC          2      TX-15                1.1              3.2             0.7              0.7              1.4             5.4             2.5            4.5            6.2
                  K5065       GBYC          3      TX-15                0.8              3.6             1.0              0.3              2.2             4.2             2.7            3.8            6.7
                  K5384       GBSC          I      TX-59             134.6             177.2            18.4             30.7             63.7          1037.4           941.9         1787.2         1560.9
                  K5385       GBSC          2      TX-59             218.3            208.6             53.1             56.3             91.3          1143.3          1046.6         2042.0         1615.1
                  K5386       GBSC          3      TX-59             203.9            201.5             46.6             48.3            100.5          1203.7          1093.8         2504.0         2001.9
                  K5039       GBHR          I      TX-17                1.0              2.5             1.0              0.9              1.3             3.2             3.5            4.7            5.9
                  K5040       GBHR          2      TX-17                0.8              2.4             0.4              0.5              0.6             6.5             3.3            5.6            5.9
                  K5041       GBHR          3      TX-17                0.5              2.8             0.9              1.1              0.8             4.7             2.8            5.9            3.4
                  K5027       SIJ313        1      TX-19                1.4              5.8             1.4              1.1              1.7             5.6             4.0           11.1            9.1
                  K5028       SLBB          2      TX-19                2.2             10.4             0.7              0.6              1.5            11.0             10.2           7.2            13.1
                  K5029       SLBB          3      TX-19                0.6              4.2             0.9              0.5              1.2             6.3             5.0            5.4            6.6
                  K5033       CLSIJ         I      LA-20                0.5              3.1             0.7              0.5              1.1             6.9             4.7           10.2            23.9
                  K5034       CLSJ          2      LA-20                1.2              4.4             0.1              0.2              0.2            10.1             9.6            9.1            16.7
                  K5035       CLSJ          3      IA-20                0.4              2.6             0.6              0.4              0.7             5.5             4.0            6.1            11.7
                  K5045       CLLC          1      IA-60                2.7              9.5             1.5              1.3              3.8             7.4             4.1            7.9            14.9
                  K5046       CLLC          2      LA-60                1.8              7.8             0.5              0.3              1.1             3.6             2.8            4.8            8.4
                  K5047       CLLC          3      IA-60                1.7              8.6             0.8              1.3              1.9            60.9            30.4           18.4            13.7
                  K5069       JHJH          1      LA-21                0.7              9.6             0.8              1.0              1.4             5.6             3.5            7.4            5.3
                  K5070       JHJH          2      IA-21                0.5              5.6             0.5              0.4              0.3             5.5             3.6            5.0            3.5
                  K5071       JHJH          3      LA-21                0.5              3.6             0.4              0.3              0.6             4.3             3.3            2.9            4.8
                  K5159       VBSP          I      IA-22                0.3              3.4             0.3              0.1              0.6             3.7             3.4            4.6            7.0
                  K5160       VBSP          2      IA-22                0.6              4.1             0.2              0.2              0.4             3.2             3.3            3.6            6.6
                  K5161       VBSP          3      IA-22                0.5              4.2             0.9              0.7              0.7             4.2             3.3            5.0            7.2
                  K5189       ABOB          1      IA-24                0.9              5.1             0.4              0.1              0.2             6.0             4.5            5.2            3.7





                                                                            MUSSEL WATCH YEAR VI - Bivalve Aromatics Data





                                                                                                                                                                                               2,3,4-TRI
                  FILE         SITE      REP LOCATION BENZO(a)                  PERYLENE           INDENO-          DIBENZ       BENZO(ghf)        2-METHYL       I-METHYL       2,6 DIME      METHYL-
                                                   # AND          PYRENE                            PYRENE        ANTHRAC         PERYLENE             NAPH            NAPH           NAPH       NAPH
                                                   STATE             (ppb)+           (ppb)+           (ppb)           (ppb)+           (ppb)          (ppb)+          (ppb)+         (ppb)+      (ppb)



                  K5190        ABOB         2      LA-24               0.2              2.5              0.3             0.1              0.2             3.9             2.3           2.4            2.0
                  K5191        ABOB         3      LA,24               0.3              3.1              0,2             0.1              0.3             2.5             1.8           2.8            2.5
                  K5195        CLCL         1      IA-25               1.2              3.7              0.2             0.3              0.3             5.3             3.1           4.7            4.2
                  K5196        CLCL         2      LA-25               0.3              3.2              0.2             0.2              0.2             3.0             2.5           2.7            2.6
                  K5197        CLCL         3      IA-25               0.2              3.5              0.1             0.1              0.3             3.6             2.3           2.1            2.8
                  K5165        TBLB         1      I.A-26              0.3              2.4              0.2             0.2              0.5             4.0             3.2           3.8            4.5
                  K5166        TBL13        2      LA-26               1.7              1.9              0.5             0.4              0.8             7.3             4.2           5.1            3.5
                  K5167        TBLB         3      LA-26               0.8              1.4              0.9             0.1              1.2             5.8             3.9           2.7            2.6
                  K5183        TBLF         1      LA-27               0.3              1.3              0.3             0.2              0.4             6.6             3.6           3.2            2.6
                  K5184        TBLF         2      LA-27               0.4              1.4              0.2             0.2              0.2             6.5             2.8           3.6            2.8
                  K5185        TBLF         3      LA-27               0.2              1.1              0.3             0.2              0.2             5.4             2.7           2.9            2.2
                  K5168        BBSD         I      IA-28               0.8              2.0              0.4             0.3              0.4             4.8             4.4           5.3            4.7
                  K5169        BBSD         2      IA-28               0.2              1.6              0.5             0.2              0.3             4.6             4.9           5.0            5.4
                  K5170        BBSD         3      IA-28               0.7              1.4              1.0             0.4              1.0             3.0             2.8           3.7            3.5
                  K5174        B13MB        1      LA-29               7.0              7.7              1.9             0.8              2.1             9.6             7.3           5.5            6.4
                  K5175        BBMB         2      LA-29               3.8              5.3              2.1             0.6              1.2             7.0             6.5           4.4            3.7
                  K5176        BBMB         3      IA-29               3.0              6.7              2.4             0.8              1.9             7.3             9.1           4.7            4.3
                  K5210        MRTP         I      LA-65               2.0             24.2              0.6             0.3              1.2             8.2             4.7          14.1            23.3
                  K5211        MRTP         2      LA-65               0.7             22.2              0.8             0.7              1.4             6.2             3.5          10.1            16.3
                  K5212        MRTP         3      LA-65               1.1             19.4              0.6             0.4              0.8             6.7             4.8          10.0            12.8
                  K5216        BSSI         I      LA-31               2.4             11.5              2.1             0.3              1.7            10.5             5.8          17.7            22.2
                  K5217        BSSI         2      LA-31               2.8             15.5              2.9             0.9              4.0             8.1             5.3          13.6            18.8
                  K5218        BSSI         3      LA-31               0.9             13.8              1.0             0.5              1.7             5.6             5.0          17.0            23.1
                  K5201        BSBG         1      IA-30               0.3              1.2              0.6             0.2              0.6             5.2             4.6           4.3            4.3
                  K5202        BSBG         2      IA-30               0.7              2.9              0.9             1.1              1.0             5.3             3.4           2.4            4.0
                  K5203        BSBG         3      IA-30               0.2              0.7              0.1             0.1              0.3             2.5             3.6           3.5            2.1
                  K5207        LBMP         I      LA-32               0.6              2.6              0.7             0.2              0.9            10.4             6.8           5.2            2.5
                  K5208        LBMP         2      IA-32               1.3              3.5              1.3             0.8              1.6             8.2             5.0           618            4.6
                  K5209        LBMP         3      IA-32               0.6              1.9              0.3             0.1              0.7             4.9             2.9           4.6            3.9
                  K5249        LPGO         I      IA-63               74.1            52.3            39.0             27.3            55.8           297.2           201.5          912.9         1278.6
                  K5250        LPGO         2      IA-63               79.7            77.9            36.1              20.1           52.2           244.4           172.2          922.0         1287.2
                  K5251        LPGO         3      IA-63               94.3            77.6            53.7              23.4           65.5           388.8           264.4         1453.2         1965.8
                  K5222        MSPC         1      MS-33               1.8              5.7              0.8             6.2              1.4             5.0             4.6          10.2            15.5
                  K5223        MSPC         2      MS-33               1.0              3.0              1.0             0.5              1.7             4.9             2.0           8.7            9.1
                  K5224        MSPC         3      MS-33               0.8              3.1              0.7             0.3              0.9             2.2             1.9           4.6            6.5
                  K5228        MSBB         I      MS-34               4.0              7.1              1.1             0.3              1.5            55.1            38.0         117.5          178.6
                  K5229        MSBB         2      MS-34               3.2              9.3              1.9             1.3              9.9            89.6            61.7         218.2          309.2
                  K5230        MSBB         3      MS-34               1.4              5.5              0.7             0.6              2.2            21.9            16.9          64.5            96.6





                                                                           MUSSEL WATCH YEAR VI - Bivalve Aromatics Data





                                                                                                                                                                                            2,3,4-TRI
                 RLE          SITE      REP LOCA'17ION BENZO(a)                PERYLENE          INDENO-           DIBENZ      BENZOWA)          2-METHYL       1-METHYL       2,6 DIME     METHYL-
                                                  #AND           PYRENE                           PYRENE        ANTHRAC         PERYLENE              NAPH           NAPH          NAPH        NAPH
                                                  STATE             (ppb)+          (ppb)+            (ppb)          (ppb)+           (ppb)           (ppb)+         (ppb)+        (ppb)+      (ppb)


                 K5246        MSP13        1      MS-35               1.7              4.6             0.8             0,4              0.6             7.3            6.9            5.6            7.3
                 K5247        MSP13        2      MS-35               1.5              4.0             1.6             1.1              1.2             5.4            3.8            8.4            7.2
                 K5248        MSP13        3      MS-35               0.8              7.1             0.6             0.9              2.1             4.1            2.6            5.7            6.4
                 K5234        MBCP         1      AL-36               2.2              6.0             0.4             0.2              0.9             6.1            3.0            4.9            5.9
                 K5235        MBCP         2      AL-36               0.6              4.9             0.9             0.5              1.1             4.0            2.3            5.1            3.4
                 K5236        MBCP         3      AL-36               0.7              4.4             0.4             6.6              0.6             3.5            1.4            3.5            2.6
                 K5240        MBHI         I      AL-66               4.0            18.1              0.6             0.3              1.5             7.9            5.1            9.2            11.3
                 K5241        MBHI         2      AL-66               2.0            19.3              1.9             1.5              5.3             5.1            3.4            7.4            10.8
                 K5242        MBHI         3      AL-66               1.1            16.8              0.5             0.3              2.0             4.9            3.7            4.8            9.2
                 K5261        P13PH        1      FL-67               6.0              3.6             3.1             1.5              3.9            42.5           29.1          30.6             15.3
                 K5262        P13PH        2      FL-67              10.0              9.2            12.5             5.2              9.7            81.9           53.6          51.3             25.0
                 K5263        PBPH         3      FL-67               3.0              5.1             2.7             1.6              4.1            56.0           38.8          41.0             20.0
                 K5255        PBIB         I      FL-37               0.6              2.4             0.7             0.2              0.6             3.2            2.5            3.7            3.3
                 K5256        PBIB         2      FL-37               1.8              6.2             1.8             0.4              1.6             7.2            4.5            4.9            4.4
                 K5257        PBIB         3      FL-37               2.2              3.8             1.3             0.8              1.8             3.5            2.3            5.9            4.4
                 K5267        CBJB         1      FL-73               7.9              7.3             8.1             2.8            10.9            105.5           52.8          55.2             23.4
                 K5268        CBJB         2      FL-73              15.1            10.4             31.6             7.4            25.3            102.5           52.9          63.6             21.9
                 K5269        CBJB         3      FL-73               5.7              6.6            11.3             2.5            13.4            114.3           59.0          71.3             27.0
                 K5273        CBSR         1      FL-38               0.3              1.7             0.5             0.3              0.4             3.0            2.7            3.3            2.7
                 K5274        CBSR         2      FL-38               0.3              4.1             0.9             0.4              0.7             3.3            4.1            5.4            2.1
                 K5275        CBSR         3      FL-38               0.7              3.5             1.3             1.4              0.6             4.4            3.1            3.8            2.8
                 K5279        CBSP         I      FL-39              27.9            10.4             18.1             8.8            29.7             22.9           14.2          11.9             5.8
                 K5280        CBSP         2      FL-39              21.0              6.9            11.9             6.3            19.4             15.7            7.7            9.6            4.7
                 K5281        CBSP         3      FL-39              14.2              8.9            12.8             5.6            24.6             36.7           19.8          31.8             11.7
                 K5303        PCLO         1      FL-74               0.3              0.9             1.3             0.6              1.2             9.5            4.6            8.0            5.5
                 K5304        PCLO         2      FL-74               1.5              5.0             2.2             0.5              2.7            32.2           16.6          26.9             12.1
                 K5305        PCLO         3      FL-74               0.3              1.0             0.7             0.3              0.7            21.2           10.3          10.8             9.4
                 K5297        SAVVB        1      FL-40               6.6              9.1             6.5             2.7              9.7            41.7           24.0          90.9           236.7
                 K5298        SAWB         2      FL-40              11.3            15.1             13.7             6.3            17.6             68.6           39.2         165.8           374.0
                 K5299        SAWB         3      FL-40               7.4            10.4              8.7             3.3            13.2             67.3           37.1         156.1           376.1
                 K5291        APDB         I      FL-41               0.3              3.3             0.6             0.2              1.1             8.8            7.2            8.1            4.0
                 K5292        APD13        2      FL-41               0.3              3.3             0.4             0.4              0.8            16.4            8.0            5.3            7.5
                 K5293        APD13        3      FL-41               0.3              3.0             0.5             0.4              0.6             9.3            7.7            8.3            6.0
                 K5285        APCP         1      FL-42               3.0              5.4             2.6             1.0              4.7            27.6           13.5          30.3             16.6
                 K5286        APCP         2      FL-42               2.6              5.9             4.3             1.0              5.4            45.5           20.3          39.8             16.4
                 K5287        APCP         3      FL-42               1.1              4.7             2.6             1.0              5.2            43.8           19.4          54.4             24.2
                 K5321        AESP         1      FL-75               0.5              1.9             0.3             0.7              0.4             5.5            6.3            5.7            2.2
                 K5322        AESP         2      FL-75               0.5              2.4             0.7             0.2              0.9             9.7            4.7            5.8            1.7





                                                                          MUSSEL WATCH YEAR VI - Bivalve Aromatics Data





                                                                                                                                                                                         2,3,4-TRI
                 FILE        SITE      REP LOCATION BENZO(a)                 PERYLENE           INDENO-          DIBENZ      BENZO(ghi)       2-METHYL       I-METHYL       2,6 DIME     METHYL-
                                                  #AND          PYRENE                          PYRENE        ANTHRAC         PERYLENE              NAPH          NAPH           NAPH       NAPH
                                                  STATE            (ppb)+          (ppb)+           (ppb)          (ppb)+            (ppb)          (Ppb)+        (ppb)+         (ppb)+     (ppb)


                 K5323       AESP         3       FL-75              0.4             1.5             1.0             0.8              0.4             8.7            5.4           5.0            2.9
                 K5315       CKBP         1       FL-43              0.2             0.6             0.3             0.2              0.4             3.9            3.8           2.9            2.0
                 K5316       CKBP         2       FL-43              0.1             0.6             0.4             0.3              0.4             7.3            3.7           2.8            2.2
                 K5317       CKBP         3       FL-43              0.1             0.9             0.2             0.3              0.2             5.5            3.1           2.0            1.1
                 K5353       TBNP         I       FL-76              1.8             2.0             2.8             0.7              6.2            26.8          12.8           19.1            27.1
                 K5351       TBNP         2       FL-76              1.2             0.9             1.9             0.8              3.7            35.8          13.8           23.9            11.7
                 K5352       TBNP         3       FL-76              1.3             1.7             2.5             1.2              4.7            43.9          21.9           22.2            10.6
                 K5333       TBMK         I       FL-47              0.4             0.2             0.2             0.5              0.7            10.2            4.1           6.0            4.1
                 K5334       TBMIK        2       FL-47              0.4             0.6             1.0             0.2              1.9            20.1          11.4           10.3            5.0
                 K5335       TBMK         3       FL-47              1.2             0.9             1.3             0.8              2.3            17.9            9.1          10.9            6.2
                 K5327       TBPB         I       FL-44              1.0             0.7             1.7             0.6              1.9             4.6            1.8           2.8            2.5
                 K5328       TBPB         2       FL-44              0.9             1.5             2.4             0.7              3.5             7.6            5.6           6,4            1.8
                 K5329       TBPB         3       FL-44              1.0             1.2             2.0             0.4              2.6             4.1            3.0           6.4            3.3
                 K5339       TBOT         1       FL-70              0.9             1.1             2.0             0.6              1.9             7.9            3.8           3.5            4.1
                 K5340       TBOT         2       FL-70              2.4             1.8             4.1             1.1              3.7             9.7            7.1           4.7            3.7
         co      K5341       TBOT         3       FL-70              1.9             1.3             3.4             2.4              2.9             9.2          14.0            5.2            6.6
                 K5309       TBKA         I       FL-77              3.6             2.6             4.5             2.4              8.5             4.5            3.9           3.4            6.2
                 K53 10      TBKA         2       FL-77              5.1             3.2             8.5             3.1              9.6             6.8            3.5           3.5            3.4
                 K5311       TBKA         3       FL-77              8.9             6.3             11.2            4.2             21.7             7.8          10.2            7.7            7.3
                 K5345       TBCB         I       FL-46              0.4             0.4             0.4             0.4              0.6            23.7          12.4            8.6            3.2
                 K5347       TBCB         2       FL-46              0.2             0.3             0.4             0.5              0.8            27.6          14.6           13.5            5.0
                 K5346       TBCB         3       FL-46              0.4             0.2             0.6             0.5              1.1            38.6          19.3           13.8            7.5
                 K5369       CBBI         I       FL-48              0.4             0.4             0.6             0.5              0.6             9.8            5.8           4.7            3.8
                 K5370       CBBI         2       FL-48              0.0             0.9             0.5             0.3              0.5             8.8            6.1           3.8            3.4
                 K5371       CBBI         3       FL-48              0.4             0.2             0.6             0.3              0.9             8.1            4.3           4.5            3.2
                 K5363       CBFM         1       FL-71              1.4             0.9             2.6             0.6              3.3            42.8          22.1           14.3            5.0
                 K5364       CBFM         2       FL-71              1.9             1.2             3.6             1.2              4.5            57.8          30.6           17.6            5.5
                 K5365       CBFM         3       FL-71              2.2             3.6             3.0             1.8              6.3             9.0            8.9           6.1            2.5
                 K5357       NBNI3        I       FL-49              1.5             1.6             2.5             0.9              6.5            10.8            5.0           7.3            5.9
                 K5358       NBNB         2       FL-49              1.8             1.8             1.9             0.7              7.4            11.1            6.5           7.1            6.4
                 K5359       NBNB         3       FL-49              1.4             1.5             2.0             0.5              6.8            13.1            7.5          10.5            7.1
                 K5381       RBHC         1       FL-50              0.3             0.2             0.3             0.5              0.8             8.7            5.1           5.4            3.9
                 K5382       RBHC         2       FL-50              0.3             0.6             0.5             0.3              1.2            14.3            9.6           5.1            3.2
                 K5383       RBHC         3       FL-50              0.4             0.5             0.5             0.6              1.0            11.3            7.4           6.3            4.3
                 K5375       EVFU         I       FL-51              0.3             0.9             0.5             0.4              0.3             7.7            3.7           4.1            2.4
                 K5376       EVFU         2       FL-51              0.1             0.2             0.7             0.3              0.8             6.6            5.5           3.8            1.7
                 K5377       EVFU         3       FL-51              0.1             0.2             0.5             0.6              0.8             6.5            4.3           5.3            2.3
                 K5396       BHKF         1       FL-81              1.0             1.8             1.5             0.4              2.3            12.1            6.2           6.5            2.2





                                                                         MUSSEL WATCH YEAR VI - Bivalve Aromatics Data





                                                                                                                                                                                         2.3,4-TRI
                F1LE         SITE      REP LOCATION BENZO(a)                 PERYLENE          INDENO-           DIBENZ      BENZO(ghi)       2-METHYL       1-METHYL       2,6 DIME     METHYL-
                                                 #AND           PYRENE                          PYPENE        ANTHRAC        PERYLENE              NAPH           NAPH           NAPH      NAPH
                                                 STATE            (ppb)+           (ppb)+           (ppb)          (ppb)+           (ppb)          (ppb)+         (ppb)+         (ppb)+    (ppb)


                K5397       BHKF         2       FL-81               0.9              0.6             0.7             0.3             1.9            12.0            7.6            6.2          3.4
                K5398       BHKF         3       FL-81                1.4             0.2             1.0             0.5             2.1            19.4           10.6            7.5           1.2





                                                                           MUSSEL WATCH YEAR VI - Bivalve Aromatics Data




                                                                                CENSORED            S&T              YR 1(+)          YR 1(+)         YR 1(+)        YR 1(+) TOTAL
                 FILE        SITE       REP LOCATION             I-MEI'lin        S&T PAH           PAH            S&T            2-3 RINGS       4-5 RINGS           RATIO ALKYL +
                                                  # AND            PHENAN        (<20ppb--O)    MEASURED        AROMATICS        AROMA71CS       AROMATICS           4-5 TO    S & T PAH
                                                  STATE               (ppb)+            (ppb)           (ppb)           (ppb)              (0h)                  2-3 RINGS         (ppb)



                 K5135       LMSB         1       Tx- 1                  6.3            20.0            85.3              79             59.7            40.3           0.68           90.3
                 K5136       LMSB         2       Tx- 1                  0.6            20.0            59.9              54             53.4            46.6           0.87           97.3
                 K5137       LMSB         3       Tx- 1                  0.6            20.0            45.4              41             54.5            45.5           0.83           62.4
                 K5087       CCIC         1       TX-3                   4.1            103.8           181.5            163             28.1            71.9           2.56          340.8
                 K5088       CCIC         2       TX-3                   3.4            91.5            172.7            156             33.1            66.9           2.02          384.3
                 K5089       CCIC         3       TX-3                   4.1            103.2           193.1            173             34.2            65.8           1.93          421.7
                 K5147       ABLR         I       TX-4                   0.7            20.0            27.2              26             85.8            14.2           0.17           70.2
                 K5148       ABLR         2       TX-4                   0.5            20.0            24.3              20             83.7            16.3           0.19           68.3
                 K5149       ABLR.        3       TX-4                   3.3            20.0            42.2              35             87.6            12.4           0.14          100.5
                 K5141       CBCR         I       TX-5                   0.7            20.0            26.8              24             82.2            17.8           0.22           32.9
                 K5142       CBCR         2       TX-5                   1.4            20.0            25.8              23             84.0            16.0           0.19           28.2
                 K5143       CBCR         3       TX-5                   1.1            20.0            36.8              33             84.5            15.5           0.18           91.9
                 K5099       MBAR         1       TX-6                   1.5            20.0            23.5              21             82.4            17.6           0.21           19.7
                 K5100       MBAR         2       TX-6                   0.5            20.0            25.2              21             77.5            22.5           0.29           22.4
                 K5101       MBAR         3       TX-6                   2.0            20.0            28.1              25             79.8            20.2           0.25           21.9
                 K51 11      SAPP         I       TX-7                   1.6            20.0            35.6              34             89.8            10.2           0.11           59.8
                 K5112       SAPP         2       TX-7                   0.6            20.0            34.6              30             87.1            12.9           0.15           54.0
                 K5113       SAPP         3       TX-7                   0.5            20.0            30.1              28             87.9            12.1           0.14           39.0
                 K5117       SAMP         1       TX-8                   3.8            20.0            43.5              38             74.0            26.0           0.35          121.2
                 K5118       SAMP         2       TX-8                   2.4            20.0            45.4              39             75.7            24.3           0.32          172.2
                 K5119       SAMP         3       TX-8                   2.7            20.0            35.2              29             78.8            21.2           0.27           85.0
                 K5105       ESSP         1       TX-9                   3.1            20.0            56.4              48             76.7            23.3           0.30          229.1
                 K5106       ESSP         2       TX-9                   3.6            20.0            70.4              60             77.0            23.0           0.30          250.0
                 K5107       ESSP         3       TX-9                   4.4            20.0            71.1              59             75.3            24.7           0.33          218.1
                 K5129       MBGP         1       TX-12                  8.4            20.0            106.8             88             49.3            50.7           1.03          283.3
                 K5130       MBGP         2       TX-12                  1.7            20.0            88.8              72             43.5            56.5           1.30          249.4
                 K5131       MBGP         3       TX-12                  1.8            20.0            86.2              69             44.3            55.7           1.26          288.7
                 K5123       MBLR         1       TX-11                  3.1            23.3            148.7            115             29.5            70.5           2.39          230.2
                 K5124       MBLR         2       TX-11                  3.7            56.1            214.2            169             39.7            60.3           1.52          382.8
                 K5125       MBLR         3       TX-11                  5.0            20.0            141.8            105             40.9            59.1           1.44          251.8
                 K5081       MBTP         1       TX-13                  3.5            20.0            30.3              27             83.9            16.1           0.19           35.5
                 K5082       M137?        2       TX-13                  0.5            20.0            32.2              26             84.3            15.7           0.19           42.2
                 K5083       MBTP         3       TX-13                  1.9            20.0            29.1              26             81.7            18.3           0.22           41.2
                 K5075       MBEM         I       TX-14                  2.7            20.0            56.3              48             70.9            29.1           0.41          207.2
                 K5o76       MBEM         2       TX-14                  1.1            20.0            44.0              40             76.3            23.7           0.31          186.1
                 K5077       MBEM         3       TX-14                  0.9            20.0            42.8              37             75.9            24.1           0.32          166.2
                 K5015       BRCL         I       TX-72                  3.7            20.0            121.1             95             54.5            45.5           0.83          244.7
                 K5016       BRCL         2       TX-72                  0.0            20.0            126.4            108             35.4            64.6           1.83          237.6





                                                                           MUSSEL WATCH YEAR VI - Bivalve Aromatics Data




                                                                                 CENSORED           S&T              YR 1(+)          YR 1(+)         YR 1(+)        YR 1(+) TOTAL
                 FILE          SITE     REP LOCATION              1-METHYL         S&T PAH          PAH            S&T            2-3 RINGS       4-5 RINGS           RATIO ALKYL +
                                                  #AND              PHENAN        (<20ppb--O)    MEASURED        AROMA71CS       AROMATICS       AROMATICS            4-5 TO   S & T PAH
                                                  STATE               (ppb)+            (ppb)           (ppb)            (ppb)            N                (0/6)  2-3 RINGS        (ppb)



                 K5017       BRCL          3      TX-72                  2.3            20.0            109.8              87             43.5           56.5            1.30         452.4
                 K5021       BRFS          1      TX-57                 16.3          1569.4           1710.2            1509             15.0           85.0            5.68        2743.1
                 K5022       BRFS          2      TX-57                  7.1            411.5           548.0             503             22.9           77.1            3.36        1267.5
                 K5023       BRFS          3      TX-57                  4.6            417.8           551.6             492             17.3           82.7            4.78        1121.0
                 K5009       GBCR          I      TX- 18                 5.3            203.8           322.5             296             24.7           75.3            3.05         746.5
                 K5010       GBCR          2      TX-18                 10.2            192.4           334.3             309             30.4           69.6            2.29         822.5
                 K5011       GBCR          3      TX-18                  7.8            250.1           396.5             352             26.4           73.6            2.79         819.0
                 K5003       GBOB          I      TX-58                 10.8            427.0           553.4             459             16.0           84.0            5.24         880.0
                 K5004       GBOB          2      TX-58                  3.0            247.3           354.9             304             18.7           81.3            4.36         773.5
                 K5005       GBOB          3      TX-58                  3.7            168.1           270.8             220             19.2           80.8            4.21         534.0
                 K5057       GBTD          1      TX-16                  9.8            20.0            138.4             115             52.8           47.2            0.89        1238.8
                 K5058       GBTD          2      TX-16                  7.0            20.0            164.4             134             60.3           39.7            0.66        1661.4
                 K5059       GBTD          3      TX- 16                10.3            184.6           316.0             264             58.8           41.2            0.70        4633.8
                 K5063       GBYC          I      TX-15                 22.6            43.6            158.3             133             55.1           44.9            0.82         518.8
                 K5064       GBYC          2      TX-15                 13.9            20.0            136.9             118             49.3           50.7            1.03         465.7
                 K5065       GBYC          3      Tx- 15                 5.0            20.6            126.4             107             42.3           57.7            1.36         446.3
                 K5384       GBSC          1      TX-59               463.3          13629.4         13647.8            11709             66.3           33.7            0.51      91581.8
                 K5385       GBSC          2      TX-59               408.1          15338.7         15338.7            13037             66.0           34.0            0.52      78726.6
                 K5386       GBSC          3      TX-59               436.7          17677.6         17677.6            15033             67.1           32.9            0.49      98997.6
                 K5039       GBHR          1      TX-17                  2.4            20.0            89.8               73             61.4           38.6            0.63         329.5
                 K5M         GBHR          2      TX-17                  6.3            20.0            102.0              89             58.0           42.0            0.72         450.5
                 K5041       GBHR          3      TX-17                  3.5            20.0            88.0               77             63.5           36.5            0.57         392.8
                 K5027       SLBB          1      TX- 19                 7.7            56.9            207.5             177             45.8           54.2            1.18        1036.2
                 K5028       SLBB          2      TX-19                  9.1            142.6           294.6             258             40.2           59.8            1.49        1375.0
                 K5029       SLBB          3      TX-19                  3.6            20.0            124.6             106             44.9           55.1            1.23         717.2
                 K5033       CLSJ          1      LA-20                 18.5            23.9            148.4             119             65.6           34.4            0.53        1332.9
                 K5034       CLSJ          2      LA-20                 18.3            20.0            164.9             144             64.9           35.1            0.54        1737.5
                 K5035       CLSJ          3      LA-20                 13.8            20.0            109.0              92             63.0           37.0            0.59        1225.5
                 K5045       CLLC          1      LA-60                 42.8            389.6           521.7             484             50.5           49.5            0.98        1669.3
                 K5046       CLLC          2      IA-60                 27.0            201.7           297.1             277             43.3           56.7            1.31        1082.0
                 K5047       CLLC          3      IA-60                  7.9            452.6           590.3             557             59.1           40.9            0.69        1591.3
                 K5069       JHJH          I      IA-21                  3.9            23.6            139.5             128             57.9           42.1            0.73         302.8
                 K5070       JHJH          2      LA-21                  2.8            20.0            106.4              98             58.1           41.9            0.72         364.5
                 K5071'      JHJH          3      IA-21                  3.7            20.0            92.4               82             63.1           36.9            0.58         217.0
                 K5159       VBSP          I      IA-22                  4.1            20.0            70.9               61             63.9           36.1            0.56         312.8
                 K5160       VBSP          2      IA-22                  3.2            20.0            65.0               53             59.2           40.8            0.69         255.8
                 K5161       VBSP          3      IA-22                  2.0            20.0            68.7               57             61.0           39.0            0.64         337.0
                 K5189       ABOB          I      IA-24                  1.2            20.0            63.1               55             72.7           27.3            0.38         100.7





                                                                           MUSSEL WATCH YEAR VI - Bivalve Aromatics Data




                                                                                 CENSORED           S&T               YR 1            YR I(+)         YR 1(+)         YR 1(+) TOTAL
                 FILE         SITE      REP LOCATION              1-ME`f1iyL       S&T PAH          PAH             S&T           2-3 RINGS        4-5 RINGS          RATIO ALKYL +
                                                   #AND             PHENAN       (<20ppb--O)     MEASURED        AROMATICS       AROMATICS       AROMATICS            4-5 TO    S & T PAH
                                                   STATE               (ppb)+           (ppb)           (ppb)           (ppb)             N                N      2-3 RINGS        (ppb)


                 K5190        ABOB         2       LA-24                 1.7            20.0            42.5               38             72.7            27.3           0.38         157.1
                 K5191        ABOB         3       IA-24                 0.5            20.0            35.3               31             66.6            33.4           0.50           77.1
                 K5195        CLCL         I       LA-25                 2.8            20.0            69.5               60             70.0            30.0           0.43         228.7
                 K5196        CLCL         2       LA-25                 1.2            20.0            46.5               40             66.5            33.5           0.50         140.7
                 K5197        CLCL         3       LA-25                 1.8            20.0            45.4               40             65.9            34.1           0.52         128.7
                 K5165        TBLI3        1       LA-26                 4.5            20.0            58.1               50             68.6            31.4           0.46         219.4
                 K5166        TBLI3        2       LA-26                 1.5            20.0            83.9               73             63.4            36.6           0.58         183.1
                 K5167        T13LB        3       LA-26                 2.1            20.0            64.7               56             65.6            34.4           0.52         173.1
                 K5183        TBLF         I       LA-27                 3.0            20.0            55.5               51             73.8            26.2           0.36         308.8
                 K5184        TBLF         2       LA-27                 2.2            20.0            55.2               49             71.3            28.7           0.40         297.5
                 K5185        TBLF         3       LA-27                 0.9            20.0            44.6               40             73.9            26.1           0.35         200.2
                 K5168        BBSD         I       LA-28                 4.7            20.0            70.0               62             74.9            25.1           0.34         357.3
                 K5169        BBSD         2       I.A-28                3.3            20.0            61.0               51             72.8            27.2           0.37         245.2
                 K5170        BBSD         3       IA-28                 3.1            20.0            58.6               50             65.2            34.8           0.53         388.6
                 K5174        BBMB         1       LA-29                10.9            752.7           873.4             787             24.5            75.5           3.08        1703.1
                 K5175        BBMB         2       LA-29                 7.7            635.0           741.7             689             18.2            81.8           4.50        1375.7
         00      K5176        BBMB         3       LA-29                 9.1            686.7           811.3             754             20.7            79.3           3.83        1409.4
                 K52 10       MRTP         I       LA-65                22.4            205.0           309.9             272             47.9            52.1           1.09        2122.3
                 K5211        MRTP         2       LA-65                12.9            45.0            197.5             168             47.2            52.8           1.12        1227.3
                 K5212        MRTP         3       LA-65                10.7            27.7            191.0             168             46.2            53.8           1.17         995.8
                 K5216        BSSI         I       LA-31                14.3            151.5           277.0             239             44.3            55.7           1.26        2273.0
                 K5217        BSSI         2       LA-31                11.4            85.8            234.8             199             40.7            59.3           1.46        1249.4
                 K5218        BSSI         3       LA-31                19.6            89.8            227.3             192             45.1            54.9           1.22        1187.8
                 K5201        BSBG         1       LA-30                 3.0            20.0            74.0               66             81.2            18.8           0.23         201.7
                 K5202        BSBG         2       LA-30                 1.5            20.0            65.4               57             70.7            29.3           0.41         177.4
                 K5203        BSBG         3       LA-30                 0.7            20.0            39.0               35             72.6            27.4           0.38         116.5
                 K5207        LBMP         I       LA-32                 2.8            28.5            122.5             110             68.5            31.5           0.46         473.2
                 K5208        LBMP         2       LA-32                 4.0            22.1            110.9              98             65.2            34.8           0.53         265.1
                 K5209        LBMP         3       LA-32                 1.9            20.0            79.9               71             63.7            36.3           0.57         241.6
                 K5249        LPGO         1       LA-63               452.5         7852.3           7852.3            5993              48.7            51.3           1.05      49392.9
                 K5250        LPGO         2       LA-63               545.3         8170.3           8170.3            6136              46.7            53.3           1.14      42799.2
                 K5251        LPGO         3       LA-63              1184.9         12069.3          12069.3           9307              54.0            46.0           0.85      69887.7
                 K5222        MSPC         1       MS-33                11.0            253.3           394.4             348             31.7            68.3           2.16        1738.2
                 K5223        MSPC         2       MS-33                 9.9            152.9           264.1             235             34.2            65.8           1.92         734.8
                 K5224        MSPC.        3       MS-33                 8.6            100.9           195.6             175             30.0            70.0           2.33         663.0
                 K5228        MSBB         1       MS-34                62.2         1118.1           1180.8              969             60.1            39.9           0.66        9560.6
                 K5229        MSBB         2       MS-34               113.1         1928.6           1964.7            1587              59.0            41.0           0.69      11293.5
                 K5230        MSBB         3       MS-34                84.8            609.7           728.8             585             55.6            44.4           0.80        3919.1






                                                                          MUSSEL WATCH YEAR VI - Bivalve Aromatics Data




                                                                                CENSORED           S&T              YR 1(+)         YR 1(+)         YR 1(+)        YR 1(+) TOTAL
                 FILE        SITE      REP LOCATION              I-METHYL         S&T PAH          PAH             S&T          2-3 RINGS        4-5 RINGS          RA710 ALKYL +
                                                  #AND             PHENAN       (<20ppb--O)    MEASURED        AROMATICS       AROMATICS       AROMATICS           4-5 TO    S & T PAH
                                                  STATE              (ppb)+            (ppb)           (ppb)          (ppb)             N                N     2-3 RINGS         (ppb)


                 K5246       MSPB         1       MS-35                10.1            113.8           227.5            209             35.1           64.9           1.85        1246.3
                 K5247       MSPB         2       MS-35                10.6            91.0            204.7            180             36.6           63.4           1.73         949.4
                 K5248       MSP13        3       MS-35                 4.1            65.8            162.2            145             28.3           71.7           2.54         735.7
                 K5234       MBCP         I       AL-36                11.7            202.8           312.4            293             32.4           67.6           2.09         941.3
                 K5235       MBCP         2       AL-36                 6.2            105.4           202.9            185             32.4           .67.6          2.08         471.1
                 K5236       MBCP         3       AL-36                 5.1            67.7            149.0            140             28.5           71.5           2.51         422.4
                 K5240       MBHI         I       AL-66                17.4            473.5           631.0            584             20.1           79.9           3.98        1944.4
                 K5241       MBHI         2       AL-66                13.9            394.5           538.6            486             19.0           81.0           4.27        1599.3
                 K5242       MBHI         3       AL-66                11.8            267.7           417.9            385             17.6           82.4           4.67        1186.6
                 K5261       P13PH        1       FL-67                36.1         2023.5          2104.3            2025              48.3           51.7           1.07        3310.2
                 K5262       PBPH         2       FL-67                51.0         3444.1          3506.3            3346              50.4           49.6           0.99        5326.3
                 K5263       PBPH         3       FL-67                41.4         2440.4          2499.3            2415              50.5           49.5           0.98        3994.8
                 K5255       PBIB         I       FL-37                 2.4            30.3            144.1            131             49.8           50.2           1.01         462.0
                 K5256       PBIB         2       FL-37                 5.2            112.5           251.2            225             49.1           50.9           1.04         632.0
                 K5257       PBIB         3       FL-37                 4.0            86.5            190.8            169             49.2           50.8           1.03         540.2
                 K5267       CBJB         1       FL-73                26.1         1224.5          1279.1            1155              44.2           55.8           1.26        3290.3
                 K5268       CI3,JI3      2       FL-73                24.4         1536.1          1586.8            1379              41.9           58.1           1.38        3726.6
                 K5269       CBJB         3       FL-73                35.5         1516.0          1608.7            1456              47.7           52.3           1.09        3595.2
                 K5273       CBSR         I       FL-38                 1.5            20.0            76.2              68             56.6           43.4           0.77         337.5
                 K5274       CBSR         2       FL-38                 2.7            20.0            95.9              87             60.3           39.7           0.66         338.8
                 K5275       CBSR         3       FL-38                 1.3            20.0            88.5              79             58.6           41.4           0.71         350.9
                 K5279       CBSP         I       FL-39                 5.8            420.7           556.6            451             30.0           70.0           2.33        1459.2
                 K5280       CBSP         2       FL-39                 8.5            204.6           368.4            305             31.3           68.7           2.20        1146.2
                 K5281       CBSP         3       FL-39                11.3            486.7           619.5            521             36.6           63.4           1.73        1537.0
                 K5303       PCLO         1       FL-74                20.9            107.3           213.1            190             49.7           50.3           1.01         830.0
                 K5304       PCLO         2       FL-74                23.3            489.2           627.9            576             46.7           53.3           1.14        2167.8
                 K5305       PCLO         3       FL-74                10.9            123.3           239.1            220             59.0           41.0           0.70         924.8
                 K5297       SAWB         1       FL-40              299.7          2516.8          2591.9            2223              42.0           58.0           1.38       25358.2
                 K5298       SAWB         2       FL-40              566.2          4257.3          4336.0            3741              42.1           57.9           1.37       36476.7
                 K5299       SAWB         3       FL-40              595.2          4105.7          4163.9            3596              42.9           57.1           1.33       37133.8
                 K5291       APDB         I       FL-41                 2.1            20.0            105.4             95             60.2           39.8           0.66         551.3
                 K5292       APDB         2       FL-41                 3.8            20.0            125.0            111             66.0           34.0           0.52         504.3
                 K5293       APDB         3       FL-41                 4.3            20.0            117.3            106             63.5           36.5           0.58         466.1
                 K5285       APCP         I       FL-42                15.6            217.5           354.3            309             47.8           52.2           1.09        1810.7
                 K5286       APCP         2       FL-42                24.0            332.2           444.8            406             51.8           48.2           0.93        2083.2
                 K5287       APCP         3       FL-42                15.4            366.6           500.5            444             49.8           50.2           1.01        2565.3
                 K5321       AESP         I       FL-75                 1.6            20.0            84.0              76             67.6           32.4           0.48         115.2
                 K5322       AESP         2       PL-75                 2.3            20.0            96.3              87             70.9           29.1           0.41         123.3





                                                                          MUSSEL WATCH YEAR VI - Bivalve Aromatics Data




                                                                                CENSORED           S&T              YR 1(+)          YR 1(+)         YR 1           YR 1(+) TOTAL
                 FILE        SITE      REP LOCATION              I-METHYL         S&T PAH          PAH            S&T            2-3 RINGS       4-5 RINGS          RATIO ALKYL +
                                                  #AND             PHENAN        (<20ppb--O)   MEASURED        AROMATICS        AROMATICS       AROMATICS           4-5 TO   S & T PAH
                                                  STATE               (ppb)+           (ppb)           (ppb)            (ppb)           N                       2-3 RINGS        (ppb)



                 K5323       AESP         3       FL-75                 3.3            20.0            93.7              84             65.6            34.4           0.52         129.6
                 K5315       CKBP         1       FL-43                 1.1            20.0            43.7              39             78.3            21.7           0.28          38.6
                 K5316       CK13P        2       FL-43                 2.0            20.0            55.1              50             80.8            19.2           0.24          65.2
                 K5317       CKBP         3       FL-43                 1.6            20.0            45.7              42             76.1            23.9           0.31          42.3
                 K5353       T13NP        I       FL-76                 10.5           391.5           536.5            471             27.9            72.1           2.58        1426.8
                 K5351       T13NP        2       FL-76                 9.5            388.7           508.6            470             30.7            69.3           2.25        1312.9
                 K5352       T13NP        3       FL-76                 10.0           450.6           568.7            M8              32.7            67.3           2.06        1524.2
                 K5333       T13MK        1       FL-47                 3.4            46.4            119.9            111.            60.2            39.8           0.66         285.6
                 K5334       TBMK         2       FL-47                 7.8            165.4           291.3            273             53.9            46.1           0.85         855.2
                 K5335       TBMK         3       FL-47                 8.5            194.9           327.4            303             52.3            47.7           0.91         796.4
                 K5327       TBPB         I       FL-44                 1.8            60.4            138.4            121             26.9            73.1           2.72         306.5
                 K5328       T13PB        2       FL-44                 3.1            133.6           237.7            211             29.6            70.4           2.38         398.3
                 K5329       TI3PI3       3       FL-44                 1.4            64.1            161.8            138             30.9            69.1           2.23         286.5
                 K5339       TBOT         I       FL-70                 3.5            24.7            132.2            112             42.5            57.5           1.35         233.7
                 K5340       TBOT         2       FL-70                 3.3            74.5            207.6            176             37.9            62.1           1.64         494.2
                 K5341       TBOT         3       FL-70                 5.2            65.3            215.7            180             43.1            56.9           1.32         355.0
         0       K5309       TBKA         I       FL-77                 9.3            296.6           456.7            399             15.1            84.9           5.62        1611.3
                 K5310       TBKA         2       FL-77                 6.0            340.3           485.2            422             18.0            82.0           4.54        1633.7
                 K5311       T13KA        3       FL-77                 13.6           905.6         1034.8             887             16.3            83.7           5.13        3040.5
                 K5345       TI3CB        1       FL-46                 3.0            47.0            126.8            118             77.5            22.5           0.29         288.2
                 K5347       TBCB         2       FL-46                 3.5            27.6            150.5            139             74.7            25.3           0.34         372.6
                 K5346       TBCB         3       FL-46                 4.4            119.1           210.4            196             75.7            24.3           0.32         596.1
                 K5369       CBBI         1       FL-48                 2.7            20.0            87.6              78             53.9            46.1           0.86         341.3
                 K5370       CBBI         2       FL-48                 2.1            20.0            86.1              78             60.3            39.7           0.66         334.2
                 K5371       CBBI         3       FL-48                 1.3            20.0            74.2              67             61.1            38.9           0.64         264.2
                 K5363       C13FM        I       FL-71                 1.5            152.3           254.0            214             63.7            36.3           0.57         583.8
                 K5364       CBFM         2       FL-71                 2.9            204.5           310.0            278             68.4            31.6           0.46         724.1
                 K5365       CI3FM        3       FL-71                 2.4            70.8            206.6            171             36.3            63.7           1.76         765.1
                 K5357       NBNB         1       FL-49                 6.0            193.1           326.9            286             20.2            79.8           3.95        1280.0
                 K5358       NBNI3        2       FL-49                 5.8            192.4           310.5            265             22.8            77.2           3.40        1268.2
                 K5359       N13NI3       3       FL-49                 5.8            196.5           361.2            314             24.8            75.2           3.04        1336.3
                 K5381       RBHC         1       FL-50                 1.5            20.0            74.6              66             58.3            41.7           0.72         335.4
                 K5382       RBHC         2       FL-50                 2.2            20.0            102.6             93             57.2            42.8           0.75         431.6
                 K5383       RI3HC        3       FL-50                 1.5            20.0            102.1             92             56.0            44.0           0.78         452.7
                 K5375       EVFU         1       FL-51                 0.8            20.0            59.2              54             71.3            28.7           0.40         135.8
                 K5376       EVFU         2       FL-51                 1.0            20.0            57.8              53             73.8            26.2           0.35          69.5
                 K5377       EVFU         3       FL-51                 1.2            20.0            58.6              53             71.9            28.1           0.39         210.2
                 K5396       BHKF         1       FL-81                 2.7            20.0            88.6              79             63.5            36.5           0.58         279.1





                                                                           MUSSEL WATCH YEAR VI - Bivalve Aromatics Data




                                                                                 CENSORED            S&T              YR 1(+)         YR 1(+)          YR 1(+)        YR 1(+) TOTAL
                 FILE         SITE      REP LOCATION              1-MET1iYL        S&T PAH          PAH             S&T           2-3 RINGS        4-5 RINGS           RATIO ALKYL +
                                                   # AND            PHENAN        (<20ppb--O)   MEASURED AROMATICS               AROMATICS        AROMATICS           4-5 TO    S & T PAH
                                                   STATE               (ppb)+            (ppb)           (ppb)           (ppb)            (0/6)             (0/6) 2-3 RINGS        (ppb)


                 K5397       BHKF         2        FL-81                  3.2            20.0            84.2               73            60.9             39.1           0.64        283.5
                 K5398       BHKF         3        FL-81                  1.2            20.0            96.2               89            69.5             30.5          0.44         310.5




I
Ii
I
I
I
I
I
I
I
                Aromatics QA/QC Data

I
I
I
I
I
I
I
I
A,                       42




 I
 I
 I
 I
 I
 I
 I
 I
 I
 I                         Aromatics Blanks, Spikes and QC Data
 I
 I
 I
 I
 I
 I
 I
 I
                                                43
 t", -





                                                                MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks, Spikes and QC Data




                                                                                                                                                                                                    2,3,4-TRI
                   FILE                 QC                  DESCRIPTION SAMPLE NAPH 2-METHYL I-METHYL BIPHENYL 2,6 DIME ACENAPH- ACENAPH- METHYL-
                                   BATCH                                         VVEIGHT                     NAPH           NAPH                         NAPH THYLENE                   THENE NAPH
                                                                                   (g dry)     (ppb)+        (ppb)+         (ppb)+         (ppb)+        (ppb)+            (ppb)          (ppb)+       (ppb)


               LABORATORY REFERENCE MATERIAL


               >W2639              P505.6              GERG SM. CHK 11                 1.0     649.9         1257.5         970.8          208.6         766.9               1.0            20.1        442.6
               >W2897              P507.8              GERG STD. CHK 11                1.0     745.8         1364.5        1065.2          216.7         867.1               1.0            20.3        423.6
               >W2961              P507.8              GERG STD. CHK 11                1.0     703.7         1273.5        1007.9          195.0         782.3               1.1            18.5        393.7
               >W4149              P512.3              GERG STD. CHK 11                1.0     580.7         1156.1         928.4          156.8         622.9               1.0            15.6        332.5
               >W4157              P514,5              GERG STD. CHK 11                1.0     637.2         1155.2         887.6          161.4         658.0               0.7            18.7        355.1
               >W4229              P518,9              GERG STD. CHK 11                1.0     594.8         1118.1         874.2          198.1         798.8               1.2            22.1        417.6
               >W4240              P520,1              GERG STD. CHK 11                1.0     594.0         1235.7         967.8          174.2         686.5               0.8            20.9        396.8
               >W4272              P522,3              GERG STD. CHK 11                1.0     650.8         1170.3         G138.0         193.9         745.1               0.7            20.5        400.0
               >W4271              P524.5              GERG SM. CHK 11                 1.0     552.0         1101.3         861.9          173.1         676.4               0.7            18.0        358.5
               >W4407            P526,7.9              GERG STD. CHK 11                1.0     689.0         1247.6         945.7          256.2         999.0               0.9            21.9        507.3
               >W4936                 P528             GERG STD. CHK 11                1.0     638.4         1241.8         985.9          183.5         652.4               1.2            15.8        362.2
               >W4807                 P531             GERG STD. CHK 11                1.0     613.7         1146.8         886.1          181.4         695.7               1.1            17.1        409.8
               >W5005                 P532             GERG STD. CHK 11                1.0     598.3         1109.6         855.4          179.5         623.5               0.5            17.1        358.4


               aver-age                                                                        634.5         1198.3         936.5          190.7         736.5               0.9            19.0        396.8
                                                                                               8.2%            6.3%          6.4%          13.2%         14.1%            23.5%            11.00/0      11.2%


               GERG chk 2 - avg. of 50                                                         646.8         1175.4         923.7          178.0         711.0               0.8            17.6        373.7
                                                                                               12.7%         11.0%          11.50/0        13.4%         12.9%            65.7%           15.7%         13.2%
               BLANKS


               >QO685              P503.4           S&T BLANK P503                   10.0           1.3          0.5           0.5           0.5            0.5              0.1             0.2            0.3
               >QO688              P503.4           S&T BLANK P504                   10.0           0.1          0.1           0.2           0.5            0.2              0.0             0.1            0.2
               >Q0740              P505.6           S&T BLANK P505                   10.0           1'3          1.6           0.7           0.5            0.6              0.1             0.4            0.3
               >Q0743              P505.6           S&T BLANK P506                   10.0           0.8          0.9           0.4           0.7            0.3              0.1             0.2            0.3
               >Q0746              P507,8           S&T BLANK P507                   10.0           0.5          0.8           0.8           0.3            0.3              0.1             0.2            0.3
               >Q0749              P507,8           S&T BLANK P508                   10.0           0.7          0.5           0.3           0.2            0.5              0.1             0.2            0.3
               >Q0770             P510,11           S&T BLANK P510                   10.0           0.2          0.8           0.3           0.7            0.3              0.3             0.4            0.5
               >Q0784             P510,11           S&T BLANK P511                   10.0           1.0          0.5           0.6           0.5            0.2              0.1             0.2            0.5
               >Q0787              P512.3           S&T BLANK P512                   10.0           0.4          0.2           0.3           0.2            0.4              0.1             0.2            0.4
               >Q0790              P512.3           S&T BLANK P513                   10.0           0.5          0.3           0.2           0.3            0.4              0.1             0.2            0.2
               >Q1022              P514.5           S&T BLANK P514                   10.0           0.7          1.0           0.6           0.3            0.8              0.2             0.5            0.4
               >Q1025              P514.5           S&T BLANK P515                   10.0           0.7          0.7           0.3           0.2            0.4              0.3             0.5            0.5
               >Q1028              P516.7           S&T BLANK P516                   1010           0.6          0.5           0.4           0.2            0.5              0.2             0.2            0.3
               >Q1040              P516,7           S&T BLANK P517                   10.0           0.9          0.6           0.5           0.5            0.2              0.1             0.2            0.3
               >Q1043              P518,9           S&T BLANK P518                   10.0           0.2          0.3           0.4           0.5            0.1              0.1             0.1            0.2





                                                         MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks, Spikes and QC Data




                                                                                                                                                                              2,3,4-TRI
                 FILE               QC               DESCRIPTION SAMPLE             NAPH 2-METHYL         1-METHYL     BIPHENYL     2.6 DIME      ACENAPH-      ACENAPH-      METHYL-
                               BATCH                                    WEIGHT                   NAPH         NAPH                      NAPH       THYLENE          THENE       NAPH
                                                                          (g dry)   (ppb)+       (ppb)+       (ppb)+       (ppb)+       (ppb)+          (ppb)         (ppb)+    (ppb)


              >QI054           P518,9         S&T BLANK P519                10.0       0.6          0.7          0.9          0.3          1.2            0.1           0.5          1.2
              >QI063           P520.1             S&T BLANK P520            10.0       1.3          0.9          0.6          0.6          0.6            0.1           0.3          0.5
              >QI066           P520,1             S&T BLANK P521            10.0       1.0          0.7          0.7          0.2          0.5            0.1           0.3          0.1
              >QI109           P522,3        S&T BLANK P522                 10.0       0.6          0.9          0.6          0.8          1.2            0.1           0.4          0.8
              >glll5           P522,3        S&T BLANK P523                 10.0       0.6          0.6          0.3          0.2          0.3            0.2           0.2          0.1
              >Q1118           P524.5    S&TTISSUE BLANK P524               10.0       1.2          1.1          0.7          0.7          0.4            0.1           0.2          0.4
              >Q 1184          P524.5    S&TTISSUE BLANK P525               10.0       0.8          0.5          0.3          0.3          0.3            0.1           0.3          0.4
              >Q1218          P526,7.9       S&T BLANK P527                 10.0       1.7          0.8          0.6          0.3          0.2            0.2           0.5          0.5
              >g 1336         P526.7.9       S&T BLANK P529                 10.0       0.8          0.6          0.4          0.8          0.5            0.2           0.5          0.1
              >Q 1258             P528  S&T TISSUE BLANK P528               10.0       1.2          0.5          0.3          0.2          0.1            0.0           0.1          0.2
              >Q1708             P531 S&TTISSUE BLANK P531                  10.0       0.8          0.4          0.5          0.2          0.1            0.3           0.1          0.7

              average                                                                  0.8          0.6          0.5          0.4          0.4            0.1           0.3          0.4
                                                                                    48.6%        48.1%        38.7%        50.4%        65.6%          50.8%         52.5%        63.3%
              NIST SRM 1974 -TISSUE SAMPLE
              Values for SRM 1974                                                                  17.0          9.0


              >QI023           P514.5             S&T NIST P514             0.60      18.3         11.3         13.7          8.5         15.8          21.3            7.9         30.3
              >QI026           P514.5             S&T NIST P515             0.60      18.5         13.3          9.5          4.7         19.5          10.8            6.8         23.9
              >Q1041           P516,7             S&T NIST P517             0.60      16.3         20.1          8.5          9.1         22.2            7.2           9.7         23.0
              >glO44           P518.9             S&T NIST P518             0.60      21.2         26.7         17.6          7.5         22.7          13.6            8.6         23.3
              >Q 1055          P518'9             S&T NIST P519             0.60      14.3         16.5         13.0          4.5         11.8            5.2           4.9         21.1
              >glO64           P520,1               S&T NIST P520           0.60      32.5         17.1         12.5          7.0         12.7            4.2           4.1         27.4
              >glO67           P520,1               S&T NIST P521           0.60      29.2         19.4         13.0          8.2         13.4            7.9           8.8         28.5
              >QIlIO           P522,3             S&T NIST P522             0.60      28.8         20.7         14.3          13.7        18.4          17.6            10.3        36.5
              >Q1119           P524,5               S&T NIST P524           0.60      25.5         25.2         17.5          10.9        21.9            8.7           6.6         27.1
              >Q 1185          P524.5               S&T NIST P525           0.60      21.8         15.5         14.2          8.3         13.4            6.7           6.6         17.5

              average                                                                 22.6         18.6         13.4          8.2         17.2          10.3            7.4         25.9
                                                                                    25.5%        24.8%        20.6%        31.5%        23.6%          51.3%          25.5%        19.5%


              REPLICATES AND SPIKED SAMPLES


              >QO684           P503.4     S&T QA/QC(K5039)P503                311      7.6          4.6          3.8          2.5          4.0            1.6           2.4          4.7
              >K5039           P503.4 StT TISSUE P503 (GBHR)                  3.1      8.8          5.3          3.5          2.5          4.7            1.8           2.3          5.8



              >QO687           P503A      S&T QA/QC(K5159)P504                2.7      7.3          4.5          2.8          3.2          5.2            0.7           0.7          7.5





                                                            MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks, Spikes and QC Data




                                                                                                                                                                                        2,3,4-TRI
                  FILE                QC                 DESCRIPTION SAMPLE              NAPH 2-METHYL 1-METHYL BIPHENYL 2.6DIME ACENAPH- ACENAPH-                                      METHYL-
                                 BATCH                                      WEIGHT                     NAPH         NAPH                        NAPH       THYLENE           THENE        NAPH
                                                                              (g dry)    (ppb)+        (ppb)+       (ppb)+        (ppb)+        (ppb)+           (ppb)        (ppb)+       (ppb)


              >K5159             P503,4   S&TTISSUE P504 (VBSP)                  2.7        6.4           3.7           3.4          3.9           4.6            1.1             1.1          7.0
              >QO689             P503.4       S&T SPIKE(K5159)PS04               2.7      43.8          45.1          45.0          41.4          40.7           31.5           36.8          47.4
                                                 Average % Recovery =       102.71%     101.1%        111.7%        112.2%      101.3%          97.6%          82.1%          96.3%        108.9%

              >Q0739             P505,6      S&T QA/QC(K5222)P505                2.1        8.9           5.7           5.1          4.5          10.6            4.5             5.3         14.6
              >K5222             P505,6 S&T TISSUE P505 (MSPC)                   2.1        8.1           5.0           4.6          4.9          10.2            4.9             7.1         15.5
              >Q0741             P505,6       S&T SPIKE(K5222)P505               2.2      57.5          67.6          68.2          64.9          67.0           62.7           73.6          76.6
                                                 Average % Recovery =       109-33%     107.0%        109.3%        116.4%      124.1%         114.0%         120.3%          132.2%       131.2%

              >Q0742             P505,6      S&T QA/QC(K504O)P506                3.3        5.4           5.5           3.8          2.5           3.8            2.1             3.9          5.3
              >K5040             P505,6 S&T TISSUE P506 (GBHR)                   3.3        4.8           6.5           3.3          3.8           5.6            3.5             3.1          5.9
              >Q0744             P505.6       S&T SPIKE(K504O)P506               3.3      33.4          35.3          40.5          35.6          31.9           29.8           32.3          37.3
                                                 Average % Recovery =       86-02%       94.7%         95.2%        122.70/6    105.1%          87.0%          87.1%          96.5%        103.9%

              >Q0745             P507.8      S&T QA/QC K5118 P507                3.4        5.3           5.0           3.1          2.0           2.9            1.0             1.7          3.6
              >K5118             P507,8 S&T TISSUE P507 (SAMP)                   3.4        4.9           4.3           3.9          2.0           2.6            1.9             1.7          1.8
              >Q0747             P507,8        S&T SPK K5118 P507                3.4      29.0          33.3          32.6          28.0          27.5           26.2           26.8          26.1
                                                 Average % Recovery =       85.84%       81.4%         97.90A       96.9%         87.9%         84.1%          82.0%          84.9%         82.1%

              >Q0748             P507.8      S&T QA/QC K5064 P508                2.7        5.2           3.7           2.4          1.9           4.0            2.9             2.1          5.2
              >K5064             P507,8 S&T TISSUE P508 (GBYC                    2.7        6.0           5.4           2.5          2.0           4.5            2.6             2.6          6.2
              >Q0750             P507,8        S&T SPK K5064 P508                2.7      33.2          36.1          37.1          33.1          34.2           33.0           34.4          34.8
                                                 Average % Recovery         82.64%       74.8%         83.9%        94.6%         85.1%         81.2%          83.0%          87.0%         78.5%

              >Q0769           P510.11       S&T QA/QC(K506S)P510                3.0        8.0           3.8           2.9          3.7           6.1            4.0             2.2          3.4
              >K5065           P510,11 S&TTISSUEP510 (GBYC)                      3.0        6.3           4.2           2.7          3.1           3.8            2.8             2.6          6.7
              >Q0771           P510.11         S&T SPK(K5065) P5 10              3.0      38.3          31.0          33.1          37.1          35.2           42.3           35.2          33.7
                                                 Average % Recovery =       91.17%       97.4%         81.5%        92.4%       103.4%          95.6%         119.8%          99.0%         82.3%

              >Q0783           P510,11       S&T QA/QC(K5119)P511                3.6        4.1           1.6           1.7          2.1           1.6            1.6             1.4          2.0
              >K5119           P510,11 S&T TISSUE P511 (SAMP)                    3.9        3.2           2.9           1.5          1.7           2.0            1.7             0.4          3.1
              >Q0785           P510,11         S&T SPK K5119 P511                3.6      23.9          25.1          26.3          21.4          22.5           22.9           20.3          23.1
                                                 Average % Recovery =       78.43%       73.3%         78.5%        88.6%         70.0%         73.1%          75.5%          71.1%         71.0%


              >Q0786             P512,3 @ QA/QC K5170 P512(BBSD)                 2.8        3.9           4.7           2.2          3.1           2.2            0.5             1.1          3.5
              >Q0788             P512,3        S&T SPK(K5170) P512               2.8      30.8          32.4          33.0          32.2          31.6           30.3           32.0          32.7
                                                 Average % Recovery =       80.42%       75.0%         77.2%        85.9%         81.3%         81.9%          83.0%          86.3%         81.3%





                                                               MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks, Spikes and QC Data




                                                                                                                                                                                                 2,3,4-TRI
                   FILE                 QC                 DESCRIPTION SAMPLE                NAPH 2-METHYL 1-METHYL BIPHENYL 2,6DIME ACENAPH- ACENAPH-                                           METHYL-
                                  BATCH                                         WEIGHT                      NAPH           NAPH                         NAPH       THYLENE             THENE        NAPH
                                                                                  (g dry)    (ppb)+         (ppb)+         (ppb)+       (ppb)+          (ppb)+            (ppb)        (ppb)+       (ppb)



               >QO789             P512.3 S&T QA/QC(K5242)P513                         1.3        5.4           4.5           2.8            1.9           4.3              2.2             3.0           7.7
               >K5242             P512.3 S&T TISSUE P513 (MBHI)                       1.4        5.4           4.9           3.7            3.3           4.8              2.7             4.1           9.2
               >Q0791             P512,3           S&T SPK(K5242) P513                1.3      62.2           73.2          70.0          59.2           58.2             51.5           61.9           64.9
                                                   Average % Recovery           80.580/6     75.2%          90.5%          88.0%        74.2%           70.6%          64.7%           76.6%          73.6%

               >K5039             P514,5 S&TTISSUE P514 (GBHR                         3.1        4.2           3.2           3.5            3.2           4.7              6.0             3.3           5.9
               >Q 1021            P514.5           S&T SPK K5039 P514                 3.1      31.1           31.8          34.2          32.1           32.8             32.8           31.7           35.0
                                                   Average % Recovery =         96.680,6     83.2%          88.2%          94.80A       89.2%           87.0%          82.9%           88.0%          89.8%

               >K5217             P514,5     S&T TISSUE P515 (BSSI)                   2.3        6.8           8.1           5.3            4.2          13.6              2.9             4.1          18.8
               >Q 1024            P514,5           S&T SPK K5217 P515                 2.3      42.5           44.1          45.8          38.9           45.0             35.8           38.2           51.2
                                                   Average % Recovery =         83.47%       81.9%          82.6%          92.8%        79.6%           72.0%          75.7%           78.2%          74.0%

               >K5057             P516,7 S&TTISSUE P516 (GBTD)                        3.2        5.1           7.5           2.9            3.0           9.0              2.8             1.5          10.3
               >QI027             P516,7           S&T SPK K5057 P516                 3.2      31.7           38.2          34.9          35.9           39.7             34.9           33.4           39.8
                                                   Average % Recovery           97.50%       85.9%          99.2%        103.1%         106.1%          99.1%          103.3%          102.7%         95.2%

               >K5255             P516,7    S&T TISSUE P517 ( PBIB                    3.7        4.8           3.2           2.5            2.1           3.7              2.5             5.9           3.3
               >Q 1039            P516.7,T QA/QC K5255 P517 JSPK)                     3.7      26.3           29.8          29.2          26.2           26.5             25.7           28.8           27.3
                                                   Average % Recovery =         91.32%       79.8%          98.7%          99.5%        89.6%           84.7%          86.3%           85.2%          89.3%

               >K5333             P518.9 S&T TISSUE P518 (TBMK)                       3.2        6.6          10.2           4.1            2.6           6.0              0.8             3.2           4.1
               >Q1042             P518,9 -T QA/QC K5333 P518 JSPK)                    3.1      30.5           36.6          34.6          32.6           33.1             24.4           31.8           31.0
                                                   Average % Recovery =         80.81%       72.2%          79.4%          92.9%        91.5%           82.4%          72.4%           87.3%          82.0%

               >K5249             P518,9 S&TTISSUEP519 (LPGO)                         2.0      27.3         297.2          201.5          57.8          912.9             27.4           67.3         1278.6
               >QI053             P518.9 -T QAIQC K5249 P519 (SPKI                    2.0      68.0         356.5          262.4          104.4         980.7             74.0           111.1        1348.5
                                                   Average % Recovery =         101.660/6    81.1%         115.5%        119.8%         92.6%          121.7%          93.0%           86.9%          125.7%

               >K5298             P520,1 S&TTISS NP520 (SAVvrB)                       1.7      31.9           68.6          39.2          30.8          165.8             14.8           42.3         374.0
               >Q1062             P520.1 AA S&T QA/QC K5298 JSPK)                     1.6      79.0         130.0          104.9          84.7          230.2             71.9           100.1        446.2
                                                   Average % Recovery =         102.040/6    74.5%          96.1%        104.1%         85.70h          97.2%          91.4%           91.3%          101.2%

               >K5346             P520,1 S&TTISS NP521 (TBCB)                         1.6      29.6           38.6          19.3            6.0          13.8              2.6             2.1           7.5
               >Q 1065            P520,1 A.A S&T QA/QC K5346 jSPK)                    1.6      82.5           99.3          84.8          66.4           75.6             64.1           66.7           70.3
                                                   Average % Recovery =         97.300,6     86.8%         100.0%        106.8%         98.1%          100.6%          99.7%           104.7%         102.0%





                                                               MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks, Spikes and QC Data




                                                                                                                                                                                                2,3,4-TRI
                   FILE                 gC                 DESCRIPTION SAMPLE                NAPH 2-METHYL           1-METHYL      BIPHENYL       2,6 DIME       ACENAPH-        ACENAPH-       METHYL-
                                  BATCH                                         WEIGHT                     NAPH           NAPH                        NAPH        THYLENE             THENE       NAPH
                                                                                  (g dry)    (ppb)+        (ppb)+         (ppb)+        (ppb)+        (ppb)+            (ppb)         (ppb)+       (ppb)


               >K5250             P522,3 S&T TISSUE P522 (LPGO)                      1.9       22.7        244.4          172.2          58.8         922.0             37.8            70.0        1287.2
               >Q 1108            P522.3 -.T QA/QC K5250 P522 (SPKI                  1.9       75.5        304.7          218.6         115.1         975.6             99.0            126.3       1374.7
                                                   Average % Recovery =         101.33%      98.5%         106.0%         82.1%        104.1%         73.00/6         113.9%          103.7%        125.9%

               >K5257           P526,7,9S&TTISSUESP529 (PBIB)                        2.8        5.0           3.5            2.3           4.7           5.9              5.1            8.0            4.4
               >QI114             P522.3 -T QA/QC K5257 P523 JSPKJ                   2.8       35.6          40.1          39.6          38.7           38.7            33.1            41.2          41.3
                                                   Average % Recovery =         91.07%       85.0%         101.7%         103.6%        94.5%         91.1%           77.9%           92.00/6       102.4%

               >K5347             P524.5)&TTISSUE NP524 (TBCB)                       2.5       16.2          27.6          14.6            4.6          13.5              2.1            1.7            5.0
               >QI117             P524.5 -T QA/QC K5347 P524 (SPK)                   2.5       52.4          67.9          55.7          47.3           46.7            40.2            41.0          44.4
                                                   Average % Recovery =         97.68%       90.0%         100.1%         102.0%       105.9%         82.4%           94.7%           97.7%         97.8%

               >K5170             P524.5 S&T TISSUE P525 (BBSD)                      2.9        4.7           3.0            2.8           3.1           3.7              0.5            1.3            3.5
               >Q1183             P524,5 -T QA/QC K5170 P525 JSPK)                   2.8       32.2          33.5          32.5          35.0           35.9            31.3            33.7          37.2
                                                   Average % Recovery =         94.93%       76.9%         85.2%          83.0%         89.1%         90.1%           86.1%           90.8%         94.2%

         00    >K5386           P526,7,9)&TnSSUES P526 (GBSC)                        2.1     147.1         1203.7         1093.8        590.4         2504.0            68.1          1078.7        2001.9
               >QI192           P526.7.9       S&T QA/QC(K5386)P526                  2.1     206.6         1198.8         1099.3        596.0         2562.9            114.2         1022.9        2042.9


               >Q1217           P526,7,9       S&T QA/QC(K5398)P527                  2.5       11.1          18.4          10.4            2.4           7.5              1.1            1.3            4.4
               >K5398           P526,7.9'5&T TISSUES P527 (BHKF)                     2.5       12.1          19.4          10.6            3.0           7.5              0.9            1.3            1.2
               >Q1219           P526,7.9         S&T SPK(K5398) P527                 2.5       48.1          61.5          53.1          46.9           51.3            39.9            43.5          45.4
                                                   Average % Recovery =         103.84%      88.7%         103.7%         104.9%       108.3%         108.0%          96.3%           104.3%        109.2%

               >Q1335           P526,7.9       S&T QA/QC(K5280)P529                  2.3        9.7          14.0            8.8           4.4           9.9              2.7            3.6            5.9
               >K5280           P526.7,9 S&T TISSUES P529 (CBSP)                     2.3        7.3          15.7            7.7           4.3           9.6              2.3            3.9            4.7
               >Q1337           P526,7.9         S&T SPK(K5280) P529                 2.2       40.3          52.2          46.1          44.5           49.9            38.8            42.6          45.6
                                                   Average % Recovery =         87.92%       73.7%         81.2%          85.8%         89.9%         90.0%           81.6%           86.5%         91.5%

               >Q1707                P531      S&T QA/QC K5135 P531                  1.6        9.5           6.5            2.3           1.6           4.0              1.3            1.9            3.7
               >K5135                P531      S&TTISS P531 (LMSP)                   1.6        7.6           7.4            2.6           2.3           3.1              2.0            0.9            1.5
               >Q 1709               P531        S&T K5135+MS P531                   1.6       65.4          77.3          74.4          62.6           52.9            59.7            54.5          59.2
                                                   Average % Recovery =         89.51%       90.9%         109.80A        112.7%        94.7%         78.4%           90.70/6         84.1%         90.7%





                                                         MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks, Spikes and QC Data




                                                                                                                                                                             2,3,4-TRI
                 FILE               QC               DESCRIPTION SAMPLE NAPH 2-METHYL 1-METHYL BIPHENYL 2.6 DIME ACENAPH- ACENAPH- METHYL-
                               BATCH                                    WEIGHT                    NAPH         NAPH                     NAPH THYLENE               THENE NAPH
                                                                          (g dry)   (ppb)+       (ppb)+       (ppb)+       (ppb)+       (ppb)+          (ppb)        (ppb)+     (ppb)










             DUPLICATE RE-EXTRACTIONS


             >K5003            P503.4 S&T TISSUE P503 (GBOB)                 2.6     10.1           4.8         3.9           2.7          2.7           4.4            6.6          3.0
             >K5003            P514,5         S&T TISSUE P514                2.5       5.4          3.4         3.9           1.6          3.3           4.8            6.6          3.8


             >K5009            P503.4&TTISSUEP503 (GBCR)                     2.4     10.8           7.7         5.3           3.1          6.3           4.6            7.0          6.3
             >K5009            P524.5         S&TTISSUE P525                 2.4       6.4          5.5         3.9           4.6          7.5           4.2            7.5          5.7


             >K5015            P503.4.&TTISSUEP503 (BRCL)                    2.6     10.7           7.2         3.5           2.5          2.7           8.7            1.2          4.5
             >K5015            P514,5         S&T TISSUE P514                2.5     10.1           6.3         3.7           6.7          6.6           9.4            1.9          7.7


             >K5039            P503,4 S&T TISSUE P503 (GBHR)                 3.1       8.8          5.3         3.5           2.5          4.7           1.8            2.3          5.8
             >K5039            P514.5         S&T TISSUE P514                3.1       4.2          3.2         3.5           3.2          4.7           6.0            3.3          5.9


             >K5075            P503.45&TIISSUEP503 (MBEM)                    2.2     10.2           4.5         3.8           2.7          2.9           1.0            1.9          3.0
             >K5075            P514.5         S&T TISSUE P514                2.2       6.3          3.2         4.3           2.4          3.9           2.4            0.7          2.2





                                                            MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks, Spikes and QC Data





                  FILE                QC                DESCRIPTION SAMPLE FLUORENE PHENAN ANTHRAC I-METHYL FLUORANTH PYRENE                                                    BENZ(a) CHRYSENE
                                 BATCH                                      WEIGHT                                                  PHENAN                                    ANTHRAC
                                                                              (g dry)         (Ppb)+       (ppb)+        (ppb)+       (ppb)+           (ppb)+        (ppb)+        (ppb)+     (ppb)+



              LABORATORY REFERENCE MATERIAL


              >W2639             P505.6            GERG STD. CHK 11              1.0          108.9        295.5            1.4       145.2              10.6         14.8           6.4           50.7
              >W2897             P507,8            GERG STD. CHK 11              1.0           99.1        269.9            1.4       177.3              11.1         14.9           5.7           47.2
              >W2961             P507,8            GERG M. CHK 11                1.0           88.8        250.9            0.6       178.5              10.6         11.9           5.0           47.1
              >W4149             P512,3            GERG SM. CHK 11               1.0           68.7        230.7            1.8       171.2              10.6         12.6           6.8           52.0
              >W4157             P514.5            GERG STD. CHK 11              1.0           77.4        187.8            1.2       129.3               9.8         11.2           5.0           39.7
              >W4229             P518,9            GERG STD. CHK 11              1.0           96.3        232.3            2.0       168.0              11.9         17.8           5.3           48.5
              >W4240             P520,1            GERG STD. CHK 11              1.0           87.6        249.2            2.5       149.4              13.2         14.8           4.6           42.5
              >W4272             P522,3            GERG STD. CHK 11              1.0           81.9        256.6            1.2       150.2              12.6         15.5           6.3           47.0
              >W4271             P524.5            GERG STD. CHK 11              1.0           71.4        226.3            2.8       150.9              10.3         14.6           5.8           40.9
              >W4407           P526,7,9            GERG STD. CHK 11              1.0          104.0        313.4            1.5       211.0              15.0         21.6           6.0           67.5
              >W4936                P528           GERG STD. CHK 11              1.0           84.8        219.0            1.0       134.5              11.0         13.0           5.9           51.6
              >W4807                P531           GERG SM. CHK 11               1.0           84.2        235.1            1.9       102.4              11.5         12.4           5.0           48.6
              >W5005                P532           GERG STD. CHK 11              1.0           78.6        201.8            2.2         97.0             12.4         13.6           5.4           44.1


              average                                                                          87.1        243.7            1.7       151.1              11.6         14.5           5.6           48.2
                                                                                              13.5%        13.8%         36.70/6      19.9%             11.9%        18.3%         10.9%          13.9%


              GERG chk 2 - avg. of 50                                                          82.9        231.1            1.8       152.5              11.0         13.0           5.9           45.2
                                                                                              15.0%        13.5%         45.5%        19.40/6           16.0%        17.3%         14.4%          11.4%
              BLANKS

              >QO685             P503.4         S&T BLANK P503                  10.0            0.2           0.@           0.1          0.2              0.1          0.2           0.1            0.1
              >QO688             P503A          S&T BLANK P504                  1010            0.1           0.2           0.0          0.1              0.1          0.1           0.0            0.0
              >Q0740             P505.6         S&T BLANK P505                  10.0            0.3           0.1           0.2          0.1              0.3          0.4           0.0            0.1
              >Q0743             P505,6         S&T BLANK P506                  10.0            0.3           0.3           0.1          0.6              0.2          011           0.1            0.1
              >Q0746             P507,8         S&T BLANK P507                  10.0            0.2           0.4           0.0          0.4              0.2          0.1           0.1            011
              >Q0749             P507,8         S&T BLANK P508                  10.0            0.1           0.3           0.1          0.2              0.1          0.3           0.1            0.1
              >Q0770            P510,11         S&T BLANK P5 10                 10.0            0.4           0.3           0.2          0.2              0.2          0.5           0.1            0.1
              >QO784            P510,11         S&T BLANK P511                  10.0            0.1           0.2           0.2          0.0              0.1          0.2           0.1            0.1
              >Q0787             P512,3         S&T BLANK P512                  10.0            0.2           0.1           0.1          0.1              0.2          0.2           0.1            0.1
              >Q0790             P512,3         S&T BLANK P513                  10.0            0.3           0.1           0.1          0.1              0.2          0.1           0.0            0.2
              >Q 1022            P514,5         S&T BLANK P514                  1010            0.3           0.4           0.2          1.1              0.2          0.3           0.2            0.1
              >Q 1025            P514,5         S&T BLANK P515                  10.0            0.4           0.3           0.1          0.3              0.1          0.2           0.1            0.4
              >g 1028            P516,7         S&T BLANK P516                  10.0            0.3           0.3           0.2          0.1              0.2          0.4           0.2            0.2
              >Q 1040            P516,7         S&T BLANK P517                  10.0            0.4           0.3           0.1          0.1              0.1          0.1           0.1            0.2
              >Q 1043            P518,9         S&T BLANK P518                  10.0            0.1           0.3           0.1          0.2              0.2          0.3           0.1            0.1





                                                            MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks, Spikes and QC Data





                  FILE                QC                DESCRIPTION SAMPLE             FLUORENE        PHENAN ANTHRAC 1-METHYL                 FLUORANTH          PYRENE        BENZ(a)    CHRYSENE
                                BATCH                                       WEIGHT                                                 PHENAN                                     ANTHRAC
                                                                             (g dry)         (ppb)+        (ppb)+        (ppb)+       (ppb)+           (ppb)+       (ppb)+        (ppb)+      (ppb)+


              >QI054            P518.9          S&T BLANK P519                  10.0            0.5          1.0           0.2           0.7             0.6           1.6           0.5            0.8
              >Q 1063           P520,1               S&T BLANK P520             10.0            0.2          0.5           0.2           0.4             0.5           0.6           0.1            0.2
              >QI066            P520.1               S&T BLANK P521             10.0            0.3          0.2           0.2           0.1             0.2           0.3           0.1            0.1
              >Q1109            P522,3         S&T BLANK P522                   10.0            0.4          1.0           0.2           0.7             0.5           1.4           0.4            1.0
              >QI115            P522,3         S&T BLANK P523                   10.0            0.1          0.3           0.1           0.2             0.2           0.3           0.1            0.1
              >QI118            P524.5     S&T TISSUE BLANK P524                10.0            0.3          0.3           0.1           0.4             0.2           0.3           0.2            0.1
              >Q1184            P524.5     S&T TISSUE BLANK P525                10.0            0.2          0.3           011           0.2             0.1           0.1           0.1            0.1
              >Q1218           P526,7.9        S&T BLANK P527                   10.0            0.1          0.3           0.1           0.1             0.3           0.2           0.1            0.0
              >Q1336           P526,7.9        S&T BLANK P529                   10.0            0.1          0.3           0.1           0.1             0.2           0.2           0.1            0.1
              >Q1258               P528   S&T TISSUE BLANK P528                 10.0            0.1          0.3           0.0           0.1             0.1           0.2           0.0            0.1
              >Q 1708             P531 S&T TISSUE BLANK P531                    10.0            0.2          0.8           0.1           0.3             0.2           0.2           0.1            0.2


              average                                                                           0.2          0.4           0.1           0.3             0.2           0.3           0.1            0.2
                                                                                             46.9%         63.3%        51.5%         88.4%            64.6%       105.00/0       89.4%         126.3%
              NIST SRM 1974 - TISSUE SAMPLE
              Values for SRM 1974                                                              12.0         45.0           6.1         19.0            272.0        276.0          37.0          124.0


              >QI023            P514.5               S&T NIST P514              0.60           13.2         47.4          22.5         19.4            246.8        247.3          34.3          118.4
              >Q 1026           P514,5               S&T NIST P515              0.60            6.9         37.1          15.3         26.7            195.0        189.2          33.1          124.0
              >QI041            P516.7               S&T NIST P517              0.60           10.5         35.7          11.6         18.7            260.3        249.3          28.3          132.4
              >Q1044            P518.9               S&T NIST P518              0.60           11.1         53.3           9.2         17.6            351.1        332.8          44.4          181.9
              >QI055            P518,9               S&T NIST P519              0.60           11.6         39.4           9.0         13.6            199.8        185.7          29.7          109.1
              >Q1064            P520.1                 S&T NIST P520            0.60            7.7         26.9           8.2         14.1            187.5        199.9          28.2          104.1
              >QI067            P520,1                 S&T NIST P521            0.60            8.3         42.2          13.6         22.2            310.4        285.2          35.7          138.5
              >Q1110            P522.3               S&T NIST P522              0.60           16.6         58.1          24.0         34.4            303.6        292.6          50.5          230.8
              >Q1119            P524,5                 S&T NIST P524            0.60           12.6         38.4          14.2         23.7            235.1        221.5          33.7          125.3
              >Q 1185           P524,5                 S&T NIST P525            0.60            8.0         27.8           8.6         12.3            195.2        185.6          26.3          102.0

              average                                                                          10.7         40.6          13.6         20.3            248.5        238.9          34.4          136.7
                                                                                             26.9%         23.5%        39.6%         31.7%            21.9%        20.5%         21.1%          27.9%


              REPLICATES AND SPIKED SAMPLES


              >QO684            P503,4      S&T QA/QC(K5039)P503                  3.1           2.7          6.5           5.1           4.6             8.2           8.8           1.6            4.5
              >K5039            P503.4 kT TISSUE P503 (GBHR)                      3.1           3.3          8.1           5.1           4.2             8.6           8.5           1.9            4.3



              >QO687            P503.4      S&T QA/QC(K5159)P504                  2.7           2.4          7.7           2.1           3.4             5.1           7.6           1.6            2.9



    mm@m@mm@mm mmm mmm
                                                               MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks, Spikes and QC Data




                   FILE                QC                  DESCRIPTION SAMPLE               FLUORENE        PHENAN ANTHRAC I-METHYL                    FLUORANTH         PYRENE BENZ(a)             CHRYSENE
                                  BATCH                                        WEIGHT                                                     PHENAN                                       ANTHRAC
                                                                                 (g dry)         (ppb)+         (ppb)+        (ppb)+        (ppb)+            (ppb)+        (ppb)+        (ppb)+        (ppb)+


               >K5159             P503.4    S&TTISSUE P504 (VBSP)                    2.7             2.4           7.2           2.0            4.1              5.0            7.7           1.2             2.7
               >QO689             P503.4         S&T SPIKE(K5159)P504                2.7           40.2          44.7           27.1          52.3              48.8          47.8          37.6            40.2
                                                   Average % Recovery =        102.71%           102.2%        101.2%         85.5%        130.2%            118.1%         108.3%        98.2%           101.2%

               >QO739             P505,6       S&T QA/QC(K5222)P505                  2.1             8.6         38.4           12.1          16.0              76.9          62.7          26.5            45.3
               >K5222             P505.6 S&T TISSUE P505 (MSPC )                     2.1           11.5          36.9           11.2          11.0              78.8          67.5          23.5            46.7
               >Q0741             P505.6         S&T SPIKE(K5222)P505                2.2           78.1          77.4           41.9          60.0            111.3           99.5          76.1            96.6
                                                   Average % Recovery =        109.33%           132.9%         88.9%         78.2%        106.4%             73.2%         71.8%         114.6%          109.8%

               >Q0742             P505,6       S&T QA/QC(K504O)P506                  3.3             4.9           8.0           4.8            8.4              7.7            7.4           1.9             5.1
               >K5040             P505,6 S&T TISSUE P506 (GBHR)                      3.3             4.9           7.2           5.9            6.3              7.1            6.8           9.3             7.6
               >Q0744             P505.6         S&T SPIKE(K504O)P506                3.3           36.5          31.0           23.5          29.7              26.1          26.1          24.7            36.4
                                                   Average % Recovery =        86.02%            104.6%         78.70/6       68.0%         77.5%             71.1%         72.6%         96.2%           95.1%

               >QO745             P507.8       S&T QA/QC K5118 P507                  3.4             1.6           5.4           3.2            3.4              1.2            1.6           1.2             2.5
        c.n    >K5118             P507,8 S&T TISSUE P507 (SAMP)                      3.4             1.8           3.6           2.7            2.4              0.9            1.8           1.1             2.9
        t,,D   >Q0747             P507,8         S&T SPK K5118 P507                  3.4           28.7          29.3           25.0          34.2              28.9          28.0          26.6            26.8
                                                   Average % Recovery =        85.84%            90.6%          86.8%         75.3%        107.7%             94.9%         88.6%         86.1%           80.7%

               >Q0748             P507,8       S&T gA/QC K5064 P508                  2.7             2.6           6.1          12.3            4.6             13.5          15.8            3.1           13.7
               >K5064             P507.8 S&T TISSUE P508 (GBYC)                      2.7             1.5           7.2          12.7          13.9              12.0          17.8            2.8           14.4
               >gO750             P507,8         S&T SPK K5064 P508                  2.7           31.8          36.8           39.4          51.1              43.9          47.0          30.3            42.6
                                                   Average % Recovery =        82.64%            82.7%          81.2%         73.4%        102.2%             87.6%         80.5%         75.1%           77.9%

               >QO769           P510.11        S&TQA/QC(K5065)P510                   3.0             2.2           7.6           9.1            5.6             12.2          21.5            3.1           14.6
               >K5065           P510.11 S&TTISSUEP510 (GBYC)                         3.0             1.9           6.4           9.3            5.0             10.2          20.6            3.2           15.6
               >Q0771           P510,11          S&T SPK(K5065) P5 10                3.0           32.1          39.6           36.8          40.2              40.6          47.8          29.9            47.5
                                                   Average % Recovery =        91.170/6          91.7%         100.80/0       84.3%        107.1%             92.9%         84.1%         81.2%           98.0%

               >QO783           P510,11        S&T QA/QC(K5119)P511                  3.6             1.4           3.2           3.0            3.4              0.8            1.8           0.8             1.1
               >K5119           P510.11    S&T TISSUE P511 (SAMP)                    3.9             1.7           3.6           3.2            2.7              0.8            1.7           1.0             1.2
               >QO785           P510,11          S&T SPK K5119 P511                  3.6           21.9          24.0           22.0          25.7              24.7          24.4          22.2            22.9
                                                   Average % Recovery =        78.43%            72.1%          72.1%         66.4%         81.6%             85.1%         80.7%         75.5%           77.3%



               >QO786             P512,3'QA/QC K5170 P512(BBSD)                      2.8             2.0           6.1           1.2            2.0              3.6            4.5           0.4             2.0
               >QO788             P512.3         S&T SPK(K5170) P512                 2.8           32.4          32.5           27.6          32.3              31.4          30.5          32.3            29.5
                                                   Average % Recovery =        80.42%            84.9%          73.4%         73.8%         84.5%             77.3%         72.5%         89.0%           76.7%



                                                               mmm MM MM MM M M @m
                                                              MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks, Spikes and QC Data



                 FILE                  QC                  DESCRIPTION SAMPLE FLUORENE PHENAN ANTHRAC 1-METHYL FLUORANTH                                                   PYRENE        BENZ(a) CHRYSENE
                                  BATCH                                        WEIGHT                                                     PHENAN                                       ANTHRAC
                                                                                 (g dry)              (ppb)+       (ppb)+          (ppb)+      (ppb)+           (ppb)+           (ppb)+       (ppb)+    (ppb)+


               >Q0789             P512,3 S&T QA/QC(K5242)P513                         1.3             4.1          15.2            7.8         12.0             114.3            125.7        19.6              43.3
               >K5242             P512,3 S&TTISSUE P513 (MBHI)                        1.4             4.6          16.0            8.2         11.8             106.0            119.3        18.1              42.4
               >Q0791             P512,3         S&T SPK(K5242) P513                  1.3             60.3         69.9            59.1        67.3             168.8            196.5        82.2              111.3
                                                   Average % Recovery =          80.58%               73.8%        70.70/6         67.2%       73.1%            77.1%            95.6%        84.2%             89.0%
               >K5039             P514.5 S&T TISSUE P514 (GBHR)                       3.1             4.3          6.8             9.0           2.4               7.3           7,9            1.7             4.5
               >Q 1021            P514.5           S&T SPK K5039 P514                 3.1             34.6         35.0            33.4        37.7              36.2            34.3         30.8              35.3
                                                   Average % Recovery =          96.68%               93.8%        87.0%           75.4%       109.2%           89.2%            81.8%        89.7%             95.0%
               >K5217             P514,5    S&TTISSUEP515 (BSSI)                      2.3             6.3          15.2            5.7         11.4              29.0            34.7           6.3             22.2
               >Q 1024            P514.5           S&T SPK K5217 P515                 2.3             40.6         51.2            34.3        52.9              65.4            72.2         43.9              62.1
                                                   Average % Recovery =          83.47%               78.6%        82.2%           65.6%       95.1%            83.0%            85.2%        86.1%             91.2%
               >K5057             P516,7 S&TTISSUE P516 (GBTD)                        3.2             2.6          10.0            9.4           9.8               9.7           15.4           2.4             13.8
        ul     >Q 1027            P516,7           S&T SPK K5057 P516                 3.2             33.6         42.7            35.8        43.8              41.7            42.0         27.6              39.6
                                                   Average % Recovery =          97.500/6             99.8%        105.60/6        85.1%       109.5%           103.3%           85.7%        81.4%             83.3%
               >K5255             P516.7    S&T TISSUE P517 (PBIB)                    3.7             7.3          19.9            13.3          2.4             30.3            17.0           4.5             8.3
               >Q 1039            P516.7,.T QA/QC K5255 P517 (SPK)                    3.7             30.7         45.6            33.3        33.6              59.5            43.3         27.2              31.1
                                                   Average % Recovery =          91.32%               87.2%        95.7%           74.1%       116.1%           108.80/6         97.8%        84.5%             84.9%
               >K5333             P518,9 S&T TISSUE P518 (TBMK)                       3.2             5.2          23.7            1.7           3.4             22.7            9.7            1.8             7.3
               >Q 1042            P518,9 -T QA/QC K5333 P518 JSPK)                    3.1             31.6         49.7            25.7        32.2              50.7            35.8         25.6              39.2
                                                   Average % Recovery =          80.81%               80.3%        76.2%           73.6%       87.8%            82.3%            78.3%        72.8%             96.9%
               >K5249             P518,9 S&TTISSUEP519 (LPGO)                         2.0             176.8        632.8           94.3        452.5            430.4            1333.2       395.9             552.6
               >Q 1053            P518,9,.T QA/QC K5249 P519 JSPK)                    2.0             230.6        674.7           156.2       519.4            498.0            1371.2       438.5             605.4
                                                   Average % Recovery =          101.66%              106.0%       77.5%           122.8%      129.3%           115.8%           62.7%        81.1%             100.1%
               >K5298             P520.1 S&TTISSNP520 (SAWB)                          1.7             99.0         462.4           70.3        566.2            895.8            641,5        156.4             368.4
               >Q 1062            P520,1 AA S&T QA/QC K5298 (SPKI                     1.6             159.3        545.8           151.6       638.2            1010.6           738,5        204.8             455.5
                                                   Average % Recovery =          102.04%              93.2%        115.80A         128.0036    93.2%            149.1%           130.5%       71.8%             125.60A
               >K5346             P520,1 S&TTISS NP521 (TBCB)                         1.6             5.3          27.3            2.1           4.4             23.7            13,6           1.3             6.5
               >Q 1065            P520,1 AA S&T QA/QC K5346 (SPK)                     1.6             71.5         78.9            48.2        73.1              86.2            69.2         55.2              63.1
                                                   Average % Recovery =          97.300/6             107.4%       84.70A          74.9036     111.5%           102.3%           90.6%        87.3%             92.0%



     M@m MM M @Mmm M M MM on M MM
                                                                MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks, Spikes and QC Data




                   FILE                 QC                  DESCRIPTION SAMPLE                FLUORENE         PHENAN ANTHRAC I-METHYL                    FLUORANTH           PYRENE         BENZ(a)    CHRYSENE
                                   BATCH                                         VVEIGHT                                                     PHENAN                                        ANTHRAC
                                                                                   (g dry)          (ppb)+        (ppb)+         (ppb)+         (ppb)+            (ppb)+        (ppb)+         (ppb)+       (ppb)+


                >K5250             P522.3 S&TTISSUEP522 (LPGO)                         1.9          190.2         558.8            83.6         545.3             359.2         1311.2         457.9           698.4
                >Q 1108            1?522@3 -T QAIQC K5250 P522 (SPKI                   1.9          236.3         609.8          120.5          591.3             406.9         1402.7         522.6           758.8
                                                    Average % Recovery =          101.33%           81.0%         79.2%          66.7%          70.1%             79.0%         132.7%        107.90/6         92.7%

                >K5257           P526,7.9 S&T TISSUES P529 (PBIB)                      2.8             8.9          26.3           15.0            4.0              37.6          22.7            5.5             9.5
                >Q1114             P522.3 -T QA/QC K5257 P523 jSPK)                    2.8            42.6          65.6           38.4          46.7               82.7          62.8           34.8            39.8
                                                    Average % Recovery =          91.07%            93.5%         108.8%         64.9%        118.6%            124.7%          111.1%         81.2%           84.1%

                >K5347             P524,5;&TT1SSUE NP524 (TBCB)                        2.5             4.1          17.2            1.0            3.5              15.7            9.4           1.9             5.8
                >QI117             P524.5 -T QA/QC K5347 P524 (SPK)                    2.5            43.4          63.2           26.4          53.7               62.3          51.5           38.6            46.7
                                                    Average % Recovery =          97.680,6          97.50,6       114.3%         63.0%        124.5%            115.6%          104.7%         91.1%          101.60/6

                >K5170             P524.5 S&T TISSUE P525 (BBSD)                       2.9             2.7           6.7            1.7            3.1                4.9           4.9           1.4             2.6
                >Q 1183            P524.5 -T QA/QC K5170 P525 JSPK)                    2.8            35.1          42.3           43.7          39.2               40.8          38.1           32.0            33.1
                                                    Average % Recovery -          94.93%            90.6%         99.3%         117.7%        101.2%            100.2%          92.6%          85.8%           85.2%

                >K5386           P526,7,9;&T TISSUES P526 (GBSC)                       2.1          1074.9        1699.8         263.7          436.7             841.7         1803.3         395.5           933.8
                >Q 1192          P526.7.9       S&T QA/QC(K5386)P526                   2.1          943.7         1792.5         301.9          571.0             953.6         2012.5         420.0           969.5



                >Q 1217          P526.7.9       S&T QA/QC(K5398)PS27                   2.5             1.4           3.9            1.8            2.0                8.5           8.6           2.6             4.8
                >K5398           P526.7,95&TTISSUES P527 (BHKF)                        2.5             0.9           4.2            1.2            1.2                7.4           8.2           2.5             4.7
                >Q 1219          P526.7,9         S&T SPK(K5398) P527                  2.5            43.4          48.9           32.8          50.1               56.8          53.5           41.0            47.6
                                                    Average % Recovery =         103.840/6          104.8%        110.1%         77.9%        120.6%            122.0%          111.70/6       95.0%          106.0%

                >Q1335           P526,7.9       S&T QA/QC(K5280)P529                   2.3             5.7          29.1            6.3            9.6              51.5          39.0           16.9            39.9
                >K5280           P526.7.9 S&T TISSUES P529 (CBSP)                      2.3             5.3          27.3            6.0            8.5              47.3          40.3           19.2            44.2
                >Q1337           P526,7.9         S&T SPK(K5280) P529                  2.2            45.4          68.0           39.2          53.0             101.7           86.3           55.5            88.4
                                                    Average % Recovery =          87.92%            89.70A        90.2%          74.3%          99.5%           120.3%          101.70/6       80.6%           97.7%

                >Q 1707               P531      S&T QA/QC K5135 P531                   1.6             1.3           7.9            1.8            3.4              11.3            5.0           1.2             4.2
                >K5135                P531      S&T TISS P531 (LMSP)                   1.6             1.7          10.1            1.4            6.3              16.3            7.3           1.0             4.3
                >Q 1709               P531        S&T K5135+MS P531                    1.6            51.6          66.9           44.2          64.2               68.9          59.3           50.2            69.4
                                                    Aver-age % Recovery =         89.51%            78.5%         89.2%          67.1%          91.0%             82.8%         81.7%          77.3%          102.2%





                                                        MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks, Spikes and QC Data





                FILE               QC                DESCRIPTION SAMPLE FLUORENE PHENAN ANTHRAC 1-ME1'HYL FLUORANTH PYRENE                                         BENZ(a) CHRYSENE
                               BATCH                                   WEIGHT                                             PHENAN                                  ANTHRAC
                                                                        (g dry)        (ppb)+       (ppbl+      (ppbl+       (ppb)+          (ppb)+      (ppb)+       (ppb)+     (ppb)+









              DUPLICATE RE-EXTRACTIONS


              >K5003           P503AS&T TISSUE P503 (GBOB)                 2.6            4.0         1.9         28.6         16.4            5.8       164.7         139.1         42.0
              >K5003           P514.5        S&T TISSUE P514               2.5            4.5         1.4         22.3         11.9            10.8      138.9         106.7         26.2

              >K5009           P503,4 &T TISSUE P503 (GBCR)                2.4            5.1         2.0         16.3         11.7            5.5       111.3         68.1          12.8
              >K5009           P524.5        S&T TISSUE P525               2.4            6.6         1.8         18.4          7.4            5.3       114.7         63.2          10.6

              >K5015           P503.4-&TTISSUEP503 (BRCL)                  2. 6           1.5         0.9          7.9          5.0            9.2          16.7       21.1            4.3
        ul    >K5015           P514,5        S&T TISSUE P514               2.5            3.2         1.1          5.9          3.8            3.7          11.7       13.9            2.3
        Cn    >K5039           P503A S&T TISSUE P503 (GBHR)                3.1            3.3         1.2          8.1          5.1            4.2          8.6         8.5            1.9
              >K5039           P514.5        S&T TISSUE P514               3.1            4.3         0.9          6.8          9.0            2.4          7.3         7.9            1.7

              >K5075           P503,45&TIISSUEP503 (MBEM)                  2.2            3.0         0.9          8.0          1.9            1.9          6.8         5.4            0.9
              >K5075           P514.5        S&T TISSUE P514               2.2            2.8         1.2          4.2          3.5            2.7          2.5         2.9            1.4





                                                               MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks, Spikes and QC Data





                   F1LE                 QC                 DESCRIPTION SAMPLE                   BENZO(b)          BENZO(k) BENZO(e) BENZO(a) PERYLENE INDENO-                                 DIBENZ BENZO(ghl)
                                   BATCH                                       WEIGHT FLUORANTH                FLUORANTH PYRENE PYRENE                                         PYRENE ANTHRAC PERYLENE
                                                                                  (g dry)             (ppb)              (ppb)        (ppb)+        (ppb)+          (ppb)+          (ppb)        (ppb)+      (ppb)



                LABORATORY REFERENCE MATERIAL


                >W2639             P505,6             GERG STI). CHK 11               1.0              5.5                3.6          14.9            2.1             2.2            0.9           0.9            4.0
                >W2897             P507,8             GERG STD. CHK 11                1.0              5.6                4.2          12.8            2.3             2.8            1.0           1.1            4.0
                >W2961             P507,8             GERG STD. CHK 11                1.0              6.1                4.1          11.4            2.3             2.5            1.0           2.0            3.2
                >W4149             P512,3             GERG STD. CHK 11                1.0              4.6                4.7          11.4            1.9             2.0            0.9           1.8            3.4
                >W4157             P514.5             GERG STD. CHK 11                1.0              3.1                5.2           9.7            2.4             0.7            1.0           4.1            5.0
                >W4229             P518.9             GERG STD. CHK 11                1.0              5.5                4.7          10.1            2.2             1.7            0.7           2.2            3.3
                >W4240             P520,1             GERG STD. CHK 11                1.0              5.0                5.1          10.1            1.9             1.9            0.8           2.3            4.1
                >W4272             P522,3             GERG STD. CHK 11                1.0              5.6                5.8          11.4            2.3             2.1            1.3           2.4            3.9
                >W4271             P524.5             GERG SM. CHK 11                 1.0              5.7                4.6          12.4            3.1             2.6            0.9           2.3            3.6
                >W4407           P526.7,9             GERG STD. CHK 11                1.0              5.2                5.2          15.5            3.1             2.8            0.8           0.9            3.8
                >W4936                P528            GERG STD. CHK 11                1.0              3.6                4.2           9.9            2.0             1.2            1.1           1.4            4.7
                >W4807                P531            GERG STI). CHK 11               1.0              3.5                4.8          10.2            1.9             1.4            0.8           1.4            3.2
                >W5005                P532            GERG STD. CHK 11                1.0              4.3                5.0          10.9            1.9             1.0            1.5           1.2            3.5


                average                                                                                4.9                4.7          11.6            2.3             1.9            1.0           1.8            3.8
                                                                                                     18.9%              11.8%         15.6%          17.70/6        34.7%          21.0%         45.1%           14.1%


                GERG chk 2 - avg. of 50                                                                4.5                4.8          11.5            2.5             2.0            1.1           2.2            4.4
                                                                                                     19.7%              21.0%         14.6%         37.7%           27.1%          74.4%         31.9%          22.1%
                BLANKS


                >QO685             P503.4          S&T BLANK P503                   10.0               0.0                0.0           0.1            0.1             0.4            0.1           0.1            0.1
                >QO688             P503,4          S&T BLANK P504                   10.0               0.0                0.0           0.1            0.1             0.0            0.0           0.1            0.0
                >Q0740             P505,6          S&T BLANK P505                   10.0               0.1                0.1           0.1            0.1             0.2            0.1           0.1            0.1
                >Q0743             P505,6          S&T BLANK P506                   10.0               0.1                0.1           0.1            0.1             0.2            0.1           0.1            0.1
                >Q0746             P507.8          S&T BLANK P507                   10.0               0.1                0.0           0.1            0.1             0.1            0.1           0.2            0.1
                >Q0749             P507.8          S&T BLANK P508                   10.0               0.1                0.1           0.0            0.1             0.2            0.1           0.0            011
                >Q0770            P510,11          S&T BLANK P5 10                  10.0               0.1                0.1           0.2            0.0             0.2            0.2           0.2            0.1
                >Q0784            P510.11          S&T BLANK P511                   10.0               0.1                0.0           0.0            0.0             0.3            0.1           0.1            0.1
                >Q0787             P512,3          S&T BLANK P512                   10.0               0.1                0.1           0.1            0.1             1.6            0.1           0.1            0.1
                >Q0790             P512.3          S&T BLANK P513                   10.0               0.0                0.0           0.1            0.0             0.8            0.1           0.1            0.0
                >Q1022             P514,5          S&T BLANK P514                   10.0               0.2                0.3           0.2            0.4             0.1            0.3           0.1            0.4
                >Q1025             P514.5          S&T BLANK P515                   10.0               0.2                0.3           0.2            0.2             0.6            0.4           0.5            0.2
                >Q 1028            P516,7          S&T BLANK P516                   10.0               0.1                0.1           0.1            0.0             1.0            0.1           0.1            0.1
                >Q 1040            P516.7          S&T BLANK P517                   10.0               0.1                0.1           0.0            0.1             0.3            0.1           0.1            0.1
                >Q 1043            P518,9          S&T BLANK P518                   10.0               0. 1               0.1           0.1            0.1             0.3            0.1           0.1            0.0





                                                                MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks, Spikes and QC Data





                   IFILE                QC                  DESCRIPTION SAMPLE                  BENZO(b)           BENZO(k)       BENZO(e)      BENZO(a)       PERYLENE        INDENO-         DIBENZ     BENZO(gW)
                                   BATCH                                        WEIGHT       FLUORANTH          FLUORANTH          PYRENE         PYRENE                        PYRENE      ANTHRAC       PERYLENE
                                                                                  (g dry)             (ppb)              (ppb)        (ppb)+         (ppb)+         (ppb)+          (ppb)        (ppb)+       (ppb)


                >QI054             P518.9          S&T BLANK P519                   10.0               0.3                 0.1           0.3           0.1             0.7           0.1            0.1             0.1
                >Q1063             P520.1               S&T BLANK P520              10.0               0.1                 0.2           0.1           0.1             0.6           0.1            0.1             0.1
                >Q1066             P520.1               S&T BLANK P521              10.0               0.1                 0.1           0.1           0.0             0.3           0.1            0.1             0.1
                >QlIO9             P522.3          S&T BLANK P522                   10.0               0.3                 0.2           0.3           0.0             0.3           0.1            0.1             0.2
                >QI115             P522,3          S&T BLANK P523                   10.0               0.0                 0.0           0.0           0.0             0.0           0.1            0.1             0.1
                >Q1118             P524.5     S&T TISSUE BLANK P524                 10.0               0.1                 0.1           0.1           0.0             0.1           0.1            0.1             0.1
                >QI184             P524,5     S&T TISSUE BLANK P525                 10.0               0.0                 0.1           0.0           0.0             0.1           0.1            0.1             0.0
                >Q 1218           P526,7.9         S&T BLANK P527                   10.0               0.1                 0.1           0.0           0.0             0.2           0.0            0.1             0.1
                >Q 1336           P526,7.9         S&T BLANK P529                   10.0               0.0                 0.0           0.0           0.0             0.1           0.1            0.1             0.0
                >Q 1258               P528   S&T TISSUE BLANK P528                  10.0               0.0                 0.0           0.1           0.0             0.3           0.2            0.1             0.1
                >Q1708               P531 S&T TISSUE BLANK P531                     10.0               0.1                 0.0           0.1           0.0             0.2           0.1            0.1             0.1


                average                                                                                0.1                 0.1           0.1           0.1             0.4           0.1            0.1             0.1
                                                                                                    82.4%               83.9%         82.5%        110.6%           98.1%         73.2%          78.0%           90.3%
                NIST SRM 1974 - MSSUE SAMPLE
         LTI    Values for SRM 1974                                                                   52.3               35.0          81.0           18.6             8.5          14.6            2.8           20.0

                >Q 1023            P514.5               S&T NIST P514               0.60              52.8               27.5          84.8           17.7             8.4          24.5            6.4           32.6
                >QI026             P514.5               S&T NIST P515               0.60              44.3               25.4          69.7           13.1             5.6          14.3            4.0           22.4
                >Q 1041            P516.7               S&T NIST P517               0.60              32.5               19.5          57.9           12.1             10.1          7.5            1.2           11.4
                >Q 1044            P518,9               S&T NIST P518               0.60              46.5               35.9          97.1           17.8             10.1         15.6            3.4           20.9
                >QI055             P518,9               S&T NIST P519               0.60              38.4               27.5          57.4            9.9             4.8          10.3            2.9           12.1
                >QI064             P520.1                  S&T NIST P520            0.60              47.2               23.5          59.0           13.1             5.7          14.8            4.3           21.2
                >Q1067             P520.1                  S&T NIST' P521           0.60              61.4               35.7          69.2           15.2             7.7          14.8            4.1           20.8
                >QlII0             P522.3               S&T NIST P522               0.60              64.6               48.6          111.6          18.1             15.2         19.6            5.6           29.7
                >QI119             P524.5                  S&T NIST P524            0.60              43.0               32.3          69.1           12.4             7.4          13.0            4.2           15.5
                >Q 1185            P524.5                  S&T NIST P525            0.60              33.2               32.1          48.1            8.4             5.0           8.0            2.2           11.6

                average                                                                               46.4               30.8          72.4           13.8             8.0          14.2            3.8           19.8
                                                                                                     22.0%              25.2%         26.0%         23.1%           37.9%         34.2%          37.3%           35.2%


                REPLICATES AND SPIKED SAMPLES


                >QO684             P503,4      S&T QA/QC(K5039)P503                   3.1              1.6                 1.6           2.6           2.5             2.9           0.6            0.5             0.8
                >K5039             P503,4 'kT TISSUE P503 (GBHR)                      3.1              1.9                 1.2           2.4           2.0             2.4           0.6            0.3             1.2



                >Q0687             P503A       S&T QA/QC(K5159)P504                   2.7              0.8                 1.3           1.4           0.5             3.8           0.4            0.2             0.9



    mm@ mmm MM M MM M M M@m MM
                                                      MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks, Spikes and QC Data




                 FILE             QC               DESCRIPTION SAMPLE             BENZO(b)        BENZO(k)    BENZO(e)    BENZO(a)    PERYLENE      INDENO-       DIBENZ   BENZO(ghl)
                              BATCH                                 WEIGHT     FLUORANTH       FLUORANTH       PYRENE      PYRENE                    PYRENE    ANTHRAC     PERYLENE
                                                                     (g dry)          (ppb)           (ppb)     (ppb)+       (ppb)+       (ppb)+        (ppb)     (ppb)+      (ppb)


             >K5159           P503,4  S&Tf1SSUE P504 (VBSP)             2.7            0.6              0.6         1.5         0.3          3.4         0.3         0.1           0.6
             >QO689           P503,4      S&T SPIKE(K5159)P504          2.7           40.2            41.0        48.6        28.0          36.9        49.5        46.4           47.1
                                            Average % Recovery =    102.71%         106.8%          109.0016    106.8%       75.00/6      90,6%       125.0%      96.7%         99.2%

             >Q0739           P505,6    S&T QA/QC(K5222)P505            2.1           10.8            10.4        14.8          3.0          3.0         0.6         0.2           0.8
             >K5222           P505,6 S&T TISSUE P505 ( MSPC )           2.1           15.2              8.1       13.9          1.8          5.7         0.8         0.2           1.4
             >Q0741           P505,6      S&T SPIKE(K5222)P505          2.2           64.4            56.9        75.9        52.9          50.8        62.8        53.0           56.9
                                            Average % Recovery =    109.33%         106.80A         105.8%      113.0036     110.4%       97.6%       125.8%      114.2%        119.9%

             >Q0742           P505,6    S&T QA/QC(K504O)P506            3.3            2.2              1.3         3.1         0.6          3.0         0.4         0.1           0.5
             >K5040           P505,6 S&T TISSUE P506 ( GBHR)            3.3            1.9              0.9         2.8         0.8          2.4         0.4         0.5           0.6
             >Q0744           P505.6      S&T SPIKE(K504O)P506          3.3           25.4            23.5        28.4        23.3          25.9        22.1        21.3           24.5
                                            Average % Recovery =    86.02%          77.5%           74.4%       84.6%        74.1%        77.8%       71.6%       69.9%         78,8%

             >Q0745           P507.8    S&T QA/QC K5118 P507            3.4            1.0              0.7         0.8         0.8          1.7         0.3         0.4           0.5
             >K5118           P507,8 S&T TISSUE P507 ( SAMP             3.4            1.4              0.4         0.8         0.6          1.3         0.2         0.2           0.4
             >Q0747           P507,8      S&T SPK K5118 P507            3.4           28.5            21.8        29.2        23.3          26.5        22.1        23.6           23.3
                                            Average % Recovery      85.84%          91.5%           72.6%       95.8%        76.7%        85.1%       74.0%       79.1%         77,7%

             >Q0748           P507.8    S&T QA/QC K5064 P508            2.7            5.0              2.1         6.4         0.9          2.1         1.4         0.7           1.6
             >K5064           P507,8 S&T TISSUE P508 (GBYC              2.7            4.7              3.1         8.0         1.1          3.2         0.7         0.7           1.4
             >Q0750           P507,8      S&T SPK K5064 P508            2.7           36.7            32.7        38.8        27.9          31.6        33.9        33.2           27.3
                                            Average % Recovery      82.64%          87.6%           81.0%       84.5%        73.3%        77.9%       90.7%       88.7%         70.8%

             >Q0769         P510,11     S&TQA/QC(K5065)P510             3.0            3.8              3.1         7.2         0.8          3.1         0.8         0.7           1.8
             >K5O65         P510.11 S&TTISSUEP510 (GBYC)                3.0            3.3              3.6         7.4         0.8          3.6         1.0         0.3           2.2
             >Q0771         P510,11       S&T SPK(K5065) P510           3.0           32.0            29.9        37.4        25.5          29.9        32.5        28.4           29.3
                                            Average % Recovery =    91.170,6        87.0%           79.9%       91.7%        75.2%        79.9%       95.6%       85.0%         82.1%

             >Q0783         P510,11     S&T QA/QC(K5119)P511            3.6            1.0              0.1         0.7         0.3          1.2         0.3         0.4           0.3
             >K5119         P510,11  S&TTISSUE P511 (SAMP)              3.9            0.4              0.3         0.4         0.2          0.6         0.5         0.3           0.5
             >g0785         P510,11       S&T SPK K5119 P511            3.6           20.9            21.5        25.0        17.9          21.2        29.8        27.3           26.9
                                            Average % Recovery =    78.43%          73.5%           75.9%       88.0%        63.4%        73.3%       105.0%      96.7%         94.5%


             >Q0786           P512.3'QA/QC K5170 P512(BBSD)             2.8            0.5              0.5         0.4         0.4          2.5         0.3         0.1           0.4
             >Q0788           P512,3      S&T SPK(K5170) P512           2.8           29.8            32.9        28.2        21.4          30.9        28.8        29.2           35.4
                                            Average % Recovery =    80.42%          82.0%           90.4%       77-50A       58.7%        79.3%       79.5%       81.2%         97.5%





                                                               MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks, Spikes and QC Data




                   FILE                 QC                 DESCRIPTION SAMPLE                  BENZO(b)           BENZON        BENZO(c)       BENZO(q)      PERYLENE         INDENO-       DIBENZ BENZO(ghi)
                                  BATCH                                        WEIGHT       FLUORANTH          FLUORANTH          PYRENE        PYRENE                        PYRENE      ANTHRAC       PERYLENE
                                                                                 (g dry)             (ppb)             (ppb)        (ppb)+        (ppb)+           (ppb)+         (ppb)       (ppb)+        (ppb)



                >Q0789            P512.3 S&T QA/QCJK5242)P513                        1.3             12.1                9.3          15.0            1.2           18.5            0.8          0.6             1.7
                >K5242            P512,3 S&TTISSUE P513 (MBHI)                       1.4              9.5                8.7          13.3            1.1           16.8            0.5          0.3             2.0
                >Q0791            P512,3           S&T SPK(K5242) P513               1.3             68.7              68.5           92.4          63.0           102.7          55.9          55.2             66.8
                                                   Average % Recovery =         80.580/6             78.2%            79.0%       104.5%          82.2%          113.2%          73.8%        73.OOA          86.1%

                >K5039            P514.5 S&T TISSUE P514 (GBHR)                      3.1              2.4                0.7           2.2            1.0            2.5            1.0          0.9             1.3
                >Q1021            P514,5           S&T SPK K5039 P514                3.1             31.6              40.9           41.3          37.5            37.3          41.1          35.1             37.3
                                                   Average % Recovery =         96.680/6             9011%           124.2%       120.7%          112.80,6       107.5%        123.8%        105.80/b       111.2%

                >K5217            P514.5    S&TTISSUE P515 (BSSI)                    2.3              5.6                1.7           6.6            2.8           15.5            2.9          0.9             4.0
                >Q 1024           P514.5           S&T SPK K5217 P515                2.3             37.7              39.9           56.6          39.0            59.4          38.4          32.1             41.7
                                                   Average % Recovery =         83.470/6             73.5%            87.8%       114.7%          83.3%          100.6%          81.5%        71.6%           86.6%

                >K5057            P516.7 S&TTISSUE P516 (GBTD)                       3.2              4.4                3.5           4.8            1.3            5.2            1.1          1.5             1.8
                >QI027            P516,7           S&T SPK K5057 P516                3.2             35.4              28.0           32.6          23.2            35.5          40.4          39.0             35.2
                                                   Average % Recovery           97.500/6             99.9%            79.0%         89.6%         70.6%            97.4%       126.8%        120.90/6       107.9%

                >K5255            P516.7    S&TTISSUE P517 ( PBIB                    3.7              2.4                3.7           2.4            0.6            2.4            0.7          0.2             0.6
                >Q1039            P516,7 -T QA/QC K5255 P517 jSPK)                   3.7             27.6              24.8           26.0          19.5            26.3          29.3          29.2             26.6
                                                   Average % Recovery =         91.32%               93.7%            78.4%         87.9%         70.1%            88.8%       106.1%        107.6%           96.5%

                >KS333            P518.9 S&TTISSUE P518 (TBMK)                       3.2              2.0                1.6           1.4            0.4            0.2            0.2          0.5             0.7
                >Q1042            P518,9 -T QA/QC K5333 P518 (SPK)                   3.1             28.2              26.2           27.0          19.2            24.4          29.3          32.3             26.3
                                                   Average % Recovery =         80,81%               80.1%            75.4%         78.4%         57.7%            74.2%         89.3%        97.6%           78.4%

                >K5249            P518,9 S&T TISSUE P519 (LPGO)                      2.0             226.8            232.1         206.5           74.1            52.3          39.0          27.3             55.8
                >Q1053            P518.9 -T QA/QC K5249 P519 (SPK)                   2.0             283.5            269.1         265.8           113.9           89.3          113.4         89.6           102.6
                                                   Average % Recovery =        101.660/6          111.0%              71.7%       116.5%          78.9%            73.5%       139.6%        124.2%           93.0%

                >K5298            P520.1 S&TTISSNP520 (SAVVB)                        1.7             145.2             29.7           69.9          11.3            15.1          13.7           6.3             17.6
                >Q 1062           P520,1 AA S&T QA/QC K5298 (SPK)                    1.6             197.1             96.4         122.1           64.3            77.9          96.0          77.9             81.8
                                                   Average % Recovery =        102.04%               77.8%           106.2%         81.3%         84.9%          100.6%        131.9%        115.2%         102.7%

                >K5346            P520.1 S&TTISS NP521 (TBCB)                        1.6              1.6                0.7           1.6            0.4            0.2            0.6          0.5             1.1
                >Q1065            P520.1 AA S&T QA/QC K5346 (SPK)                    1.6             71.2              51.8           58.0          48.9            56.8          77.3          68.3             64.2
                                                   Average % Recovery =         97.300/6          112.8%              82.8%         91.5%         70.5%            91.7%       124.4%        109.90/0       102.4%





                                                                MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks, Spikes and QC Data





                    FILE                QC                  DESCRIPTION SAMPLE                   BENZO(b)           BENZO(k)       BENZO(e)      BENZO(a)       PERYLENE         INDENO-         DIBENZ     BENZO(ghl)
                                   BATCH                                         WEIGHT      FLUORANTH           FLUORANTH          PYRENE         PYRENE                         PYRENE      ANTHRAC       PERYLENE
                                                                                   (g dry)             (ppb)              (ppb)        (ppb)+         (ppb)+          (ppb)+          (ppb)       (Ppb)+        (ppb)


                >K5250             P522,3 S&TTISSUE P522 (LPGO)                        1.9           377.5                243.5        263.8           79.7            77.9           36.1          20.1            52.2
                >Q 1108            P522,3 -.T QA/QC K5250 P522 jSPK)                   1.9           445.3                312.1        322.4          127.0           144.1           107.9         88.6           108.7
                                                   Average % Recovery            101.33%           116.2%              121.7%        102.3%           86.5%          122.1%       133.8%          128.2%          104.6%

                >K5257           P526,7,9 S&T TISSUES P529 ( PBIB                      2.8              3.4                5.5            4.0            2.2             3.8           1.3           0.8              1.8
                >Q1114             P522.3,T QA/QC K5257 P523 JSPK)                     2.8             35.5               34.5          35.3           18.4            37.0           32.9          29.3            34.0
                                                   Average % Recovery =          91.070/6            89.2%                80.3%        87.2%          44.9%           92.1%         88.0%         79.2%            89.5%

                >K5347             P524,5;&T TISSUE NP524 (TBCB)                       2.5              1.8                1.0            1.5            0.2             0.3           0.4           0.5              0.8
                >Q1117             P524.5,.T QA/QC K5347 P524 (SPK)                    2.5             48.8               39.4          43.6           23.9            35.2           44.8          36.5            41.3
                                                   Average % Recovery =          97.68%            116.6%                 95.3%      104.5%           59.0%           86.5%       109.9%          89.3%          100.3%

                >K5170             P524.5 S&T TISSUE P525 (BBSD)                       2.9              1.6                0.9            1.0            0.7             1.4           1.0           0.4              1.0
                >Q1183             P524.5-T QA/QC K5170 P525 (SPK)                     2.8             39.3               33.2          35.0           29.1            29.3           45.5          48.1            38.2
                                                   Average % Recovery =          94.930/6          105.6%                 90.6%        95.0%          79.3%           77.9%       124.4%         133.5%          104.1%

                >K5386           P526.7,9)&TTISSUESP526 (GBSC)                         2.1           266.3                160.9        512.6          203.9           201.5           46.6          48.3           100.5
                >Q1192           P526.7,9       S&T QA/QC(K5386)P526                   2.1           275.7                190.0        525.2          231.8           225.9           86.2          84.9           121.4


                >Q1217           P526,7.9       S&T QA/gC(K5398)P527                   2.5              1.5                2.0            2.5            1.7             0.5           1.5           0.5              3.1
                >K5398           P526,7,9;&T TISSUES P5V (BHKF)                        2.5              1.4                1.1            2.1            1.4             0.2           1.0           0.5              2.1
                >Q 1219          P526,7.9         S&T SPK(K5398) P527                  2.5             47.6               30.9          54.3           40.5            38.5           52.2          37.9            40.0
                                                   Average % Recovery =          103.84%           114.2%                 73.4%      129.1%           96.5%           94.5%       126.5%          92.60/6          93.6%

                >Q 1335          P526.7,9       S&T QA/QC(K5280)P529                   2.3             10.2               10.5          18.4           13.7              5.2          11.0           4.6            13.8
                >K5280           P526.7,9 S&TTISSUES P529 (CBSP)                       2.3             14.5               10.4          24.3           21.0              6.9          11.9           6.3            19.4
                >Q1337           P526,7,9         S&T SPK(K5280) P529                  2.2             47.7               47.5          65.3           55.1            41.1           57.5          50.0            53.9
                                                   Average % Recovery =          87.92%              74.0%                82.9%        91.0%          75.7%           76.5%       101.7%          97.7%            76.7%

                >Q 1707               P531      S&T QA/QC K5135 P531                   1.6              0.8                1.2            1.4            1.0             1.4           0.5           0.2              0.4
                >K5135                P531      S&TTISS P531 (LMSP)                    1.6              0.8                1.4            0.7            0.9             0.9           0.5           0.4              0.5
                >Q 1709               P531       S&T K5135+MS P531                     1.6             51.1               69.1          72.5           46.6            63.8           58.8          50.6            56.1
                                                   Average % Recovery =          89.51%              79.0%             106.3%        112.8%           71.8%           98.7%         91.6%         78.9%            87.3%





                                                            MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks. Spikes and QC Data





                   FILE               QC                DESCRIPTION SAMPLE                BENZO(b)         BENZO(k) BENZO(e) BENZO(a) PERYLENE INDENO-                           DIBENZ BENZO(ght)
                                 BATCH                                    WEIGHT FLUORANTH FLUORANTH PYRENE PYRENE                                                  PYRENE ANTHRAC PERYLENE
                                                                             (g dry)           (ppb)             (ppb)       (ppb)+        (ppb)+         (ppb)+        (ppb)        (ppb)+     (ppb)










               DUPLICATE RE-EXTRACTIONS


               >K5003            P503.4 S&T TISSUE P503 ( GBOB)                 2.6            73.3               42.1         27.7         35.4            14.3         17.9          6.5            18.9
               >K5003            P514,5          S&T TISSUE P514                2.5            66.5               38.2         14.3         28.3            9.9          13.7          6.5            19.4


               > K5009           P503,4!kT TISSUE P503 (GBCR)                   2.4            23.8                7.2          6.0          7.0            1.5           1.5          0.7            1.7
               >K5009            P524,5          S&TTISSUE P525                 2.4            25.9                6.8          6.6          4.9            1.2           1.7          0.7            1.7


               >K5015            P503,4.&TTlSSUEP503 (BRCL)                     2.6             9.3                1.7          2.9          3.1            0.7           0.6          0.3            1.4
               >K5015            P514,5          S&TTISSUE P514                 2.5             7.8                3.3          2.1          3.2            1.6           1.8          0.4            1.5


               >K5039            P503,4 S&T TISSUE P503 (GBHR)                  3.1             4.3                1.9          1.2          2.4            2.0           0.6          0.3            1.2
               >K5039            P514,5          S&T TISSUE P514                3.1             4.5                2.4          0.7          2.2            1.0           1.0          0.9            1.3


               >K5075            P503,45&TTISSUEP503 (MBEM)                     2.2             2.3                1.2          0.6          0.8            1.3           0.3          0.2            0.2
               >K5075            P514,5          S&TTISSUE P514                 2.2             3.6                1.6          0.4          2.3            0.3           0.8          0.6            1.0





                                                                MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks, Spikes and QC Data




                                                                                                   TOTAL              TOTAL       2-3 RINGS         4-5 RINGS             RA710          CI-       C2- C3-
                   FILE                 QC                  DESCRIPTION SAMPLE AROMATICS                       AROMATICS          MEASURED          MEASURED             4-5 TO NAPH NAPH NAPH
                                   BATCH                                         WEIGHT       MEASURED           AS YR 1 (+)      AS YR 1(+)        AS YR 1(+)       2-3 RINGS
                                                                                   (g dry)             (Ppb)           (ppb)                (0h)             N       AS YR 1(+)        (ppb)      (ppb)     (ppb)


                LABORATORY REFERENCE MATERIAL


                >W2639             P505.6              GERG STD. CHK 11                1.0         4984.9              4527               97.7               2.3            0.02    2228.2     2112.9       1674.2
                >W2897             P507,8              GERG STD. CHK 11                1.0         5364.3              4925               98.0               2.0            0.02    2429.7     2110.7       1578.0
                >W2961             P507,8              GERG STD. CHK 11                1.0         5001.4              4592               98.0               2.0            0.02    2281.3     2009.5       1553.9
                >W4149             P512.3              GERG STD. CHK 11                1.0         4378.9              4032               97.5               2.5            0.03    2084.5     1398.7       1129.2
                >W4157             P514.5              GERG STD. CHK 11                1.0         4366.1              3996               97.9               2.1            0.02    2042.8     1317.5       993.1
                >W4229             P518,9              GERG STD. CHK 11                1.0         4637.3              4204               97.6               2.4            0.02    1992.3     1686.6       1401.7
                >W4240             P520.1              GERG STD. CHK 11                1.0         4671.6              4259               97.9               2.1            0.02    2203.5     1804.3       1530.5
                >W4272             P522.3              GERG STD. CHK 11                1.0         4725.3              4308               97.7               2.3            0.02    2108.3     1723.5       1413.8
                >W4271             P524.5              GERG SID. CHK 11                1.0         4299.9              3926               97.7               2.3            0.02    1963.2     1652.1       1339.8
                >W4407            P526.7.9             GERG STD. CHK 11                1.0         5444.9              4922               97.3               2.7            0.03    2193.3     1767.7       1450.9
                >W4936                P528             GERG STD. CHK 11                1.0         4629.8              4253               97.7               2.3            0.02    2227.6     1846.3       1602.6
                >W4807                P531             GERG STD. CHK 11                1.0         4479.8              4057               97.7               2.3            0.02    2032.9     1604.1       1297.2
                >W5005                P532             GERG STD. CHK 11                1.0         4226.7              3854               97.7               2.3            0.02    1965.0     1601.4       1470.4


                average                                                                            4708.5             4296.5              97.7               2.3              0.0   2134.8     1741.2       1418.1
                                                                                                       8.OOA           7.9%               0.2%              8.1%            8.3%       6.3%      13.4%      13.0%

                GERG chk 2 - avg. of 50                                                            4603.3              4214               97.8               2.2            0,02    2099.1     1829.2       1527.0
                                                                                                                                                                                      11.1%      18.00/0    19.0%
                BLANKS


                >QO685             P503.4           S&T BLANK P503                   10.0               5.9                 5             81.7              18.3            0.22         1.1       0.0         0.0
                >QO688             P503.4           S&T BLANK P504                   10.0               2.5                 2             78.2              21.8            0.28         0.3       0.0         0.0
                >Q0740             P505,6           S&T BLANK P505                   10.0               7.9                 7             83.3              16.7            0.20         2.3       0.0         0.0
                >Q0743             P505,6           S&T BLANK P506                   10.0               6.0                 5             85.0              15.0            0.18         1.3       0.0         0.0
                >Q0746             P507,8           S&T BLANK P507                   10.0               5.3                 5             83.0              17.0            0.20         1.6       0.0         0.0
                >QO749             P507,8           S&T BLANK P508                   10.0               4.6                 4             78.7              21.3            0.27         0.8       0.0         0.0
                >Q0770            P510,11           S&T BLANK P510                   10.0               6.7                 5             70.2              29.8            0.42         1.2       0.0         0.0
                >Q0784            P510.11           S&T BLANK P511                   10.0               5.0                 4             79.0              21.0            0.27         1.1       0.0         0.0
                >Q0787             P512.3           S&T BLANK P512                   10.0               5.5                 5             46.3              53.7            1.16         0.4       0.0         0.0
                >Q0790             P512,3           S&T BLANK P513                   10.0               4.1                 4             60.4              39.6            0.65         0.5       0.0         0.0
                >Q 1022            P514,5           S&T BLANK P514                   10.0               9.2                 8             78.7              21.3            0.27         1.6       0.0         0.0
                >Q 1025            P514,5           S&T BLANK P515                   10.0               8.2                 6             63.1              36.9            0.59         1.1       0.0         0.0
                >Q 1028            P516.7           S&T BLANK P516                   10.0               6.0                 5             59.8              40.2            0.67         0.8       0.0         0.0
                >Q 1040            P516.7           S&T BLANK P517                   10.0               5.2                 5             80.0              20.0            0.25         1.0       0.0         0.0
                >Q 1043            P518.9           S&T BLANK P518                   10.0               4.3                 4             64.8              35.2            0.54         0.6       0.0         0.0





                                                               MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks, Spikes and QC Data




                                                                                                    TOTAL            TOTAL       2-3 RINGS         4-5 RINGS             RATIO         Cl-        C2- C3-
                   FILE                 QC                 DESCRIPTION SAMPLE                AROMATICS        AROMATICS         MEASURED          MEASURED             4-5 TO       NAPH        NAPH       NAPH
                                  BATCH                                         WEIGHT       MEASURED          AS YR 1(+)        AS YR 1(+)        AS YR 1(+)      2-3 RINGS
                                                                                  (g dry)            (ppb)            (ppb)                                        AS YR I(+)        (ppb)      (ppb)      (ppb)


               >QI054             P518.9           S&T BLANK P519                   10.0             13.3                11              58.5             41.5            0.71         1.6        0.0         0.0
               >QI063             P520.1                S&T BLAM P520               10.0               8.6                8              72.2             27.8            0.38         1.5        0.0         0.0
               >Q1066             P520,1                S&T BLANK P521              10.0               5.9                5              77.9             22.1            0.28         1.4        0.0         0.0
               >QI109             P522,3          S&T BLANK P522                    10.0             12.6                11              62.6             37.4            0.60         1.5        0.0         0.0
               >Q1115             P522,3          S&T BLANK P523                    10.0               4.3                4              77.4             22.6            0.29         1.0        0.0         0.0
               >Q1118             P524.5      S&T TISSUE BLANK P524                 10.0               7.5                7              82.5             17.5            0.21         1.8        0.0         0.0
               >Q 1184            P524,5      S&T TISSUE BLANK P525                 10.0               4.7                4              84.2             15.8            0.19         0.8        0.0         0.0
               >Q1218            P526.7.9         S&T BLANK P527                    10.0               6.3                5              82.1             17.9            0.22         1.4        0.0         0.0
               >Q 1336           P526.7.9         S&T BLANK P529                    10.0               5.1                5              84.5             15.5            0.18         1.0        0.0         0.0
               >Q 1258               P!528  S&T TISSUE BLANK P528                   10.0               4.3                4              77.5             22.5            0.29         0.8        0.0         0.0
               >Q 1708              P531 S&T TISSUE BLANK P531                      10.0               5.7                4              78.0             22.0            0.28         1.0        0.0         0.0


               average                                                                                 6.3              5.4              74.2             25.8              0.4        1.1        0.0         0.0
                                                                                                    38.3%            37.5%             13.5%             39.0%           60.5%      40.0%       0.0%       0.0%
               NIST SRM 1974 - TISSUE SAMPLE
               Values for SRM 1974


               >Q 1023            P514,5                S&T NIST P514               0.60            1130.8              942              18.9             81.1            4.29       25.0       69.6       137.2
               >Q1026             P514,5                S&T NIST P515               0.60            933.2               792              20.0             80.0            4.00       22.9       54.7       96.5
               >Q1041             P516.7                S&T NIST P517               0.60            1015.1              914              17.8             82.2            4.63       28.6       52.5       108.8
               >QI044             P518.9                S&T NIST P518               0.60            1389.9            1234               15.8             84.2            5.32       44.3       50.2       95.2
               >Q 1055            P518.9                S&T NIST P519               0.60            852.7               738              18.8             81.2            4.32       29.5       39.8       102.8
               >Q 1064            P520.1                 S&T NIST P520              0.60            883.0               745              19.2             80.8            4.22       29.6       40.4       82.1
               >Q 1067            P520,1                 S&T NIST P521              0.60            1213.2            1044               17.1             82.9            4.86       32.4       54.6       97.5
               >Q1110             P522.3                S&T NIST P522               0.60            1484.0            1267               18.9             81.1            4.29       35.0       89.1       159.4
               >Q1119             P524,5                 S&T NIST P524              0.60            1044.8              905              21.7             78.3            3.61       42.7       60.2       106.5
               >QI185             P524.5                 S&T NIST P525              0.60            818.4               709              19.2             80.8            4.20       29.7       48.6       81.9


               average                                                                              1076.5            929.1              18.7             81.3              4.4      32.0       56.0       106.8
                                                                                                    20,0%            20.4%               8.1%             1.9%           10.20/6    20.6%       24.7%      21.5%


               REPLICATES AND SPIKED SAMPLES


               >QO684             P503.4       S&T QA/QC(K5039)P503                   3.1            86.2                75              58.2             41.8            0.72         8.5      16.6       30.5
               >K5039             P503,4 kT TISSUE P503 (GBI-iR)                      3.1            90.6                78              61.1             38.9            0.64         8.8      20.8       43.7


               >QO687             P503,4       S&T QA/QC(K5159)P504                   2.7            73.9                62              62.9             37.1            0.59         7.3      13.1       29.5



                                                    MM MM M = M M M M = mmm
                                                               MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks, Spikes and QC Data




                                                                                                    TOTAL            TOTAL       2-3 RINGS         4-5 RINGS             RATIO         CI-        C2- C3-
                   FILE                 QC                 DESCRIPTION SAMPLE               AROMATICS AROMATICS                 MEASURED          MEASURED             4-5 TO        NAPH      NAPH NAPH
                                   BATCH                                        WEIGHT       MEASURED           AS YR 1(+)       AS YR 1(+)        AS YR 1 (+)     2-3 RINGS
                                                                                  (g dry)            (ppb)             (ppb)              N                 (96)   AS YR 1(+)         (ppb)       (ppb)   (ppb)


               >K5159              P503,4   S&TTISSUE P504 (VBSP)                    2.7             70.9                61             63.9              36.1             0.56        7.1        10.6      22.9
               >QO689              P503.4       S&T SPIKE(K5159)P504                 2.7                                                                                               0.0        0.0          010
                                                   Average % Recovery =         102.71%

               >QO739              P505.6      S&T QA/QC(K5222)P505                  2.1             389.1              347             33.1              6619             2.02        10.7       31.7      72.2
               >K5222              P505.6 S&T TISSUE P505 (MSPC )                    2.1             394.4              348             31.7              68.3             2.16        9.6        22.7      57.5
               >Q0741              P505,6       S&T SPIKE(K5222)P505                 2.2                                                                                               0.0        0.0          0.0
                                                   Average % Recovery =         109.33%

               >QO742              P505,6      S&T QA/QC(K504O)P506                  3.3             91.6                80             63.8              36,2             0.57        9.3        15.3      35.9
               >K5040              P505,6 S&T TISSUE P506 (GBHR)                     3.3             102.0               89             58.0              42.0             0.72        9.9        15.0      31.7
               >Q0744              P505,6       S&T SPIKE(K504O)P506                 3.3                                                                                               0.0        0.0          0.0
                                                   Average % Recovery =         86.02%

               >Q0745              P507,8      S&T QA/QC K5118 P507                  3.4             50.6                44             76.7              23.3             0.30        8.1        0.0          0.0
               >K5118              P507.8 S&T TISSUE P507 (SAMP)                     3.4             45.4                39             75.7              24.3             0.32        8.2        15.8         0.0
               >Q0747              P507,8        S&T SPK K5118 P507                  3.4                                                                                               0.0        0.0          0.0
                                                   Average % Recovery =         85.84%

               >Q0748              P507,8      S&T QA/QC K5064 P508                  2.7             119.0              101             44.3              55.7             1.26        6.0        9.8       21.6
               >K5064              P507,8 S&T TISSUE P508 (GBYC                      2.7             136.9              118             49.3              50.7             1.03        8.0        9.0       24.7
               >Q0750              P507.8        S&T SPK K5064 P508                  2.7                                                                                               0.0        0.0          0.0
                                                   Average % Recovery           82.64%

               >Q0769            P510.11       S&T QA/QC(K5065)P510                  3.0             131.5              115             44.7              55.3             1.24        6.8        8.7       23.2
               >K5065            P510,11    S&TTISSUE P510 (GBYC)                    3.0             126.4              107             42.3              57.7             1.36        6.9        8.6       17.3
               >Q0771            P510.11         S&T SPK(K5065) P5 10                3.0                                                                                               0.0        0.0          0.0
                                                   Average % Recovery =         91.170/6

               >Q0783            P510,11       S&T QA/QC(K5119)P511                  3.6             36.0                30             77.1              22.9             0.30        3.3        0.0          0.0
               >K5119            P510.11    S&TTISSUE P511 (SAMP)                    3.9             35.2                29             78.8              21.2             0.27        4.4        0.0          0.0
               >Q0785            P510.11         S&T SPK K5119 P511                  3.6                                                                                               0.0        0.0          0.0
                                                   Average % Recovery =         78.43%


               >Q0786              P512,3'QA/QC K5170 P512(BBSD)                     2.8             47.8                42             67.1              32.9             0.49        6.9        6.7       12.2
               >Q0788              P512,3        S&T SPK(K5170) P512                 2.8                                                                                               010        0.0          0.0
                                                   Average % Recovery           80.420,6





                                                                MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks, Spikes and QC Data




                                                                                                     TOTAL             TOTAL       2-3 RINGS         4-5 RINGS              RATIO         Cl-        C2- C3-
                   FILE                 QC                  DESCRIPTION SAMPLE AROMATICS                        AROMATICS         MEASURED          MEASURED              4-5 TO        NAPH         NAPH NAPH
                                   BATCH                                         WEIGHT        MEASURED          AS YR 1(+)        AS YR 1 (+)       AS YR 1 (+)      2-3 RINGS
                                                                                   (g dry)             (ppb)             (ppb)              (0/0)             (0h)    AS YR 1 (+)        (ppb)       (ppb)  (ppb)



                >Q0789             P512.3      S&T QA/QC(K5242)P513                    1.3             432.8              399               15.3              84.7            5.55        7.3        10.2      27.5
                >K5242             P512.3 S&T TISSUE P513 ( MBHI                       1.4             416.7              384               17.4              82.6            4.75        8.6        12.5      24.4
                >Q0791             P512.3         S&T SPK(K5242) P513                  1.3                                                                                                0.0        0.0         0.0
                                                    Average % Recovery =          80.58%

                >K5039             P514.5 S&T TISSUE P514 (GBHR)                       3.1             89.8                 73              61.4              38.6            0.63        6.8        0.0         0.0
                >Q 1021            P514.5           S&T SPK K5039 P514                 3.1                                                                                                0.0        0.0         010
                                                    Average % Recovery =          96.68%

                >K5217             P514.5    S&T TISSUE P515 (BSSI)                    2.3             234.8              199               40.7              59.3            1.46        13.4       21.6      61.6
                >Q1024             P514.5           S&T SPK K5217 P515                 2.3                                                                                                0.0        0.0         0.0
                                                    Average % Recovery =          83.47%

                >K5057             P516,7 S&T TISSUE P516 (GBTD)                       3.2             138.4              115               52.8              47.2            0.89        10.4       18.4      42.1
                >QI027             P516.7           S&T SPK K5057 P516                 3.2                                                                                                0.0        0.0         0.0
                                                    Average % Recovery =          97.50%

                >K5255             P516.7    S&T TISSUE P517 (PBIB)                    3.7             144.1              131               49.8              50.2            1.01        5.7        10.7      18.5
                >QI039             P516,7 -T QA/QC K5255 P517 JSPK)                    3.7                                                                                                0.0        0.0         0.0
                                                    Average % Recovery =          91.32%
                >K5333             P518.9 S&T TISSUE P518 (-IBMK)                      3.2             119.9              ill               60.2              39.8            0.66        14.3       11.8      14.9
                >Q1042             P518.9 -T QA/QC K5333 P518 JSPK)                    3.1                                                                                                0.0        0.0         0.0
                                                    Average % Recovery =          80.81%
                >K5249             P518.9 S&T TISSUE P519 (LPGO)                       2.0           7852.3              5993               48.7              51.3            1.05      498.7     1819.0     4806.6
                >QI053             P518.9 -T QA/QC K5249 P5 19 JSPK)                   2.0                                                                                                0.0        0.0         0.0
                                                    Average % Recovery =          101.66%

                >K5298             P520,1 S&T TISS NP520 (SAWB)                        1.7           4336.0              3741               42.1              57.9            1.37       107.8       401.6   1432.3
                >Q 1062            P520,1 AA S&T gA/QC K5298 JSPK)                     1.6                                                                                                0.0        0.0         0.0
                                                    Average % Recovery =          102,04%

                >K5346             P520.1 S&TTISS NP521 (-FBCB)                        1.6             210.4              196               75.7              24.3            0.32        57.9       37.2      36.0
                >QI065             P520.1 AA S&T QA/QC K5346 JSPKJ                     1.6                                                                                                0.0        0.0         0.0
                                                    Average % Recovery =          97,300/6





                                                               MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks, Spikes and QC Data




                                                                                                    TOTAL            TOTAL       2-3 RINGS         4-5 RINGS             RATIO         Ci-        C2- C3-
                   FILE                 QC                  DESCRIPTION SAMPLE              AROMATICS AROMATICS                 MEASURED          MEASURED             4-5 TO       NAPH NAPH NAPH
                                   BATCH                                        WEIGHT       MEASURED           AS YR I(+)       AS YR 1 (+)       AS YR 1 (+)     2-3 RINGS
                                                                                  (g dry)            (ppb)             (ppb)              (0/6)             (0h)   AS YR I(+)        (ppb)      (ppb)    (ppb)


                >K5250             P522,3 S&TTISSUEP522 (LPGO)                        1.9          8170.3              6136             46.7              53.3            1.14       416.6     1545.5    3945.3
                >Q1108             P522.3 -T QA/QC K5250 P522 JSPK)                   1.9                                                                                              0.0        0.0          0.0
                                                   Average % Recovery           101-33%

                >K5257          P526,7,9 S&T TISSUES P529 ( PBIB                      2.8            190.8              169             49.2              50.8            1.03         5.8      13.3        19.9
                >QI114             P522,3 -T QA/QC K5257 P523 JSPK)                   2.8                                                                                              0.0        0.0          0.0
                                                   Average % Recovery           91-07%

                >K5347             P524,5 @)&T TISSUE NP524 (TBCB                     2.5            150.5              139             74.7              25.3            0.34       42.2       25.5        33.8
                >Q1117             P524,5 T QA/QC K5347 P524 JSPK)                    2.5                                                                                              0.0        0.0          0.0
                                                   Average % Recovery =         97-680/6

                >K5170             P524,5 S&T TISSUE P525 (BBSD)                      2.9            58.6                50             65.2              34.8            0.53         5.8      10.4        17.9
                >Q 1183            P524,5 -T QA/QC K5170 P525 JSPK)                   2.8                                                                                              0.0        0.0          0.0
                                                   Average % Recovery =         94-93%

                >K5386          P526,7,93)&TTISSUESP526 (GBSC)                        2.1         17677.6             15033             67.1              32.9            0.49     2297.6     5626.9     7213.3
                >Q 1192         P526,7,9       S&T QA/QC(K5386)P526                   2.1         18549.3             15719             65.5              34.5            0.53     2298.0     5425.8     6740.0



                >Q1217          P526,7,9       S&T QA/QC(K5398)P527                   2.5            103.3               90             67.0              33.0            0.49       28.9       18.4        25.6
                >K5398          P526,7,9)&TnSSUES P527 (BHKF)                         2.5            96.2                89             69.5              30.5            0.44       30.0       17.6        21.8
                >Q1219          P526,7.9         S&T SPK(K5398) P527                  2.5                                                                                              0.0        0.0          0.0
                                                   Average % Recovery =         103-840/6

                >Q1335          P526.7.9       S&T QA/QC(K5280)P529                   2.3            344.6              290             34.8              65.2            1.87         0.0      23.6        27.6
                >K5280          P526.7.9 S&T TISSUES P529 ( CBSP)                     2.3            368.4              305             31.3              68.7            2.20         0.0      22.3        23.7
                >Q1337          P526,7.9         S&T SPK(K5280) P529                  2.2                                                                                              0.0        0.0          0.0
                                                   Average % Recovery =         87.92%

                >Q1707                P531     S&T QA/QC K5135 P531                   1.6            73.7                66             61.2              38.8            0.63         8.8        0.0          0.0
                >K5135                P531     S&TTISS P531 (LMSP)                    1.6            81.8                75             57.8              42.2            0.73       12.7         0.0          0.0
                >Q 1709               P531       S&T K5135+MS P531                    1.6                                                                                              0.0        0.0          0.0
                                                   Average % Recovery =         89-51%





                                                               MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks, Spikes and QC Data




                                                                                                   TOTAL            TOTAL       2-3 RINGS        4-5 RINGS             RATIO         CI_        C2- C3-
                   FILE                 QC                 DESCRIPTION SAMPLE AROMATICS AROMATICS MEASURED MEASURED                                                   4-5 TO NAPH NAPH NAPH
                                  BATCH                                       WEIGHT MEASURED                  AS YR 1(+)       AS YR 1(+)       AS YR 1 (+)     2-3 RINGS
                                                                                 (g dry)            (ppb)             (ppb)              N                 (0/b) AS YR 1            (ppb)     (ppb) (ppb)









               DUPLICATE RE-EXTRACTIONS


               >K5003             P503AS&TTISSUEP503 (GBOB)                          2.6            676.8              517             15.8             84.2             5.33        8.7        9.9       15.0
               >K5003             P514,5           S&TTISSUE P514                    2.5            552.1              406             15.8             84.2             5.31        7.3        0.0       0.0

               >K5009             P503A &T TISSUE P503 (GBCR)                        2.4            333.0              288             26.1             73.9             2.83       12.9      15.3        28.5
               >K5009             P524,5           S&T TISSUE P525                   2.4            322.7              277             25.1             74.9             2.98        9.4      16.0        28.2

               >K5015             P503,4.&TTISSUEP503 (BRCL)                         2.6            127.7              102             42.5             57.5             1.35       10.6      12.7        19.6
               >K5015             P514.5           S&T TISSUE P514                   2.5            119.7               88             55.9             44.1             0.79       10.1        0.0       0.0

               >K5039             P503A S&T TISSUE P503 (GBHR)                       3.1            89.4                74             60.6             39.4             0.65        8.8      20.8        43.7
               >K5039             P514,5           S&T TISSUE P514                   3.1            88.2                67             64.2             35.8             0.56        6.8        5.7       7.9

               >K5075             P503,45&TTISSUEP503 (MBEM)                         2.2            65.7                58             68.8             31.2             0.45        8.3      12.9        14.9
               >K5075             P514.5           S&T TISSUE P514                   2.2            57.0                45             71.6             28.4             0.40        7.5        0.0       0.0





                                                        MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks, Spikes and QC Data




                                                                                     C4-       ci-       C2-       C3-          CI-          C2-         C3-          C4-       Cl- C2-
                 FILE              QC                DESCRIPTION SAMPLE NAPH. FLUOR FLUOR FLUOR                            PHEN +       PHEN +       PHEN +      PHEN +        DBT DBT
                              BATCH                                    WEIGHT                                              ANTHRA       ANTHRA      ANTHRA       ANTHRA
                                                                         (g dry)     (ppb)   (ppb)      (ppb)     (ppb)        (ppb)        (ppb)       (ppb)       (ppb)      (ppb)   (ppb)



             LABORATORY REFERENCF, AkTERIAL


             >W2639           P505.6            GERG STD. CHK 11            1.0    1099.8    289.6    464.1     603.6        741.1        974.7        674.1        455.9      368.4   638.0
             >W2897           P5D7,8            GERG STD. CHK 11            1.0    774.0     293.1    388.0     314.9        572.2        638.6        420.9        216.5      366.2   534.7
             >W2961           P507.8            GERG STD. CHK 11            1.0    789.2     233.9    358.3     302.5        562.9        650.6        466.7        223.2      362.9   531.0
             >W4149           P512.3            GERG STD. CHK 11            1.0    667.4     187.0    305.1     270.4        527.9        653.4        312.8        193.6      251.8   350.4
             >W4157           P514, 5           GERG STD. CHK 11            1.0    601.2     196.3    313.6     304.1        417.7        499.3        294.7        172.0      195.8   259.9
             >W4229           P518'@)           GERG STD. CHK 11            1.0    866.8     223.3    406.7     471.0        575.0        753.1        510.8        331.7      317.6   510.0
             >W4240           P520,1            GERG SM. CHK 11             1.0    1000.7    231.3    369.6     471.1        602.5        819.8        624.6        366.2      332.4   536.2
             >W4272           P522,S            GERG SM. CHK 11             1.0    883.3     207.8    336.3     372.0        346.7        698.6        479.2        297.4      306.6   486.3
             >W4271           P524,5            GERG STD. CHK 11            1.0    876.2     199.0    340.6     357.3        528.7        714.3        530.3        437.0      294.0   457.5
             >W4407          P526.7.9           GERG STD. CHK 11            1.0    844.8     307.6    473.6     471.8        775.1        976.7        586.0        365.9      427.7   646.3
             >W4936              P52S           GERG STI). CHK 11           1.0    948.3     199.9    315.5     327.1        508.9        605.2        440.3        225.1      227.8   401.2
             >W4807              P531           GERG STD. CHK 11            1.0    702.3     196.0    326.8     318.4        538.0        642.4        483.3        361.4      295.0   417.9
             >W5005              P532           GERG STD. CHK 11            1.0    899.4     198.1    357.3     415.8        463.8        627.4        490.4        271.2      254.6   403.1


        00   average                                                               842.6     227.9    365.8     384.6        550.8        711.8        485.7        301.3      307.8   474.8
                                                                                   15.6%     17.7%    14.3%     24.0%        20.2%        18.8%        21.4%        29.60/6    20.2%   22.1%


             GERG chk 2 - avg. of 50                                               908.5     217.5    354.4     363.1        529.1        686.8        427.0        250.1      288.3   424.6
                                                                                   21.7%     14.2%    18.1%     23.8%        19.5%        17.8%        23.5%        31.7%      23.9%   25.7%
             BLANKS


             >QO685           P502A          S&T BLANK P503                10.0      0.0       0.0       0.0       0.0          0.0          0.0         0.0          0.0       0.0        0.0
             >QO688           P503A          S&T BLANK P504                10.0      0.0       0.0       0.0       0.0          0.0          0.0         0.0          0.0       0.0        0.0
             >Q0740           P505,C         S&T BLANK P505                10.0      0.0       0.0       0.0       0.0          0.0          0.0         0.0          0.0       0.0        0.0
             >Q0743           P505,6         S&T BLANK P506                10.0      0.0       010       0.0       0.0          0.0          0.0         0.0          0.0       0.0        0.0
             >Q0746           P507.8         S&T BLANK P507                10.0      0.0       0.0       0.0       0.0          0.0          0.0         0.0          0.0       0.0        0.0
             >Q0749           P5078          S&T BLANK P508                10.0      0.0       0.0       0.0       0.0          0.0          0.0         0.0          0.0       0.0        0.0
             >Q0770           P510,11        S&T BLANK P5 10               1010      0.0       0.0       0.0       0.0          0.0          0.0         0.0          0.0       0.0        0.0
             >Q0784           P510,11        S&T BLANK P511                10.0      0.0       0.0       0.0       0.0          0.0          0.0         0.0          0.0       0.0        0.0
             >Q0787           P512,3         S&T BLANK P512                10.0      0.0       0.0       0.0       0.0          0.0          0.0         0.0          0.0       0.0        0.0
             >Q0790           P512,S         S&T BLANK P513                10.0      0.0       0.0       0.0       0.0          0.0          0.0         0.0          0.0       0.0        0.0
             >Q1022           P514,5         S&T BLANK P514                10.0      0.0       0.0       0.0       0.0          0.0          0.0         0.0          0.0       0.0        0.0
             >Q 1025          P514,5         S&T BLANK P515                10.0      0.0       0.0       0.0       0.0          0.0          0.0         0.0          0.0       0.0        0.0
             >Q 1028          P516.7         S&T BLANK P516                10.0      0.0       0.0       0.0       0.0          0.0          0.0         0.0          0.0       0.0    -   0.0
             >Q 1040          P516,7         S&T BLANK P517                10.0      0.0       0.0       0.0       0.0          0.0          0.0         0.0          0.0       0.0        0.0
             >Q1043           P518,9         S&T BLANK P518                10.0      0.0       0.0       0.0       0.0          0.0          0.0         0.0          0.0       0.0        0.0





                                                                  MUSSEL WATCH YEAR V1 - Bivalve Aromatics Blanks, Spikes and QC Data




                                                                                                     C4-        Cl-         C2-        C3-            Cl-            C2-            C3-            C4-         Cl-      C2-
                    FILE                  QC                  DESCRIPTION SAMPLE                   NAPH     FLUOR       FLUOR      FLUOR        PHEN +          PHEN +         PHEN +         PHEN +          DBT       DBT
                                    BATCH                                          WEIGHT                                                       ANTHRA         ANTHRA          ANTHRA         ANTHRA
                                                                                     (g dry)       (ppb)        (ppb)     (ppb)      (ppb)            (ppb)         (ppb)           (ppb)         (ppb)       (ppb)     (ppb)


                >Q1054              P518.9           S&T BLANK P519                     10.0         0.0        0.0         0.0        0.0            0.0            0.0            0.0            0.0         0.0          0.0
                >Q1063              P520,1                 S&T BLANK P520               10.0         0.0        0.0         0.0        0.0            0.0            0.0            0.0            0.0         0.0          0.0
                >Q 1066             P520.1                 S&T BLANK P521               10.0         0.0        0.0         0.0        0.0            0.0            0.0            0.0            0.0         0.0          0.0
                >Q 1109             P522,3           S&T BLANK P522                     10.0         0.0        0.0         0.0        0.0            0.0            0.0            0.0            0.0         0.0          0.0
                >Q1115              P522.3           S&T BLANK P523                     10.0         0.0        0.0         0.0        0.0            0.0            0.0            0.0            0.0         0.0          0.0
                >Q1118              P524,5      S&T TISSUE BLANK P524                   10.0         0.0        0.0         0.0        0.0            0.0            0.0            0.0            0.0         0.0          0.0
                >9 1184             P524.5      S&T TISSUE BLANK P525                   10.0         0.0        0.0         0.0        0.0            0.0            0.0            0.0            0.0         0.0          0.0
                >Q 1218            P526.7,9          S&T BLANK P527                     10.0         0.0        0.0         0.0        0.0            0.0            0.0            0.0            0.0         0.0          0.0
                >Q1336             P526,7,9          S&T BLANK P529                     10.0         0.0        0.0         0.0        0.0            0.0            0.0            0.0            0.0         0.0          0.0
                >g 1258                P528   S&T'IISSUE BLANK P528                     10.0         0.0        0.0         0.0        0.0            0.0            0.0            0.0            0.0         0.0          0.0
                >Q1708                P531 S&T TISSUE BLANK P531                        10.0         0.0        0.0         0.0        0.0            0.0            0.0            0.0            0.0         0.0          0.0

                average                                                                              0.0        0.0         0.0        0.0            0.0            0.0            0.0            0.0         0.0          0.0
                                                                                                   0.0016       0.00/6    0.00/6     0.00/6           0.0%          0.0%            0.00/0        0.0%        0.0%      0.0%
                NIST SRM 1974 - TISSUE SAMPLE
                Values for SRM. 1974


                >Q 1023             P514,5                 S&T NIST PS 14               0.60       206.5        54.3      286.4      747.5            126.4         374.1           368.9         266.7       41.5      161.6
                >Q 1026             P514.5                 S&T NIST P515                0.60       135.3        37.2      182.2      387.4            92.4          297.0           216.5         148.8       24.4      108.1
                >Q 1041             P516.7                 S&T NIST P517                0.60       230.0        23.7      225.8      486.3            126.6         372.6           491.3         273.7       43.4      186.7
                >Q 1044             P518,9                 S&T NIST P518                0.60       230.6        48.4      245.3      563.2            147.6         509.7           748.6         372.2       50.1      265.6
                >Q 1055             P518'9                 S&T NIST PS 19               0.60       122.8        16.8      117.8      220.5            79.3          235.0           353.0         220.7       31.1      149.1
                >Q1064              P520,1                  S&T NIST P520               0.60       116.9        38.7      142.5      329.1            66.0          260.4           366.6         188.1       29.9      144.4
                >Q 1067             P520,1                  S&T NIST P521               0.60       218.6        43.3      258.8      567.3            113.5         421.1           644.3         326.3       29.0      210.4
                >Q1110              P522,3                 S&T NIST P522                0.60       307.9        71.9      346.8      791.9            196.0         691.7           664.6         503.9       50.6      335.8
                >Q1119              P524.5                  S&T NIST P524               0.60       170.9        40.3      174.9      431.6            88.4          350.6           491.1         257.6       37.7      152.7
                >Q 1185             P524.5                  S&T NIST P525               0.60       139.8        30.6      130.9      382.6            71.2          223.7           328.8         201.7       26.4      120.9

                average                                                                            187.9        40.5      211.1      490.7            110.7         373.6           467.4         275.9       36.4      183.5
                                                                                                   31.0%      36.6%       33.4%      34.9%         34.4%            36.2%           34.9%         35.6%     25.1%       36.3%


                REPLICATES AND SPIKED SAMPLES

                >QO684              P503,4       S&T QA/QC(K503O)P503                     3.1      34.0         0.0         0.0        0.0            20.6          27.8            24.9          25.1         0.0        19.3
                >K5039              P503,4 ScT TISSUE P503 (GBHR)                         3.1      55.7         0.0         0.0        0.0            26.7          33.8            28.6          38.5         0.0        18.4


                >Q0687              P503A        S&T QA/QC(K5159)P504                     2.7      34.9         11.0      66.6       105.4            17.8          28.1            18.4          17.2         6.5        13.9



                                                                 mmummm M M M mmmmm M
                                                               MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks, Spikes and QC Data




                                                                                                 C4-        Cl-        C2-        C3-           Ci-            C2-           C3-            C4-        Cl-     C2-
                   FILE                QC                  DESCRIPTION SAMPLE                    NAPH FLUOR FLUOR FLUOR                    PHEN +        PHEN +         PHEN +        PHEN +         DBT      DBT
                                  BATCH                                         WEIGHT                                                    ANTHRA         ANTHRA         ANTHRA        ANTHRA
                                                                                  (g dry)        (ppb)    (ppb)      (ppb)        (ppb)         (ppb)          (ppb)         (ppb)          (ppb)    (ppb)    (ppb)


               >K5159             P503,4    S&T TISSUE P504 (VBSP)                   2.7         21.2       7.6      51.5         68.0          19.0           26.9          16.8           16.5       4.5        12.0
               >gO689             P503,4        S&T SPIKE(K5159)P504                 2.7         0.0        0.0        0.0        0.0           0.0            0.0           0.0            0.0        0.0        0.0
                                                   Average % Recovery =         102.71%

               >g0739             P505,6       S&T QA/QC(K5222)P505                  2.1         113.8     20.3      121.2      248.8           63.3           150.9         140.6          55.9     28.4       135.9
               >K5222             P505.6 S&T TISSUE P505 ( MSPC )                    2.1         77.8      21.5      119.4      250.9           62.5           133.6         130.8          78.3     30.4       146.9
               >g0741             P505,6        S&T SPIKE(K5222)P505                 2.2         0.0        0.0        0.0        0.0           0.0            0.0           0.0            0.0        0.0        0.0
                                                   Average % Recovery =         109.33%

               >Q0742             P505,6       S&T QA/QC(K504O)P506                  3.3         33.8       6.8      35.6         99.5          31.2           42.1          49.6           31.2       2.5        17.9
               >K5040             P505,6 S&T TISSUE P506 (GBHR)                      3.3         32.7       7@9      26.7         71.3          21.3           36.2          34.2           27.3       4.5        11.5
               >g0744             P505.6        S&T SPIKE(K504O)P506                 3.3         0.0        0.0        0.0        0.0           0.0            0.0           0.0            0.0        010        0.0
                                                   Average % Recovery =         86.02%

               >Q0745             P507,8       S&T QA/QC K5118 P507                  3.4         0.0        0.0        0.0        0.0           15.1           22.1          22.4           29.8       0.0        15.6
               >K5118             P507,8 S&T TISSUE P507 (SAMP)                      3.4         0.0        0.0        0.0        0.0           15.5           22.8          19.2           24.7       0.0        9.4
               >Q0747             P507,8         S&T SPK K5118 P507                  3.4         0.0        0.0        0.0        0.0           0.0            0.0           0.0            0.0        0.0        0.0
                                                   Average % Recovery =         85.84%

               >Q0748             P507,8       S&T QA/QC K50664 P508                 2.7         23.8       9.2      21.0         0.0           25.9           33.9          31.5           37.0       0.0        14.5
               >K5064             P507,8 S&T TISSUE P508 (GBYC)                      2.7         16.3       8.4      28.2         0.0           26.3           25.7          46.9           44.6       0.0        26.1
               >Q0750             P507,8         S&T SPK K5064 P508                  2.7         0.0        0.0        0.0        0.0           0.0            0.0           0.0            0.0        0.0        0.0
                                                   Average % Recovery =         82.64%

               >Q0769            P510.11       S&TgA/gC(K5065)P510                   3.0         29.4       9.5      42.5         46.4          19.6           48.3          39.3           39.3       3.9        15.9
               >K5065            P510.11    S&TTISSUE P510 (GBYC)                    3.0         25.9       7.3      29.0         28.3          20.0           42.0          34.0           29.8       6.0        14.6
               >Q0771            P510.11         S&T SPK(K5065) P5 10                3.0         0.0        0.0        0.0        0.0           0.0            0.0           0.0            0.0        0.0        0.0
                                                   Average % Recovery =         91.17%

               >QO783            P510,11       S&T QA/gC(K5119)P511                  3.6         8.4        7.4        0.0        0.0           7.0            17.4          12.0           15.4       0.0        0.0
               >K5119            P510,11    S&T TISSUE P511 (SAMP)                   3.9         9.2        5.5        0.0        0.0           7.2            12.2          9.7            8.5        0.0        4.6
               >QO785            P510,11         S&T SPK K5119 P511                  3.6         0.0        0.0        0.0        0.0           0.0            0.0           0.0            0.0        0.0        0.0
                                                   Average % Recovery =         78.43%


               >Q0786             P512,3    QA/QC K5170 P512(BBSD)                   2.8         17.0       5.8      20.8         33.3          10.9           24.9          17.4           16.1       OD         8.2
               >g0788             P512,3         S&T SPK(K5170) P512                 2.8         010        0.0        0.0        0.0           0.0            0.0           0.0            0.0        0.0        0.0
                                                   Average % Recovery =         80.42%



     mmm MM mmm MM MM M M MIM @
                                                                MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks, Spikes and QC Data




                                                                                                 C4-         Ci-        C2-        C3-           Ci-            C2-           C3-            C4-        Cl- C2-
                    FILE                 QC                 DESCRIPTION SAMPLE                   NAPH FLUOR FLUOR FLUOR                     PHEN +        PHEN +         PHEN +        PHEN +           DBT    DBT
                                   BATCH                                         VVEIGHT                                                    ANTHRA        ANTHRA         ANn-IRA       ANTHRA
                                                                                   (g dry)       (ppb)     (ppb)        (ppb)    (ppb)          (ppb)           (ppb)        (ppb)         (ppb)        (Ppb)  (ppb)




                >Q0789             P512,3       S&T QA/QC(K5242)P513                   1.3       48.7        18.1       72.3     135.2          40.9            113.0        68.5          38.0         10.4      53.3
                >K5242             P512,3 S&TI7ISSUE P513 ( MBHI                       1.4       63.1        15.4       76.2     136.1          41.1            104.0        64.5          50.5         11.8      52.7
                >Q0791             P512.3           S&T SPK(K5242) P513                1.3       0.0         0.0        0.0        0.0           0.0            0.0           0.0            0.0        0.0         0.0
                                                    Average % Recovery =         80.58%

                >K5039             P514,5 S&T17ISSUE P514 (GBHR)                       3.1       18.1        0.0        0.0      508.2          27.6            31.9         32.8          23.1         0.0         9.6
                >Q 1021            P514.5           S&T SPK K5039 P514                 3.1       0.0         0.0        0.0        0.0           0.0            0.0           0.0            0.0        0.0         0.0
                                                    Average % Recovery =         96.6896

                >K5217             P514,5     S&TTISSUEP515 (BSSI)                     2.3       117.0       18.1       95.8     186.8          57.6            164.3     1047.5           59.5         12.8      40.7
                >Q 1024            P514,5           S&T SPK K5217 P515                 2.3       0.0         0.0        0.0        0.0           0.0            0.0           0.0            0.0        0.0         0.0
                                                    Average % Recovery           83.47%

                >K5057             P516.7 S&T TISSUE P516 (GBTD                        3.2       53.3        13.3       57.4     116.1          40.4            102.0        126.0         214.7        11.4      52.6
                >Q 1027            P516,7           S&T SPK K5057 P516                 3.2       0.0         0.0        0.0        0.0           0.0            0.0           0.0            0.0        0.0         0.0
                                                    Average % Recovery =         97.500/6

                >K5255             P516.7    S&T71SSUEP517 (PBIB)                      3.7       22.9        7.5        17.6     31.5           25.3            24.9         53.4          28.0         4.5       10.8
                >Q 1039            P516,7 -T QA/QC K5255 P517 (SPK)                    3.7       0.0         0.0        0.0        0.0           0.0            0.0           0.0            0.0        0.0         0.0
                                                    Average % Recovery =         91.32%

                >K5333             P518,9 S&TIISSUE P518 (TBMK)                        3.2       18.4        4.8        15.4       0.0          20.5            17.2          0.0            0.0        0.0         8.7
                >Q1042             P518,9 -T QA/QC K5333 P518 (SPK)                    3.1       0.0         0.0        0.0        0.0           0.0            0.0           0.0            0.0        0.0         0.0
                                                    Average % Recovery =         80.81%

                >K5249             P518,9 S&TTISSUEP519 (LPGO)                         2.0    5336.1      892.6     3176.1     4261.3         3078.6        5959.9        4895.8         2250.2       884.9    2293.1
                >Q 1053            P518.9 -T QA/QC K5249 P519 JSPK)                    2.0       0.0         0.0        010        0.0           0.0            0.0           0.0            0.0        0.0         0.0
                                                    Average % Recovery =         101.66%

                >K5298             P520,1 S&TTISSNP520 (SAWB)                          1.7    3668.5      660.1     2618.4     4707.5          322.8        6721.2        4081.9          1453.0      759.4    2727.1
                >Q 1062            P520,1 AA S&T QA/QC K5298 (SPK)                     1.6       0.0         0.0        0.0        0.0           0.0            0.0           0.0            0.0        0.0         0.0
                                                    Average % Recovery =         102.040/6

                >K5346             P520,1 S&T7ISS NP521 (TBCB)                         1.6       30.5        16.8       26.4     86.2           27.6            30.5         44.5            0.0        0.0       11.4
                >Q 1065            P520.1 AA S&T QA/QC K5346 JSPKJ                     1.6       0.0         0.0        0.0        0.0           0.0            0.0           0.0            0.0        0.0         0.0
                                                    Average % Recovery =         97.30%





                                                               MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks, Spikes and QC Data




                                                                                                C4-         CI-        C2-        C3-           Ci-            C2-           C3-            C4-        Cl-    C2-
                   FILE                 QC                 DESCRIPTION SAMPLE NAPH FLUOR FLUOR FLUOR                                       PHEN +        PHEN +         PHEN +        PHEN +          DBT     DBT
                                  BATCH                                         WEIGHT                                                     ANTHRA        ANTHRA         ANTHRA        ANTHRA
                                                                                  (g dry)      (ppb)      (ppb)        (ppb)    (ppb)           (ppb)          (ppb)        (ppb)          (ppb)      (ppb)   (ppb)


               >K5250             P522,3 S&TTISSUEP522 (LPGO)                         1.9   4322.3 1033.0 3302.7 3869.0                      3038.1        5237.4         3362.8         1440.9      740.2    1850.2
               >Q 1108            P522,3 -T QA/QC K5250 P522 (SPK)                    1.9       0.0         0.0        0.0        0.0           0.0            0.0           0.0            0.0        0.0         0.0
                                                   Average % Recovery =         101.33%

               >K5257           P526,7,9S&TTISSUESP529 (PBIB)                         2.8      25.4         9.9        27.3       0.0           24.3           36.3         63.2           42.5        7.4      20.8
               >Q1114             P522,3 .T QA/QC K5257 P523 (SPK)                    2.8       0.0         0.0        0.0        0.0           0.0            0.0           0.0            0.0        0.0         0.0
                                                   Average % Recovery =         91.070/6

               >K5347             P524.5)&T TISSUE NP524 (TBCB)                       2.5      25.9         9.8        18.3     32.3            14.3           19.6         --32.5         12.1        0.0         0.0
               >QI117             P524,5 -.T QA/QC K5347 P524 JSPK)                   2.5       0.0         0.0        0.0        0.0           0.0            0.0           0.0            0.0        0.0         0.0
                                                   Average % Recovery           97.68%

               >K5170             P524,5 S&T TISSUE P525 ( BBSD                       2.9      25.7         7.5        36.3     59.9            15.6           29.4         39.5           30.5        5.0      14.8
               >Q 1183            P524.5,.T QA/QC K5170 P525 jSPK)                    2.8       0.0         0.0        0.0        0.0           0.0            0.0           0.0            0.0        0.0         0.0
                                                   Average % Recovery =         94.93%

               >KS386           P526.7,9;&TTISSUES P526 (GBSC)                        2.1    7067.2     2365.1     5092.8     7659.2         3266.0        6289.1        12037.5        8399.3       552.5    1788.5
               >Q 1192          P526,7,9       S&T QA/QC(K5386)P526                   2.1    6526.9     2010.2     4165.1     6534.3         3667.6        6899.1        13389.4        9737.8       574.0    1900.5


               >Q 1217          P526,7.9       S&T QA/QC(K5398)P527                   2.5      29.3         0.0        0.0        0.0           13.3           28.0         26.8           17.2        0.0         7.3
               >K5398           P526,7,95&TnSSUESP527 (BHKF)                          2.5      24.2         0.0        14.7     30.9            11.8           31.3         23.1           14.6        0.0         5.6
               >Q 1219          P526,7.9         S&T SPK(K5398) P527                  2.5       0.0         010        0.0        0.0           0.0            0.0           0.0            0.0        0.0         0.0
                                                   Average % Recovery =         103.840/6

               >Q 1335          P526,7,9       S&T QA/QC(K5280)P529                   2.3      26.7         810        30.9     50.1            39.3           73.5         69.6           42.3       12.4      32.8
               >K5280           P526,7,9 S&T TISSUES P529 (CBSP)                      2.3      31.4         8.7        33.2       0.0           45.5           78.3         80.3           55.3       11.8      38.9
               >Q 1337          P526.7,9         S&T SPK(K5280) P529                  2.2       0.0         0.0        0.0        0.0           0.0            0.0           0.0            0.0        0.0         0.0
                                                   Average % Recovery =         87.92%

               >Q 1707               P531      S&T QA/QC K5135 P531                   1.6       0.0         0.0        0.0        0.0           0.0            0.0           0.0            0.0        0.0         0.0
               >K5135                P531      S&TTISSP531 (LMSP)                     1.6       0.0         0.0        0.0        0.0           0.0            0.0           0.0            0.0        0.0         0.0
               >Q1709                P531        S&T K5135+MS P531                    1.6       0.0         0.0        0.0        0.0           0.0            0.0           0.0            0.0        0.0         0.0
                                                   Average % Recovery =         89.51%





                                                          MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks. Spikes and QC Data




                                                                                        C4-       CI_       C2-       C3-          CI_          C2-          C3-           C4-      Cl- C2-
                  FILE               QC               DESCRIPTION SAMPLE NAPH FLUOR FLUOR FLUOR                               PHEN +       PHEN +       PHEN +       PHEN +        DBT DBT
                                BATCH                                    WEIGHT                                              ANTHRA ANTHRA ANTHRA ANTHRA
                                                                           (g dry)      (ppb)    (ppb)      (ppb)    (ppb)         (ppb)        (ppb)        (ppb)       (ppb)    (ppb) (ppb)










              DUPLICATE RE-EXTRACTIONS


              >K5W3             P503.4 S&T TISSUE P503 (GBOB)                 2.6       19.5      6.7       21.4      0.0          31.0         48.9         54.3        37.4       7.8      23.4
              >K5003            P514,5         S&T TISSUE P514                2.5       0.0       0.0       31.7     37.0          22.9         47.1         45.5        33.8       4.5      14.5

              >K5009            P503,4!kT TISSUE P503 (GBCR)                  2.4       28.6      10.3      30.7      0.0          28.6         44.0         40.4        27.0       9.4      19.1
              >K5009            P524.5         S&T TISSUE P525                2.4       25.4      11.7      39.9     73.8          23.9         52.7         48.1        27.9       3.5      15.3


              >K5015            P503,4 .&TTISSUE P503 (BRCL)                  2.6       23.3      0.0       15.1      0.0          15.7         33.0         37.2        31.7       0.0      16.1
              >K5015            P514,5         S&T TISSUE P514                2.5       0.0       0.0       29.5      0.0          11.8         24.0         27.6          0.0      4.8      11.5
        co
              >K5039            P503,4 S&T TISSUE P503 (GBHR)                 3.1       55.7      0.0       0.0       0.0          26.7         33.8         28.6        38.5       010      18.4
              >K5039            P514,5         S&T TISSUE P514                3.1       18.1      6.5       0.0      50.8          27.6         31.9         32.8        23.1       0.0        9.6

              >K5075            P503,45&TTISSUEP503 (MBEM)                    2.2       20.9      0.0       0.0       0.0          10.1         19.8         17.0        16.1       0.0      11.7
              >K5075            P514,5         S&T TISSUE P514                2.2       22.1      0.0       23.0      0.0          13.8         20.2         31.8        14.4       0.0        9.3





                                                              MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks, Spikes and QC Data




                                                                                               C3-               Ci-          ci-         C2-          C3-         C4-       DBT         TOTAL
                  FILE                 QC                  DESCRIPTION SAMPLE                 DBT FLUORANTH              CHRYS CHRYS CHRYS CHRYS                                       ALKYL +
                                  BATCH                                        WEIGHT                   +PYRENES                                                                      S & T PAH
                                                                                 (g dry)      (ppb)            (ppb)        (ppb)        (ppb)       (ppb)        (ppb)      (ppb)       (ppb)



              LABORATORY REFERENCE MATERIAL


              >W2639              P505,6             GERG STD. CHK 11                1.0    542.6              104.8        103.7        193.6       105.7        111.8      187.5         16430.6
              >W2897              P507.8             GERG STD. CHK 11                1.0    452.0              72.8         76.4         108.5       45.9         43.0       196.3         14566.9
              >W2961              P507,8             GERG M. CHK 11                  1.0    485.3              81.9         86.4         107.1       54.5         42.8       188.2         14092.0
              >W4149              P512.3             GERG STD. CHK 11                1.0    326.1              70.5         87.0         85.2        47.5         34.5       145.5         11422.6
              >W4157              P514.5             GERG STD. CHK 11                1.0    220.8              63.9         62.3         79.8        42.7         104.4      133.0         10638.0
              >W4229              P518,9             GERG STI), CHK 11               1.0    507.0              87.4         74.9         124.9       102.8        71.7       141.5         13801.9
              >W4240              P520.1             GERG STD. CHK 11                1.0    521.4              105.1        84.2         126.3       69.7         52.2       152.4         14471.9
              >W4272              P522,3             GERG STD. CHK 11                1.0    488.5              91.3         87.2         133.5       63.3         34.3       173.4         13348.4
              >W4271              P524.5             GERG SM. CHK 11                 1.0    471.1              87.3         74.7         134.5       77.3         72.3       128.9         13072.6
              >W4407            P526.7.9             GERG STD. CHK 11                1.0    673.5              150.3        89.7         158.2       81.3         86.3       214.0         15992.2
              >W4936                 P528            GERG STD. CHK 11                1.0    333.5              83.1         70.4         84.9        40.3         24.7       131.4         13046.2
              >W4807                 P531            GERG STD. CHK 11                1.0    377.4              91.7         67.4         88.8        66.2         65.8       145.7         12565.5
              >W5005                 P532            GERG STD. CHK 11                1.0    394.2              104.1        77.7         104.0       44.4         53.7       124.7         12582.4


              average                                                                       445.6              91.9         80.1         117.6       64.7         61.4       158.7         13540.9
                                                                                            24.9%             22.8%         13.2%       26.7%       32.7%        42.6%       17.9%            11.6%


              GERG chk 2 - avg. of 50                                                       398.0              83.7         81.6         103.2       52.9         50.7       152.4         13331.2
                                                                                            28.2%             24.6%         19.4%       28.5%       34.5%        42.4%       17.2%
              BLANKS


              >QO685              P503.4          S&T BLANK P503                   10.0        0.0               0.0          0.0         0.0          0.0         0.0         0.1               6.0
              >QO688              P503.4          S&T BLANK P504                   10.0        010               0.0          0.0         0.0          0.0         0.0         0.1               2.6
              >QO740              P505,6          S&T BLANK P505                   10.0        0.0               0.0          0.0         0.0          0.0         0.0         0.1               7.9
              >Q0743              P505.6          S&T BLANK P506                   10.0        0.0               010          0.0         0.0          0.0         0.0         0.1               6.1
              >QO746              P507,8          S&T BLANK P507                   10.0        0.0               0.0          0.0         0.0          0.0         0.0         0.1               5.3
              >Q0749              P507,8          S&T BLANK P508                   10.0        0.0               0.0          0.0         0.0          0.0         0.0         0.2               4.8
              >Q0770             P510,11          S&T BLANK P510                   10.0        0.0               0.0          0.0         0.0          0.0         0.0         0.1               6.7
              >QO784             P510,11          S&T BLANK P511                   10.0        0.0               0.0          0.0         0.0          0.0         0.0         0.1               5.1
              >QO787              P512,3          S&T BLANK P512                   10.0        0.0               0.0          0.0         0.0          0.0         0.0         0.1               5.7
              >Q0790              P512.3          S&T BLANK P513                   10.0        0.0               0.0          0.0         0.0          0.0         0.0         0.1               4.2
              >Q 1022             P514.5          S&T BLANK P514                   10.0        0.0               0.0          0.0         0.0          0.0         0.0         0.1               9.3
              >Q 1025             P514,5          S&T BLANK PSI 5                  10.0        0.0               0.0          0.0         0.0          0.0         0.0         0.1               8.3
              >Q1028              P516.7          S&T BLANK P516                   10.0        0.0               0.0          0.0         0.0          0.0         0.0         0.1               6.1
              >Q 1040             P516,7          S&T BLANK P517                   10.0        0.0               0.0          0.0         0.0          0.0         0.0         0.1               5.3
              >Q1043              P518,9          S&T BLANK P518                   10.0        0.0               0.0          0.0         0.0          0.0         0.0         0.1               4.4





                                                              MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks, Spikes and QC Data




                                                                                               C3-              Ci-          Ci-          C2-         C3-          C4-       DBT        TOTAL
                   FILE                QC                  DESCRIPTION SAMPLE                  DBT    FLUORANTH          CHRYS        CHRYS       CHRYS        CHRYS                  ALKYL +
                                  BATCH                                        WEIGHT                   +PYRENES                                                                     S & T PAH
                                                                                 (g dry)       (ppb)          (ppb)        (ppb)          (ppb)       (ppb)       (ppb)      (ppb)       (ppb)


               >Q 1054            P518,9          S&T BLANK P519                   10.0        0.0              0.0          0.0          0.0         0.0          0.0        0.2              13.4
               >Q1063             P520,1               S&T BLANK P520              10.0        0.0              0.0          0.0          0.0         0.0          0.0        0.1              8.6
               >Q1066             P520,1               S&T BLANK P521              10.0        0.0              0.0          0.0          0.0         0.0          0.0        0.1              6.0
               >Q 1109            P522.3          S&T BLANK P522                   10.0        0.0              0.0          0.0          0.0         0.0          0.0        0.2              12.8
               >Q1115             P522,3          S&T BLANK P523                   10.0        0.0              0.0          010          0.0         0.0          0.0        0.1              4.4
               >Q1118             P524,5     S&T TISSUE BLANK P524                 10.0        0.0              0.0          0.0          0.0         010          0.0        0.1              7.6
               >Q 1184            P524,5     S&T TISSUE BLANK P525                 10.0        0.0              0.0          0.0          0.0         0.0          0.0        011              4.8
               >Q 1218           P526.7.9         S&T BLANK P527                   10.0        0.0              0.0          0.0          0.0         0.0          0.0        0.2              6.5
               >Q 1336           P526,7.9         S&T BLANK P529                   10.0        0.0              0.0          0.0          0.0         0.0          0.0        0.0              5.2
               >Q1258                P528   S&T 71SSUE BLANK P528                  10.0        0.0              0.0          0.0          0.0         0.0          0.0        0.1              4.4
               >Q 1708              P531 S&T TISSUE BIANK P531                     10.0        0.0              0.0          0.0          0.0         0.0          0.0        0.1              5.8

               average                                                                         0.0              0.0          0.0          0.0         0.0          0.0        0.1              6.4
                                                                                               0.096          0.0%         0.00/0         0.0%        0.0%        0.0%     40.3%            38.0%
               NIST SRM 1974 - TISSUE SAMPLE
               Values for SRM 1974


               >Q1023             P514.5               S&T NIST P514               0.60        187.0          191.9        73.7           62.3        0.0          0.0        5.9          4492.2
               >Q 1026            P514,5               S&T NIST P515               0.60        116.2          133.1        59.0           39.8        0.0          0.0        5.5          3067.2
               >Q1041             P516.7               S&T NIST P517               0.60        204.0          194.2        61.7           49.2        0.0          0.0        6.8          4152.6
               >Q 1044            P518,9               S&T NIST P518               0.60        329.8          285.4        85.0           61.9        0.0          0.0        7.2          5485.8
               >Q 1055            P518.9               S&T NIST P519               0.60        151.3          129.5        47.5           36.1        0.0          0.0        3.6          2909.2
               >Q 1064            P520,1                 S&T NIST P520             0.60        148.4          134.9        52.7           40.8        0.0          0.0        5.4          3070.1
               >Q 1067            P520.1                 S&T NIST P521             0.60        255.9          230.3        79.3           55.0        16.8        28.7        8.0          4871.7
               >Q1110             P522.3               S&T NIST P522               0.60        413.4          375.1        132.0          96.2        38.7         0.0        15.5         6764.5
               >Q1119             P524.5                 S&T NIST P524             0.60        214.7          199.0        51.4           46.7        34.7        63.6        8.0          4025.3
               >Q 1185            P524,5                 S&T NIST P525             0.60        173.2          134.6        46.5           32.7        20.5        19.1        4.6          3036.5

               average                                                                         219.4          200.8        68.'9          52.1        27.7        37.1        7.0          4187.5
                                                                                               39.4%          37.6%       35.7%        33.9%        33.4%       51.5%      44.2%            28.6%


               REPLICATES AND SPIKED SAMPLES


               >QO684             P503.4      S&T QA/QC(K5039)P503                   3.1       15.8             9.1          4.4          18.0        0.0          0.0        1.1           333.3
               >K5039             P503.4 SrT TISSUE P503 (GBHR )                     3.1       18.7             14.4         4.4          23.0        010          0.0        1.2           418.5



               >QO687             P503,4      S&T QA/QC(K5159)P504                   2.7       14.1             7.7          3.0          6.0         0.0          0.0        1.0           468.1





                                                           MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks, Spikes and QC Data




                                                                                         C3-              Ci-        Cl-         C2-         C3-         C4-      DBT       TOTAL
                  FILE               QC                DESCRIPTION SAMPLE                DBT    FLUORANTH         CHRYS       CHRYS       CHRYS       CHRYS                ALKYL +
                                BATCH                                     WEIGHT                  +PYRENES                                                                S & T PAH
                                                                            (g dry)      (ppb)          (ppb)       (ppb)        (ppb)      (ppb)       (ppb)     (ppb)      (ppb)


              >K5159            P503,4   S&T 71SSUE P504 (VBSP)                2.7       12.6             7.1        0.0         0.0         0.0         0.0       0.7           368.8
              >g0689            P503.4        S&T SPIKE(K5159)P504             2.7       0.0              0.0        0.0         0.0         0.0         0.0      32.1
                                               Average % Recovery =       102.71%                                                                               84.9%

              >Q0739            P505,6     S&T QA/QC(K5222)P505                2.1       150.8          49.7         0.0         0.0         0.0         0.0       5.7           1778.1
              >K5222            P505,6 S&T TISSUE P505 (MSPC)                  2.1       146.7          57.3         17.8        11.9        0.0         0.0       5.2           1765.2
              >Q0741            P505.6        S&T SPIKE(K5222)P505             2.2       0.0              0.0        0.0         0.0         0.0         0.0      43.1
                                               Average % Recovery =       109.33%                                                                               82.2%

              >Q0742            P505,6     S&T QA/QC(K504O)P506                3.3       20.7             9.9        0.0         0.0         0.0         0.0       1.5           525.0
              >K5040            P505,6 S&TnSSUE P506 (GBHR)                    3.3       16.6             9.0        7.8         11.7        0.0         0.0       0.9           468,3
              >Q0744            P505,6        S&T SPIKE(K504O)P506             3.3       0.0              0.0        0.0         0.0         0.0         0.0      18.3
                                               Average % Recovery =       86.02%                                                                                57.4%

              >Q0745            P507,8     S&T QA/QC K5118 P507                3.4       16.5           11.0         6.3         6.6         0.0         0.0       1.1           197.1
              >K5118            P507,8 S&T TISSUE P507 (SAMP)                  3.4       14.3             7.2        3.8         0.0         0.0         0.0       0,7           178.7
              >Q0747            P507,8        S&T SPK K5118 P507               3.4       0.0              0.0        0.0         0.0         0.0         0.0      25.2
                                               Average % Recovery =       85.84%                                                                                82.8%

              >Q0748            P507,8     S&T QA/QC K5064 P508                2.7       20.0           23.2         13.1        16.7        10.8        6.8       2.1           439.7
              >K5064            P507.8 S&T TISSUE P508 (GBYC)                  2.7       27.5           32.0         13.7        20.2        10.0        6.5       3.8           506.8
              >Q0750            P507,8        S&T SPK K5064 P508               2.7       0.0              0.0        0.0         0.0         0.0         0.0      32.1
                                               Average % Recovery =       82.64%                                                                                77.5%

              >Q0769          P510.11      S&T QA/QC(K5065)P510                3.0       20.2           31.1         12.8        6.2         7.4         0.0       4.5           539.6
              >K!5065         P510.11   S&TTISSUEP510 (GBYC)                   3.0       24.5           17.6         13.8        14.1        3.8         0.0       2.6           465.5
              >Q0771          P510.11         S&T SPK(K5065) P5 10             3.0       0.0              0.0        0.0         0.0         0.0         0.0      35.1
                                               Average % Recovery =       91.17%                                                                                98.7%

              >Q0783          P510.11      S&T QA/QC(K5119)P511                3.6       7.5              0.0        0.0         010         0.0         0.0       0,7           11118
              >K5119          P510.11   S&T TISSUE P511 (SAMP)                 3.9       5.8              0.0        0.0         0.0         0.0         0.0       0.3             98.2
              >Q0785          P510,11         S&T SPK K5119 P511               3.6       0.0              0.0        0.0         0.0         0.0         0.0      22.3
                                               Average % Recovery =       78.43%                                                                                78.7%


              >Q0786            P512.3'QA/QC K5170 P512(BBSD)                  2.8       6.5              0.0        2.6         5.7         0.0         6.2       0.7           242.8
              >Q0788            P512,3        S&T SPK(K5170) P512              2.8       0.0              0.0        0.0         0.0         0.0         0.0      24.2
                                               Average % Recovery =       80.42%                                                                                65.6%





                                                              MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks, Spikes and QC Data




                                                                                                C3-              ci-          ci-          C2-         C3-          C4-       DBT       TOTAL
                   FILE                QC                  DESCRIPTION SAMPLE                   DBT    FLUORANTI-i        CHRYS        CHRYS       CHRYS        CHRYS                  ALKYL +
                                  BATCH                                        WEIGHT                   +PYRENES                                                                      S & T PAH
                                                                                 (g dry)        (ppb)            (ppb)       (ppb)       (ppb)        (ppb)        (ppb)      (ppb)      (ppb)



               >Q0789             P512,3      S&T QA/QC(K5242)P513                   1.3        56.5             76.3         16.0         7.6         3.6          0.0        2.3           1231.0
               >K5242             P512,3 S&TTISSUEP513 (MBHI)                        1.4        53.0             64.5         14.8         7.8         0.0          0.0        2.3           1211.3
               >QO791             P512,3           S&T SPK(K5242) P513               1.3        0.0              0.0          0.0          0.0         0.0          0.0       44.8
                                                   Average % Recovery =         80.580A                                                                                     56.4%

               >K5039             P514,5 S&TTISSUE P514 (GBHR)                       3.1        12.3             9.8          5.2          10.5        0.0          0.0        0.9            779.8
               >Q1021             P514.5           S&T SPK K5039 P514                3.1        0.0              0.0          0.0          0.0         0.0          0.0       25.2
                                                   Average % Recovery =         96.68%                                                                                      75.2%

               >K5217             P514,5    S&TTISSUEP515 (BSSI)                     2.3        38.4             42.4         16.6         16.5        0.0          0.0        4.2           2236.3
               >Q 1024            P514,5           S&T SPK K5217 P515                2.3        0.0              0.0          0.0          0.0         0.0          0.0       31.2
                                                   Average % Recovery =         83.47%                                                                                      61.8%

               >K5057             P516.7 S&T TISSUE P516 (GBTD)                      3.2        141.2            37.5         27.1         42.1        19.8         10.4       3.4           1267.8
               >QI027             P516.7           S&T SPK K5057 P516                3.2        0.0              0.0          0.0          0.0         0.0          0.0       26.6
                                                   Average % Recovery =         97.50%                                                                                      74.7%

               >K5255             P516,7    S&TTISSUEP517 (PBIB)                     3.7        9.9              18.4         4.9          0.0         0.0          0.0        1.7            434.5
               >QI039             P516,7 -T QA/QC K5255 P517 JSPK)                   3.7        0.0              0.0          0.0          0.0         0.0          0.0       21.4
                                                   Average % Recovery =         91.32%                                                                                      73.0%

               >K5333             P518,9 S&T TISSUE P518 (TBMK)                      3.2        5.9              9.2          0.0          0.0         0.0          0.0        1.7            248.5
               >QI042             P518,9 -r QA/QC K5333 P518 (SPKI                   3.1        0.0              0.0          0.0          0.0         0.0          0.0       22.6
                                                   Average % Recovery =         80-81%                                                                                      63.9%

               >K5249             P518,9 S&T TISSUE P519 (LPGO)                      2.0    2412.2            1457.2        250.4        186.0         58.1         44.4      122.3         52036.9
               >QI053             P518,9,T QA/QC K5249 P519 JSPK)                    2.0        0.0              0.0          0.0          0.0         0.0          0.0       159.2
                                                   Average % Recovery =        101.66%                                                                                      72.6%

               >K5298             P520,1 S&TTISSNP520 (SAWB)                         1.7    2511.6               833.9      143.3          70.5        30.4         25.3      78.0          37582.7
               >Q 1062            P520, 1AA S&T QA/QC K5298 (SPK)                    1.6        0.0              0.0          0.0          0.0         0.0          0.0       144.4
                                                   Average % Recovery =        102.04%                                                                                     103.8%

               >K5346             P520,1 S&TTISS NP521 (TBCB)                        1.6        0.0              13.1         4.7          10.5        0.0          0.0        3.0            588.6
               >Q1065             P520.1 AA S&T QA/QC K5346 (SPK)                    1.6        0.0              0.0          0.0          0.0         0.0          0.0       44.8
                                                   Average % Recovery =         97.30%                                                                                      67.9%





                                                             MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks, Spikes and QC Data




                                                                                             C3-             Cl-         Ci-          C2-         C3-         C4-       DBT       TOTAL
                  FILE                QC                 DESCRIPTION SAMPLE                  DBT   FLUORANTH          CHRYS       CHRYS       CHRYS        CHRYS                 ALKYL +
                                 BATCH                                       WEIGHT                  +PYRENES                                                                  S & T PAH
                                                                               (g dry)       (ppb)           (ppb)      (ppb)        (ppb)       (ppb)        (ppb)     (ppb)      (ppb)


               >K5250            P522.3 S&TTISSUE P522 (LPGO)                     1.9     1821.7          1118.8       357.3        192.2        56.3         41.8      108.1        45553.7
               >Q1108            P522,3,T QA/QC K5250 P522 JSPKI                  1.9        0.0             0.0         0.0          0.0         0.0         0.0       146.7
                                                 Average % Recovery =        101.33%                                                                                 69.4%

               >K5257          P526,7.9S&T TISSUES P529 (PBIB)                    2.8        15.2            26.4        0.0          0.0         0.0         0.0        2.4           525.0
               >Q1114            P522.3 -T QA/QC K5257 P523 JSPK)                 2.8        0.0             0.0         0.0          0.0         0.0         0.0       24.5
                                                 Average % Recovery =        91.07%                                                                                  61.2%

               >K5347            P524.5)&T71SSUENP524 (TBCB)                      2.5        0.0             9.9         2.6          6.7         0.0         0.0        1.0           394.6
               >QI117            P524.5 Ir QA/QC K5347 P524 (SPK)                 2.5        0.0             0.0         0.0          0.0         010         0.0       24.9
                                                 Average % Recovery          97-68%                                                                                  59.2%

               >K5170            P524.5 S&T TISSUE P525 (BBSD                     2.9        12.6            11.6        2.4          7.5         5.9         6.8        1.0           398.8
               >Q 1183           P524,5 -T QA/QC K5170 P525 (SPK)                 2.8        0.0             0.0         0.0          0.0         0.0         0.0       26.3
                                                 Average % Recovery =        94.93%                                                                                  70.7%

         00    >K5386          P526,7.9')&T TISSUES P526 (GBSC)                   2.1    4805.0           7070.1      2737.8      2798.2       1118.5       246.0       129.6       103940.1
               >Q 1192         P526,7.9       S&T gA/QC(K5386)PS26                2.1    5044.5           9044.9      2857.0      2766.9        850.1       272.7       148.9       107104.9


               >Q 1217         P526,7.9       S&T QA/QC(K5398)P527                2.5        9.8             15.8        4.2          8.6         0.0         0.0        0.8           308.3
               >K5398          P526,7.9;&TTISSUESP527 (BHKF)                      2.5        7.9             14.1        0.0          0.0         0.0         0.0        1.2           315.0
               >Q1219          P526,7,9        S&T SPK(K5398) P527                2.5        0.0             0.0         0.0          0.0         0.0         0.0       33.7
                                                 Average % Recovery =        103.84%                                                                                 80.2%

               >Q1335          P526.7,9       S&T gA/QC(K5280)P529                2.3        37.3            57.7        49.6        53.9        20.2         0.0        2.2           1002.2
               >K5280          P526,7.9 S&T TISSUES P529 ( CBSP)                  2.3        47.5            71.2        82.4        82.1        40.8         15.9       2.2           1139.8
               >Q1337          P526,7,9        S&T SPK(K5280) P529                2.2        0.0             0.0         0.0          0.0         0.0         0.0       40.1
                                                 Average % Recovery =        87.92%                                                                                  84.90/6

               >Q1707               P531      S&T QA/QC K5135 P531                1.6        0.0             10.5        0.0          0.0         0.0         0.0        1.4             85.6
               >K5135               P531      S&TTISSP531 (LMSP)                  1.6        0.0             14.9        0.0          0.0         0.0         0.0        0.8             97.5
               >Q1709.              P531       S&T K5135+MS P531                  1.6        0.0             0.0         0.0          0.0         0.0         0.0       44.8
                                                 Average % Recovery =        89.51%                                                                                  69.1%





                                                          MUSSEL WATCH YEAR VI - Bivalve Aromatics Blanks, Spikes and QC Data




                                                                                         C3-             Ci-         Ci-         C2-         C3-         C4-       DBT     TOTAL
                 FILE                QC                DESCRIPTION SAMPLE                DBT FLUORANTH CHRYS CHRYS CHRYS CHRYS                                            ALKYL +
                                BATCH                                     WEIGHT                 +PYRENES                                                                S & T PAH
                                                                            (g dry)      (ppb)           (ppb)       (ppb)      (ppb)       (ppb)       (ppb)     (ppb)      (ppb)









              DUPLICATE RE-EXTRACTIONS


              >K5003            P503,4S&TTISSUEP503 (GBOB)                     2.6       30.2            94.3        26.0        13.0        0.0         0.0       5.0          1120.7
              >K5003            P514.5         S&T TISSUE P514                 2.5       16.9            65.6        12.5        11.3        0.0         0.0       2.7           897.9

              >K5009            P503,4&TIISSUEP503 (GBCR)                      2.4       18.7            45.0        0.0         0.0         0.0         0.0       2.0           680.5
              >K5009            P524.5         S&T TISSUE P525                 2.4       16.2            46.0        5.0         7.2         0.0         0.0       1.6           765.1

              >K5015            P503,4 .&T TISSUE P503 (BRCL)                  2.6       18.7            22.7        0.0         0.0         010         0.0       2.1           375.5
              >K5015            P514.5         S&T TISSUE P514                 2.5       14.2            17.3        0.0         0.0         0.0         0.0       2.4           262.6

              >K5039            P503.4 S&T TISSUE P503 (GBHR)                  3.1       18.7            14.4        0.0         0.0         0.0         0.0       2.4           391.1
              >K5039            P514,5         S&T TISSUE P514                 3.1       12.3            9.8         5.2         10.5        0.0         0.0       2.5           342.5

              >K5075            P503,45&TTISSUEP503 (MBEM)                     2.2       9.9             8.0         0.0         0.0         0.0         0.0       2.6           209.5
              >K5075            P514,5         S&T TISSUE P514                 2.2       15.1            8.7         0.0         0.0         0.0         0.0       0.5           215.9




I
I
I
I
I
I


I
I
I             Pesticides and PCBs Data
I
I
I
I
I
I
I
I
1                       80






                                                                          MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Data





                   SITE       RAW        DESIGNATOR FOLDER                     HCB LINDANE          HEPTA-    ALDRIN HEPTA                    ALPHA-           TRANS-      DIELDRIN        MIREX     2,4'DDE
                   AND        FILE            AND                                                   CHLOR                 EPOMDE       CHLORDANE         NONACHLOR                                  (0,P'DDE)
                   STATE                     STATION                           (ppb)       (ppb)       (ppb)       (ppb)                         (ppb)             (ppb)         (ppb)       (ppb)       (ppb)


                   01 TX      K5135P         LMS13-1           P505            0.00        0.00        0.00        0.00        0.03              0.01              0.01          0.01        0.04            0.00
                   01 TX      K5136P         LMSB-2            P508            0.00        0.00        0.00        0.00        0.09              2.54              0.26          0.45        0.03            0.00
                   01 TX      K5137P         LMSB-3            P511            0.00        0.00        0.00        0.00        0.00              3.10              0.33          0.31        0.00            0.18
                   03 TX      K5087P         CCIC-1            P504            0.01        0.19        0.00        0.00        0.13              1.68              0.18          2.15        0.00            1.55
                   03 TX      K5088P         CCIC-2            P507            0.05        0.16        0.00        0.41        0.01              0.61              0.35          1.69        0.00            0.01
                   03 TX      K5089P         CCIC-3            13510           0.00        0.59        0.00        0.00        0.00              1.64              0.20          1.05        0.00            0.18
                   04 q-X     K5147P         ABLR- I           P504            0.01        0.00        0.26        0.00        0.00              1.72              0.33          0.00        0.03            0.00
                   04 TX      K5148P         ABLR-2            P508            0.00        0.00        0.38        0.00        0.00              1.22              0.40          0.00        0.04            0.00
                   04 TX      K5149P         ABLR-3            P511            0.00        0.00        0.29        0.23        0.00              1.82              0.65          0.13        0.00            0.29
                   05 TX      K514 1 P       CBCR-1            P504            0.00        0.00        0.00        0.00        0.03              1.21              0.19          0.00        0.00            0.00
                   05 TX      K5142P         CBCR-2            P508            0.01        0.21        0.00        0.00        0.00              1.03              0.00          0.00        0.00            0.00
                   05 TX      K5143P         CBCR-3            P511            0.00        0.14        0.00        0.10        0.00              0.85              0.51          0.13        0.00            0.00
                   06 TX      K5099P         MBAR-1            P504            0.01        0.14        0.00        0.00        0.10              3.24              0.22          0.00        0.01            0.00
                   06 TX      K5100P         MBAR-2            P507            0.00        0.10        0.10        0.00        0.17              0.61              0.49          0.61        0.02            0.00
                   06 TX      K5101P         MBAR-3            13511           0.00        0.29        0.00        0.06        0.03              0.17              0.31          0.49        0.00            0.09
                   07 TX      K5111P         SAPP-1            P504            0.01        0.25        0.23        0.00        0.12              2.40              0.19          0.91        0.00            1.19
        00         07 TX      K5112P         SAPP-2            P507            0.01        0.15        0.117       0.00        0.32              0.30              0.59          0.93        0.00            0.08
                   07 TX      K5113P         SAPP-3            P525            0.00        0.66        0.27        0.16        0.16              1.21              0.64          0.92        0.04            0.58
                   08 TX      K5117P         SAMP-1            P504            0.00        0.41        0.00        0.00        0.28              1.15              0.29          1.90        0.00            0.37
                   08 TX      K5118P         SAMP-2            P507            0.00        0.57        0.00        0.00        0.29              0.67              0.66          1.03        0.00            0.00
                   08 TX      K5119P         SAMP-3            P511            0.00        0.53        0.01        0.18        0.66              2.61              0.91          0.69        0.00            0.00
                   09 TX      K5105P         ESSP-1            P504            0.02        0.14        0.00        0.00        0.21              0.22              0.28          0.64        0.00            2.36
                   09 TX      K5106P         ESSP-2            P507            0.00        0.10        0.07        0.00        0.29              0.47              0.66          0.81        0.00            0.00
                   09 TX      K5107P         ESSP-3            P511            0.00        0.28        0.00        0.00        0.11              0.46              0.40          0.47        0.00            0.00
                   12 TX      K5129P         MBGP-1            P504            0.01        0.27        0.12        0.00        0.62              1.15              1.35          1.75        0.00            0.00
                   12 TX      K5130P         MBGP-2            P508            0.00        0.01        0.39        0.00        0.09              3.33              0.91          0.58        0.00            0.00
                   12 TX      K5131P         MBGP-3            P511            0.00        0.27        0.54        0.10        0.06              2.58              1.12          0.58        0.00            0.00
                   11 TX      K5123P         MBLR-1            P504            0.02        0.14        0.00        0.00        0.00              1.39              0.53          0.93        0.07            2.92
                   11 TX      K5124P         MBLR-2            P507            0.00        0.07        0.00        0.00        0.07              1.09              0.58          0.50        0.00            2.77
                   11 TX      K5125P         MBLR-3            P511            0.00        0.00        0.00        0.34        0.05              2.96              0.90          0.41        0.00            3.15
                   13 TX      K508 1 P       MBTP-1            P504            0.00        0.00        0.00        0.00        0.04              3.53              0.34          1.06        0.83            0.47
                   13 TX      K5082P         MBTP-2            P507            0.00        0.04        0;11        0.00        0.04              0.49              0.63          0.30        0.61            0.13
                   13 TX      K5083P         MBTP-3            P525            0.02        0.42        0.15        0.02        0.00              1.83              0.73          0.91        0.14            0.67
                   14 TX      K5075P         MBEM-1            P514            0.00        0.53        0.00        0.00        0.29              0.47              0.67          0.96        0.00            0.12
                   14 TX      K5076P         MBEM-2            P507            0.01        0.16        0.00        0.00        0.30              0.75              0.46          0.60        0.07            0.34
                   14 TX      K5077P         MBEM-3            P510            0.00        0.34        0.00        0.00        0.08              2.28              0.52          1.20        0.06            0.12
                   72 TX      K5015P         BRCL- 1           P514            0.40        0.63        0.23        0.11        0.00              0.74              0.78          0.83        0.47            0.20
                   72 TX      K5016P         BRCL-2            P506            0.09        0.25        0.00        0.00        0.00              0.68              0.38          0.78        0.33            0.37
                   72 TX      K5017P         BRCL-3            P525            0.06        0.50        0.08        0.08        0.00              2.04              0.70          0.95        0.60            0.30






                                                                     MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Data






                  SITE      RAW        DESIGNATOR FOLDER                 HC13 LINDANE         HEPTA-    ALDRIN HEPTA                 ALPI-IA-        TRANS-     DIELDRIN       MIREX    2.4'DDE
                  AND       FILE            AND                                               CHLOR                EPOYJDE     CHLORDANE       NONACHLOR                                 (O.P'DDE)
                  STATE                   STATION                        (ppb)        (ppb)     (ppb)      (ppb)                        (ppb)           (ppb)        (ppb)       (ppb)      (ppb)



                  57 TX     K5021P        BRFS-1           P514          0.32         0.69      0.00       0.00        0.00             1.11            1.16         1.53        4.72           0.41
                  57 TX     K5022P        BRFS-2           P506          0.09         0.20      0.00       0.00        0.00             1.39            1.07         2.27        2.29           0.51
                  57 TX     K5023P        BRFS-3           P510          0.73         0.46      0.04       0.00        0.00             4.25            0.61         2.43        1.72           2.41
                  18 TX     K5009P        G13CR-1          P525          0.01         0.39      0.20       0.10        0.00             1.32            0.99         1.45        0.06           0.24
                  18 TX     K5010P        GBCR-2           P506          0.47         0.17      0.61       0.00        0.00             1.45            1.52         1.21        0.29           0.00
                  18 TX     K501 1P       GBCR-3           P515          0.00         0.73      0.13       0.00        0.12             0.98            1.02         1.20        0.00           0.00
                  58 TX     K5003P        GBOB-1           P514          0.05         1.31      0.20       0.09        0.86             15.53           21.07        5.31        0.21           0.00
                  58 TX     K5004P        GBOB-2           P506          0.00         0.93      0.22       0.00        0.65             32.04           42.53        6.95        0.13           0.00
                  58 TX     K5005P        GBOB-3           P515          0.00         1.33      0.10       0.08        0.52             26.32           34.91        6.88        0.25           0.00
                  16 TX     K5057P        GBTD-1           P516R         0.00         1.76      0.19       0.00        1.10             2.61            2.73         3.75        0.00           0.27
                  16 TX     K5058P        GBTT)-2          P516R         0.00         1.98      0.00       0.00        1.63             2.87            2.96         4.91        0.07           0.23
                  16 TX     K5059P        GBTT)-3          P516R         0.00         1.53      0.00       0.00        1.12             1.76            1.67         3.38        0.00           0.21
                  15 TX     K5063P        GBYC-1           P514          0.00         2.81      0.16       0.00        2.99             5.21            5.46         9.60        0.00           0.00
                  15 TX     K5064P        GBYC-2           P508          0.00         4.00      0.00       0.00        2.81             9.19            5.48         11.70       0.00           0.53
                  15 TX     K5065P        GBYC-3           P510          0.00         2.63      0.08       0.00        2.56             6.82            4.91         7.63        0.00           0.67
                  59TX      K5384P        GBSC - 1         P519          0.00         8.32      4;78       0.00       36.49             63.45           42.75        45.80       0.00           4.66
        00        59 TX     K5384S        GBSC-1           P519R         0.37         8.57      4.77       0.00       40.09             63.68           45.47        51.92       0.00           4.72
        t'D       59 TX     K5385P        GBSC-2           P522          0.00         8.83      5.29       0.00       38.76             61.67           41.40        52.63       0.00           2.07
                  59 TX     K5385S        GBSC-2           P522R         0.00         10.64     5.41       0.00       49.16             80.75           59.49        75.40       0.00           2.91
                  59 TX     K5386P        GBSC-3           P526          0.00         9.48      5.72       0.00       40.84             74.69           47.59        63.83       0.00           9.09
                  17 TX     K5039P        G13HR-1          P514          0.00         1.08      0.86       0.00        0.35             0.75            1.08         2.06        0.04           0.00
                  17TX      K5040P        GBHR-2           P506          0.00         0.69      0.35       0.00        0.51             1.38            1.13         2.12        0.12           0.00
                  17 TX     K5041P        GBHR-3           P510          0.00         1.17      0.25       0.00        0.35             1.93            1.08         2.44        0.05           0.67
                  19TX      K5027P        SI,1313-1        P514          0.00         0.93      0.00       0.00        0.68             0.56            2.20         4.75        0.00           0.68
                  19 TX     K5028P        SLBB-2           P506          0.00         0.65      0.00       0.00        0.63             2.71            2.06         3.93        0.15           0.79
                  19 TX     K5029P        SLBB-3           P525          0.01         0.59      0.20       0.23        0.27             2.74            1.15         2.37        0.28           0.92
                  20 LA     K5033P        CLSIJ-1          P514          0.00         0.75      0.03       0.00        0.21             0.16            0.36         1.55        0.14           0.00
                  20 LA     K5034P        CLSJ-2           P506          0.00         0.00      0.00       0.00        0.00             0.78            0.40         1.39        0.09           1.54
                  20 LA     K5035P        CLSJ-3           P510          0.00         1.06      0.00       0.00        0.20             2.79            0.28         2.09        0.22           0.34
                  60 LA     K5045P        CLLC-1           P514          0.51         1.25      0.00       0.00        3.31             1.73            2.70         4.42        0.15           0.00
                  60 LA     K5046P        CLLC-2           P507          0.40         0.81      0.00       0.00        4.96             2.76            2.07         3.61        0.28           3.97
                  60 LA     K5047P        CLLC-3           P510          0.43         0.89      0.00       0.00        3.73             3.05            2.37         3.58        0.22           3.35
                  21LA      K5069P        JHJH- 1          P514          0.00         0.57      0.08       0.04        0.74             0.82            1.26         5.97        0.30           0.00
                  21LA      K5070P        JHJH-2           P507          0.00         0.28      0.13       0.00        0.84             1.23            0.96         5.26        0.26           0.38
                  21 LA     K5071P        JHJH-3           P510          0.00         0.63      0.06       0.00        0.48             2.01            0.49         3.78        0.20           0.40
                  22 LA     K5159P        VBSP-1           P504          0.00         0.73      0.00       0.00        0.75             4.92            1.80         9.50        0.34           1.87
                  22 LA     K5160P        VBSP-2           P508          0.00         0.54      0.40       0.00        0.93             4.57            1.11         6.62        0.25           0.71
                  22 LA     K5161P        VBSP-3           P512          0.00         0.38      0.65       0.00        0.99             10.78           1.65         7.77        0.44           1.74
                  24 LA     K5189P        ABOB-1           P505          0.00         0.75      0.00       0.00        1.00             1.16            1.17         3.68        0.16           0.00






                                                                            MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Data






                    SITE       RAW        DESIGNATOR FOLDER                     HCB LINDANE           HEPTA-     ALDRIN HEPTA                    ALPHA-           TRANS-       DIELDRIN        MIREX     2,4'DDE
                    AND        FILE            AND                                                     CHLOR                 EPOXIDE      CHLORDANE         NONACHLOR                                   (0,P'DDE)
                    STATE                     STATION                           (ppb)         (ppb)      (ppb)       (ppb)                          (ppb)             (ppb)          (ppb)       (ppb)       (ppb)



                    24 LA      K5190P         ABOB-2            P508            0.00          0.29       0.00        0.00         0.39              2.59              1.24           3.36        0.15            0.00
                    24 LA      K5191P         ABOB-3            P512            0.00          0.33       0.09        0.00         0.44              3.25              1.04           4.31        0.14            0.00
                    25 LA      K5195P         CLCL-1            P505            0.00          0.80       0.00        0.00         0.19              1.06              0.76           2.63        0.00            0.37
                    25 LA      K5196P         CLCL-2            P508            0.00          0.00       0.00        0.00         0.24              2.90              0.23           0.56        0.00            0.00
                    25 LA      K5197P         CLCL-3            P512            0.00          0.07       0.00        0.00         0.26              2.17              0.65           0.98        0.19            0.06
                    26 LA      K5165P         TBLB-1            P505            0.00          0.29       0.20        0.00         0.27              1.03              0.37           0.27        0.02            0.62
                    26 LA      K5166P         T131,13-2         P508            0.00          0.29       0.33        0.00         0.19              1.36              0.26           0.74        0.14            0.51
                    26 LA      K5167P         T131,13-3         P525            0.00          0.17       0.21        0.40         0.11              1.80              0.56           0.86        0.11            0.78
                    27 LA      K5183P         TBLF-1            P525            0.00          0.22       0.15        0.06         0.14              2.63              0.59           0.75        0.06            0.59
                    27 LA      K5184P         TBLF-2            P508            0.00          0.22       0.52        0.00         0.27              1.89              0.42           0.33        0.00            0.28
                    27 LA      K5185P         TBLF-3            P512            0.00          0.10       0.21        0.00         0.34              1.21              0.53           0.68        0.06            0.30
                    28 LA      K5168P         BBSD-1            P505            0.00          1.33       0.03        0.00         1.17              1.16              1.18           3.85        0.04            0.00
                    28 LA      K5169P         BBSD-2            P508            0.00          0.60       0.82        0.00         0.59              2.67              0.71           2.93        0.00            0.00
                    28 LA      K5170P         BBSD-3            P525            0.00          0.47       0.18        0.18         0.30              1.69              1.04           2.34        0.07            0.68
                    29 LA      K5174P         1313MB-1          P505            0.00          0.43       0.32        0.00         0.00              1.78              1.59           4.86        0.00            0.94
                    29 LA      K5175P         BBMB-2            P508            0.00          0.00       0.25        0.00         0.00              3.86              0.89           3.83        0.00            0.00
         00         29 LA      K5176P         1313MB-3          P512            0.00          0.13       0.04        0.00         0.00              1.46              1.05           2.76        0.04            0.00
                    65 LA      K5210P         MRTP- 1           P505            0.00          0.67       0.00        0.00         3.71              8.59              6.95           28.12       0.00            0.00
                    65 LA      K521 1 P       MRTP-2            P515            0.00          0.77       0.09        0.32         3.35              5.81              4.92           18.66       0.11            0.00
                    65 LA      K5212P         MR'I?-3           P512            0.00          0.69       0.12        1.22         3.16              6.48              4.74           16.93       0.18            5.22
                    31LA       K5216P         BSSI-1            P505            0.07          0.94       0.00        0.26         1.74              7.66              5.79           18.95       0.07            4.94
                    31 LA      K5217P         BSSI-2            P515            0.00          1.04       0.09        0.37         2.26              5.15              4.45           13.38       0.05            0.20
                    31 LA      K5218P         BSSI-3            P512            0.00          0.56       0.14        0.00         2.28              18.51             6.04           16.41       0.10            4.51
                    30 LA      K5201P         BSBG-1            P505            0.00          1.24       0.00        0.00         0.67              2.22              0.91           1.34        0.00            0.00
                    30 LA      K5202P         BSBG-2            P515            0.00          0.29       0.06        0.00         0.20              0.60              0.55           0.99        0.00            0.00
                    30 LA      K5203P         BSBG-3            P512            0.00          0.02       0.03        0.00         0.14              1.07              0.59           1.04        0.02            0.00
                    32 LA      K5207P         LBMP-1            P505            0.00          0.31       0.26        0.00         0.21              0.93              0.66           0.92        0.03            0.53
                    32 LA      K5208P         LBMP-2            P515            0.00          0.41       0.14        0.00         0.29              0.63              0.79           1.21        0.00            0.22
                    32 LA      K5209P         LBMP-3            P512            0.00          0.07       0.10        0.00         0.16              2.75              0.67           1.44        0.00            0.13
                    62 LA      K5249P         LPGO-1            P519            0.00          1.39       10.86       9.28        15.79           146.00               98.85          60.80       0.50            2.14
                    62 LA      K5249S         LPGO- 1          P519R            0.00          1.40       10.23       10.11       17.95           163.68             116.58           67.11       0.73            3.64
                    62 LA      K5250P         LPGO-2            P522            0.00          1.25       8.99        7.58        13.50           119.94               80.75          49.60       0.44            1.32
                    62 LA      K5250S         LPGO-2           P522R            0.00          1.30       8.31        7.55        15.18           142.04               97.06          59.38       1.10            2.47
                    62 LA      K5251P         LPGO-3            P526            0.00          1.51       11.15       10.75       16.25           185.88             127.67           75.31       1.20            6.72
                    33 MS      K5222P         mSpC-i            P505            0.00          1.15       0.79        0.00         2.95              10.21             3.88           5.99        1.64            0.55
                    33 MS      K5223P         MSPC-2            P515            0.00          1.09       0.49        0.04         1.93              6.10              4.94           4.87        0.91            2.13
                    33 MS      K5224P         MSPC-3            P513            0.00          0.87       0.57        0.21         2.21              5.18              4.50           4.38        0.98            0.37
                    34 MS      K5228P         MS1313-1          P506            0.00          1.77       0.46        0.71         1.01              8.78              7.41           9.37        0.71            0.00
                    34 mS      K5229P         MS1313-2          P515            0.00          2.79       0.10        0.20         3.50              20.57             13.33          12.42       0.41            0.17






                                                                        MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Data






                   SITE       RAW       DESIGNATOR FOLDER                    HCB LINDANE          HEPTA-    ALDRIN HEPTA                  ALPHA-           TRANS-      DIELDRIN       MIREX     2XDDE
                   AND        FILE           AND                                                  CHLOR                EPO)aDE      CHLORDANE        NONACHLOR                                  (0,P'DDE)
                   STATE                    STATION                          (ppb)       (ppb)      (ppb)       (ppb)                         (ppb)           (ppb)          (ppb)      (ppb)      (ppb)


                   34 NIS     K5230P        MSBB-3           P513            0.00        1.29       0.12        0.29        1.61              9.97            5.89           5.16       0.31            0.32
                   35 MS      K5246P        MSPB-I           P506            0.00        0.36       0.41        0.00        0.12              1.72            1.30           1.70       0.14            3.23
                   35 NIS     K5247P        MSPB-2           P515            0.00        0.40       0.11        0.00        0.13              1.40            1.06           1.25       0.21            1.27
                   35 NIS     K5248P        MSPB-3           P513            0.00        0.31       0.17        0.00        0.11              0.94            1.10           1.14       0.17            1.02
                   36 AL      K5234P        M13CP-1          P506            0.00        1.36       0.20        0.00        0.80              4.03            3.76           7.07       0.00          44.12
                   36 AL      K5235P        MBCP-2           P515            0.00        1.04       0.16        0.00        0.59              1.53            1.92           3.71       0.00          22.13
                   36 AL      K5236P        MBCP-3           P513            0.00        1.16       0.17        0.00        0.47              2.34            1.69           3.32       0.10          26.00
                   66 AL      K5240P        MBHI- 1          P506            0.00        2.51       0.56        0.00        0.59              7.89            9.68           11.21      0.00          82.07
                   66 AL      K5241P        MBHI-2           P515            0100        2.50       0.26        0.00        1.25              6.51            6.88           7.41       0.00          66.49
                   66 AL      K5242P        MBHI-3           P513            0.00        2.01       0.21        0.00        0.82              6.07            6.02           6.40       0.00          65.42
                   67 FL      K5261P        PBPH-1           P517            0.00        1.88       0.47        0.11        2.50              4.46            5.03           13.03      0.00            0.00
                   67 FL      K5262P        PBPH-2           P520            0.00        2.97       0.61        1.13        4.90              7.38            8.83           21.97      0.16            1.05
                   67 FL      K5263P        PBP14-3          P523            0.15        3.50       0.30        0.22        3.10              5.70            7.53           18.30      0.21            0.76
                   37 FL      K5255P        PBIB- 1          P517            0.00        0.89       0.09        0.00        0.89              1.02            1.99           4.06       0.01            6.04
                   37 FL      K5256P        1313113-2        P520            0.00        1.36       0.37        0.00        0.98              2.06            2.82           7.34       0.00            7.06
                   37 FL      K5257P        PBIB-3           P529            0.00        1.17       0.27        0.00        0.14              0.99            2.59           7.58       0.07          10.05
        00         73 FL      K5267P        CBJB-1           P517            0.00        0.41       0.14        0.73        1.29              2.02            2.38           16.98      0.74            0.00
                   73 FL      K5268P        CBJB-2           P520            0.00        0.64       0.99        0.52        1.38@             2.41            3.20           15.99      1.00            0.26
                   73 FL      K5269P        CBJB-3        P527(P523)         0.05        0.42       0.25        0.80        0.96              2.11            2.67           14.91      1.21            0.12
                   38 FL      K5273P        CBSR-1           P517            0.00        0.20       0.03        0.00        0.61              1.76            1.38           1.92       0.00            0.16
                   38 FL      K5274P        CBSR-2           P520            0.02        0.42       0.33        0.11        0.47              2.93            1.44           2.08       0.00            0.20
                   38 FL      K5275P        CBSR-3        P527(P523)         0.10        0.22       0.14        0.13        0.14              2.68            1.30           1.75       0.10            0.45
                   39 FL      K5279P        CBSP- 1          P517            0.00        0.37       0.13        0.00        0.54              4.00            3.61           4.18       0.09            0.27
                   39 FL      K5280P        CBSP-2           P529            0.01        0.57       0.19        0.34        0.28              3.10            5.16           5.60       0.06            2.97
                   39 FL      K5281P        CBSP-3           P523            0.04        0.63       0.13        0.05        0.12              21.13           17.60          5.26       0.55            7.64
                   74 FL      K5303P        PCLO-1           P529            0.00        0.71       0.05        0.00        0.09              0.86            1.62           2.69       0.00            9.70
                   74 FL      K5303P        PCLO-1           P517            0.00        0.53       0.09        0.00        0.18              1.14            1.43           1.68       0.00            6.11
                   74 FL      K5304P        PCLO-2           P520            0.00        2.29       0.76        0.00        1.20              4.54            7.08           8.17       0.18            3.49
                   74 FL      K5305P        PCLO-3           P523            0.27        1.26       0.29        0.00        0.40              3.30            2.26           2.87       0.73            0.71
                   40 FL      K5297P        SAWB-1           P517            0.00        1.42       0.75        0.70        2.00              16.34           13.86          8.68       0.06            0.58
                   40 FL      K5298P        SAWB-2           P520            0.00        1.70       0.79        0.42        3.65              30.49           24.38          11.91      0.40            2.54
                   40 FL      K5299P        SAWB-3           P523            0.00        1.25       0.55        1.91        3.16              23.08           19.10          8.84       0.33            2.62
                   41 FL      K5291P        APDB-1           P517            0.00        0.73       0.15        0.14        0.18              1.26            1.26           2.45       0.00            0.00
                   41 FL      K5292P        APDB-2           P520            0.02        0.84       0.44        0.25        0.31              3.08            1.55           3.25       0.32            0.00
                   41 FL      K5293P        APDB-3           P523            0.19        0.88       0.12        0.01        0.37              1.26            1.02           2.01       0.29            0.12
                   42 FL      K5285P        APCP-1           P517            0.00        0.26       0.21        0.03        0.09              0.75            0.92           0.72       0.00            0.00
                   42 FL      K5286P        APCP-2           P520            0.01        0.22       0.13        0.06        0.11              1.14            1.22           1.23       0.00            0.00
                   42 FL      K5287P        APCP-3           P523            0.04        0.24       0.57        0.31        0.12              1.98            1.50           1.12       0.24            0.41
                   75 FL      K5321P        AESP-1           P517            0.00        0.16       0.20        0.00        0.00              0.75            0.57           0.87       0.00            0.53






                                                                        MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Data






                   SITE       RAW       DESIGNATOR FOLDER                    HC13 LINDANE        HEPTA-     ALDRIN HEPTA                  ALPHA-           TRANS-     DIELDRIN        MIREX     2.4' DDE
                   AND        FILE            AND                                                 CHLOR                EPOXIDE      CHLORDANE       NONACHLOR                                   (0,P'DDE)
                   STATE                    STA'nON                          (ppb)       (ppb)      (ppb)       (ppb)                        (ppb)            (ppb)         (ppb)       (ppb)      (ppb)


                   75 FL      K5322P        AESP-2           P520            0.02        0.40       0.48        0.06        0.00             0.17             0.85          1.15        0.00           0.96
                   75 FL      K5323P        AESP-3           P523            0.04        0.42       0.12        0.00        0.00             0.82             0.57          0.62        0.00           0.20
                   43 FL      K5315P        CKBP-1           P517            0.02        0.25       0.03        0.00        0.09             0.38             0.30          0.30        0.07           0.04
                   43 FL      K5316P        CKBP-2           P520            0.00        0.39       0.06        0.04        0.00             1.40             0.96          0.84        0.30           0.20
                   43 FL      K5317P        CKBP-3           P523            0.03        0.32       0.14        0.05        0.00             1.77             0.65          0.69        0.07           0.22
                   76 FL      K535 1 P      TBNP-1           P518            0.00        0.60       0.18        0.00        1.48             14.43            21.52         5.55        1.93           0.00
                   76 FL      K5352P        TBNP-2           P521            0.00        0.47       0.31        0.00        0.70             21.40            34.77         7.88        4.90           0.12
                   76 FL      K5353P        TBNP-3           P524            0.00        0.80       0.33        0.34        0.64             16.46            24.30         5.72        4.74           0.62
                   47 FL      K5333P        TBMK-1           P518            0.00        0.44       0.17        0.00        0.39             2.16             3.56          1.64        0.41           1.33
                   47 FL      K5334P        TBMK-2           P521            0.00        0.30       0.33        0.19        0.24             6.55             10.02         3.63        2.31           0.97
                   47 FL      K5335P        TBMK-3           P524            0.00        0.54       0.53        0.89        0.10             7.34             8.08          2.34        1.66           3.23
                   44 FL      K5327P        TBPB-1           P518            0.00        1.02       0.12        0.00        1.16             8.27             14.03         3.17        3.57           0.19
                   44 FL      K5328P        TBPB-2           P521            0.15        2.95       0.26        0.00        1.09             13.10            26.77         3.34        8.92           0.40
                   44 FL      K5329P        TBPB-3           P524            0.03        0.65       0.00        0.15        0.44             7.44             12.86         2.53        3.89           0.75
                   70 FL      K5339P        TBOT-1.          P518            0.00        0.95       0.00        0.00        0.21             4.20             5.11          1.04        0.36           0.86
                   70 FL      K5340P        TBOT-2           P521            0.00        0.95       0.21        0.00        0.13             5.46             6.86          0.65        0.87           0.51
        00         70 FL      K5341P        TBOT-3           P524            0.01        0.76       0.34        0.30        0.00             5.25             4.00          1.17        0.62           1.53
        C-n        77 FL      K5309P        T13KA-1          P518            0.00        1.84       0.15        0.00        1.46             26.51            32.29         4.73        1.44           0.28
                   77 FL      K5310P        TBKA-2           P521            0.00        1.55       0.05        0.12        0.06             7.37             7.89          3.50        1.31           0.11
                   77 FL      K531 1P       TBKA-3           P524            0.00        2.37       0.45        0.96        1.47             45.14            57.67         9.28        3.27           2.51
                   46 FL      K5345P        TBCB-1           P518            0.00        0.89       0.00        0.00        0.42             8.30             17.89         1.56        7.07           0.76
                   46 FL      K5346P        TBCB-2           P521            0.00        1.15       0.42        0.24        0.30             23.47            47.05         1.61        17.45          16.33
                   46 FL      K5347P        TBCB-3           P524            0.00        0.61       0.23        0.46        0.29             14.73            26.21         1.02        8.30           8.01
                   48 FL      K5369P        CBBI-1           P518            0.00        0.45       0.00        0.00        0.27             2.03             2.70          1.99        0.00           0.00
                   48 FL      K5370P        C13131-2         P521            0.00        0.20       0.00        0.00        0.06             2.75             3.22          1.63        0.00           1.14
                   48 FL      K5371P        CBBI-3           P525            0.02        0.24       0.00        0.09        0.16             2.47             2.17          1.80        0.03           0.82
                   71 FL      K5363P        CBFM-1           P518            0.00        1.02       0.06        0.00        0.68             6.35             9.22          4.75        0.00           1.26
                   71 FL      K5364P        CBFM-2           P521            0.00        1.26       0.05        0.00        0.30             7.88             10.77         6.74        0.05           0.25
                   71 FL      K5365P        CBFM-3           P524            0.04        0.65       0.19        0.06        0.24             11.35            14.29         3.42        0.04           1.26
                   49 FL      K5357P        NBNB-1           P518            0.00        0.52       0.10        0.31        0,34             7.54             8.53          6.32        0.00           1.04
                   49 FL      K5358P        NBNB-2           P521            0.00        0.47       0.11        0.13        0.21             7.43             8.19          5.50        0.01           1.78
                   49 FL      K5359P        NBNB-3           P524            0.00        0.55       0.25        0.77        0.34             7.80             8.29          6.12        0.09           2.34
                   50 FL      K538 1 P      RBHC-1           P518            0.37        1.20       0.82        0.99        1.18             2.02             2.28          2.21        0.89           0.93
                   50 FL      K5382P        RBHC-2           P521            0.01        0.13       0.12        0.03        0.04             2.26             2.31          0.73        0.01           1.62
                   50 FL      K5383P        RBHC-3           P524            0.03        0.39       0.12        0.25        0.10             3.08             2.11          1.10        0.00           1.97
                   51 FL      K5375P        EVFU-1           P518            0.00        0.00       0.00        0.00        0.00             0.79             0.16          0.00        0.00           0.00
                   51 FL      K5376P        EVFU-2           P521            0.00        0.00       0.06        0.00        0.00             0.80             0.21          0.00        0.00           0.16
                   51 FL      K5377P        EVFU-3           P524            0.02        0.18       0.08        0.00        0.00             1.28             0.33          0.00        0.00           0.45
                   81 FL      K5396111      BHKF-1           P527            0.03        0.14       0.00        o.bo        0.00             0.57             0.12          0.91        0.00           1.54






                                                                      MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Data






                  SITE      RAW        DESIGNATOR FOLDER                  HCB LINDANE HEPTA- ALDRIN HEPTA                            ALPHA-         TRANS- DIELDRIN MIREX                2,4'DDE
                  AND       FILE            AND                                               CHLOR                EP0)(IDE    CHLORDANE       NONACHLOR                                (0,P'DDE)
                 STATE                   STATION                          (ppb)      (ppb)       (ppb)     (ppb)                        (ppb)           (ppb)        (ppb)       (ppb)     (ppb)


                  81 FL     K5397P        BHKF-2           P527           0.03        0.21       0.00      0.00         0.00            0.57             0.17        0.86        0.00           1.72
                  81 FL     K5398P        BHKF-3           P527           0.04        0.34       0.00      0.00         0.00            0.77             0.14         1.17       0.00          2.70

















        00





                                                                      MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Data





                  SITE      RAW        DESIGNATOR FOLDER                  4XDDE        2.4'DDD       ENDRIN      4.4'DDD       2,4'DDT      4,4'DDT         TOTAL   PC13 #8      PCB # 18   PC13 #28
                  AND       FILE            AND                         (P,P'DDE)    (O.P DDD)                  (P,P'DDD)    (O,P'DDT)     (P,P'DDD         DDTS        (CL2)        (CL3)     (CL3)
                  STATE                   STATION                             (ppb)        (ppb)        (ppb)         (ppb)        (ppb)        (ppb)       (ppb)       (ppb)         (ppb)    (ppb)


                  01 TX     K5135P        LMSB-1           P505               0.07         0.01         0.00          0.00         0.00         0.00        0.08         0.0           0.0          0.0
                  01 TX     K5136P        LMSB-2           P508               4.14         0.00         0.00          0.00         0.00         0.00        4.14         0.6           0.0          0.0
                  01 TX     K5137P        LMSB-3           P511               2.32         0.00         0.00          0.00         0.00         0.00        2.50         0.0           0.0          0.0
                  03 TX     K5087P        CCIC-1           P504               2.74         0.00         0.00          0.35         0.00         0.00        4.64         0.0           0.0          1.6
                  03 IX     K50881)       CCIC-2           P507               2.75         0.15         0.00          0.36         0.00         0.25        3.51         0.4           0.0          1.5
                  03 TX     K5089P        CCIC-3           P510               3.13         0.03         0.00          0.69         0.08         0.00        4.11         0.0           0.0          0.0
                  04 TX     K5147P        ABLR-1           P504               2.09         0.01         0.02          0.00         0.07         1.90        4.07         0.4           0.0          0.0
                  04 TX     K5148P        ABLR-2           P508               4.14         0.00         0.00          0.00         0.00         1.07        5.21         1.0           0.0          0.0
                  04 TX     K5149P        ABLR-3           P511               5.99         0.00         0.00          0.00         0.00         0.41        6.69         0.0           0.0          0.0
                  05 TX     K514 I P      CBCR-1           P504               2.78         0.00         0.00          0.21         0.00         0.00        3.00         0.1           0.5          2.2
                  05 TX     K5142P        CBCR-2           P508               3.90         0.00         0.00          0.00         0.00         0.00        3.90         0.2           0.0          0.0
                  05 TX     K5143P        CBCR-3           P511               4.44         0.00         0.00          0.00         0.00         0.00        4.44         0.0           0.0          0.0
                  06'IX     K509913       M BAR- 1         P504               3.65         0.00         0.00          0.00         0.00         0.00        3.65         0.0           0.0          0.0
                  06 TX     K5100P        MBAR-2           P507               4.11         0.00         0.00          0.00         0.00         0.34        4.45         0.2           0.0          0.0
                  06 TX     K5101P        MBAR-3           P511               3.17         0.00         0.00          0.04         0.00         0.11        3.41         0.7           0.0          0.0
                  07 TX     K5111P        SAPP-1           P504               2.70         0.00         0.34          0.13         0.00         1.27        5.30         0.0           0.2          0.2
                  07 TX     K5112P        SAPP-2           P507               4.05         0.00         0.00          0.20         0.16         0.22        4.72         0.3           0.0          0.2
                  07 TX     K5113P        SAPP-3           P525               3.61         0.03         0.98          0.52         0.03         0.37        5.13         0.0           0.1          0.0
                  08 TX     K5117P        SAMP-1           P504               5.05         0.00         0.37          0.43         0.00         0.96        6.81         0.0           0.0          0.0
                  08 TX     K5118P        SAMP-2           P507               9.92         0.00         0.14          0.72         0.08         0.43        11.15        1.0           0.0          0.1
                  08 TX     K5119P        SAMP-3           P511               5.70         0.00         1.93          0.45         0.00         0.56        6.70         0.6           0.0          0.0
                  09 TX     K5105P        ESSP-1           P504               4.05         0.00         0.14          0.17         0.00         0.00        6.58         0.0           0.0          0.0
                  09 TX     K5106P        ESSP-2           P507               6.38         0.00         0.00          0.24         0.14         0.28        7.04         0.4           0.0          0.0
                  09 TX     K5107P        ESSP-3           P511               3.53         0.00         0.00          0.20         0.07         0.00        3.80         1.0           0.0          0.0
                  12 TX     K5129P        MBGP-1           P504               21.33        0.10         0.00          1.39         0.02         0.27        23.11        0.0           0.0          0.6
                  12 TX     K5130P        MBGP-2           P508               20.18        0.22         0.00          1.08         0.00         1.13        22.61        0.0           0.0          0.3
                  12 TX     K5131P        MBGP-3           P511               18.66        0.00         0.43          0.73         0.00         0.50        19.88        0.0           0.0          0.0
                  11 TX     K5123P        MBLR-1           P504               10.70        0.26         0.00          1.25         0.00         0.48        15.62        0.5           1.6          3.2
                  11 TX     K5124P        MBLR-2           P507               12.30        0.39         0.00          1.20         0.04         0.50        17.20        2.0           1.5          2.5
                  11 TX     K5125P        MBLR-3           P511               15.92        0.00         0.00          1.96         0.00         0.33        21.37        0.0           1.0          1.1
                  13 TX     K5081P        MBTP-1           P504               30.02        0.00         0.13          O@73         0.00         1.50        32.72        0.0           0.0          0.0
                  13 TX     K5082P        MBTP-2           P507               34.96        0.02         0.00          1.44         0.18         0.23        36.96        0.3           0.2          0.0
                  13 TX     K5083P        MBTP-3           P525               33.43        0.16         1.14          1.80         0.02         0.73        36.80        0.0           0.1          0.0
                  14 TX     K5075P        MBEM-1           P514               7.12         0.00         2.91          0.16         0.00         0.38        7.78         0.4           0.0          0.1
                  14 TX     K5076P        MBEM-2           P507               6.05         0.00         3.33          0.38         0.09         0.20        7.06         0.3           0.0          0.0
                  14 TX     K5077P        MBEM-3           13510              5.23         0.01         2.57          0.42         0.00         0.95        6.74         0.1           0.0          0.0
                  72 TX     K5015P        BRCL-1           P514               27.76        0.31         0.00          1.50         0.00         0.33        30.10        0.0           0.0          0.1
                  72 Tx     K5016P        BRCL-2           P506               22.14        0.48         0.16          1.57         0.00         1.02        25.58        0.0           0.0          0.9
                  72 TX     K5017P        BRCL-3           P525               40.69        0.17         0.28          2.23         0.03         0.35        43.77        0.0           0.0          0.1






                                                                       MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Data






                   SITE      RAW       DESIGNATOR FOLDER                   4,4'DDE      2,4'DDD        ENDRIN      4,4'DDD       2.4'DDT      4,4'DDT         TOTAL    PCB #8      PCB #18     PCB #28
                   AND       FILE            AND                         (P,P'DDE)    (0,P DDD)                   (P.P'DDD)    (O,P'DDT)     (P,P'DDT)        DDTS         (CL2)        (CL3)     (CM)
                   STATE                   STATION                             (ppb)        (ppb)         (ppb)        (ppb)         (ppb)        (ppb)       (ppb)        (ppb)        (ppb)     (ppb)



                   57 TX     K5021P        BRFS-1           P514            113.70          0.65          0.00         3.23          0.00         0.98        118.97        0.0          0.0           0.2
                   57 TX     K5022P        BRFS-2           P506            110.89          1.47          0.00         2.71          0.00         1.95        117.52        0.5          0.0           0.2
                   57 TX     K5023P        BRFS-3           P510               75.42        0.87          0.00         2.73          0.31         1.91        83.65         0.1          0.0           0.1
                   18 TX     K5009P        G13CR-1          P525               4.99         0.24          0.49         2.27          0.04         0.62        8.40          0.0          0.1           0.1
                   18 TX     K5010P        GBCR-2           P506               3.35         0.77          0.00         1.62          0.00         1.10        6.85          0.0          0.0           0.2
                   18 TX     K5011P        GBCR-3           P515               4.30         0.36          0.00         1.52          0.00         0.26        6.44          0.0          0.0           0.3
                   58 TX     K5003P        GBOB-1           P514               19.80        0.49          0.00         6.90          0.53         2.03        29.75         0.1          0.7           1.0
                   58 TX     K5004P        GBOB-2           P506               29.09        1.42          0.00         11.84         0.00         2.71        45.06         0.4          0.4           1.5
                   58 TX     K5005P        GBOB-3           P515               25.88        0.89          0.00         10.92         0.00         2.17        39.86         0.0          0.5           1.6
                   16 TX     K5057P        GBTD-1           P516R              7.74         0.94          0.03         5.07          0.00         0.00        14.03         0.0          0.0           0.6
                   16 TX     K5058P        GBTD-2           P516R              8.58         0.95          0.00         4.85          0.00         0.00        14.61         0.0          0.0           0.3
                   16 TX     K5059P        GBTD-3           P516R              6.49         0.67          0.00         5.20          0.00         0.00        12.58         0.0          0.0           0.2
                   15 TX     K5063P        GBYC-1           P514               13.19        1.55          0.00         13.80         0.00         1.30        29.84         0.0          0.1           1.0
                   15 TX     K5064P        GBYC-2           P508               11.67        0.97          0.00         13.91         0.00         1.74        28.82         0.0          0.1           1.7
                   15 TX     K5065P        GBYC-3           P510               11.29        1.55          0.00         13.35         0.85         0.87        28.58         0.0          0.2           2.7
                   59 TX     K5384P        GBSC-1           P519               73.83        8.04          0.00         61.32         14.84        8.88        171.57        0.0         13.1         25.8
        Co         59 TX     K5384S        GBSC-1           P519R           101.79          10.92         0.22         69.52         16.30        9.31        212.56        0.0         12.3         25.6
        00         59'IX     K5385P        GBSC-2           P522               80.89        7.72          0.00         60.12         16.09        8.29        175.18        0.0         14.5         23.0
                   59 TX     K5385S        GBSC-2           P522R           134.57          11.94         0.00         82.92         18.86        10.33       261.53        0.0         15.2         32.1
                   59 TX     K5386P        GBSC-3           P526               98.52        12.70         1.04         72.74         19.43        12.14       224.62        0.0         13.4         28.8
                   17 TX     K5039P        GBHR-1           P514               5.64         0.11          0.00         1.25          0.28         0.47        7.75          0.0          0.0           0.1
                   17 TX     K5040P        GBHR-2           P506               4.18         0.37          0.00         1.64          0.00         0.96        7.14          0.0          0.0           0.0
                   17 TX     K5041P        GBHR-3           P510               5.11         0.32          0.08         2.04          0.14         0.82        9.10          0.0          0.0           0.3
                   19 TX     K5027P        SI,1313-1        P514               3.50         0.00          0.00         0.69          0.00         2.54        7.41          0.0          0.2           0.5
                   19 TX     K5028P        SL1313-2         P506               9.14         0.28          0.00         2.91          0.00         1.59        14.71         0.0          0.1           0.8
                   19 TX     K5029P        SI,1313-3        P525               5.99         0.15          2.11         2.66          0.06         0.50        10.28         0.0          0.4           0.3
                   20 LA     K5033P        CLSJ-1           P514               5.73         0.00          0.14         0.88          0.00         0.16        6.78          0.0          0.0           0.1
                   20 LA     K5034P        CLSJ-2           P506               5.68         0.00          0.00         1.30          0.00         0.75        9.28          0.0          0.0           0.6
                   20 LA     K5035P        CLSJ-3           P510               6.20         0.00          0.09         1.52          0.06         1.18        9.29          0.0          0.0           0.2
                   60 LA     K5045P        CLLC- 1          P5 14              11.45        0.88          0.31         2.44          0.51         0.00        15.27         0.0          0.8           1.5
                   60 LA     K5046P        CLLC-2           P507               12.03        1.55          0.19         3.07          0.00         0.00        20.62         0.0          0.5           1.8
                   60 LA     K5047P        CLLC-3           P510               12.14        2.25          0.63         2.58          0.26         0.00        20.58         0.0          0.2           2.4
                   21 LA     K5069P        JHJH- 1          P514               22.16        0.18          1.36         6.17          0.00         0.56        29.07         0.0          0.0           0.2
                   21 LA     K5070P        JHJH-2           P507               27.05        0.27          0.38         8.58          0.27         0.24        36.80         0.8          0.0           0.2
                   21 LA     K5071P        JHJH-3           P510               17.66        0.38          0.39         5.91          0.24         0.00        24.60         0.0          0.0           0.2
                   22 LA     K5159P        VBSP-1           P504               25.12        0.42          3.30         10.67         0.66         0.00        38.74         0.0          0.0           0.0
                   22 L-A    K5160P        VBSP-2           P508               21.83        0.47          0.00         8.87          0.00         0.61        32.49         0.0          0.0           0.0
                   22 LA     K5161P        VBSP-3           P512               33.71        0.41          0.60         15.60         0.80         1.10        53.35         0.7          0.0           0.3
                   24 LA     K5189P        ABOB-1           P505               6.37         0.20          0.64         4.91          0.45         2.49        14.41         0.0          0.0           0.7





                                                                             MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Data






                    SITE       RAW        DESIGNATOR FOLDER                      4ADDE         2.4'DDD         ENDRIN        4,4'DDD        2.4'DDT        4ADDT            TOTAL    PC13 #8      PC13 # 18    PCI3 #28
                    AND        FILE             AND                            (P,11' DDE)   (0,P DDD)                    (P,P' DDD)     (0,13' DDT)    (P,P' DD'Ij         DDT'S        (CL2)          (CL3)      (CU3)
                    STATE                      STATION                                (ppb)         (ppb)          (ppb)          (ppb)         (ppb)          (ppb)        (ppb)        (ppb)          (ppb)      (ppb)


                    24 LA      K5190P          ABOB-2            P508                 11.44         0.06           0.00           5.30          0.00           1.20         18.01          0.0           0.0            0.0
                    24 LA      K519 1 P        ABOB-3            P512                 14.96         0.44           0.83           8.63          0.46           2.81         27.30          0.2           0.0            0.2
                    25 LA      K5195P          CLCL- 1           P505                 1.02          0.00           0.00           1.69          0.23           1.52         4.83           0.0           0.4            0.0
                    25 LA      K5196P          CLCL-2            P508                 2.16          0.00           0.00           1.21          0.00           1.95         5.32           0.6           0.0            0.0
                    25 LA      K5197P          CLCL-3            P512                 2.19          0.04           0.14           1.68          0.00           0.70         4.68           0.0           0.0            0.0
                    26 LA      K5165P          TBLB-1            P505                 1.82          0.24           0.04           0.64          0.00           0.65         3.97           0.5           0.0            0.2
                    26 LA      K5166P          T131,13-2         P508                 3.60          0.03           1.51           0.84          0.00           0.91         5.89           0.9           0.0            0.5
                    26 LA      K5167P          TBLB-3            P525                 2.40          0.04           0.91           0.87          0.00           0.22         4.30           0.1           0.1            0.1
                    27 LA      K5183P          TBLF-1            P525                 1.71          0.01           0.88           0.68          0.03           0.36         3.39           0.1           0.0            0.2
                    27 LA      K5184P          TBLF-2            P508                 0.74          0.00           0.53           0.47          0.00           0.45         1.95           0.3           0.0            0.6
                    27 LA      K5185P          TBLF-3            P512                 1.69          0.00           0.33           0.43          0.00           0.65         3.07           0.3           0.0            0.1
                    28 LA      K5168P          BBSD-1            P505                 1.98          0.00           0.09           1.54          0.06           1.70         5.27           0.0           0.0            0.2
                    28 LA      K5169P          BBSD-2            P508                 3.53          0.00           0.53           0.86          0.00           1.29         5.68           0.4           0.0            0.1
                    28 LA      K5170P          BBSD-3            P525                 3.34          0.04           0.70           1.47          0.03           0.42         5.97           0.0           0.2            0.2
                    29 LA      K5174P          BBMB-1            P505                 4.95          0.74           0.41           2.19          0.25           1.72         10.79          0.3           0.0            1.5
                    29 LA      K5175P          BBMB-2            P508                 4.10          0.00           0.00           0.99          0.00           1.40         6.49           1.0           0.0            0.2
                    N LA       K5176P          BBMB-3            P512                 5.87          0.00           0.11           1.90          0.23           0.66         8.66           0.5           0.0            0.6
                    65 LA      K52 1 OP        MRTP- 1           P505                 30.43         2.33           7.65           23.97         0.00           5.25         61.97          0.3           0.3            1.6
                    65 LA      K521 1P         MRIP-2            P515                 22.51         1.37           2.98           17.67         0.92           2.66         45.13          1.3           0.2            0.7
                    65 LA      K5212P          MRTP-3            P512                 27.63         1.91           2.01           24.42         0.51           4.63         64.33          1.6           0.1            0.9
                    31 LA      K5216P          BSSI - 1          P505                 30.75         1.43           4.82           16.41         0.92           6.39         60.83          0.2           0.3            0.9
                    31 LA      K5217P          BSSI-2            P515                 20.49         1.02           1.78           13.65         0.45           2.83         38.64          0.2           0.0            0.4
                    31 LA      K5218P          BSSI-3            P512                 43.17         0.97           2.10           18.48         0.00           8.95         76.08          0.6           0.0            0.7
                    30 LA      K5201P          BSBG-1            P505                 1.22          0.26           0.00           0.00          0.00           0.81         2.29           0.4           0.0            0.5
                    30 LA      K5202P          BSBG-2            P515                 2.16          0.02           0.00           0.47          0.00           0.21         2.86           0.0           0.0            0.1
                    30 LA      K5203P          BSBG-3            P5 12                2.46          0.02           0.00           0.53          0.00           0.52         3.53           0.0           0.0            0.0
                    32 LA      K5207P          LBMP-1            P505                 2.11          0.35           0.08           0.85          0.00           1.39         5.23           0.3           0.1            0.4
                    32 LA      K5208P          LBMP-2            P515                 2.20          0.04           0.00           0.99          0.00           0.31         3.76           0.0           0.0            0.0
                    32 LA      K5209P          LBMP-3            P512                 3.23          0.00           0.00           0.96          0.00           0.87         5.19           0.1           0.0            0.0
                    62 LA      K5249P          LPGO- I           P519                 78.49         14.56          7.73           98.54         8.06           11.72        213.50         0.0           5.6          17.7
                    62 LA      K5249S          LPGO-1           P519R               108.03          20.14          15.25       117.42           8.77           15.24        273.25         0.0           8.5          19.2
                    62 LA      K5250P          LPGO-2            P522                 61.82         10.78          7.00           73.11         6.11           8.80         161.94         0.0           4.5          14.9
                    62 LA      K5250S          LPGO-2           P522R                 98.43         15.61          15.54        102.29          6.36           12.54        237.70         0.0           4.7          16.5
                    62 LA      K5251P          LPGO-3            P526               125.35          21.23          11.52        121.41          10.59          16.24        301.54         0.0           6.8          21.5
                    33 NIS     K5222P          mSpC-1            P505                 23.37         1.58           0.00           10.36         0.88           3.84         40.58          0.2           0.2            3.3
                    33 NIS     K5223P          MSPC-2            P515                 12.28         0.47           0.00           5.66          0.29           1.34         22.17          0.3           0.0            1.8
                    33 MS      K5224P          MSPC-3            P513                 11.64         0.63           0.00           5.15          0.81           1.38         19.99          1.7           0.6            1.1
                    34 NIS     K5228P          MS1313-1          P506                 17.53         2.25           0.00           13.46         0.00           1.49         34.73          0.6           1.4            5.0
                    34 MS      K5229P          MS1313-2          P515                 23.58         2.57           0.00           11.25         0.00           0.67         38.25          1.8           1.4            5.2





                                                                           MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Data






                    SITE       RAW        DESIGNATOR FOLDER                     4,4'DDE       2,4'DDD        ENDRIN       4.4'DDD        2,4'DDT        4,4'DDrr      TOTAL       PCB #8       PCB # 18    PC13 #28
                    AND        FILE             AND                           (P,P'DDE)     (0,P DDD)                   (P,PI DDD)     (O,P'DDT)      (P,P'DDD        DDrS           (CL2)          (CL3)      (CL,3)
                    STATE                     STATION                               (ppb)          (ppb)         (ppb)         (ppb)          (ppb)         (ppb)       (ppb)         (ppb)         (ppb)      (ppb)



                    34 MS      K5230P         MSBB-3            P513                11.27          1.14          0.00          6.05           0.00          0.64        19.42          1.6           0.9            1.9
                    35 MS      K5246P         MSPB-1            P506                7.07           0.73          0.00          3.22           0.00          1.51        15.75          0.0           0.2            1.2
                    35 MS      K5247P         MSPB-2            P515                6.90           0.37          0.00          1.94           0.00          0.75        11.21          0.0           0.1            0.3
                    35 MS      K5248P         MSPB-3            P513                5.18           0.44          0.00          0.99           0.25          1.50        9.39           0.0           0.1            0.3
                    36 AL      K5234P         MBCP-1            P506                72.18          12.99         3.17          29.98          1.23          2.98      163.48           0.2           0.0            0.9
                    36 AL      K5235P         MBCP-2            PS 15               37.41          6.75          0.81          13.28          0.23          0.66        80.47          0.5           0.0            0.4
                    36 AL      K5236P         MBCP-3            P513                35.44          5.55          0.94          13.35          0.55          0.67        81.56          1.1           0.0            0.8
                    66 AL      K5240P         MBHI- I           P506             124.27            18.32         1.51          45.57          3.31          4.81      278.36           0.3           0.5            2.0
                    66 AL      K5241P         M13HI-2           P515                88.93          12.52         0.87          34.35          2.31          1.79      206.39           0.0           0.3            1.2
                    66 AL      K5242P         MBHI-3            P513                77.83          10.60         1.70          31.58          4.51          1.72      191.66           0.0           0.8            1.4
                    67 FL      K5261P         PI3PH-1           P517                18.09          0.84          0.00          4.19           0.79          1.90        25.81          0.1           0.6            2.0
                    67 FL      K5262P         PBPH-2            P520                33.36          1.34          1.50          7.34           0.79          5.16        49.03          0.4           1.1            3.7
                    67 FL      K5263P         PBPH-3            P523                32.90          1.00          0.91          6.61           1.13          3.34        45.73          0.7           0.9            2.6
                    37 FL      K5255P         P13113-1          P517                15.77          1.61          0.14          2.61           0.35          0.36        26.75          0.4           0.6            1.6
                    37 FL      K5256P         PBIB-2            P520                23.33          1.61          1.03          5.40           2.22          1.39        41.01          0.3           1.5            2.8
                    37 FL      K5257P         P13113-3          P529                25.82          1.70          0.84          8.31           1.18          0.67        47.73          0.7           0.2            1.4
                    73 FL      K5267P         CBJB-1            P517                12.72          3.09          0.05          19.28          0.00          1.76        36.86          0.0           0.0            0.2
                    73 FL      K5268P         CBJB-2            P520                15.30          4.30          0.60          29.28          0.00          3.00        52.13          0.0           0.3            0.5
                    73 FL      K5269P         CBJB-3         P527(P523)             13.72          3.24          0.54          23.79          0.19          2.15        43.22          0.1           0.2            0.5
                    38 FL      K5273P         CBSR- I           PS 17               16.36          0.00          0.00          2.05           0.00          0.60        19.16          0.0           0.0            0.0
                    38 FL      K5274P         CBSR-2            P520                18.59          0.00          0.34          3.01           0.00          1.22        23.01          0.1           0.0            0.1
                    38 FL      K5275P         CBSR-3         P527(PS23)             17.52          0.00          0.81          2.62           0.03          0.99        21.61          0.4           0.0            0.0
                    39 FL      K5279P         CBSP-1            P517                39.74          2.93          0.00          29.77          0.63          5.45        78.78          0.0           0.0            0.0
                    39 FL      K5280P         CBSP-2            P529                67.03          4.63          0.15          58.23          0.37          6.96      140.18           0.0           0.0            0.2
                    39 FL      K528 1 P       CBSP-3            P523             506.09            92.12         0.29        685.62           12.56       110.02     1414.05           0.1           0.4            0.6
                    74 FL      K5303P         PCLO-1            P529             710.97            53.33         0.36        506.30           3.99          63.54    1347.82           0.0           0.1            0.3
                    74 FL      K5303P         PCLO- I           P517             717.11            38.02         0.00        436.28           6.95          47.08    1251.55           0.0           0.0            0.1
                    74 FL      K5304P         PCLO-2            P520             132.37            6.37          8.10          63.48          0.00          13.26     218.97           0.0           0.7            2.3
                    74 FL      K5305P         PCLO-3            P523                62.38          2.22          1.75          21.18          0.60          5.93        93.02          0.0           1.0            0.5
                    40 FL      X5297P         SAW13-1           P517                61.91          4.96          0.00          39.57          2.03          9.83      118.89           0.0           3.1            6.3
                    40 FL      K5298P         SAWB-2            P520             129.74            10.40         0.00          67.75          6.69          28.29     245.42           0.0           4.8           10.2
                    40 FL      K5299P         SAWB-3            P523             108.05            8.72          0.00          60.70          3.53          13.26     196.87           0.0           4.0            7.6
                    41 FL      K5291P         APDB-1            P517                16.75          0.14          0.00          4.45           0.00          1.34        22.68          0.0           0.0            0.0
                    41 FL      K5292P         APDB-2            P520                12.65          0.14          0.00          3.40           0.00          1.52        17.71          0.0           0.1            0.0
                    41 FL      K5293P         APDB-3            P523                11.33          0.22          0.00          2.98           0.14          0.48        15.26          0.0           0.0            0.0
                    42 FL      K5285P         APCP- 1           P517                6.37           0.07          0.00          2.23           0.00          1.25        9.92           0.0           0.0            0.4
                    42 FL      K5286P         APCP-2            P520                7.55           0.16          0.00          3.64           0.00          2.68        14.04          0.0           0.1            0.6
                    42 FL      K5287P         APCP-3            P523                11.09          0.30          0.00          4.03           0.10          2.07        18.01          0.0           0.0            0.6
                    75 FL      K532 1 P       AESP-1            P517                10.39          0.00          0.00          1.10           0.00          0.77        12.79          0.0           0.0            0.0






                                                                                 MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Data






                      SITE        RAW         DESIGNATOR FOLDER                       4ADDE          2.4'DDD         ENDRIN        4,4'DDD         2.4'DDT         4,4'DDT        TOTAL        PC13 #8       PCB # 18     PC13 #28
                      AND         FILE             AND                              (P,P'DDE)      (O.P DDD)                     (P,P' DDD)      (0,P'DDT)       (P,P'DDT)        DDTS             (CL2)          (CL3)       (CL,3)
                      STATE                       STATION                                  (ppb)          (ppb)          (ppb)           (ppb)          (ppb)          (ppb)         (ppb)         (ppb)          (ppb)       (ppb)



                      75 FL       K5322P          AESP-2             P520                  .11.70         0.29           0.40            3.80           0.00           1.17          17.91           0.0            0.2            0.0
                      75 FL       K5323P          AESP-3             P523                  10.47          0.19           0.27            2.66           0.00           1.05          14.56           0.0            0.2            0.0
                      43 FL       K5315P          CKBP-1             P517                  1.90           0.00           0.00            0.19           0.00           0.15          2.27            0.0            0.0            0.0
                      43 FL       K5316P          CKBP-2             P520                  2.87           0.00           0.29            0.28           0.00           0.93          4.28            0.0            0.2            0.0
                      43 FL       K5317P          CKBP-3             P523                  2.83           0.16           0.33            0.48           0.00           0.32          4.02            0.0            0.1            0.0
                      76 FL       K5351P          TBNP-1             P518                  17.69          0.19           0.00            3.86           0.00           0.50          22.24           0.0            0.9            1.7
                      76 FL       K5352P          TBNP-2             P521                  40.04          0.40           0.28            7.53           0.00           1.66          49.75           0.0            1.7            2.6
                      76 FL       K5353P          TBNP-3             P524                  27.84          0.44           0.75            5.41           0.00           1.12          35.43           0.0            0.5            2.0
                      47 FL       K5333P          TBMK-1             P518                  2.82           0.02           0.00            0.38           0.00           0.42          4.07            0.0            0.4            0.2
                      47 FL       K5334P          TBMK-2             P521                  11.01          0.16           0.00            2.82           0.00           1.14          16.10           0.0            1.3            0.2
                      47 FL       K5335P          TBMK-3             P524                  9.43           0.22           0.53            3.48           0.00           1.04          17.40           0.0            0.3            0.3
                      44 FL       K5327P          TBPB-1             P518                  12.98          0.11           0.00            0.85           0.00           0.53          14.65           0.0            0.2            0.2
                      44 FL       K5328P          T131`13-2          P521                  25.54          0.22           0.00            2.39           0.00           1.12          29.67           0.0            1.1            0.3
                      44 FL       K5329P          TBPB-3             P524                  14.60          0.06           0.37            1.78           0.00           0.72          17.92           0.0            0.6            0.4
                      70 FL       K5339P          TBOT- 1            P518                  13.64          0.08           0.00            0.94           0.00           0.29          15.80           0.4            1.0            1.4
                      70 FL       K5340P          TBOT-2             P521                  19.87          0.05           0.51            2.26           0.00           0.68          23.37           0.2            0.9            2.4
                      70 FL       K5341P          TBOT-3             P524                  11.63          0.17           0.87            1.80           0.00           0.28          15.41           0.1            0.3            1.2
                      77 FL       K5309P          TBKA-1             P518                  96.90          1.97           0.00            17.16          0.55           2.45       119.31             1.4            3.1            9.5
                      77 FL       K531 OP         TBKA-2             P521                  61.09          1.49           0.00            12.14          0.51           1.98          77.32           0.2            3.0            7.0
                      77 FL       K531 1 P        TBKA-3             P524                171.91           3.83           0.00            30.40          2.25           3.99       214.89             0.6            3.9           17.1
                      46 FL       K5345P          TBCB-1             P518                  36.62          0.08           0.23            2.24           0.00           0.82          40.52           0.0            0.0            0.0
                      46 FL       K5346P          TBCB-2             P521                  95.38          0.26           2.18            6.41           0.00           0.62       119.01             0.0            1.6            0.0
                      46 FL       K5347P          TBCB-3             P524                  51.72          0.16           1.90            3.72           0.00           0.56          64.18           0.0            0.4            0.8
                      48 FL       K5369P          C13131-1           P518                  8.30           0.00           0.00            0.00           0.00           0.00          8.30            2.2            0.1            0.0
                      48 FL       K5370P          C13131-2           P521                  11.33          0.00           0.42            0.75           0.00           0.47          13.70           0.0            0.5            0.1
                      48 FL       K537 1 P        C13131-3           P525                  7.92           0.06           1.57            1.02           0.02           0.50          10.34           0.3            0.1            0.1
                      71 FL       K5363P          CBFM-1             P518                  26.51          0.13           0.59            2.33           0.00           0.75          30.97           0.0            0.1            0.2
                      71 FL       K5364P          CBFM-2             P521                  35.41          0.13           1.25            4.51           0.00           1.66          41.94           0.0            0.1            0.3
                      71 FL       K5365P          CBFM-3             P524                  42.90          0.63           0.81            12.40          0.19           1.23          58.62           0.0            0.1            0.4
                      49 FL       K5357P          NBNB-1             P518                  10.63          0.11           0.00            1.88           0.00           0.44          14.10           0.8            0.0            0.4
                      49 FL       K5358P          NBNB-2             P521                  11.35          0.14           0.49            2.11           0.00           0.90          16.28           0.1            0.1            0.4
                      49 FL       K5359P          NBNB-3             P524                  11.56          0.08           0.85            2.46           0.00           0.45          16.89           1.0            0.0            0.7
                      So FL       K538 I P        RBHC-1             P518                  3.74           0.95           1.14            1.02           0.00           0.91          7.55            0.0            0.4            0.9
                      50 FL       K5382P          RBHC-2             P521                  5.51           0.00           0.40            0.67           0.00           0.44          8.24            0.0            0.1            0.2
                      50 FL       K5383P          RBHC-3             P524                  4.59           0.06           0.92            0.87           0.00           0.36          7.84            0.0            0.2            0.2
                      51 FL       K5375P          EVFU-1             P518                  1.49           0.00           0.00            0.00           0.00           0.00          1.49            0.0            0.0            0.0
                      51 FL       K5376P          EVFU-2             P521                  1.67           0.00           0.00            0.15           0.00           0.17          2.15            0.0            0.0            0.0
                      51 FL       K5377P          EVFU-3             P524                  1.79           0.02           0.54            0.37           0.00           0.28          2.91            0.0            0.1            0.0
                      81 FL       K5396P          BHKF-1             P527                  0.19           0.00           0.25            0.23           0.00           0.00          1.96            0.0            0.3            0.3



    m m = m m m m = m m m m m m m m m m m
                                                                       MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Data






                   SITE      RAW        DESIGNATOR FOLDER                  4ADDE        2.4'DDD        ENDRIN      4,4'DDD       2.4'DDT       4,4'DDT       TOTAL     PCB #8      PCB#18 PC13#28
                   AND       FILE            AND                          (P,P'DDE)   (O,P DDD)                  (P,P' DDD)    (O,P'DDT)     (P,P'DDT)       DDTS          (CL2)        (CL3)     (CL3)
                  STATE                   STATION                              (ppb)         (ppb)        (ppb)         (ppb)        (ppb)         (ppb)       (ppb)       (ppb)        (ppb)     (ppb)



                  81 FL      K5397P        BHKF-2           P527                0.26         0100          0.39         0.32          0.00         0.00        2.29          0.0          0.3          0.3
                  81 FI,     K5398P        BHKF-3           P527                0.18         0.00          0.52         0.26          0.00         0.00        3.14          0.0          0.2          0.3



















        CD
         N)





                                                                      MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Data





                   SITE      RAW       DESIGNATOR FOLDER                  PC13 #44     PCB #52      PCB #66     PC13 #101    PC13 #105    PCB# 110/ 77     PC13 # 118    PC13 # 128  PC13 #138
                   AND       FILE           AND                               (CL4)         (CL4)        (CIA)        (CL5)         (CL5)        (CL5/4)         (CL5)         (CL6)     (CL6)
                   STATE                   SrATION                            (ppb)         (ppb)        (ppb)        (ppb)         (ppb)           (ppb)         (ppb)        (ppb)     (ppb)


                   01 TX     K5135P        LMSB-1           P505               0.0           0.0          0.0           0.0          0.0              0.0          0.0          0.0          0.9
                   01 TX     K5136P        LMSB-2           P508               0.0           0.2          0.0           0.5          0.6              0.0          1.3          0.1          3.2
                   01 TX     K5137P        LMSB-3           P511               0.0           0.1          0.0           0.2          0.1              0.0          0.2          0.0          7.4
                   03 TX     K5087P        CCIC-1           P504               0.3           0.3          0.4           0.5          0.1              0.8          1.1          0.1          3.4
                   03 TX     K5088P        CCIC-2           P507               0.4           0.4          0.3           1.1          0.1              0.9          1.9          0.5          10.0
                   03 TX     K5089P        CCIC-3           P510               0.4           0.4          0.1           0.5          0.2              0.7          0.9          0.1          2.5
                   04 TX     K5147P        ABLR-1           P504               0.1           0.0          0.0           0.1          0.0              0.2          0.2          0.0          2.2
                   04 TX     K5148P        ABLR-2           P508               0.0           0.0          0.0           0.1          0.2              0.0          0.3          0.0          2.2
                   04 TX     K5149P        ABLR-3           P511               0.0           0.0          0.0           0.3          0.0              0.0          0.2          0.0          5.4
                   05 TX     K5141P        C13CR-1          P504               0.2           0.0          0.1           0.0          0.0              0.2          0.5          0.0          2.3
                   05 TX     K5142P        CBCR-2           P508               0.5           0.0          0.2           0.0          0.0              0.0          0.9          0.0          2.7
                   05 TX     K5143P        CBCR-3           P511               0.5           0.0          0.0           0.1          0.0              0.6          0.1          0.0          4.4
                   06 TX     K5099P        MBAR-1           P504               0.2           0.1          0.3           0.0          0.0              0.3          0.2          0.1          2.7
                   06 TX     K5100P        MBAR-2           P507               0.2           0.2          0.1           0.2          0.1              1.8          1.0          0.2          2.0
                   06 TX     K5101P        MBAR-3           P511               0.2           0.1          0.0           0.1          0.0              0.4          0.0          0.2          1.4
                   07 TX     K511 IP       SAPP-1           P504               0.3           0.1          0.1           0.1          0.1              0.3          0.2          0.1          2.8
                   07 TX     K5112P        SAPP-2           P507               0.4           0.4          0.2           0.2          0.2              1.8          2.1          0.2          2.4
                   07 TX     K5113P        SAPP-3           P525               0.4           0.4          0.1           0.1          0.1              2.0          0.2          0.1          1.6
                   08 TX     K5117P        SAMP-1           P504               0.3           0.9          0.0           0.3          0.1              0.4          0.2          0.1          3.0
                   08 TX     K5118P        SAMP-2           P507               0.6           1.4          0.0           0.3          0.3              2.7          0.4          0.5          3.8
                   08 TX     K51 1 9P      SAMP-3           P511               0.2           0.4          0.4           1.3          0.1              0.5          0.0          0.1          5.9
                   09 TX     K5105P        ESSP-1           P504               0.3           0.0          0.0           0.1          0.1              0.5          0.4          0.1          2.7
                   09 TX     K5106P        ESSP-2           P507               0.4           0.3          0.0           0.3          0.1              2.8          1.8          0.4          3.9
                   09 TX     K510711'      ESSP-3           P511               0.4           0.1          0.0           0.1          0.0              0.5          0.4          0.2          2,1
                   12 TX     K5129P        MBGP-1           P504               0.8           1.1          1.3           1.3          0.2              3.8          2.6          0.3          3.7
                   12 TX     K5130P        MBGP-2           P508               0.3           0.4          0.0           2.1          0.8              3.6          2.5          0.4          4.5
                   12 TX     K513 I P      MBGP-3           P511               0.9           0.7          0.4           1.4          0.2              3.3          0.7          0.5          5.0
                   11 TX     K5123P        MBLR-1           P504               4.9          18.7          5.4           8.1          1.0              7.7          7.2          0.3          6.1
                   11 TX     K5124P        MBLR-2           P507               3.4          13.6          4.9           9.6          1.3              9.8          8.8          0.6          5.3
                   11 TX     K5125P        MBLR-3           P511               5.2          13.3          2.6           6.7          0.7             10.4          4.5          0.5          7.7
                   13 TX     K508 1 P      MBTP-1           P504               0.2           0.1          0.1           0.3          0.1              0.7          0.5          0.2          2.8
                   13 TX     K5082P        MBTP-2           P507               0.2           0.4          0.1           0.5          0.1              2.1          0.1          0.3          4.2
                   13 TX     K5083P        MBTP-3           P525               0.2           0.3          0.1           0.5          0.2              3.1          0.6          0.3          3.6
                   14 TX     K5075P        MBEM-1           P514               0.4           0.3          0.1           0.4          0.1              0.2          1.4          0.3          1.6
                   14 TX     K5076P        MBEM-2           P507               0.2           0.1          0.6           0.6          0.1              2.2          1.5          0.2          3.5
                   14 TX     K5077P        MBEM-3           13510              0.1           0.1          0.1           0.1          0.1              0.2          0.7          0.1          2.0
                   72 TX     K5015P        BRCL- 1          P514               0.8           1.4          0.8           2.0          0.5              2.4          1.9          0.5          2.8
                   72 TX     K5016P        BRCL-2           P506               0.8           1.2          0.9           3.5          1.4              3.0          2.1          0.6          4.4
                   72 TX     K5017P        BRCL-3           P525               0.5           1.2          0.5           2.5          0.3              5.5          2.6          0.5          4.6






                                                                       MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Data






                    SITE      RAW       DESIGNATOR FOLDER                 PCB #44       PC13 #52     PC13 #66    PC13 #101    PC13 #105    PCB# 110/ 77     PC13 #118     PCB # 128   PCB #138
                    AND       FILE           AND                                 (CL4)      (CL4)         (CIA)        (CLS)        (CL5)         (CL5/4)         (CL5)         (CL6)     (CL6)
                    STATE                  STATION                               (ppb)      (ppb)         (ppb)        (ppb)        (ppb)            (ppb)        (ppb)         (ppb)     (ppb)



                    57 TX     K502 I P     BRFS-1           P514                 1.0          3.9          1.5          7.3           1.0            10.7           6.2          1.6          6.9
                    57 TX     K5022P       BRFS-2           P506                 1.9          4.4          1.9          6.9           2.6              7.9          5.2          1.2          8.2
                    57 TX     K5023P       BRFS-3           P510                 0.5          1.4          0.8          3.9           0.9              5.2          3.7          0.6          5.0
                    18 TX     K5009P       GBCR-1           P525                 1.0          0.8          0.6          2.9           0.4              6.4          2.7          0.5          5.2
                    18 TX     K5010P       GBCR-2           P506                 1.9          1.7          0.9          4.6           1.4              4.7          3.0          1.1          6.3
                    18 TX     K501 1P      GBCR-3           P515                 0.5          1.0          0.4          3.0           0.4              6.2          2.6          0.6          3.5
                    58 TX     K5003P       GBOB-1           P514                 3.7          4.6          3.2          5.6           1.9              6.0          7.3          0.7          6.6
                    58 TX     K5004P       GBOB-2           P506                 6.8          6.6          4.5         14.0           5.3            14.9         12.4           1.2         12.6
                    58 TX     K5005P       GBOB-3           P515                 4.9          4.9          4.5          7.0           2.5            17.1         11.6           1.1          6.8
                    16 TX     K5057P       GBTD-1           P516R                2.1          4.1          1.0          5.6           1.5            10.6           5.6          0.6          5.8
                    16 `I'X   K5058P       GBTD-2           P516R                2.4          4.2          0.7          6.5           1.3            11.1           6.0          0.7          6.7
                    16 TX     K5059P       GBTD-3           P516R                1.4          2.8          0.8          4.7           1.1              7.2          4.1          0.4          4.5
                    15 TX     K5063P       GBYC-1           P514                 7.5        12.5           2.3         13.9           2.6            21.0           8.8          1.5         1110
                    15 TX     K5064P       GBYC-2           P508                 6.9        10.4           2.3         17.1           6.0            17.3           9.3          1.6         16.9
                    15 TX     K5065P       GBYC-3           P510                 6.5        13.0           2.3         13.5           3.8            14.6           9.0          1.3         11.6
                    59 TX     K5384P       GBSC-1           P519                 39.2       68.7          15.7         58.7         34.5             121.8        37.4           5.2         36.7
                    597X      K5384S       GBSC-I           P519R                43.3       76.6          14.0         60.8         34.7             80.3         43.9           4.1         45.4
                    59 TX     K5385P       GBSC-2           P522                 41.4       72.1          13.6         56.5         32.8             128.3        37.5           5.5         37.9
                    59 TX     K5385S       GBSC-2           P522R                55.5       86.0          15.8         79.1         42.8             95.5         54.8           5.0         57.4
                    59 TX     K5386P       GBSC-3           P526                 43.2       78.0          17.0         63.8         38.8             89.0         45.8           4.0         46.4
                    17 TX     K5039P       GBHR-1           P514                 0.6          0.9          0.7          1.4           0.2              3.5          0.8          0.5          3.6
                    17 TX     K5040P       GBHR-2           P506                 0.8          1.3          0.6          1.8           1.1              2.6          1.3          0.8          5.2
                    17 TX     K5041P       G13HR-3          P510                 0.6          0.9          0.3          0.8           0.4              2.1          1.4          0.5          4.2
                    19 TX     K5027P       SLBB-I           P514                 2.8          1.4          0.6          1.4           0.0              1.5          1.6          0.6          6.2
                    19 TX     K5028P       S 1,1313-2       P506                 1.6          2.2          0.9          5.0           2.8              6.9          3.0          1.1          8.7
                    19 TX     K5029P       SL1313-3         P525                 1.0          1.0          0.3          1.2           0.7              6.9          1.6          0.6          5.1
                    20 LA     K5033P       CLSJ-1           P514                 0.4          0.5          0.5          0.8           0.1.             0.0          0.7          0.4          2.4
                    20 IA     K5034P       CLSJ-2           P506                 0.8          1.5          0.8          2.8           1.4              0.0          1.3          0.5          4.4
                    20 LA     K5035P       CL&J-3           P510                 0.5          0.7          0.1          1.0           0.2              1.1          1.0          0.3          3.2
                    60 LA     K5045P       CLLC-1           P514                 7.0          9.6          2.6         13.9           1.0              1.8        13.6           1.6         13.8
                    60 LA     K5046P       CLLC-2           P507                 5.5        12.7           3.3         17.1           2.4            17.5         13.7           1.6         12.9
                    60 LA     K5047P       CLLC-3           P510                 .3.2         6.7          1.9         11.6           1.3            12.0         11.5           0.9         10.1
                    21 LA     K5069P       JHJH- 1          P514                 0.5          0.7          0.5          3.0           0.3              4.7          1.6          0.7          5.3
                    21 LA     K5070P       JHJH-2           P507                 0.7          1.1          0.9          3.3           0.7              7.1          2.3          1.0          7.2
                    21 LA     K5071P       JHJH-3           P510                 0.6          0.9          0.4          2.2           0.5              2.7          1.5          0.4          5.2
                    22 LA     K5159P       VBSP- I          P504                 0.8          0.6          0.5          1.7           0.8              5.9          1.5          1.1          8.7
                    22 LA     K5160P       VBSP-2           P508                 0.9          0.9          0.7          3.6           2.3              8.1          2.2          1.3          9.5
                    22 LA     K516 1 P     VBSP-3           P512                 1.2          o.5          1.0          3.7           0.8              8.6          2.3          1.8          8.0
                    24 LA     K5189P       ABOB-1           P505                 0.7          1.6          0.7          1.8           1.4              1.2          3.1          1.3          6.8






                                                                     MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Data






                   SITE      RAW       DESIGNATOR FOLDER                 PCB #44      PCB #52      PCB #66     PCB #101     PCB #105     PCB# 110/77     PCB # 118    PCB # 128    PCB #138
                   AND       FILE           AND                              (CL4)        (CL4)         (CIA)        (CL5)        (CL5)        (CL5/4)         (CL5)        (CL6)     (CL6)
                   STATE                  SrATION                            (ppb)        (ppb)         (ppb)        (ppb)        (ppb)           (ppb)        (ppb)         (ppb)    (ppb)


                   24 LA     K5190P       ABOB-2           P508                0.5          0.4          0.8          1.4          1.2              1.7          1.4          0.7          4.9
                   24 LA     K519 1 P     ABOB-3           P512                0.8          0.7          0.8          3.5          0.5              4.9          2.3          1.4          6.5
                   25 LA     K5195P       CLCL-1           P505                0.7          1.1          0.0          0.8          0.6              0.0          2.4          0.5          6.2
                   25 LA     K5196P       CLCL-2           P508                0.4          0.2          0.0          0.6          0.0              0.0          0.4          0.4          3.4
                   25 LA     K5197P       CLCL-3           P512                0.6          0.5          0.4          0.5          0.4              0.4          1.4          0.6          3.8
                   26 LA     K5165P       TBLB-1           P505                0.4          0.6          0.2          0.5          0.4              0.9          2.4          0.1          1.3
                   26 LA     K5166P       TBLB-2           P508                0.3          0.3          0.4          1.3          0.6              2.1          1.2          0.8          3.7
                   26 LA     K5167P       TBLB-3           P525                0.9          0.4          0.2          0.6          0.1              3.4          1.0          0.2          2.4
                   27 LA     K5183P       TBLF-l           P525                0.4          0.4          0.4          0.7          0.1              0.2          0.6          0.2          2.8
                   27 LA     K5184P       TBLF-2           P508                0.2          0.2          0.1          0.8          0.3              0.8          1.3          0.1          3.0
                   27 LA     K5185P       TBLF-3           P512                0.5          0.3          0.4          0.4          0.6              0.9          1.1          0.4          3.1
                   28 LA     K5168P       BBSD-1           P505                0.3          0.9          0.2          0.5          0.3              1.7          2.1          0.3          3.6
                   28 LA     K5169P       BBSD-2           P508                0.4          0.1          0.2          0.7          0.3              1.8          0.8          0.1          3.4
                   28 LA     K5170P       BBSD-3           P525                0.5          0.6          0.1          0.6          0.1              3.1          0.6          0.2          2.7
                   29 LA     K5174P       BBMB-1           P505                1.5          2.0          2.0          1.7          1.0              0.5          5.9          0.5          4.4
                   29 LA     K5175P       BBMB-2           P508                0.6          0.6          0.6          1.7          0.0              1.1          2.3          0.3          3.9
                   29 LA     H5176P       BBMB-3           P512                0.8          1.2          1.0          1.7          0.3              4.6          3.0          0.4          3.7
                   65 LA     K521 OP      MRTP-1           P505                4.2          6.3          1.9          7.9          4.9            20.0           6.3          3.2        17.0
                   65 LA     K521 I P     MRTP-2           P515                2.6          4.1          0.7          6.3          2.7            18.0           3.5          2.2          9.9
                   65 LA     K5212P       MRTP-3           P512                2.4          3.5          1.2          5.0          2.8            18.3           5.6          3.3        13.5
                   31 LA     K5216P       BSSI-I           P505                2.5          4.8          1.4          9.2          4.4            14.8           5.1          2.5        13.9
                   31 LA     K5217P       BSSI-2           P515                2.9          3.6          ill          5.4          1.1            11.9           3.2          1.9          8.6
                   31 LA     K5218P       BSSI-3           P512                0.7          2.8          0.3          7.0          1.9              9.0          8.2          3.4        12.3
                   30 LA     K520 I P     BSBG-1           P505                0.1          0.2          0.5          0.4          0.2              0.0          0.4          0.2          4.6
                   30 LA     K520213      BSBG-2           P515                0.1          0.2          0.1          0.3          0.1              0.6          0.2          0.1          1.0
                   30 LA     K5203P       BSBG-3           P512                0.1          0.1          0.2          0.4          0.2              0.2          0.8          0.1          2.2
                   32 LA     K5207P       LBMP-1           P505                0.6          0.9          0.5          0.9          0.7              1.5          1.6          0.3          3.1
                   32 LA     K5208P       LBMP-2           P515                0.2          0.3          0.2          0.3          0.1              1.2          0.2          0.1          1.3
                   32 LA     K52091-1     LBMP-3           P512                0.4          0.2          0.1          0.5          0.2              1.1          0.6          0.3          2.4
                   62 LA     K5249P       LPGO-1           P519              28.2         35.0           5.8         61.6         17.4            125.1        33.6           7.7        77.1
                   62 LA     K5249S       LPGO-1           P519R             32.9         38.6           9.0         76.6         11.2            86.1         41.5           8.4        112.2
                   62 LA     K5250P       LPGO-2           P522              23.0         28.0           5.7         51.2          5.8            99.4         25.9           5.5        56.6
                   62 LA     K5250S       LPGO-2           P522R             30.2         29.4           8.1         61.7         10.2            70.2         34.8           6.4        87.9
                   62 LA     K5251P       LPGO-3           P526              36.5         43.7           12.9        93.6         14.7            104.6        49.0           9.0        116.5
                   33 MS     K5222P       mSpC-i           P505                2.9          4.9          2.7          4.2          2.3              8.5          5.6          0.9          7.4
                   33 MS     K5223P       MSPC-2           P515                1.3          1.9          0.9          5.2          0.7              4.1          1.7          0.7          2.8
                   33 MS     K5224P       MSPC-3           P513                1.5          2.0          1.2          2.6          1.1              4.3          2.1          0.6          4.1
                   34 MS     K5228P       MSBB-1           P506                5.3        10.0           4.4         15.7          5.7            13.4         12.5           1.3        17.0
                   34 MS     K5229P       MSBB-2           P515                8.2          7.9          3.6         15.8          3.7            30.1         15.9           1.8        16.9






                                                                              MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Data






                     SITE       RAW        DESIGNATOR FOLDER                     PCB #44        PCB #52       PC13 #66      PC13 #101     PC13 # 105     PCB# 110/ 77      PC13 #118      PC13 # 128    PC13 #138
                     AND        FILE             AND                                   (CL4)         (CL4)          (CIA)         (CL5)          (CL5)          (CL5/4)           (CL5)          (CL6)      (CL6)
                     STATE                      STATION                                (ppb)         (ppb)          (ppb)         (ppb)          (ppb)             (ppb)          (ppb)          (ppb)      (ppb)



                     34 MS      K5230P          MSBB-3            P513                  3.2            5.1            2.6           7.2            1.9             10.9             6.1           0.7          10.2
                     35 MS      K5246P          MSPI3-1           P506                  1.5            3.8            1.3           4.5          10.8                5.5            3.6           0.8            7.8
                     35 MS      K5247P          MSPB-2            P515                  0.4            1.1            0.5           1.6            8.9               3.3            2.0           0.8            3.3
                     35 MS      K5248P          MSPB-3            P513                  0.4            1.6            0.4           2.1            7.2               4.0            1.5           0.3            4.3
                     36 AL      K5234P          MBCP-1            P506                  1.7            3.8            1.0           5.3          16.6                7.4            3.8           2.0          11.0
                     36 AL      K5235P          MBCP-2            P515                  0.9            1.3            0.5           6.0            8.3               5.0            1.7           1.0            4.8
                     36 AL      K5236P          MBCP-3            P513                  0.6            1.4            2.8           3.0            1.6               4.5            2.1           1.1            5.3
                     66 AL      K5240P          MBHI- I           P506                  3.1            8.7            2.0           7.3          24.9              15.9             8.0           2.2          14.7
                     66 AL      K5241P          MBHI-2            P515                  1.7            4.9            0.8           5.9          19.4              15.3             4.4           1.3            8.9
                     66 AL      K5242P          M131-11-3         P513                  1.5            4.3            0.4           4.3          11.5              13.5             4.1           1.0            9.9
                     67 FL      K5261P          PBPH-1            P517                  2.8            9.5            2.6         19.9             3.9             34.0           14.1            3.1          19.8
                     67 FL      K5262P          PBPH-2            P520                  4.4          17.1             5.0         30.7             5.5             38.6           28.2            7.4          40.7
                     67 FL      K5263P          PBPH-3            P523                  4.3          14.4             4.4         32.0             4.2             29.7           24.6            5.1          36.8
                     37 FL      K5255P          P13113-1          P517                  3.3          14.0             4.1         38.7             7.5             57.5           26.4            5.7          36.1
                     37 FL      K525613         P13113-2          P520                  4.4          20.7             7.8         52.4             6.4             55.7           38.6            10.6         60.8
                     37 FL      K5257P          1313113-3         P529                  3.3          17.1             4.9         51.7             5.4             51.4           36.8            7.7          55.4
                     73 FL      K5267P          CBJB-1            P517                  0.9            1.3            1.5           3.3            0.9               6.7            2.6           0.4            2.9
                     73 FL      K5268P          CEUB-2            P520                  1.1            1.6            1.8           3.7            1.2               6.7            5.0           1.0            9.6
                     73 FL      K5269P          CBJB-3        P527(P523)                0.7            1.2            1.2           3.0            1.0               3.0            3.0           0.8            4.9
                     38 FL      K5273P          CBSR- 1           P517                  0.1            0.1            0.1           0.4            0.1               0.0            0.0           0.3            1.9
                     38 FL      K5274P          CBSR-2            P520                  0.1            0.1            0.0           0.6            0.1               0.0            0.0           0.5            3.4
                     38 FL      K5275P          CBSR-3        P527(P523)                0.1            0.1            0.0           0.5            0.2               0.0            0.0           0.5            3.9
                     39 FL      K5279P          CBSP-1            PS 17                 0.4            1.1            0.3           1.6            0.3               3.5            2.9           0.3            4.7
                     39 FL      K5280P          CBSP-2            P529                  0.3            1.6            0.4           2.2            0.4               5.1            1.6           0.5            4.8
                     39 FL      K5281P          CBSP-3            P523                  1.5            1.4            0.1           3.8            0.5               3.6            2.4           0.7          10.4
                     74 FL      K5303P          PCLO-i            P529                  0.5            0.2            0.1           2.8            0.2               5.4            0.9           0.3            3.9
                     74 FL      K5303P          PCLO-1            P517                  0.3            0.5            0.2           2.1            0.2               0.0            1.7           0.3            2.2
                     74 FL      K5304P          PCLO-2            P520                  1.7            4.6            2.2           7.7            1.9               2.3          11.7            3.0          21.6
                     74 FL      K5305P          PCLO-3            P523                  0.5            3.2            4.0           6.5            1.3               3.0            4.5           0.9          12.0
                     40 FL      K5297P          SAW13- 1          P517                  11.5         22.0             5.7         48.1           14.6              56.9           39.5            4.2          33.0
                     40 FL      K5298P          SAWB-2            P520                  14.6         27.7            12.0         75.7           26.1              76.1           74.8            9.2          68.0
                     40 FL      K5299P          SAWB-3            P523                  14.4         26.5            10.5         64.1           19.7              75.4           61.8            5.1          48.7
                     41 FL      K5291P          APDB-I            P517                  0.1            0.4            1.6           0.3            0.6               0.0            2.2           0.4            2.6
                     41 FL      K5292P          APDB-2            P520                  0.5            0.6            0.2           0.6            0.4               0.0            0.0           0.9          10.1
                     41 FL      K5293P          APDB-3            P523                  0.6            1.0            1.3           0.8            0.1               0.0            0.3           0.4            4.4
                     42 FL      K5285P          APCP-1            P517                  0.9            0.4            0.6           6.5            0.1               0.0            1.2           0.2            1.9
                     42 FL      K5286P          APCP-2            P520                  1.4            0.6            0.6           0.6            0.4               0.0            2.5           0.3            8.2
                     42 FL      K5287P          APCP-3            P523                  1.1            1.1            0.2           1.2            0.1               0.0            0.5           0.1            5.1
                     75 FL      K532 1 P        AESP-1            P517                  0.0            0.0            0.1           0.1            0.0               0.0            0.3           0.2            1.8





                                                                         MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Data





                    SITE       RAW       DESIGNATOR FOLDER                   PC13 #44      PC13 #52     PC13 #66     PCB #101     PC13 # 105     PCB#110/77       PC13 #118    PC13 # 128   PC13 #138
                    AND        FILE           AND                                 (CL4)         (CL4)        (CIA)         (CLS)         (CL5)          (CL5/4)         (CL5)         (CL6)     (CL6)
                    STATE                    STATION                              (ppb)         (ppb)         (ppb)        (ppb)         (ppb)            (ppb)         (ppb)         (ppb)     (ppb)


                    75 FL      K5322P        AESP-2           P520                  0.1          0.0           0.0           0.7           0.0              0.0           3.2          0.3           5.3
                    75 FL      K5323P        AESP-3           P523                  0.1          0.2           0.0           0.8           0.0              0.2           0.3          0.2           3.1
                    43 FL      K5315P        CK13P-1          P517                  0.0          0.0           0.0           0.1           0.0              0.0           0.8          0.1           0.9
                    43 FL      K5316P        CKBP-2           P520                  0.0          0.0           0.0           0.3           0.0              0.3           0.4          0.2           6.8
                    43 FL      K5317P        CKBP-3           P523                  0.0          0.1           0.0           0.3           0.0              0.2           0.4          0.2           2.0
                    76 FL      K5351P        TBNP- 1          P518                  2.0          3.5           1.2           3.4           1.1              0.0           5.9          0.4           5.6
                    76 FL      K5352P        TBNP-2           P521                  2.7          4.2           2.4           6.9           1.4              0.0           9.3          0.8          11.7
                    76 FL      K5353P        TBNP-3           P524                  3.3          2.9           1.7           6.3           1.3              0.5           6.7          0.7           9.5
                    47 FL      K5333P        TBMK-1           P518                  0.4          0.2           0.1           0.1           0.2              0.0           1.7          0.0           1.0
                    47 FL      K5334P        TBMK-2           P521                  0.6          0.7           0.0           0.7           0.5              0.0           1.8          0.2           4.9
                    47 FL      K5335P        TBMK-3           P524                  0.4          0.9           0.0           1.1           0.3              0.0           1.3          0.1           4.0
                    44 FL      K5327P        TBPB-1           P518                  1.1          0.7           0.3           2.2           0.4              0.0           2.5          0.0           4.0
                    44 FL      K5328P        TBPB-2           P521                  1.7          1.7           3.7           3.6           0.4              0.0           3.8          0.5           9.0
                    44 FL      K5329P        TBPB-3           P524                  0.9          0.5           0.2           2.2           0.4              0.0           2.6          0.1           5.4
                    70 FL      K5339P        TBOT-1           P518                  1.1          1.5           1.5           1.3           0.5              0.9           4.1          0.0           3.3
                    70 FL      K5340P        TBOT-2           P521                  2.0          2.3           1.7           1.9           0.4              1.2           2.2          0.3           4.9
                    70 FL      K5341P        TBOT-3           P524                  1.3          1.1           0.8           1.9           0.2              3.0           1.0          0.1           3.8
                    77 FL      K5309P        TBKA-1           P518                 12.9         22.6          10.0         28.8            6.2            48.5          28.6           1.4          20.7
                    77 FL      K531 OP       T13KA-2          P521                  9.0         16.3           8.3         24.5            4.7            25.5          26.7           1.4          24.1
                    77 FL      K531 1 P      TBKA-3           P524                 22.9         43.7          20.5         56.6           11.8            50.7          54.3           3.2          45.4
                    46 FL      K5345P        TBCB-1           P518                  0.7          2.7           0.9           0.3           0.2              0.0           2.5          0.0           1.9
                    46 FL      K5346P        TBCB-2           P521                  2.7          8.8           2.0           2.0           0.6              0.0           4.2          0.3           4.1
                    46 FL      K5347P        TBCB-3           P524                  1.0          5.0           0.3           1.6           0.3              0.0           2.2          0.2           2.3
                    48 FL      K5369P        C13131-1.        P518                  0.1          0.7           2.5           0.4           0.2              0.0           1.4          0.0           1.0
                    48 FL      K5370P        C13131-2         P521                  0.2          0.4           3.8           0.9           0.2              0.0           1.6          0.0           1.8
                    48 FL      K5371P        C13131-3         P525                  0.3          0.3           0.2           0.6           0.2              0.0           1.4          0.1           2.3
                    71 FL      K5363P        CBFM-1           P518                  0.9          1.4           0.0           2.1           0.1              4.1           4.3          0.3           2.9
                    71 FL      K5364P        CBFM-2           P521                  1.6          2.4           0.0           3.2           0.4              0.8           4.1          0.7           5.4
                    71 FL      K5365P        CBFM-3           P524                  1.2          1.5           0.0           2.8           0.7              2.9           4.8          0.3           5.5
                    49 FL      K5357P        N13NI3-1         P518                  1.5          2.6           0.9           2.0           0.3              4.1           3.5          0.4           2.5
                    49 FL      K5358P        NBNB-2           P521                  1.5          2.2           0.5           2.5           0.2              3.6           3.0          0.6           3.4
                    49 FL      K5359P        NBNB-3           P524                  1.8          2.4           0.8           3.0           0.4              3.7           3.3          0.9           3.0
                    50 FL      K538 1 P      RI3HC-1          P518                  1.0          0.7           1.5           0.9           0.4              0.7           1.5          1.1           1.6
                    50 FL      K5382P        R13HC-2          P521                  0.3          0.2           0.0           0.4           0.3              0.3           0.2          0.1           2.5
                    50 FL      K5383P        RBHC-3           P524                  0.3          0.2           0.1           0.2           0.2              0.3           0.7          0.2           1.3
                    51 FL      K5375P        EVFU-1           P518                  0.0          0.0           0.0           0.0           0.0              0.0           0.0          0.0           0.8
                    51 FL      K5376P        EVFIJ-2          P521                  0.1          0.0           0.0           0.1           0.1              0.0           0.0          0.0           1.2
                    51 FL      K5377P        EVFU-3           P524                  0.0          0.1           0.0           0.2           0.1              0.3           0.1          0.0           2.0
                    81 FL      K5396P        BHKF-1           P527                  0.1          0.2           0.1           0.1           0.2*             0.0           0.3          0.1           2.5



     m m m m m m m m m m m m m m m m m m m
                                                                      MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Data






                   SITE      RAW       DESIGNATOR FOLDER                 PC13 #44     PCB #52      PC13 #66 PC13 #101       PC13#105 PCB#110/77 PCB#118                PCB # 128 PC13 # 138
                   AND       FILE #         AND                               (CL4)        (CL4)        (CIA)        (CLS)        (CL5)         (CL5/4)         (CL5)        (CL6)     (CL6)
                  STATE                   STATION                             (ppb)        (ppb)        (ppb)         (ppb)        (ppb)           (ppb)        (ppb)        (ppb)     (ppb)



                   81 FL     K5397P        BHKF-2           P527                0.1          0.3          0.1          0.2           0.2             0.0          0.0          0.0         2.3
                   81 FL     K5398P        BHKF-3          P527                 0.2          0.1          0.1          0.4           0.0             0.0          0.0          0.0         3.3



















         (o
         00





                                                                       MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Data






                   SITE       RAW      DESIGNATOR FOLDER                 PCB# 126     PCB #153     PC13 # 170   PCB #180      PC13 #187    PC13 # 195   PC13 #206     PC13 #209    TOTAL TOTAL
                   AND        FILE          AND                                (CL5)        (CL6)        (CL7)        (CL7)         (CL7)        (CL8)         (CL9)       (CLIO)    PCB'S    ISOMERS
                   STATE                   STATION                             (ppb)        (ppb)        (ppb)         (ppb)        (ppb)        (ppb)         (ppb)        (ppb)     (ppb)    (ppb)


                   01 TX      K5135P       LMS13-1          P505                0.0          0.0          0.0           0.0          0.0          0.0           0.0          0.0      15.6              1
                   017X       K5136P       LMSB-2           P508                0.0          0.9          0.0           0.2          0.4          0.1           0.0          0.0      29.3              8
                   01TX       K5137P       LMSB-3           P511                0.0          0.8          0.0           0.5          0.4          0.0           0.0          0.0      32.2            10
                   03 TX      K5087P       CCIC-1           P504                0.1          1.9          0.0           1.3          0.9          0.0           0.0          0.1        39            13
                   03 TX      K5088P       CCIC-2           P507                0.5          1.6          0.3           0.9          1.3          0.7           0.7          0.5        59            24
                   03 TX      K5089P       CCIC-3           P510                0.0          2.4          0.0           0.0          0.7          0.2           0.0          0.2        31              9
                   04 TX      K5147P       ABLR-1           P504                0.0          0.0          0.0           0.1          0.1          0.0           0.0          0.0        21              4
                   04TX       K5148P       ABLR-2           P508                0.0          0.0          0.0           0.1          0.1          0.0           0.0          0.0        22              4
                   04 TX      K5149P       ABLR-3           P511                0.0          0.0          0.0           0.5          INT          0.0           0.0          0.0        26              6
                   05 TX      K5141P       C13CR-1          P504                0.2          0.0          0.0           0.1          0.1          0.0           0.0          0.1        26              7
                   05TX       K5142P       C13CR-2          P508                0.0          0.0          0.0           0.0          0.1          0.0           0.0          0.0        23              5
                   05 TX      K5143P       CBCR-3           P511                0.0          0.0          0.0           0.2          0.0          0.0           0.0          0.0        25              6
                   06 TX      K5099P       MBAR-1           P504                0.1          0.1          0.0           0.6          0.2          0.0           0.0          0.1        23              5
                   06 TX      K5100P       MBAR-2           P507                0.0          0.0          0.0           0.5          0.3          0.0           0.0          0.1        27              7
                   06 TX      K5101P       MBAR-3           P511                0.0          0.0          0.0           0.0          0.0          0.0           0.0          0.0        19              3
                   07 TX      K5111P       SAPP-1           P504                0.2          0.4          0.0           0.1          0.1          0.0           0.0          0.0        23              5
                   07 TX      K5112P       SAPP-2           P507                0.0          0.2          0.0           0.5          0.4          0.0           0.0          0.1        32            10
                   07 TX      K5113P       SAPP-3           P525                0.0          0.4          0.0           0.2          0.4          0.1           0.0          0.1        26              6
                   08 TX      K5117P       SAMP-1           P504                0.1          0.6          0.0           0.1          0.7          0.0           0.0          0.0        27              7
                   08 TX      K5118P       SAMP-2           P507                0.5          0.7          0.0           0.9          1.1          0.0           0.0          0.0        41            14
                   08 TX      K5119P       SAMP-3           P511                0.0          0.3          0.0           0.6          0.0          0.3           0.0          0.0        34            11
                   09 TX      K5105P       ESSP-1           P504                0.1          0.7          0.0           0.1          0.4          0.0           0.0          0.0        24              5
                   09TX       K5106P       ESSP-2           P507                0.0          0.8          0.0           1.0          0.8          0.0           0.0          0.2        39            13
                   09 TX      K5107P       ESSP-3           P511                0.0          0.5          0.0           0.1          0.6          0.0           0.0          0.0        25              6
                   12 TX      K5129P       MBGP-1           P504                0.0          1.3          0.0           0.1          1.8          0.0           0.0          0.0        50            19
                   12TX       K5130P       MBGP-2           P508                0.5          1.9          0.0           0.1          2.5          0.0           0.0          0.0        52            20
                   12 TX      K5131P       MBGP-3           P511                0.0          1.2          0.0           1.6          1.9          0.0           0.0          0.2        48            18
                   11 TX      K5123P       MBLR-1           P504                0.1          7.1          0.0           0.1          2.7          0.0           0.0          0.0        155           75
                   11 TX      K5124P       MBLR-2           P507                0.0          7.3          0.0           0.8          3.6          0.0           0.0          0.0        155           75
                   11 TX      K5125P       MBLR-3           P511                0.0          5.8          0.0           0.9          4.2          0.0           0.0          0.0        136           64
                   13 TX      K5081P       MBTP-1           P504                0.1          0.5          0.0           0.1          0.5          0.0           0.0          0.0        25              6
                   13 TX      K5082P       MBTP-2           P507                0.1          0.7          0.0           0.4          0.6          0.0           0.0          0.0        33            10
                   13 TX      K5083P       MBTP-3           P525                0.0          1.7          0.0           0.5          0.9          0.0           0.0          0.0        36            12
                   14 TX      K5075P       MBEM-1           P514                0.0          0.2          0.0           0.1          0.8          0.0           0.0          0.0        25              6
                   14 TX      K5076P       MBEM-2           P507                0.2          0.6          0.0           0.2          0.4          0.0           0.0          0.0        34            11
                   14 TX      K5077P       MBEM-3           P510                0.1          0.8          0.0           0.2          0.3          0.0           0.0          0.0        23              5
                   72 TX      K5015P       BRCL-1           P514                0.0          3.4          0.0           0.2          0.9          0.1           0.0          0.2        48            18
                   72 TX      K5016P       BRCL-2           P506                0.0          4.3          0.3           1.1          1.4          0.0           0.0          0.2        63            26
                   72 TX      K5017P       BRCL-3           P525                0.7          5.0          0.0           0.4          1.5          0.0           0.0          0.2        63            26






                                                                       MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Data






                   SITE      RAW       DESIGNATOR FOLDER                 PCB# 126     PC13 #153    PC13 #170    PC13 #180     PCB #187     PC13 # 195   PC13 #206     PC13 #209    TOTAL TOTAL
                   AND       FILE           AND                                (CL5)        (CL6)        (CL7)        (CL7)         (CL7)        (CL8)         (CL9)      (CLIO)     PCB'S    ISOMERS
                   STATE                   STATION                             (ppb)        (ppb)        (ppb)        (ppb)         (ppb)        (ppb)         (ppb)        (ppb)    (ppb)      (ppb)



                   57 TX     K5021P        BRFS-1           P514                0.0          6.7          0.0           1.0          3.1           0.0          0.0          0.1       ill            51
                   57 TX     K5022P        BRFS-2           P506                0.0          8.4          0.5           1.5          3.1           0.0          0.0          0.0       116            54
                   57 TX     K5023P        BRFS-3           P510                0.1          5.9          0.0           0.7          1.2           0.0          0.0          0.2        71            30
                   18 TX     K5009P        G13CR-I          P525                1.2          7.5          0.0           0.4          2.9           0.0          0.0          0.0        75            33
                   18 TX     K5010P        GBCR-2           P506                0.1          6.1          0.6           1.9          3.4           0.0          0.3          0.4        87            39
                   18 TX     K5011P        GBCR-3           P515                0.0          6.3          0.1           0.3          2.6           0.2          0.3          0.4        68            29
                   58 TX     K5003P        GBOB-1           P514                0.0          8.7          0.0           1.8          2.6           0.0          0.0          0.0       117            54
                   58 TX     K5004P        GBOB-2           P506                0.0         12.8          0.5           3.3          4.1           0.0          0.0          0.0       205            101
                   58 TX     K5005P        GBOB-3           P515                0.0          9.7          0.0           1.1          2.5           0.0          0.0          0.0       157            76
                   16 TX     K5057P        GBTD-l           P516R               0.0         10.4          0.0           0.3          3.9           0.0          0.0          0.0       112            52
                   16 TX     K5058P        GBTD-2           P516R               0.0         12.6          0.0           0.4          4.4           0.0          0.0          0.0       122            57
                   16 TX     K5059P        GBTD-3           P516R               0.0          8.9          0.0           0.4          2.5           0.0          0.0          0.0        88            39
                   15 TX     K5063P        GBYC-1           P514                0.0         11.5          010           2.2          5.2           0.0          0.0          0.0       205            101
                   15 TX     K5064P        GBYC-2           P508                0.0         16.3          0.0           2.6          5.1           0.0          0.0          0.1       229            114
                   15 TX     K5065P        GBYC-3           P510                0.0         16,2          0.0           2.5          4.3           0.0          0.0          0.1       206            102
                   59 TX     K5384P        GBSC-l           P519                15.8        53.2          0.0         19.8          11.4           0.0          0.0          0.0     1067             557
                   591X      K5384S        GBSC-1           P519R               5.0         56.5          0.0         25.9          11.2           0.0          1.9          0.0     1037             541
                   59 TX     K5385P        GBSC-2           P522                17.2        52.0          0.0         20.0          12.2           0.0          0.0          0.0     1081             565
                   59 TX     K5385S        GBSC-2           P522R               9.2         66.4          0.0         31.9          14.0           0.4          2.8          5.0     1278             669
                   59 TX     K5386P        GBSC-3           P526                4.9         59.7          0.0         25.9          11.9           1.1          3.9          5.7     1112             581
                   17 TX     K5039P        GBHR-1           P514                0.0          2.1          0.1           0.3          2.0           0.0          0.1          0.0        45            17
                   17 TX     K5040P        GBHR-2           P506                0.0          4.7          0.2           0.8          2.3           0.0          0.0          0.0        58            24
                   17 TX     K5041P        GBHR-3           P510                0.0          3.8          0.1           0.1          2.0           0.0          0.0          0.0        47            17
                   1 9TX     K502711       SI,1313- I       P514                0.0          1.9          0.0           0.4          1.0           0.0          0.0          0.0        52            20
                   19 TX     K5028P        SLBB-2           P506                0.0          8.9          0.7           1.6          2.9           0.0          0.0          0.0       103            47
                   19 TX     K5029P        SI,1313-3        P525                0.7          3.6          0.4           0.5          1.6           0.4          0.2          0.5        65            27
                   20 LA     K5033P        CLSJ-l           P514                0.0          1.4          0.0           0.3          1.9           0.0          0.2          0.3        33            10
                   20 LA     K5034P        CLSJ-2           P506                0.0          4.0          0.2           1.1          1.9           0.0          0.0          0.0        54            21
                   20 LA     K5035P        CLSJ-3           P510                0.0          3.2          0.0           0.2          1.2           0.0          0.0          0.1        38            13
                   60 LA     K5045P        CLLC-1           P514                0.0         14.0          0.0           3.1          4.0           0.0          0.0          0.0       181            88
                   60 LA     K5046P        CLLC-2           P507                2.1         13.9          0.2           3.7          4.0           0.0          0.0          0.3       228            113
                   60 LA     K5047P        CLLC-3           13510               0.0         12.6          0.0           3.4          2.6           0.0          0.0          0.2       167            81
                   21 LA     K5069P        JHJH-1           P514                0.0          3.3          0.0           0.4          3.5           0.0          0.0          0.0        61            25
                   21 LA     K5070P        JHJH-2           P507                1.7          5.0          0.1           0.8          4.8           0.0          0.0          0.0        85            38
                   21 LA     K5071P        JHJH-3           P510                0.0          5.4          0.0           0.1          2.2           0.0          0.0          0.0        56            22
                   22 LA     K5159P        VBSP-l           P504                0.2          6.1          0.0           0.5          4.1           0.0          0.0          0.2        76            33
                   22 LA     K5160P        VBSP-2           P508                2.1          6.2          0.0           0.8          3.1           0.0          0.0          0.1        93            42
                   22 LA     K5161P        VBSP-3           P512                2.5          7.9          0.4           1.4          4.8           0.0          0.1          0.4       101            46
                   24 LA     K5189P        ABOB-1           P505                0.4          3.6          0.4           0.7          2.1           0.0          0.0          0.0        64            26





                                                                         MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Data






                    SITE       RAW       DESIGNATOR FOLDER                  PCB# 126     PCB # 153    PCB # 170     PCB # 180     PCB # 187    PCB # 195     PCB #206      PCB #209      TOTAL TOTAL
                    AND        FILE           AND                                (CL5)         (CL6)         (CL7)        (CL7)         (CL7)         (CL8)        (CL9)        (CLIO)     PCB'S   ISOMERS
                    STATE                    STATION                             (ppb)         (ppb)         (ppb)        (ppb)         (ppb)         (ppb)         (ppb)        (ppb)     (ppb)      (ppb)


                    24 LA      K5190P        ABOB-2           P508                 0.0           3.7          0.0           0.9           2.3          0.0           0.0           0.0        52            20
                    24 LA      K5191P        ABOB-3           P512                 0.0           7.0          0.0           0.6           2.7          0.0           0.0           0.7        76            33
                    25 LA      K5195P        CLCL- 1          P505                 0.3           1.5          0.3           0.5           1.0          0.0           0.0           0.0        45            16
                    25 LA      K5196P        CLCL-2           P508                 0.0           0.7          0.1           0.1           0.8          0.0           0.0           0.0        28              8
                    25 LA      K5197P        CLCL-3           P512                 0.0           1.4          0.2           0.2           0.6          0.2           0.3           0.4        37            12
                    26 LA      K5165P        TBLB- 1          P505                 0.0           0.3          0.1           0.3           0.3          0.0           0.0           0.0        30              9
                    26 LA      K5166P        TBLB-2           P508                 0.0           0.4          0.2           0.7           0.4          0.0           0.0           0.0        40            14
                    26 LA      K5167P        TBLB-3           P525                 0.0           0.8          0.0           0.2           0.5          0.0           0.0           0.0        35            11
                    27 LA      K5183P        TBLF- 1          P525                 0.0           1.1          0.0           0.4           0.5          0.0           0.0           0.0        29              8
                    27 LA      K5184P        TBLF-2           P508                 0.2           0.5          0.0           0.2           0.4          0.0           0.0           0.1        31              9
                    27 LA      K5185P        TBLF-3           P512                 0.3           0.5          0.1           0.3           0.4          0.0           0.0           0.1        32            10
                    28 LA      K5168P        BBSD-1           P505                 0.1           0.1          0.0           0.1           0.7          0.0           0.0           0.0        35            11
                    28 LA      K5169P        BBSD-2           P508                 0.0           0.3          0.0           0.1           0.9          0.0           0.0           0.0        32            10
                    28 LA      K5170P        BBSD-3           P525                 0.3           1.2          0.0           0.2           0.8          0.1           0.0           0.0        36            11
                    29 LA      K5174P        BBMB-1           P505                 0.9           1.8          0.0           1.0           1.4          0.0           0.0           0.1        64            26
                    29 LA      K5175P        BBMB-2           P508                 0.0           0.9          0.0           0.7           1.2          0.0           0.0           0.1        43            15
                    29 LA      K5176P        BBMB-3           P512                 0.2           2.3          0.0           0.0           0.8          0.0           0.0           0.2        54            21
                    65 LA      K52 1 OP      MRTP-1           P505                 0.0         17.2           0.9           3.7           8.1          0.0           0.0           0.9      212           105
                    65 LA      K521 IP       MRTP-2           P515                 0.0         11.3           0.4           1.3           4.9          0.0           0.0           0.6      147             71
                    65 LA      K5212P        MR'f?-3          P512                 0.0         12.1           0.5           2.0           6.8          0.4           0.3           1.5      168             82
                    31 LA      K5216P        BSSI-I           P505                 0.0         12.9           0.5           1.8           6.5          0.0           0.0           0.0      168             82
                    31 LA      K5217P        BSSI-2           P515                 0.0         10.0           0.1           0.6           4.1          0.0           0.0           0.0      118             55
                    31 LA      K5218P        BSSI-3           P512                 2.7           7.9          0.0           0.9           6.1          0.2           0.5           0.3      138             65
                    30 LA      K5201P        BSBG-1           P505                 0.0           0.0          0.2           0.8           0.4          0.0           0.0           0.0        30              9
                    30 LA      K5202P        BSBG-2           P515                 0.0           0.4          0.0           0.1           0.2          0.0           0.0           0.0        21              4
                    30 LA      K5203P        BSBG-3           P512                 0.0           0.7          0.0           0.0           0.1          0.0           0.0           0.0        24              5
                    32 LA      K5207P        LBMP-1           P505                 0.0           1.0          0.2           0.8           0.6          0.0           0.0           0.1        39            14
                    32 LA      K5208P        LBMP-2           P515                 0.0           0.2          0.0           0.1           0.3          0.0           0.0           0.0        23              5
                    32 LA      K5209P        LBMP-3           P512                 0.0           0.7          0.0           0.1           0.3          0.0           0.0           0.0        27              7
                    62 LA      K5249P        LPGO-I           P519                 0.0         131.6          5.5           6.8         46.6           0.0           0.0           0.0     1158           605
                    62 LA      K5249S        LPGO-1          P519R                12.6         181.9          7.0         10.4          63.1           0.2           0.0           0.3     1374           720
                    62 LA      K5250P        LPGO-2           P522                 0.0         110.1          4.4           5.1         36.3           0.0           0.0           0.0      914           476
                    62 LA      K5250S        LPGO-2          P522R                 0.0         142.1          6.1           8.8         52.8           0.5           0.1           1.2     1094           572
                    62 LA      K5251P        LPGO-3           P526                 0.0         198.6          9.1         12.8          68.3           0.5           0.0           0.0     1522           798
                    33 MS      K5222P        MSpC-1           P505                 0.0           2.9          0.4           0.8           1.2          0.1           0.0           0.0      105             48
                    33 MS      K5223P        MSPC-2           P515                 0.0           2.2          0.2           0.3           1.4          0.6           0.7           0.7        66            27
                    33 MS      K5224P        MSPC-3           P513                 0.0           3.0          0.4           0.6           1.1          0.3           0.2           0.2        68            29
                    34 MS      K5228P        MSBB-1           P506                 0.0         26.2           0.6         20.4          15.6           0.0           0.0           0.0      307           155
                    34 MS      K5229P        MSBB-2           P515                 0.0         29.5           0.2           6.1         10.4           0.0           0.0           0.0      313           158






                                                                              MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Data






                      SITE       RAW        DESIGNATOR FOLDER                    PC13#126     PC13 #153     PCB # 170     PC13 #180      PCB #187      PCB # 195      PC13 #206     PC13 #209     TOTAL TOTAL
                      AND        FILE            AND                                  (CL5)          (CL6)         (CL7)         (CL7)         (CL7)          (CL8)         (CL9)        (CLIO)     PCB'S     ISOMERS
                      STATE                     STATION                               (ppb)          (ppb)         (ppb)         (ppb)         (ppb)          (ppb)         (ppb)          (ppb)      (ppb)      (ppb)



                      34 MS      K5230P         MS1313-3          P513                  0.0          12.3           0.0            3.9           4.7           0.0            0.0           0.0       152             73
                      35MS       K5246P         MSPB- I           P506                  0.0           5,6           0.4            3.0           3.1           0.0            0.2           0.0       115             54
                      35 MS      K5247P         MSP13-2           P515                  0.0           8.4           0.0            1.4           1.8           0.0            0.2           0.0         78            34
                      35MS       K5248P         MSPB-3            P513                  0.0           4.0           0.2            0.8           2.3           0.3            0.6           0.2         72            31
                      36 AL      K5234P         MBCP-1            P506                  0.0          11.7           0.0            4.9           5.6           0.0            0.0           0.0       157             76
                      36 AL      K5235P         MBCP-2            P515                  0.0           4.5           0.0            2.2           3.8           0.0            0.0           0.0         91            41
                      36 AL      K5236P         MBCP-3            P513                  0.0           5.3           0.0            1.9           2.8           0.0            0.0           0.0         79            34
                      66 AL      K5240P         M13HI- I          P506                  0.0          19.1           0.7            3.7           6.7           0.0            0.4           0.0       241            120
                      66 AL      K5241P         M13HI-2           P515                  0.0          10.4           0.0            1.6           4.4           0.0            0.7           0.0       167             81
                      66 AL      K5242P         M13HI-3           P513                  0.0          11.9           0.0            1.6           3.4           0.0            0.3           0.0       146             70
                      67 FL      K5261P         PBPH-1            P517                  0.0          31.9           0.0            0.5           4.0           0.0            0.0           0.0       295            149
                      67 FL      K5262P         PBPH-2            P520                  0.0          48.7           0.0            2.3           8.5           0.0            0.0           0.0       471            242
                      67 FL      K5263P         PBPH-3            P523                  0.0          50.9           0.0            1.2           7.5           0.0            0.0           0.0       429            219
                      37 FL      K5255P         PBIB- 1           P517                  0.0          59.5           0.1            0.2           5.5           0.0            0.0           0.0       508            261
                      37 FL      K5256P         P13113-2          P520                  0.0          89.4           0.6            0.5         10.1            0.2            0.0           0.0       700            363
                      37 FL      K5257P         P13113-3          P529                  0.0          73.9           0.2            0.2           8.8           0.0            0.0           0.0       617            319
                      73FL       K5267P         CBJB-1            P517                  0.0           2.6           0.0            0.3           1.0           0.0            0.0           0.0         61            25
           0
           N)         73 FL      K5268P         CBJB-2            P520                  0.0           3.6           0.0            1.5           2.0           0.0            0.0           0.0         89            40
                      73 FL      K5269P         CBJB-3        P527(P523)                0.0           2.9           0.0            0.5           1.1           0.0            0.0           0.0         59            24
                      38 FL      K5273P         CBSR-I            P517                  0.0           0.6           0.0            0.0           0.8           0.0            0.0           0.0         22               5
                      38 FL      K5274P         CBSR-2            P520                  0.0           0.8           0.0            0.2           0.5           0.0            0.0           0.0         26               7
                      38 FL      K5275P         CBSR-3        P527(P523)                0.2           0.9           0.3            0.2           0.8           0.3            0.2           0.1         30               9
                      39 FL      K5279P         CBSP-1            P517                  0.0           6.7           0.0            0.3           3.1           0.0            0.0           0.0         61            25
                      39 FL      K5280P         CBSP-2            P529                  0.5           7.4           0.0            0.3           3.2           0.0            0.0           0.0         67            28
                      39 FL      K5281P         CBSP-3            P523                  0.0          12.7           1.0            1.3           6.8           0.2            0.0           0.3       104             48
                      74 FL      K5303P         PCLO-1            P529                  0.8           1.4           0.0            1.0           1.5           0.0            0.0           0.0         51            20
                      74 FL      K5303P         PCLO-1            P517                  0.0           1.7           0.0            0.3           0.6           0.0            0.0           0.0         33            10
                      74 FL      K5304P         PCLO-2            P520                  0.0          14.8           0.0            3.6           7.3           0.0            0.0           0.0       175             86
                      74 FL      K5305P         PCLO-3            P523                  0.0           9.4           0.0            1.1           2.7           0.0            0.0           0.0       110             51
                      40 FL      K5297P         SAWB-1            P517                  0.0          51.6           0.0            3.4         16.1            0.0            0.4           0.3       612            317
                      40 FL      K5298P         SAWB-2            P520                  0.0          92.0           0.0           10.1         35.7            0.0            0.0           0.6       1030           537
                      40 FL      K5299P         SAWB-3            P523                  0.0          71.0           0.0            4.5         26.0            0.0            0.0           0.0       844            439
                      41 FL      K5291P         APDB-1            P517                  0.0           2.1           0.0            0.1           2.0           0.0            0.0           0.0         37            12
                      41 FL      K5292P         APDB-2            P520                  0.0           2.6           0.0            0.9           3.1           0.0            0.0           0.0         52            20
                      41 FL      K5293P         APDB-3            P523                  0.0           1.5           0.0            0.7           0.9           0.0            0.0           0.0         37            12
                      42 FL      K5285P         APCP-1            P517                  0.0           0.7           0.0            0.5           0.7           0.0            0.0           0.0         29               8
                      42 FL      K5286P         APCP-2            P520                  0.0           1.5           0.0            1.2           1.3           0.0            0.0           0.0         50            19
                      42 FL      K5287P         APCP-3            P523                  0.0           0.9           0.0            0.9           1.3           0.0            0.0           0.0         39            13
                      75 FL      K5321P         AESP-1            P517                  0.0           0.0           0.0            0.0           0.3           0.0            0.0           0.0         19               3






                                                                            MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Data






                     SITE       RAW        DESIGNATOR FOLDER                   PCB# 126     PC13 #153      PC13 # 170    PCB #180      PC13 # 187    PC13 # 195    PC13 #206      PCB #209      TOTAL TOTAL
                     AND        FILE            AND                                  (CL5)         (CL6)         (CL7)         (CL7)         (CL7)          (CL8)         (CL9)        (CL10)     PCB'S    ISOMERS
                     STATE                     STATION                               (ppb)         (ppb)         (ppb)         (ppb)          (ppb)         (ppb)         (ppb)          (ppb)      (ppb)     (ppb)


                     75 FL      K5322P         AESP-2            P520                 0.0            0.0           0.0           0.5           0.5           0.0            0.0           0.0         34            11
                     75 FL      K5323P         AESP-3            P523                 0.1            0.1           0.0           0.3           0.2           0.0            0.0           0.0         25              6
                     43 FL      K5315P         CKBP-1            P517                 0.0            0.2           0.0           0.2           0.1           0.0            0.2           0.0         19              3
                     43 FL      K5316P         CKBP-2            P520                 0.2            0.0           0.0           0.3           0.6           0.0            0.2           0.0         32              9
                     43 FL      K5317P         CKBP-3            P523                 0.0            0.3           0.0           0.2           0.4           0.0            0.0           0.0         22              4
                     76 FL      K5351P         TBNP- 1           P518                 0.0          10.1            0.0           0.1           3.9           0.0            0.0           0.0         89            40
                     76 FL      K5352P         TBNP-2            P521                 0.0          18.0            0.0           2.4           7.9           0.0            0.0           0.0       150             72
                     76 FL      K5353P         TBNP-3            P524                 0.0          13.2            0.0           2.0           6.2           0.0            0.0           0.3       122             57
                     47 FL      K5333P         TBMK-1            P518                 0.0            0.2           0.0           0.0           0.3           0.0            0.0           0.0         23              5
                     47 FL      K5334P         TBMK-2            P521                 0.0            3.2           0.0           4.1           1.0           0.0            0.0           0.0         50            19
                     47 FL      K5335P         TBMK-3            P524                 0.0            1.6           0.0           2.5           1.2           0.0            0.0           0.0         40            14
                     44 FL      K5327P         TBPB-1            P518                 0.0            7.7           0.0           0.0           3.2           0.0            0.0           0.0         56            22
                     44 FL      K5328P         TBPB-2            P521                 0.0          12.0            0.0           2.1           8.3           0.0            0.0           0.0       105             48
                     44 FL      K5329P         TBPB-3            P524                 0.0            7.2           0.0           1.7           3.7           0.0            0.0           0.0         63            26
                     70 FL      K5339P         TBOT-1            P518                 0.0            1.5           0.0           0.5           1.0           0.0            0.0           0.0         52            20
                     70 FL      K5340P         TBOT-2            P521                 0.0            2.3           0.0           1.8           2.4           0.0            0.0           0.0         65            27
                     70 FL      K5341P         TBOT-3            P524                 0.0            1.7           0.0           1.0           1.1           0.0            0.0           0.0         49            19
                     77 FL      K5309P         T13KA-1           P518                 0.0          45.6            0.1           2.1           12.7          0.0            0.0           0.0       494           254
                     77 FL      K5310P         TBKA-2            P521                 0.0          38.6            0.2           6.0           14.5          0.0            0.0           0.0       411           210
                     77 FL      K5311P         TBKA-3            P524                 0.0          73.7            1.1           7.2          26.8           0.0            0.0           0.0       844           439
                     46 FL      K5345P         TBCB-1            P518                 0.0            0.0           0.0           0.0           0.0           0.0            0.0           0.0         31              9
                     46 FL      K5346P         TBCB-2            P521                 0.0            3.2           0.0           0.9           0.0           0.0            0.0           0.0         71            30
                     46 FL      K5347P         TBCB-3            P524                 0.0            1.4           0.0           0.9           0.0           0.0            0.0           0.0         44            16
                     48 FL      K5369P         C13131-1          P518                 0.0            0.9           0.0           0.0           0.3           0.0            0.0           0.0         32            10
                     48 FL      K5370P         C13131-2          P521                 0.0            1.4           0.0           1.1           0.7           0.0            0.0           0.0         38            13
                     48 FL      K5371P         CBBI-3            P525                 0.0            0.9           0.0           0.7           0.5           0.0            0.0           0.0         29              8
                     71 FI,     K5363P         CBFM-1            P518                 0.0            3.6           0.0           0.7           1.3           0.0            0.0           0.0         55            22
                     71 FL      K5364P         CBFM-2            P521                 0.0            5.5           0.0           2.6           3.8           0.0            0.0           0.0         72            31
                     71 FL      K5365P         CBFM-3            P524                 0.0            3.9           0.0           1.9           1.2           0.0            0.0           0.0         65            27
                     49 FL      K5357P         NBNB-1            P518                 0.0            2.1           0.0           0.2           0.6           0.0            0.0           0.0         55            22
                     49 FL      K5358P         NBNB-2            P521                 0.0            2.5           0.0           1.1           1.3           0.0            0.0           0.0         57            23
                     49 FL      K5359P         NBNB-3            P524                 0.0            2.3           0.0           1.2           1.1           0.0            0.0           0.0         62            26
                     50 FL      K5381P         RBHC-1            P518                 0.7            0.3           0.7           0.8           1.3           1.5            1.0           1.6         48            18
                     50 FL      K5382P         RBHC-2            P521                 0.0            0.9           0.0           0.4           0.3           0.0            0.0           0.0         25              6
                     50 FL      K5383P         RBHC-3            P524                 0.0            0.7           0.0           0.5           0.1           0.0            0.0           0.0         24              5
                     51 FL      K5375P         EVFU-1            P518                 0.0            0.0           0.0           0.0           0.0           0.0            0.0           0.0         15              1
                     51 FL      K5376P         EVFIJ-2           P521                 0.0            0.1           0.0           0.4           0.0           0.0            0.0           0.0         17              2
                     51 FL      K5377P         EVFU-3            P524                 0.0            0.3           0.0           0.7           0.0           0.0            0.0           0.0         21              4
                     81 FL      K5396P         BHKF-1            P527                 0.0            0.7           0.0           0.5           0.2           0.4            0.0           0.0         25              6






                                                                        MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Data






                     SITE      RAW       DESIGNATOR FOLDER                PC13#126 PCB#153 PCB#170 PCB#180 PCB#187 PCB#195                                PC13 #206 PCB #209          TOTAL    TOTAL
                     AND       FILE           AND                               (CL5)        (CL6)         (CL7)        (CL7)        (CL7)        (CL8)         (CL9)      (CLIO) PCB'S       ISOMERS
                    STATE                  STATION                              (ppb)        (ppb)         (ppb)        (ppb)        (ppb)        (ppb)         (ppb)        (ppb)      (ppb)   (ppb)


                    81 FL      K5397P       BHKF-2           P527                 0.0          0.8           0.0          0.5          0.3          0.5           0.0          0.0        25            6
                    81 FL      K5398P       BHKF-3           P527                 0.0          0.5           0.0          0.4          0.2          0.3           0.0          0.0        25            6




I
I
I
I
I
I
I
I
I
I          Pesticides and PCBs QA/QC Data
I
I
I
I
I
I
I
1
                       105
 I




I
I
I
I
I
I
I
I
I
I              Pesticides and PCBs Duplicates
I
I
I
I
I
I
I
1
                       106
I





                                                                 MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Duplicates




                    SITE     RAW       DESIGNATOR FOLDER               HC13 LINDANE          HEPTA-      ALDRIN        HEPTA          ALPHA-         TRANS- DIELDRIN MIREX 2,4'DDE
                    AND      FILE           AND                                               CHLOR                EPOYJDE CHLORDANE            NONACHLOR                             (0,P' DDE)
                    STATE                  STATION                     (ppb)         (ppb)      (ppb)       (ppb)                        (ppb)            (ppb)        (ppb)     (ppb)    (ppb)


                    08 TX    K5118P        SAMP-2          P507        0.00          0.57       0.00        0.00         0.29            0.67             0.66         1.03      0.00         0.00
                    08 TX    90745P        SAMP-2          P507        0.01          0.33       0.00        0.00         0.29            0.74             0.59         1.07      0.00         0.00

                    08 TX    K5119P        SAMP-3          P511        0.00          0.53       0.01        0.18         0.06            2.61             0.91         0.69      0.00         0.00
                    08 TX    Q0783P        SAMP-3          P511        0.00          0.72       0.00        0.20         0.06            2.19             0.88         0.87      0.00         0.00

                    15 TX    K5064P        GBYC-2          P508        0.00          4.00       0.00        0.00         2.81            9.19             5.48         11.70     0.00         0.53
                    15 TX    Q0748P        GBYC-2          P508        0.00          3.20       0.00        0.00         2.43            8.87             5.78         10.22     0.00         0.87

                    15 TX    K5065P        GBYC-3          P510        0.00          2.63       0.08        0.00         2.56            6.82             4.91         7.63      0.00         0.67
                    15 TX    Q0769P        GBYC-3          P510        0.00          2.58       0.05        0.00         2.77            7.03             5.00         8.37      0.00         0.90

                    17 TX    K5040P        GBHR-2          P506        0.00          0.69       0.35        0.00         0.51            1.38             1.13         2.12      0.12         0.00
                    17 TX    Q0742P        GBHR-2          P506        0.00          0.86       0.35        0.00         0.50            1.46             1.33         2.31      0.07         0.00

                    22 LA    K5159P        VBSP-1          P504        0.00          0.73       0.00        0.00         0.75            4.92             1.80         9.50      0.34         1.87
                    22 LA    Q0687P        VBSP- 1         P504        0.10          0.67       0.00        0.00         0.79            4.07             1.81         8.94      0.31         1.47
            4       281A     K5170P        BBSD-3          P525        0.00          0.47       0.18        0.18         0.30            1.69             1.04         2.34      0.07         0.68
                    28 LA    Q0786P        BBSD-3          P512        0.00          0.31       0.15        0.00         0.39            2.86             0.95         2.18      0.02         0.00

                    33 MS    K5222P        MSPC- 1         P505        0.00          1.15       0.79        0.00         2.95            10.21            3.88         5.99      1.64         0.55
                    33 MS    Q0739P        MSPC- 1         P505        0.00          1.36       0.99        0.00         3.79            9.89             5.46         7.31      1.63         0.67


                    66 AL    K5242P        M13HI-3         P513        0.00          2.01       0.21        0.00         0.82            6.07             6.02         6.40      0.00        65.42
                    66 AL    90789P        MBHI-3          P513        0.00          2.13       0.27        0.00         0.83            6.12             6.21         7.15      0.00        68.08

                    39 FL    91335P        CBSP-2          P529        0.00          0.57       0.19        0.27         0.30            3.81             5.58         5.90      0.07         3.20
                    39 FL    K5280P        CBSP-2          P529        0.01          0.57       0.19        0.34         0.28            3.10             5.16         5.60      0.06         2.97

                    81 FL    K5398P        BHKF-3          P527        0.04          0.34       0.00        0.00         0.00            0.77             0.14         1.17      0.00         2.70
                    81 FL    Q1217P        BHKF-3          P527        0.05          0.32       0.00        0.00         0.00            0.75             0.18         0.98      0.04         2.64





                                                                 MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Duplicates




                   SITE      RAW       DESIGNATOR FOLDER                4A'DDE       2,4'DDD      ENDRIN      4.4'DDD       2,4'DDT     4,4'DDT TOTAL           PC13 #8 PCB # 18     PC13 #28
                   AND       FILE           AND                       (P,P DDE)    (0,13 DDD)               (13,13' DDD) (07 DDT)       (P,P'DDT)    DDT`S         (CL2)       (CL3)    (CI,3)
                   STATE                   STATION                          (ppb)         (ppb)       (ppb)        (ppb)        (ppb)         (ppb)     (ppb)       (ppb)      (ppb)     (ppb)


                   08 TX     K5118P        SAMP-2          P507             9.92          0.00        0.14         0.72         0.08          0.43      11.15        110         0.0         0.1
                   08 TX     Q0745P        SAMP-2          P507             9.10          0.00        0.00         0.90         0.10          0.48      10.58        0.6         0.0         0.5

                   08 TX     K5119P        SAMP-3          P511             5.70          0.00        1.93         0.45         0.00          0.56      6.70         0.6         0.0         0.0
                   08 TX     g0783P        SAMP-3          P511             5.47          0.00        2.22         0.29         0.00          0.37      6.13         0.8         0.0         0.0

                   15 TX     K5064P        GBYC-2          P508             11.67         0.97        0.00         13.91        0.00          1.74      28.82        0.0         0.1         1.7
                   15 TX     Q0748P        GBYC-2          P508             11.18         0.99        0.00         14.18        0.00          1.40      28.62        0.0         0.1         119

                   15 TX     K5065P        GBYC-3          P510             11.29         1.55        0.00         13.35        0.85          0.87      28.58        0.0         0.2         2.7
                   15 TX     Q0769P        GBYC-3          P510             11.45         1.55        0.00         13.21        0.84          0.86      28.82        0.0         0.2         2.6

                   17 TX     K5040P        GBHR-2          P506             4.18          0.37        0.00         1.64         0.00          0.96      7.14         0.0         0.0         0.0
                   17 TX     Q0742P        GBHR-2          P506             4.97          0.39        0.00         1.80         0.00          0.36      7.51         0.0         0.0         0.0

                   22 LA     K5159P        VBSP- I         P504             25.12         0.42        3.30         10.67        0.66          0.00      38.74        0.0         0.0         0.0
                   22 LA     90687P        VBSP- 1         P504             24.77         0.61        3.45         10.71        0.47          0.34      38.37        0.0         0.1         0.0
          0
          00       28 LA     K5170P        BBSD-3          P525             3.34          0.04        0.70         1.47         0.03          0.42      5.97         0.0         0.2         0.2
                   28 LA     Q0786P        BBSD-3          P512             3.63          0.18        0.18         2.28         0.20          0.69      6.99         0.3         0.0         0.3

                   33 MS     K5222P        MSPC- I         P505             23.37         1.58        0.00         10.36        0.88          3.84      40.58        0.2         0.2         3.3
                   33 NIS    Q0739P        MSPC- 1         P505             23.09         1.66        0.00         10.45        0.70          3.67      40.23        0.3         0.3         2.8


                   66 AL     K5242P        MBHI-3          P513             77.83         10.60       1.70         31.58        4.51          1.72   191.66          0.0         0.8         1.4
                   66 AL     90789P        M13HI-3         P513             81.41         10.41       1.80         33.56        5.50          1.80   200.76          0.0         0.9         1.1

                   39 FL     g 1335P       CBSP-2          P529             71.34         5.01        0.10         62.01        0.39          7.30   149.25          0.0         0.0         0.2
                   39 FL     K5280P        CBSP-2          P529             67.03         4.63        0.15         58.23        0.37          6.96   140.18          0.0         0.0         0.2

                   81 FL     K5398P        BHKF-3          P527             0.18          0.00        0.52         0.26         0.00          0.00      3.14         0.0         0.2         0.3
                   81 FL     Q1217P        BHKF-3          P527             0.20          0.00        0.34         0.32         0.00          0.00      3.16         0.0         0.7         0.2





                                                                  MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Duplicates



                    SITE      RAW       DESIGNATOR FOLDER PC13#44 PCB#52 PC13#66 PCB#101                                PCB # 105     PCB# 110/77      PCB # 118 PC13 # 128 PC13 # 138 PCB# 126
                    AND       FILE           AND                            (CL4)        (CIA)     (CIA)          (CL5)      (CL5)           (CL5/4)         (CL5)         (CL6)         (CL6)    (CL5)
                    STATE                  STATION                          (ppb)        (ppb)      (ppb)         (ppb)      (ppb)               (ppb)        (ppb)        (ppb)         (ppb)    (ppb)


                    08 TX     K5118P       SAMP-2           P507             0.6         1.4         0.0          0.3          0.3               2.7          0.4           0.5          3.8          0.5
                    08 TX     Q0745P       SAMP-2           P507             0.5         1.6         0.2          0.4          0.3               2.7          0.8           0.6          3.7          0.2

                    08 TX     K5119P       SAMP-3           P511             0.2         0.4         0.4          1.3          0.1               0.5          0.0           0.1          5.9          0.0
                    08 TX     Q0783P       SAMP-3           P511             0.3         0.5         0.3          2.2          0.1               0.8          0.0           0.3          4.9          0.0

                    15 TX     K5064P       GBYC-2           P508             6.9         10.4        2.3          17.1         6.0               17.3         9.3           1.6          16.9         0.0
                    15 TX     Q0748P       GBYC-2           P508             5.9         10.6        2.7          15.5         5.6               16.8         8.8           1.6          15.2         0.0

                    15 TX     K5065P       GBYC-3           P5 10            6.5         13.0        2.3          13.5         3.8               14.6         9.0           1.3          11.6         0.0
                    15 TX     90769P       GBYC-3           P5 10            6.1         13.5        3.1          13.9         3.7               14.1         8.5           1.3          10.9         0.0

                    17 TX     K5040P       GBHR-2           P506             0.8         1.3         0.6          1.8          1.1               2.6          1.3           0.8          5.2          0.0
                    17 TX     Q0742P       GBHR-2           P506             0.9         1.2         0.6          1.9          1.0               2.5          1.3           0.8          5.9          0.0

                    22 LA     K5159P       VBSP- I          P504             0.8         0.6         0.5          1.7          0.8               5.9          1.5           ill          8.7          0.2
                    22 I-A    g068713      VBSP- I          P504             0.5         0.4         0.3          2.0          0.8               5.7          1.8           1.1          9.5          0.0
          0
                    28 LA     K5170P       BBSD-3           P525             0.5         0.6         0.1          0.6          0.1               3.1          0.6           0.2          2.7          0.3
                    28 LA     90786P       BBSD-3           P512             0.3         0.5         0.3          1.4          0.2               2.7          1.0           0.4          4.1          0.2

                    33 MS     K5222P       MSPC- I          P505             2.9         4.9         2.7          4.2          2.3               8.5          5.6           019          7.4          0.0
                    33 MS     Q0739P       mSPC- 1          P505             2.9         4.3         2.5          3.2          1.8               8.2          4.4           0.9          6.4          0.0


                    66 AL     K5242P       MBHI-3           P513             1.5         4.3         0.4          4.3        11.5                13.5         4.1           1.0          9.9          0.0
                    66 AL     90789P       MBHI-3           P513             1.5         4.6         0.8          4.5        12.8                12.5         4.9           0.9          10.9         0.0

                    39 FL     91335P       CBSP-2           P529             0.4         1.4         0.3          2.5          0.5               4.9          1.1           0.5          4.8          0.5
                    39 FL     K5280P       CBSP-2           P529             0.3         1.6         0.4          2.2          0.4               5.1          1.6           0.5          4.8          0.5

                    81 FL     K5398P       BHKF-3           P527             0.2         0.1         0.1          0.4          0.0               0.0          0.0           0.0          3.3          0.0
                    81 FL     Q 1217P      BHKF-3           P527             0.1         0.2         0.1          0.4          0.0               0.0          0.0           0.0          2.9          0.0





                                                                 MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Duplicates




                    SITE     RAW       DESIGNATOR FOLDER PCB#153 PCB#170 PCB#180 PCB#187 PCB#195 PCB#206 PCB#209                                                     TOTAL      TOTAL
                    AND      FILE           AND                             (CL6)        (CL7)        (CL7)         (CL7)        (CL8)        (CL9)       (CL10)      PCB'S    ISOMERS
                    STATE                  STATION                          (ppb)         (ppb)        (ppb)        (ppb)        (ppb)        (ppb)        (ppb)       (ppb)      (ppb)



                    08 TX    K5118P        SAMP-2          P507               0.7         0.0           0.9          1.1          0.0          0.0          0.0          41              14
                    08 TX    90745P        SAMP-2          P507               0.8         0.0           0.5          1.1          0.0          0.0          0.0          41              14

                    08 TX    K5119P        SAMP-3          P511               0.3         0.0           0.6          0.0          0.3          0.0          0.0          34              11
                    08 TX    Q0783P        SAMP-3          P511               0.3         0.0           0.9          0.0          0.3          0.0          0.0          36              12

                    15 TX    K5064P        GBYC-2          P508             16.3          0.0           2.6          5.1          0.0          0.0          0.1         229              114
                    15 TX    Q0748P        GBYC-2          P508             15.7          0.0           2.3          4.6          0.0          0.0          0.2         217              108

                    15 TX    K5065P        GBYC-3          P510             16.2          0.0           2.5          4.3          0.0          0.0          0.1         206              102
                    15 TX    Q0769P        GBYC-3          P510             17.9          0.0           2.8          4.6          0.0          0.0          0.1         209              103

                    17 TX    K5040P        GBHR-2          P506               4.7         0.2           0.8          2.3          0.0          0.0          0.0          58              24
                    17 TX    Q0742P        GBHR-2          P506               4.9         0.0           0.6          2.8          0.0          0.0          0.0          60              24


                    22 LA    K5159P        VBSP- 1         P504               6.1         0.0           0.5          4.1          0.0          0.0          0.2          76              33
                    22 LA    P0687P        VBSP-I          P504               5.9         0.0           0.4          4.2          0.0          0.0          0.1          76              33

                    28 LA    K5170P        BBSD-3          P525               1.2         0.0           0.2          0.8          0.1          0.0          0.0          36              11
                    28 LA    Q0786P        BBSD-3          P512               2.0         0.0           0.1          0.6          0.1          0.0          0.0          41              14


                    33 MS    K5222P        MSPC- I         P505               2.9         0.4           0.8          1.2          0.1          0.0          0.0         105              48
                    33 MS    Q0739P        MSPC- 1         P505               3.3         0.9           0.9          1.5          0.1          0.0          0.0          98              45



                    66 AL    K5242P        M13HI-3         P513             11.9          0.0           1.6          3.4          0.0          0.3          0.0         146              70
                    66 AL    Q0789P        MBHI-3          P513             12.7          0.0           1.5          3.6          0.0          0.3          0.0         153              74

                    39 FL    Q 1335P       CBSP-2          P529               7.6         0.0           0.3          3.5          0.0          0.0          0.0          67              28
                    39 FL    K5280P        CBSP-2          P529               7.4         0.0           0.3          3.2          0.0          0.0          0.0          67              28


                    81 FL    K5398P        BHKF-3          P527               0.5         0.0           0.4          0.2          0.3          0.0          0.0          25              6
                    81 FL    Q 1217P       BHKF-3          P527               0.3         0.0           0.4          0.2          0.3          0.0          0.0          25              6




I
I
I
I
I
I
I
I
I
I               Pesticides and PCBs Blanks
I
I
I
I
I
I
I
I
 I                     III






                                                                   MUSSEL WATCH YEAR V1 - Bivalve Pesticides and PCBs Blanks




                   RAW DESIGNATOR FOLDER                    HCB      LINDANE        HEPTA-       ALDRIN        HEPTA           ALPHA-          TRANS-     DIELDRIN        MIREX 2XDDE
                  FILE           AND                                                CHLOR                   EPOXIDE     CHLORDANE        NONACHLOR                                  (0,P'DDE)
                               STATION                      (ppb)        (ppb)         (ppb)        (ppb)                        (ppb)            (ppb)        (ppb)        (ppb)     (ppb)


                 90688P         BLANK          P504         0.00         0.00          0.00         0.00         0.00            0.03             0.03         0.00         0.09          0.00
                 90740P         BLANK          P505         0,00         0.00          0.00         0.00         0.00            0.11             0.00         0.00         0.00          2.05
                 90743P         BLANK          P506         0.00         0.00          0.00         0.00         0.00            0.00             0.00         0.00         0.00          0.61
                 90746P         BLANK          P507         0.02         0.00          0.00         0.29         0.00            0.00             0.00         0.00         0.00          0.00
                 Q0749P         BLANK          P508         0.00         0.00          0.00         0.00         0.00            0.00             0.00         0.00         0.00          0.57
                 90770P         BLANK          P510         0100         0.00          0.00         0.00         0.00            0.00             0.00         0.54         0.00          0.81
                 g0784P         BLANK          P511         0.00         0.00          0.00         0.00         0.00            0.00             0.00         0.00         0.00          0.00
                 90787P         BLANK          P512         0.00         0.00          0.00         0,00         0.00            0.00             0.00         0,00         0.00          0.00
                 Q0790P         BLANK          P513R        0.00         0.00          0.00         0.00         0.00            0.00             0.00         0.00         0100          0.11
                 Q1022P         BLANK          P514         0.02         0.15          0.04         0.00         0.00            0.00             0.00         0.00         0.00          0.00
                 Q1025P         BLANK          P515         0.00         0.15          0.00         0.00         0.00            0.00             0.00         0.00         0.00          0.00
                 91028P         BLANK          P516R        0.00         0.00          0.00         0.00         0.00            0.00             0.00         0.00         0.00          0.00
                 Q1040P         BLANK          P517         0.00         0.00          0.00         0.00         0.00            0.00             0.00         0.00         0.00          0.00
                 Q1043P         BLANK          P518         0.00         0.14          0.00         0.06         0.00            0.00             0.00         0.00         0.00          0.00
                 91054P         BLANK          P519         O.Do         0.00          0.13         0.16         0.12            0.47             0.35         0.26         0.10          0.06
                 Q 1054S        BLANK          P519R        0.02         0.24          0.22         0.09         0.13            0.64             0.51         0.38         0.15          0.11
                 Q1063P         BLANK          P520         0.02         0.18          0.12         0.00         0.09            0.00             0.17         0.16         0.00          0.00
                 Q1066P         BLANK          P521         0.00         0.00          0.00         0.00         0.00            0.30             0.22         0.00         0.15          0.00
                 Q1 109P        BLANK          P522         0.00         0.30          0.17         0.24         0.16            0.42             0.30         0.26         0.09          0.09
                 gilogs         BLANK          P522R        0.03         0.33          0.21         0.26         0.20            0.61             0.46         0.40         0.25          0.32
                 Q1115P         BLANK          P523         0.00         0.17          0.06         0.14         0.00            0.11             0.14         0.14         0.07          0.11
                 gi 118P        BLANK          P524         0.00         0.26          0.09         0.00         0.05            0.28             0.25         0.07         0.12          0.72
                 Q 1 184P       BLANK          P525         0.02         0.25          0.10         0.15         0.06            0.11             0.14         0.16         0.09          0.58
                 Q I 193P       BLANK          P526         0.02         0.39          0.12         0.00         0.14            0.70             0.30         0.00         0.09          0.00
                 Q1218P         BLANK          P527         0.01         0.07          0.00         0.00         0.00            0.00             0.00         0.00         0.01          0.00
                 Q1336P         BLANK          P529         0.01         0.32          0.02         0.00         0.00            0.00             0.07         0.00         0.00          0.00





                                                                    MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Blanks




                   RAW DESIGNATOR FOLDER 4,4* DDE                       2N DDD         ENDRIN      4X DDD       2,4@ DDrr      4.4'DDT         TOTAL       PCB #8      PCB # 18    PCB #28 PCB #44
                  FILE           AND                     (P,P' DDE)    (OX DDD)                  (P.1- DDD)     (O,P'DDT)     (P,P'DD-n        DDTS           (CL2)         (CL3)     (CL3)        (CIA)
                               STATION                     (ppb)             (ppb)        (ppb)         (ppb)        (ppb)         (ppb)         (ppb)        (ppb)         (ppb)     (ppb)        (ppb)


                  Q0688P        BLANK          P504             0.04         0.00         0.00          0.22         0.00          0.00          0.26          0.0           0.0          0.0           0.0
                  Q0740P        BLANK          P505             0.06         0.00         0.00          0.00         0.00          0.83          2.94          011           0.0          011           0.1
                  90743P        BLANK          P506             0.00         0.21         0.00          0.00         O.Co          0.00          0.83          0.0           0.1          0.0           0.3
                  90746P        BLANK          P507             0.00         0.00         0.00          0.00         0.00          0.00          0.00          0.0           0.0          0.0           0.1
                  90749P        BLANK          P508             0.00         0.00         0.00          0.00         0.00          0.00          0.57          0.0           0.0          0.0           0.0
                  Q0770P        BLANK          P510             0.06         0.00         0.00          0.00         0.00          0.00          0.87          0.0           0.0          0.0           0.0
                  90784P        BLANK          P511             0.00         0.00         0.00          0.00         0.00          0.00          0.00          0.0           0.0          0.0           0.0
                  Q0787P        BLANK          P512             0.00         0.00         0.00          0.00         0.00          0.00          0.00          0.0           0.0          0.0           0.0
                  90790P        BLANK          P513R            0.18         0.00         0.00          0.00         0.00          0.00          0.30          0.0           0.0          0.0           0.1
                  Q1022P        BLANK          P514             0.00         0.00         0.00          0100         0.00          0.00          0.00          0.0           0.0          0.0           0.0
                  Q1025P        BLANK          P515             0.00         0.00         0.00          0.00         0.00          0.00          0.00          0.0           0.0          0.0           0.0
                  Q1028P        BLANK          P516R            0.00         0.00         0.00          0.00         0.00          0.00          0.00          0.0           0.0          0.0           0.0
                  Q 1040P       BLANK          P517             0.00         0.00         0.00          0.00         0.00          0.00          0.00          0.0           0.0          0.0           0.0
                  Q1043P        BLANK          P518             0.00         0.05         0.00          0.00         0.00          0.00          0.05          0.0           0.0          0.0           0.0
                  91054P        BLANK          P519             0.40         0.10         0.00          0.20         0.11          0100          0.88          0.0           0.1          0.0           0.2
                  Q 1054S       BLANK          P519R            0.71         0.15         0.14          0.55         0.06          0.29          1.88          0.0           0.1          0.1           0.2
                  Q1063P        BLANK          P520             0.33         0.09         0.00          0.48         0.00          0.31          1.21          0.0           0.1          0.0           0.4
                  Q1066P        BLANK          P521             0.00         0.00         0.00          0.00         0.00          0.00          0.00          0.0           0.0          0.0           0.0
                  Qll()gp       BLANK          P522             0.25         0.10         0.00          0.15         0.00          0.00          0.58          0.0           0.1          0.0           0.2
                  Q1109S        BLANK          P522R            0.70         0.21         0.45          0.81         0.10          0.44          2.57          0.1           0.1          0.1           0.3
                  Q1115P        BLANK          P523             0.42         0.09         0.20          0.19         0.08          0.21          1.10          0.0           0.2          0.0           0.1
                  Q1118P        BLANK          P524             0.59         0.04         0.23          0.20         0.09          0.00          1.63          0.0           0.2          0.1           0.0
                  Q I 194P      BLANK          P525             0.27         0.10         0.41          0.27         0.07          0.12          1.40          0.0           0.2          0.1           0.2
                  Q 1 193P      BLANK          P526             0.81         0.14         0.28          0.79         0.16          0.00          1.90          0.0           0.2          0.2           0.4
                  Q1218P        BLANK          P527             0.05         0.00         0.29          0.00         0.00          0.00          0.05          0.0           0.0          0.0           0.0
                  Q1336P        BLANK          P529             0.45         0.00         0.32          0.66         0.00          0.00          1.11          010           0.0          0.1           0.5






                                                                     MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Blanks





                   RAW       DESIGNATOR FOLDER             PCB #52       PCB #66     PCB #101     PCB # 105     PCB#110/77      PCB # 118    PCB # 128     PCB # 138    PCB# 126     PCB # 153
                  FILE            AND                           (CIA)         (CIA)        (CL5)        (CL5)         (CL5/4)         (CL5)         (CL6)        (CL6)     (CL5)         (CLO
                               STATION                          (ppb)         (ppb)        (ppb)         (ppb)           (ppb)        (ppb)         (ppb)        (ppb)      (ppb)        (ppb)



                  Q0688P        BLANK          P504              0.0           0.0          0.0           0.0             0.0          0.0           0.0           2.2          0.2          0.0
                  90740P        BLANK          P505              0.1           0.1          0.2           0.3             0.0          0.1           0.0           0.7          0.1          0.2
                  90743P        BLANK          P506              0.9           0.0          0.4           0.0             0.5          0.2           0.1           1.6          0.0          0.5
                  90746P        BLANK          P507              0.1           0.0          0.3           0.1             0.0          0.2           0.0           0.9          0.0          0.1
                  90749P        BLANK          P508              0.0           010          0.0           0.0             0.0          0.0           0.0           2.5          0.0          0.0
                  90770P        BLANK          P510              0.0           0.0          0.0           0.0             0.0          0.0           0.0           0.0          0.1          0.0
                  90784P        BLANK          P511              0.0           0.0          0.0           0.0             0.0          0.0           0.0           3.7          0.0          0.0
                  Q0787P        BLANK          P512              0.0           0.0          0.0           0.0             0.0          0.1           0.0           0.0          0.0          0.0
                  90790P        BLANK          P513R             0.0           0.0          0.0           0.0             0.0          0.0           0.0           1.7          0.0          0.0
                  Q1022P        BLANK          P514              0.0           0.0          0.0           0.0             0.0          0.0           0.0           0.8          0.0          0.0
                  91025P        BLANK          P515              0.0           0.0          0.0           0.0             0.0          0.0           0.0           0.5          0.0          0.0
                  91028P        BLANK          P516R             0.0           0.0          0.0           0.0             0.0          0.0           0.0           0.4          0.0          0.0
                  Q1040P        BLANK          P517              0.0           0.0          0.0           0.0             0.0          0.0           0.0           0.7          0.0          0.0
                  Q1043P        BLANK          P518              0.0           0.0          0.0           0.0             0.0          0.0           0.0           0.3          0.0          0.0
                  Q1054P        BLANK          P519              011           0.0          0.3           0.0             0.6          0.2           0.2           0.6          0.0          0.4
                  91054S        BLANK          P519R             0.2           0.1          0.4           0.2             0.6          0.3           0.2           1.2          0.0          0.8
                  Q1063P        BLANK          P520              0.0           0.0          010           0.0             0.0          0.0           0.2           2.1          0.0          0.0
                  91066P        BLANK          P521              0.0           0.0          0.0           0.0             0.0          0.0           0.1           1.5          0.0          0.0
                  Q 1 109P      BLANK          P522              0.2           0.0          0.2           0.0             0.0          0.0           0.0           0.8          0.0          0.2
                  Q1109S        BLANK          P522R             013           0.3          0.3           0.5             0.6          0.3           0.3           1.8          0.5          0.7
                  Q1 115P       BLANK          P523              0.1           0.1          0.3           0.1             0.2          0.2           0.1           2.0          0.1          0.3
                  Q1118P        BLANK          P524              0.0           0.2          0.2           0.1             0.1          0.1           0.1           2.2          0.2          0.0
                  Q 1 184P      BLANK          P525              0.1           0.1          0.1           0.1             0.5          0.1           0.1           1.3          0.7          0.2
                  Q I 193P      BLANK          P526              0.3           0.1          0.5           0.4             2.6          0.3           0.1           2.1          0.0          0.7
                  Q 1218P       BLANK          P527              0.0           0.0          0.0           0.0             0.0          0.2           0.0           1.6          0.1          0.0
                  Q 1336P       BLANK          P529              0.0           0.0          0.0           0.0             0.0          0.0           0.0           0.7          0.5          0.0





                                                                     MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Blanks




                    RAW DESIGNATOR FOLDER                   PCB # 170     PCB # 180    PCB # 187    PCB #195      PCB #206      PCB #209     TOTAL TOTAL
                   FILE           AND                              (CL7)        (CL7)        (CL7)         (CLS)        (CL9)        (CLIO)   PCB'S ISOMERS
                                STATION                            (ppb)        (ppb)         (ppb)        (ppb)        (ppb)         (ppb)     (ppb)    (ppb)


                   Q0688P        BLANK          P504                0.0          0.0           0.0          0.0           0.0          0.0         19            3
                   90740P        BLANK          P505                0.0          0.2           0.0          0.1           0.0          0.0         18            2
                   Q0743P        BLANK          P506                0.1          0.6           0.2          0.1           0.0          0.0         24            6
                   Q0746P        BLANK          P507                0.0          0.2           0.1          0.0           0.0          0.0         18            2
                   Q0749P        BLANK          P508                0.0          0.0           0.0          0.0           0.0          0.0         18            2
                   90770P        BLANK          P510                0.0          0.0           0.0          0.0           0.0          0.0         14            0
                   Q0784P        BLANK          P511                0.0          0.0           0.0          0.4           0.0          0.0         22            4
                   Q0787P        BLANK          P512                0.0          0.0           0.0          0.1           0.0          0.0         14            0
                   Q0790P        BLANK          P513R               0.0          0.0           0.0          0.0           0.0          0.0         17            2
                   Q 1022P       BLANK          P514                0.0          0.0           0.0          0.0           0.0          0.0         15            1
                   Q1025P        BLANK          P515                0.0          0.0           0.0          0.0           0.0          0.0         15            0
                   Q1028P        BLANK          P516R               0.0          0.0           0.1          0.0           0.0          0.0         15            1
                   Q1040P        BLANK          P517                0.0          0.0           0.0          0.0           0.0          0.0         15            1
                   Q1043P        BLANK          P518                0.0          0.0           0.0          0.0           0.0          0.0         14            0
                   Q 1054P       BLANK          P519                0.0          0.3           0.2          0.0           0.0          0.0         20            3
                   Q 1054S       BLANK          P519R               0.2          0.3           0.4          0.2           0.2          0.3         25            6
                   Q1063P        BLANK          P520                0.0          0.3           0.2          0.4           0.4          0.3         22            4
                   Q1066P        BLANK          P521                0.0          0.3           0.3          0.4           0.0          0.0         19            3
           L"      Q1109P        BLANK          P522                0.0          0.0           0.2          0.0           0.0          0.0         18            2
                   Q1109S        BLANK          P522R               0.4          0.4           0.4          0.4           0.3          0.4         30            9
                   Q1115P        BLANK          P523                0.1          0.1           0.2          0.2           0.1          0.2         23            5
                   Q1118P        BLANK          P524                0.3          0.3           0.2          0.4           0.2          0.2         23            5
                   Q1 184P       BLANK          P525                0.3          0.2           0.2          0.3           0.2          0.2         23            5
                   Q1193P        BLANK          P526                0.0          0.5           0.2          0.3           0.2          0.3         32            9
                   Q1218P        BLANK          P527                0.0          0.0           0.0          0.1           0.1          0.1         18            2
                   Q 1336P       BLANK          P529                0.0          0.0           0.0          0.0           0.0          0.0         17            2




I
I
I
I
I
I
I
I
I
I                Pesticide and PCB Spikes
I
I
I
I
I
I
I
1
                       116
J, -





                                                             MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Spikes





                    FILE               DESCRIPTION           DRY WT HCB LINDANE HEPTA- ALDRIN FIEPTA                          ALPFIA-      TRANS- DIELDRIN ENDRIN MIREX
                                                              (grams)                      CHLOR               EPO)GDE CHLORDANE NONACHLOR


              SPIKED SAMPLES ES 08 TX SAMP-2            P507
                AMOUNT SPIKED (ug)                                     0.0409     0.0454     0.0421   0.0469      0.0462        0.0441         0.0443    0.0431     0.0421   0.0421

              Q0745P                   ORIG SAMPLE               3.38
              Q0747P                     SPK SAMP                3.38  0.0000     0.0003     0.0000   0.0000      0.0003        0.0007         0.0006    0.0011     0.0000   0.0000
              RECOVERED SPIKE (ug)                                     0.0125     0.0117     0.0124   0.0120      0.0126        0.0123         0.0121    0.0126     0.0114   0.0118
              % RECOVERY                                                  0.04       0.04      0.04      0.04        0.04         0.04           0.04       0.04      0.04      0.04
                                                                            104        85         99       86          90           89             88         91         92        95
              SPIKED SAMPLES ES 08 TX SAMP-3 P511
                AMOUNT SPIKED (ug)                                     0.0409     0.0454     0.0421   0.0469      0.0462        0.0441         0.0443    0,0431     0.0421   0.0421

              Q0783P                   ORIG SAMPLE               3.59  0.0000     0.0007     0.0000   0.0002      0.0001        0.0022         0.0009    0.0009     0.0022   0.0000
              Q0785P                     SPK SAMP                3.58  0.0049     0.0120     0.0114   0.0112      0.0120        0.0130         0.0105    0.0113     0.0146   0.0124
              RECOVERED SPIKE (ug)                                        0.02       0.04      0.04      0.04        0.04         0.04           0.03       0.04      0.04      0.04
              % RECOVERY                                                    43         89         97       84          93           87             78         86       105       105


              SPIKED SAMPLES T-S 16TX GBTD-1 P516R
                AMOUNT SPIKED (ug)                                     0.0409     0.0454     0.0421   0.0469      0.0462        0.0441         0.0443    0.0431     0.0421   0.0421

              K5057P                   ORIG SAMPLE               3.21  0.0000     0.0017     0.0002   0.0000      0.0011        0.0026         0,0027    0.0038     0.0000   0.0000
              Q1027P                     SPK SAMP                3.22  0.0053     0.0166     0.0133   0.0153      0.0145        0.0153         0.0155    0.0171     0.0134   0.0139
              RECOVERED SPIKE (ug)                                        0.02       0.05      0.04      0.05        0.04         0.04           0.04       0.04      0.04      0.04
              % RECOVERY                                                    42         105       101       105         93           93             93         100      102       107


              SPIKED SAMPLES ES 15 TX GBYC-2 P508
                AMOUNT SPIKED (ug)                                     0.0409     0.0454     0.0421   0.0469      0.0462        0.0441         0.0443    0.0431     0.0421   0.0421

              Q0748                    ORIG SAMPLE               2.72  0.0000     0.0028     0.0000   0.0000      0.0024        0.0089         0.0058.   0.0102     0.0000   0.0000
              Q0750                      SPK SAMP                2.72  0.0058     0.0190     0.0157   0.0141      0.0185        0.0227         0.0194    0.0240     0.0200   0.0156
              RECOVERED SPIKE (ug)                                        0.02       0.04      0.04      0.04        0.04         0.04           0.04       0.04      0.05      0.04
              % RECOVERY                                                    39         97        101       82          94           85             84         87       129       101


              SPIKED SAMPLES ES 15 TX GBYC-3 P5 10
                AMOUNT SPIKED (ug)                                     0.0409     0.0454     0.0421   0.0469      0.0462        0.0441         0.0443    0.0431     0.0421   0.0421

              Q0769P                   ORIG SAMPLE               3.02  0.0000     0.0026     0.0000   0.0000      0.0028        0.0070         0.0050    0.0084     0.0000   0.0000
              Q0771P                     SPK SAMP                3.03  0.0048     0.0156     0.0128   0.0130      0.0171        0.0202         0.0183    0.0200     0.0140   0.0161
              RECOVERED SPIKE (ug)                                        0.01       0.04      0.04      0.04        0.04         0.04           0.04       0.04      0.04      0.05
              % RECOVERY                                                    35         87         92       84          94           90             91         82       101       116





                                                                MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Spikes





                    FILE                 DESCRIPTION            DRY Wr HCB LINDANE HEPTA- ALDRIN HEPTA                             ALPHA-        TRANS- DIELDRIN ENDRIN MIREX
                                                                (grams)                        CHLOR                EPO)GDE    CHLORDANE, NONACHLOR




              SPIKED SAMPLES ES 17 TX GBHR- I P514
                AMOUNT SPIKED (ug)                                        0.0409      0.0454     0.0421    0.0469      0.0462        0.0441          0.0443     0.0431     0.0421    0.0421

              K5039P                     ORIG SAMPLE                3.09  0.0000      0.0011     0.0009    0.0000      0.0003        0.0008          0.0011     0.0021     0.0000    0.0000
              Q1021P                      SPK SAMP                  3.09  0.0141      0.0184     0.0161    0.0166      0.0178        0.0124          0.0157     0.0180     0.0164    0.0156
              RECOVERED SPIKE (ug)                                           0.04       0.05       0.05      0.05         0.05          0.04            0.05      0.05       0.05      0.05
              % RECOVERY                                                       106        118        112       109          117           82             102        114         120      114


              SPIKED SAMPLES ES 17 TX GBHR-2 P506
                AMOUNT SPIKED (ug)                                        0.0409      0.0454     0.0421    0.0469      0.0462        0.0441          0.0443     0,0431     0.0421    0.0421

              gO742                      ORIG SAMPLE                3.27  0.0000      0.0009     0.0004    0.0000      0.0005        0.0015          0.0014     0.0023     0.0000    0.0001
              gO744                       SPK SAMP                  3.30  0.0099      0.0099     0.0109    0.0116      0.0139        0.0130          0.0133     0.0146     0.0221    0.0124
              RECOVERED SPIKE (ug)                                           0.03       0.03       0.03      0.04         0.04          0.04            0.04      0.04       0.07      0.04
              % RECOVERY                                                        80         66         83        81          96            86              89         94          M        97


              SPIKED SAMPLES ES 22 LA VBSP- 1 P504
         Go     AMOUNT SPIKED (ug)                                        0.0409      0.0454     0.0421    0.0469      0.0462        0.0441          0.0443     0.0431     0.0421    0.0421

              90687P                     ORIG SAMPLE                2.74  0.0001      0.0007     0.0000    0.0000      0.0008        0.0041          0.0018     0.0089     0.0035    0.0003
              Q0689P                      SPK SAMP                  2.70  0.0082      0.0121     0.0136    0.0151      0.0158        0.0175          0.0156     0.0178     0.0277    0.0164
              RECOVERED SPIKE (ug)                                           0.02       0.03       0.04      0.04         0.04          0.04            0.04      0.02       0.07      0.04
              % RECOVERY                                                        54         68         87        87          88            82              84          M          M       103


              SPIKED SAMPLES ES 28 LA BBSD-3 P525
                AMOUNT SPIKED (ug)                                        0.0409      0.0454     0.0421    0.0469      0.0462        0.0441          0.0443     0.0431     0.0421    0.0421

              K5170P                     ORIG SAMPLE                2.85  0.0000      0.0005     0.0002    0.0002      0.0003        0.0017          0.0010     0.0023     0.0007    0.0001
              Q 1 183P                    SPK SAMP                  2.80  0.0090      0.0232     0.0231    0.0228      0.0254        0.0219          0.0243     0.0260     0.0334    0.0295
              RECOVERED SPIKE NO                                             0.03       0.06       0.06      0.06         0.07          0.06            0.07      0.07       0.09      0.08
              % RECOVERY DIVIDED BY 2                                           31         70         76        68          76            64               73         77        109       98


              SPIKED SAMPLES ES 31 LA BSSI-2 P515
                AMOUNT SPIKED (ug)                                        0.0409      0.0454     0.0421    0.0469      0.0462        0.0441          0.0443     0.0431     0.0421    0.0421

              K5217P                     ORIG SAMPLE                2.33  0.0000      0.0010     0.0001    0.0004      0.0023        0,0052          0.0044     0.0134     0.0018    0, 0001
              Q1024P                      SPK SAMP                  2.30  0.0119      0.0215     0.0197    0.0231      0.0276        0.0256          0.0248     0.0315     0.0245    0.0229
              RECOVERED SPIKE (ug)                                           0.03       0.05       0.04      0.05         0.06          0.05            0.05      0.04       0.05      0.05





                                                                MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Spikes





                     FILE                DESCRIPTION            DRY Wr HCB LINDANE HEPTA- ALDRIN HEPTA,                             ALPHA-        TRANS- DIELDRIN ENDRIN MIREX
                                                                  (grams)                       CHLOR                 EPOXIDE   CHLORDANE NONACHLOR



              % RECOVERY                                                       67          104        107       112          126           107             106        97         124      125


              SPIKED SAMPLES ES 33 MS MSPC- 1 P505
                AMOUNT SPIKED (ug)                                         0.0409     0.0454      0.0421    0.0469      0.0462        0.0441          0.0443     0.0431     0.0421    0.0421

              Q0739P                     ORIG SAMPLE                 2.12  0.0000     0.0014      0.0010    0.0000      0.0038        0.0099          0.0055     0.0073     0.0000    0.0016
              Q0741P                       SPK SAMP                  2.16  0.0081     0.0150      0.0184    0.0171      0.0190        0.0269          0.0254     0.0246     0.0260    0.0218
              RECOVERED SPIKE (ug)                                           0.02        0.03       0.04      0.04         0.03          0.04           0.04        0.04       0.06      0.04
              % RECOVERY                                                       43          65          89        79          71            83              97         86           M      103


              SPIKED SAMPLES ES 66 AL MBHI-3 P513R
                AMOUNT SPIKED (ug)                                         0.0409     0.0454      0.0421    0.0469      0.0462        0.0441          0.0443     0.0431     0.0421    0.0421

              K5242P                     ORIG SAMPLE                 1.39  0.0000     0.0024      0.0002    0.0000      0.0008        0.0073          0.0073     0.0077     0.0017    0.0000
              Q0791P                       SPK SAMP                  1.33  0.0146     0.0303      0.0284    0.0307      0.0307        0.0397          0.0387     0.0398     0.0268    0.0304
              RECOVERED SPIKE (ug)                                           0.02        0.04       0.04      0.04         0.04          0.04           0.04        0.04       0.03      0.04
              % RECOVERY                                                       47          82          89        87          86            98              94         99          79        96


              SPIKEDSAMPLES ES 37FL P13113-1 P517
                AMOUNT SPIKED (ug)                                         0.0409     0.0454      0.0421    0.0469      0.0462        0.0441          0.0443     0.0431     0.0421    0.0421

              K5255P                     ORIG SAMPLE                 3.72  0.0000     0.0009      0.0001    0.0000      0.0009        0.0010          0.0020     0.0041     0.0001    0.0000
              Q 1039P                      SPK SAMP                  3.72  0.0070     0.0115      0.0119    0.0126      0.0142        0.0113          0.0135     0.0163     0.0123    0.0122
              RECOVERED SPIKE (ug)                                           0.03        0.04       0.04      0.05         0.05          0.04           0.04        0.05       0.05      0.05
              % RECOVERY                                                       64          87         104       100          107           87              97         105        107      107


              SPIKED SAMPLES ES 39 FL CBSP-2 P529
                AMOUNT SPIKED (ug)                                         0.0409     0,0454      0.0421    0.0469      0.0462        0.0441          0.0443     0.0431     0.0421    0.0421

              K5280P                     ORIG SAMPLE                 2.27  0.0000     0.0006      0.0002    0.0003      0.0003        0.0031          0.0052     0.0056     0.0002    0.0001
              Q 1337P                      SPK SAMP                  2.24  0.0067     0.0173      0.0165    0.0179      0.0155        0.0179          0.0219     0.0207     0.0197    0.0191
              RECOVERED SPIKE NO                                             0.01        0.04       0.04      0.04         0.03          0.03           0.04        0.03       0.04      0.04
              % RECOVERY                                                       37          83          87        84          74            75              85         79         104      101


              SPIKED SAMPLES ES 40 FL SAWB-2 P520
                AMOUNT SPIKED NO                                           0.0409     0.0454      0.0421    0.0469      0.0462        0.0441          0.0443     0.0431     0.0421    0.0421

              K5298P                     ORIG SAMPLE                 1.65  0.0000     0.0017      0.0008    0.0004      0.0037        0.0305          0.0244     0.0119     0.0000    0.0004
              Q 1062P                      SPK SAMP                  1.61  0.0153     0.0312      0.0308    0.0297      0.0394        0.0552          0.0498     0.0419     0.0436    0.0561





                                                               MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Spikes





                     FILE               DESCRIPTION            DRY Wr HCB LINDANE HEPTA- ALDRIN HEPTA                             ALPHA-        TRANS- DIELDRIN ENDRIN MIREX
                                                                (grams)                       CHLOR                 EPOXIDE   CHLORDANE NONACHLOR


              RECOVERED SPIKE (ug)                                          0.02        0.05       0.05     0.05         0.06          0.04           0.04       0.05       0.07       0.09
              % RECOVERY                                                      60          105        115      101          125           90              92        112        56         71


              SPIKED SAMPLES ES 47 FL TBMK- 1 P518
                AMOUNT SPIKED (ug)                                        0.0409     0.0454     0.0421    0.0469      0.0462        0.0441          0.0443     0.0431     0.0421   0.0421

              K5333P                    ORIG SAMPLE                 3.23  0.0000     0.0004     0.0002    0.0000      0.0004        0.0022          0.0036     0.0015     0.0000   0.0004
              Q1042P                      SPKSAMP                   3.07  0.0125     0.0163     0.0157    0.0157      0.0181        0.0168          0.0181     0.0154     0,0131   0.0144
              RECOVERED SPIKE (ug)                                          0.04        0.05       0.05     0.05         0.05          0.04           0.04       0.04       0.04       0.04
              % RECOVERY                                                      94          108        113      103          118           102            100         99        96        102


              SPIKED SAMPLES ES 46 FL TBCB-2 P521
                AMOUNT SPIKED (ug)                                        0.0409     0.0454     0.0421    0.0469      0.0462        0.0441          0.0443     0.0431     0.0421   0.0421

              K5346P                    ORIG SAMPLE                 1.58  0.0000     0.0012     0.0004    0.0002      0.0003        0.0235          0.0471     0.0016     0.0022   0.0175
              Q1065P                      SPK SAMP                  1.62  0.0154     0.0432     0.0423    0.0389      0.0451        0.0608          0.0885     0.0455     0.0481   0.0789
              RECOVERED SPIKE (ug)                                          0.02        0.07       0.07     0.06         0.07          0.06           0.07       0.07       0.07       0.10
              % RECOVERY DIVIDED BY 2                                         31           75         81       67           78           69              76         82        88        118


              SPIKED SAMPLES ES 46 FL TBCB-3 P524
                AMOUNT SPIKED (ug)                                        0.0409     0.0454     0.0421    0.0469      0.0462        0.0441          0.0443     0.0431     0.0421   0.0421


              K5347P                    ORIG SAMPLE                 2.47  0.0000     0.0006     0.0002    0.0005      0.0003        0.0147          0.0262     0.0010     0.0019   0.0083
              Q1117P                      SPK SAMP                  2.48  0.0090     0.0253     0.0266    0.0260      0.0278        0.0400          0.0515     0.0261     0.0270   0.0420
              RECOVERED SPIKE (ug)                                          0.02        0.06       0.07     0.06         0.07          0.06           0.06       0.06       0.06       0.08
              % RECOVERY DIVIDED BY 2                                         27           67         78       68           74           71              71         72        74         99





                                                                MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Spikes





                     FILE                DESCRIPTION             2.4'DDE    4,4'DDE 2.4! DDD 4,4'DDD 2.4'DDT 4,4'DDT AVG. % PCB
                                                               (O.P' DDE)   (P.P'DDE)  (O,P'DDD) (P.P'DDD) (O,P'DDT)       (P,P' DDT)   RECOVERY



               SPIKED SAMPLES ES 08 TX SAMP-2             P507
                 AMOUNT SPIKED (ug)                                0.0449      0.0423      0.0427     0.0434      0.0435      0.0463        0.0423

               Q0745P                    ORIG SAMPLE
               Q0747P                      SPK SAMP                0.0000      0.0091      0.0000     0.0009      0.0001      0.0005        0.0000
               RECOVERED SPIKE (ug)                                0.0094      0.0207      0.0127     0.0140      0.0115      0.0142        0.0137
               % RECOVERY                                            0.03        0.04        0.04        0.04        0.04        0.05          0.04
                                                                        70          93         100         102         89          100           104
               SPIKED SAMPLES ES 08 TX SAMP-3 P511
                 AMOUNT SPIKED (ug)                                0.0449      0.0423      0.0427     0.0434      0.0435      0.0463        0.0423

               Q0783P                    ORIG SAMPLE               0.0000      0.0075      0.0000     0.0003      0.0000      0.0005        0.0004
               Q0785P                      SPK SAMP                0.0130      0.0200      0.0127     0.0103      0.0106      0.0134        0.0118
               RECOVERED SPIKE (ug)                                  0.05        0.04        0.05        0.04        0.04        0.05          0.04
               % RECOVERY                                              104         105         107         83          87          100            97


               SPIKED SAMPLES 3,S 16TX GBTD-1 P516r,
          N)     AMOUNT SPIKED (ug)                                0.0449      0.0423      0.0427     0.0434      0.0435      0.0463        0.0423

               K5057P                    ORIG SAMPLE               0.0003      0.0094      0.0009     0.0061      0.0000      0.0000        0.0025
               Q1027P                      SPK SAMP                0.0135      0.0223      0.0141     0.0189      0.0132      0.0128        0.0155
               RECOVERED SPIKE (ug)                                  0.04        0.04        0.04        0.04        0.04        0.04          0.04
               % RECOVERY                                               94          99          99         95          97           89            99


               SPIKED SAMPLES ES 15 TX GBYC-2 P508
                 AMOUNT SPIKED (ug)                                0.0449      0.0423      0.0427     0.0434      0,0435      0.0463        0.0423

               Q0748                     ORIG SAMPLE               0.0009      0.0112      0.0010     0.0142      0.0000      0.0014        0.0000
               Q0750                       SPK SAMP                0.0112      0.0258      0.0160     0.0272      0.0125      0.0170        0.0191
               RECOVERED SPIKE (ug)                                  0.03        0.04        0.04        0.04        0.03        0.04          0.04
               % RECOVERY                                               63          94          96         82          78           91            94


               SPIKED SAMPLES ES 15 TX GBYC-3 P510
                 AMOUNT SPIKED (ug)                                0.0449      0.0423      0.0427     0.0434      0.0435      .0.0463       0.0423

               Q0769P                    ORIG SAMPLE               0.0009      0.0115      0.0016     0.0132      0.0008      0.0009        0.0053
               Q0771P                      SPK SAMP                0.0132      0.0257      0.0159     0.0272      0.0138      0.0143        0.0200
               RECOVERED SPIKE (ug)                                  0.04        0.04        0.04.       0.04        0.04        0.04          0.04
               % RECOVERY                                               83         102         102         98          90           88           105





                                                                MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Spikes





                     FILE                DESCRIPTION            2,4'DDE 4.4'DDE 2.4'DDD 4,4'DDD 2,4'DDT 4,4'DDT AVG. % PC13
                                                               (O,P' DDE)   (P.P'DDE)  (O,P'DDD) (P,P'DDD) (07 DDT)         (P,P'DErr)  RECOVERY




               SPIKED SAMPLES ES 17 TX GBHR- 1 P514
                 AMOUNT SPIKED (ug)                                0.0449      0.0423      0.0427     0.0434      0.0435      0.0463        0.0423

               K5039P                    ORIG SAMPLE               0.0000      0.0056      0.0001     0.0013      0.0003      0.0005        0.0005
               Q1021P                      SPHSAMP                 0.0080      0.0184      0.0158     0.0132      0.0101      0.0151        0.0147
               RECOVERED SPIKE (ug)                                  0.02        0.04        0.05        0.04        0.03        0.05          0.04
               % RECOVERY                                               55          93         113         85          70          98           103


               SPIKED SAMPLES ES 17 TX GBHR-2 P506
                 AMOUNT SPIKED (ug)                                0.0449      0.0423      0.0427     0.0434      0.0435      0.0463        0.0423

               Q0742                     ORIG SAMPLE               0.0000      0.0053      0.0004     0.0019      0.0000      0.0004        0.0000
               Q0744                       SPK SAMP                0.0067      0.0162      0.0130     0.0138      0.0097      0.0128        0.0130
               RECOVERED SPIKE (ug)                                  0.02        0.04        0.04        0.04        0.03        0.04          0.04
               % RECOVERY                                               49          85          98         90          74          89             92


               SPIKED SAMPLES ES 22 LA VBSP- I P504
                 AMOUNT SPIKED (ug)                                0.0449      0.0423      0.0427     0.0434      0.0435      0.0463        0.0423

               Q0687P                    ORIG SAMPLE               0.0015      0.0248      0.0006     0.0107      0.0005      0.0003        0.0009
               Q0689P                      SPK SAMP                0.0066      0.0320      0.0175     0.0216      0.0132      0.0143        0.0172
               RECOVERED SPIKE (ug)                                  0.01        0.02        0.05        0.03        0.03        0.04          0.04
               % RECOVERY                                               M           M          107         68          79          81           103


               SPIKED SAMPLES ES 28 LA BBSD-3 P525
                 AMOUNT SPIKED (ug)                                0.0449      0.0423      0.0427     0.0434      0.0435      0.0463        0.0423

               K5170P                    ORIG SAMPLE               0.0007      0.0033      0.0000     0.0015      0.0000      0.0004        0.0006
               Q I 183P                    SPK SAMP                0.0208      0.0273      0.0253     0.0256      0.0200      0.0280        0.0279
               RECOVERED SPIKE (ug)                                  0.06        0.07        0.07        0.07        0.06        0.08          0.08
               % RECOVERY DIVIDED BY 2                                  63          79          83         78          64          84             91


               SPIKED SAMPLES ES 31 LA BSSI-2 P515
                 AMOUNT SPIKED (ug)                                0.0449      0.0423      0.0427     0.0434      0.0435      0.0463        0.0423

               K5217P                    ORIG SAMPLE               0.0002      0.0205      0.0010     0.0137      0.0004      0.0028        0.0022
               Q 1024P                     SPK SAMP                0.0194      0.0349      0.0241     0.0299      0.0196      0.0225        0.0228
               RECOVERED SPIKE (ug)                                  0.04        0.03        0.05        0.04        0.04        0.05          0.05





                                                             MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Spikes





                    FILE               DESCRIPTION           2.4'DDE 4.4'DDE 2,4'DDD 4,4'DDD 2XDDT 4.4'DDT AVG. % PC13
                                                             (O,P'DDE)   (P.P'DDE) (O,P'DDD) (P,P'DDD) (O,P'DDT)      (P,P'DEM   RECOVERY



              % RECOVERY                                             99        78          124       86          101        98            112


              SPIKED SAMPLES ES 33MS MSPC-1 P505
                AMOUNT SPIKED (ug)                              0.0449     0.0423     0.0427     0.0434     0.0435      0.0463       0.0423

              90739P                   ORIG SAMPLE              0.0007     0.0231     0.0017     0.0104     0.0007      0.0037       0.0017
              Q0741P                     SPK SAMP               0.0167     0.0382     0.0208     0.0257     0.0201      0.0221       0.0212
              RECOVERED SPIKE (ug)                                0.03       0.03        0.04      0.03        0.04       0.04         0.04
              % RECOVERY                                             77        77          97        76           96        86          100,


              SPIKED SAMPLES ES 66 AL M13HI-3 P513R
                AMOUNT SPIKED (ug)                              0.0449     0.0423     0.0427     0.0434     0.0435      0.0463       0.0423

              K5242P                   ORIG SAMPLE              0.0654     0.0778     0.0106     0.0382     0.0055      0.0021       0.0035
              90791P                     SPK SAMP               0.0947     0.1047     0.0412     0.0644     0.0383      0.0327       0.0337
              RECOVERED SPIKE (ug)                                0.04       0.04        0.04      0.03        0.04       0.04         0.04
              % RECOVERY                                             87        85          95        80          100        88            95
         ND
         C4   SPIKEDSAMPLES ES 37FL PBIB-1 P517
                AMOUNT SPIKED (ug)                              0.0449     0.0423     0.0427     0.0434     0.0435      0.0463       0.0423

              K5255P                   ORIG SAMPLE              0.0079     0.0205     0.0016     0.0026     0.0004      0.0005       0.0147
              Q1039P                     SPK SAMP               0.0115     0.0316     0.0132     0.0133     0.0106      0.0137       0.0260
              RECOVERED SPIKE (ug)                                0.01       0.04        0.04      0.04        0.04       0.05         0.04
              % RECOVERY                                             M         97         101        92           87        107           99


              SPIKED SAMPLES ES 39 FL CBSP-2 P529
                AMOUNT SPIKED (ug)                              0.0449     0.0423     0.0427     0.0434     0.0435      0.0463       0.0423


              K5280P                   ORIG SAMPLE              0.0030     0.0670     0.0046     0.0582     0.0004      0.0070       0.0013
              Q1337P                     SPKSAMP                0.0177     0.0901     0.0231     0.0806     0.0130      0.0265       0.0186
              RECOVERED SPIKE NO                                  0.03       0.05        0.04      0.05        0.03       0.04         0.04
              % RECOVERY                                             74        122         97        116          65        95            92


              SPIKED SAMPLES ES 40 FL SAWB-2 P520
                AMOUNT SPIKED (ug)                              0.0449     0.0423     0.0427     0.0434     0.0435      0.0463       0.0423


              K5298P                   ORIG SAMPLE              0.0025     0.1297     0.0104     0.0677     0.0067      0.0283       0.0229
              Q1062P                     SPK SAMP               0.0347     0.1350     0.0464     0.0898     0.0386      0.0628       0.0619





                                                             MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs Spikes




                    FILE                DESCRIPTION          2,4'DDE 4,4'DDE 2ADDD 4.4'DDD 2,4'DDT 4,4'DDT AVG. % PCB
                                                              (O,P'DDE)  (P,P'DDE) (O.P'DDD) (P,P'DDD) (O,P' DDT)     (P,P'DDT)   RECOVERY


              RECOVERED SPIKE (ug)                                  0.05       0.01       0.06       0.04        0.05        0.06         0.06
              % RECOVERY                                             115         M           m          82        118         120            M

              SPIKED SAMPLES ES 47 FL TBMK- I P5 18
                AMOUNT SPIKED (ug)                               0.0449     0.0423      0.0427     0.0434     0.0435      0.0463       0.0423
              K5333P                    ORIG SAMPLE              0.0013     0.0028      0.0000     0.0004     0.0000      0.0004       0.0000
              Q1042P                     SPK SAMP                0.0145     0.0159      0.0142     0.0146     0.0145      0.0140       0.0146
              RECOVERED SPIKE (ug)                                  0.04       0.04       0.04       0.04        0.04        0.04         0.04
              % RECOVERY                                              90         95         102        100        102          90          104

              SPIKED SAMPLES ES 46 FL TBCB-2 P521
                AMOUNT SPIKED (ug)                               0.0449     0.0423      0.0427     0.0434     0.0435      0.0463       0.0423

              K5346P                    ORIG SAMPLE              0.0163     0.0954      0.0003     0.0064     0.0000      0.0006       0.0016
              Q 1065P                    SPK SAMP                0.0484     0.1416      0.0484     0.0514     0.0365      0.0516       0.0516
              RECOVERED SPIKE (ug)                                  0.05       0.07       0.08       0.07        0.06        0.08         0.08
         ND   % RECOVERY DIVIDED BY 2                                  M         88          91         84         68          89           96

              SPIKED SAMPLES ES 46 FL TBCB-3 P524
                AMOUNT SPIKED (ug)                               0.0449     0.0423      0.0427     0.0434     0.0435      0.0463       0.0423
              K5347P                    ORIG SAMPLE              0.0080     0.0517      0.0002     0.0037     0.0000      0.0006       0.0008
              Q1117P                     SPK SAMP                0.0324     0.0784      0.0306     0.0309     0.0274      0.0355       0,0339
              RECOVERED SPIKE (ug)                                  0.06       0.07       0.08       0.07         0.07       0.09         0.08
              % RECOVERY DIVIDED BY 2                                 67         78          88         78          78         94            97




I
I
I


I
I
I
I
I
I              Pesticides and PCBs - NIST Data
I
I
I
I
I
I
I
1
                        125





                                                               MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs - NIST Data




                 RAW     DESIGNATOR FOLDER               HCB      LINDANE         HEPTA-       ALDRIN        HEPTA         ALPHA-          TRANS-    DIELDRIN      MIREX    *2.4'DDE     4ADDE
                FILE          AND                                                  CHLOR                 EPO)UDE CHLORDANE NONACHLOR                                        (0,P'DDE)   (P,P' DDE)
                           STATION                       (ppb)         (ppb)         (ppb)       (ppb)                        (ppb)          (ppb)        (ppb)      (ppb)        (ppb)    (ppb)


               Q 1023P        NIST         P514          0.00          0.58          0.00        0.00         0.00            19.29          19.94        9.38       0.00           M         44.35
               91026P         NIST         P515          0.00          0.48          0.00        0.00         0.00            18.08          14.41        7.71       0.30           M         34.85
               Q1041P         NIST         P517          0.00          0.85          0.00        0.00         0.00            17.45          14.89        8.32       0.00           M         32.12
               Q1044P         NIST         P518          0.00          1.44          0.00        0.00         0.00            28.34          23.13        11.28      0.00           M         50.31
               Q 1064P        NIST         P520          0.00          0.55          0.00        0.00         0.00            13.94          11.49        10.81      0.74           M         31.62
               Q1067P         NIST         P521          0.01          0.75          0.94        0.00         0.00            25.35          21.01        12.17      0.66           M         49.29
               Q1110P         NIST         P522          0.00          1.11          0.98        0.00         0.57            29.32          23.50        12.81      0.67           M         44.25
               'Q 1067P       NIST         P523          0.01          0.95          0.80        0.00         0.00            22.93          18.49        11.90      0.56           M         48.90
               Q1119P         NIST         P524          0.00          0.98          0.93        0.00         0.00            19.40          16.15        13.21      0.64           M         41.44
               Q I 185P       NIST         P525          0.03          0.73          0.35        0.00         0.00            16.06          12.59        11.21      0.36           m         32.62
               Q 1 194P       NIST         P526          0.02          1.27          0.65        0.00         0.00            22.78          18.67        15.81      1.48           M         45.88
               TVG                                       0.01          0.88          0.42        0.00         0.05            21.18          17.66        11.33      0.49                     41.42
               STD DEV                                   0.01          0.29          0.42        0.00         0.16            4.76           3.89         2.20       0.42                       6.98
               Cv                                       159.87        33.15         99.15        0.00        316.23           22.49          22.03        19.39     84.48                     16.86

                                                     M = Matrix interference, larger peak (PC13 84) with retention time slightly less than OP DDE.
          N)                                         No peak found for OP DDE.






                                                                MUSSEL WATCH YEAR V1 - Bivalve Pesticides and PCBs - NIST Data





                  RAW    DESIGNATOR FOLDER                 2.4'DDD       ENDRIN        4.4'DDD        2.4'DDT       4.4'DDT      TOTAL   PCB #8    PCB # 18    PCB #28    PCB #44     PCB #52
                 FILE         AND                        (OY DDD)                    (P,P'DDD)      (0,P'DEM       (P.P'DDT)     DDTS       (CL2)       (CL,3)     (CI-3)      (CIA)    (CL4)
                            STATION                            (ppb)        (ppb)          (ppb)         (ppb)          (ppb)    (ppb)       (ppb)      (ppb)      (ppb)       (ppb)    (ppb)


                9 1023P       NIST          P514               7.24         0.00           50.68         7.84           5.09     115.19       6.5       24.1       94.7        88.7       130.6
                Q 1026P       NIST          P515               4.27         0.00           38.35         4.23           2.93     84.63        6.3       15.9       64.9        59.0         92.8
                Q1041P        NIST          P517               5.12         0.00           35.03         3.75           3.09     79.12        5.6       17.9       79.4        60.4       101.5
                g 1044P       NIST          P518               7.30         0.00           58.73         5.84           3.90     126.08       8.2       30.1       106.6       93.0       154.7
                9 1064P       NIST          P520               4.38         0.00           37.71         3.96           4.49     82.17        1.2       10.5       61.1        43.1         69.8
                g 1067P       NIST          P521               7.33         0.00           55.80         6.66           5.14     124.22       3.2       21.5       98.6        78.9       115.2
                Q111op        NIST          P522               7.89         0.00           48.26         6.38           4.08     110.87       6.8       35.5       113.3       112.4      171.2
                Q 1067P       NIST          P523               6.38         0.00           52.56         5.54           4.45     153.96       3.1       21.3       85.9        77.0       113.9
                Q1119P        NIST          P524               5.17         0.00           46.01         3.86           2.87     99.35        0.9       16.4       83.8        63.2       105.2
                Q 1 185P      NIST          P525               3.05         0.00           37.51         2.83           1.80     105.06       1.2       14.9       60.0        45.7         75.5
                Q 1 194P      NIST          P526               6.15         0.00           50.93         4.19           2.25     109.39       3.4       22.2       88.5        74.9       120.2


                AVG                                            5.84         0.00           46.51         5.01           3.64     108.18      4.22       20.93      85.17       72.39     113.68
                STD DEV                                        1.49         0.00           7.80          1.46           1.07     21.09       2.46       6.80       17.05       19.87      29.18
                CV                                            25.43         0.00           16.77         29.25          29.48    19.50      58.39       32.47      20.02       27.45      25.67



          tQ






                                                                  MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs - NIST Data





                  RAW     DESIGNATOR FOLDER PC13 #66                PC13 #101     PCB #105 PCB# 110/77         PCB #118       PC13 # 128     PCB # 138       PCB# 126      PCB # 153    PCB # 170
                  FILE         AND                           (CIA)        (CL5)         (CL5)       (CL5/4)          (CL5)          (CL6)          (CL6)          (CL5)         (CL6)       (CL7)
                             STATION                         (ppb)        (ppb)         (ppb)         (ppb)          (ppb)          (ppb)          (ppb)          (ppb)         (ppb)       (ppb)


                Q 1023P        NIST          P514            91.6         130.9         50.3          293.1          122.3          18.1           128.2           0.0          169.0            0.0
                Q 1026P        NIST          P515            72.4         104.7         31.7          240.0          88.1           14.0           90.1            0.0          118.7            0.8
                Q1041P         NIST          P517            80.8         104.0         43.2          229.9          99.9           12.8           92.5            0.0          114.3            0.7
                91044P         NIST          P5 18           125.4        177.5         50.4          447.7          140.1          18.8           144.2           0.0          226.4            0.0
                Q 1064P        NIST          P520            71.8         85.1          35.9          135.6          92.5           16.3           91.3            0.0          109.4            1.2
                Q 1067P        NIST          P521            118.4        141.5         61.3          221.0          137.7          21.6           152.9           0.0          177.1            2.7
                Q111op         NIST          P522            95.4         169.1         50.6          376.4          115.4          14.8           126.3           0.0          170.6            0.0
                Q 1067P        NIST          P523            128.7        135.4         53.8          234.0          137.2          20.1           148.7           0.0          172.3            2.7
                Q1119P         NIST          P524            105.5        124.2         49.7          196.1          123.0          20.8           138.9           0.0          150.7            2.4
                Q 1 185P       NIST          P525            86.7         94.2          38.2          153.1          90.9           13.1           97.7            0.0          114.7            1.5
                Q 1 194P       NIST          P526            108.5        131.0         50.1          205.3          127.7          19.6           133.3           0.0          169.4            2.8
                TVG                                          98.66       127.05         46.85        248.38         115.89          17.28        122.19           0.00         153.88           1.35
                STD DEV                                      19.27        27.80         8.28          88.35          18.93          3.05           23.45          0.00          34.66           1.09
                CV                                           19.54        21.88         17.68         35.57          16.34          17.67          19.19          0.00          22.52          80.54




          00



                                                           mmmm m =am mm
                                                                 MUSSEL WATCH YEAR VI - Bivalve Pesticides and PCBs - NIST Data





                  RAW     DESIGNATOR FOLDER               PCB # 180      PCB # 187      PC13 # 195    PCB #206       PCB #209           TOTAL TOTAL
                 FILE          AND                              (CL7)          (CL7)         (CL8)          (CI,9)        (CLIO)         PCB'S    ISOMERS
                            STATION                             (ppb)          (ppb)         (ppb)          (ppb)           (ppb)         (ppb)     (ppb)


                Q1023P         NIST          P514               13.2           29.3            0.0            0.0            0.0          2642           1391
                Q1026P         NIST          P515                 9.1          20.6            0.0            0.0            0.0          1959           1029
                Q1041P         NIST          P517                 9.2          20.4            0.0            0.0            0.0          2041           1073
                Q1044P         NIST          P518               13.6           34.2            0.0            0.0            0.0          3361           1771
                Q1064P         NIST          P520               13.1           22.5            0.6            0.3            0.0          1642             861
                Q1067P         NIST          P521               18.0           33.4            0.4            0.3            0.0          2667           1404
                Q111op         NIST          P522               12.0           27.7            0.0            0.0            0.0          3033           1598
                Q1067P         NIST          P523               16.4           31.5            0.3            0.3            0.0          2627           1383
                Q1119P         NIST          P524               14.6           28.5            0.5            0.2            0.0          2328           1225
                Q 1 185P       NIST          P525               10.9           20.6            0.3            0.2            0.1          1752             919
                Q1194P         NIST          P526               16.0           30.4            1.0            0.9            1.6          2484           1307


                AVG                                             13.30          27.18         0.28           0.20            0.16       2412.27        1269.03
                STD DEV                                         2.75           5.02          0.32           0.25            0.46        507.65         268.60
                CV                                              20.68          18.49        112.84         124.14        288.76           21.04          21.17



          N)




I
I
I
I
I
I
I
I
I
                 Trace Metals Data
I
I
I
I
I
I
I
I
1
                        130
 "I





                                                         MUSSEL WATCH YEAR VI - Bivalve Trace Metals Data





                        SAMPLE              Ag      As       Cd       Cr     Cu        Fe         Hg      Mn       Ni        Pb      Se      Sn Zn


                        LMSB-I           1.41     10.8    2.24     0.72      94.    409.     127.00      12.3      1.1    0.62      3.1    <0.2   1270.
                        LMSB-2          0.980       9.5   2.25     1.18      74.    704.     116.00      16.6      1.3    0.78      3.1    <0.2   1000.
                        LMSB-3           1.72       8.8   3.01     0.66     104.    398.     122.00      16.9      1.1    0.66      2.4    <0.2   1210.
                        CCIC- 1         0.631       7.2   3.77     0.75      68.    430.      46.00      13.0      1.3    0.75      3.2      0.5  3400.
                        CCIC-2          0.663       8.4   3.74     0.95      75.    527.      49.00      14.2      1.6    0.75      3.1      0.4  3630.
                        CCIC-3          0.506       9.6   3.50     0.41      66.    221.      45.00       9.2      1.2    0.53      3.5      0.3  2780.
                        ABLR-1          0.432     10.9    2.40     0.46      20.    268.      72.00      11.1      1.0    0.69      3.1    <0.2     187.
                        ABLR-2          0.413     10.1    2.73     0.41      20.    239.      68.00      10.0      1.2    0.68      2.9    <0.2     186.
                        ABLR-3          0.403     10.1    2.55     0.48      20.    268.      74.00      10.7      1.1    0.62      2.9    <0.2     179.
                        CBCR-1           3.92       8.1   8.26     0.79     159.    405.     121.00      17.1      2.7    1.11      2.7    <0.2   1310.
                        CBCR-2           2.46       7.6   6.82     0.61     111.    334.     101.00      16.3      2.8    0.93      2.7    <0.2     945.
                        CBCR-3           2.56       8.0   7.35     0.94     105.    468.     102.00      20.2      2.9    1.20      2.8    <0.2     990.
                        MBAR-1          0.791       7.1   3.35     0.43      27.    296.      41.00      14.4      1.4    0.45      2.7      0.2    208.
                        MBAR-2          0.754       7.2   3.21     0.59      28.    360.      52.00      15.5      2.0    0.50      2.3    <0.2     227.
                        MBAR-3          0.594       7.1   2.58     0.35      23.    216.      66.00      10.0      1.4    0.47      2.4    <0.2     183.
                        SAPP- 1          1.25       8.0   4.33     0.30      36.    199.      70.00       9.1      1.8    0.46      3.5    <0.2     390.
                        SAPP-2           1.06       7.6   4.14     0.27      33.    214.      57.00       9.4      1.8    0.56      4.0    <0.2     376.
                        SAPP-3           1.15       7.7   4.18     0.31      29.    212.      96.00      10.5      1.9    0.53      3.9    <0.2     345.
                        SAMP-1          0.828       4.6   2.42     0.32      33.    213.      33.00      11.1      2.0    0.47      3.0      0.3    397.
                        SAMP-2          0.759       4.8   2.90     0.40      34.    247.      32.00      10.4      1.4    0.40      3.5    <0.2     389.
                        SAMP-3          0.788       4.6   2.84     0.37      34,    218.      35.00      10.4      1.2    0.43      3.8    <0.2     337.
                        ESSP- 1          1.42       9.4   3.90     0.96      53.    457.      64.00      15.1      1.9    0.62      3.8    <0.2     569.
                        ESSP-2           1.78     10.5    4.50     1.96      71.    929.      90.00      28.5      2.2    0.90      3.1    <0.2     762.
                        ESSP-3           1.60     10.6    4.34     0.60      58.    306.      90.00      11.0      1.8    0.50      3.8    <0.2     590.
                        MBGP-1           2.30       6.8   5.47     0.91     115.    505.     630.00      14.7      2.9    1.04      3.3      0.2    991.
                        MBGP-2           2.83       7.9   5.50     1.03     140.    534.     696.00      18.4      3.3    1.15      5.1    <0.2   1220.
                        MBGP-3           2.63     11.1    6.05     1.45     129.    629.     692.00      18.9      3.2    1.22      2.6      0.4    983.
                        MBLR- 1          1.84       6.0   4.72     0.56     112.    352.     1190.00     15.1      2.8    0.91      3.9      0.4    999.
                        MBLR-2           1.91       6.5   4.55     0.88     119.    467,     1340.00     17.5      3.7    0.82      3.0      0.2    974.
                        MBLR-3           1.99       5.7   4.73     0.73     124.    355.     1280.00     13.4      3.5    0.75      4.2    <0.2   1140.
                        MBTP- 1          1.41       7.7   4.30     0.51      58.    260.      82.00      12.3      2.7    0.40      4.1    <0.2     510.



                                                                 All concentrations in ppm, gg/g dry wt.






                                                            MUSSEL WATCH YEAR VI - Bivalve Trace Metals Data





                         SAMPLE               Ag      As        Cd        Cr      Cu        Fe          Hg      Mn        Ni       Pb       Se       Sn    Zn


                         MBTP-2            2.36       7.0     5.68     0.99       84.    417.      71.00      19.5        2.5   0.70       3.9    <0.2      683.
                         MBTP-3            2.56       8.9     5.47     0.88       69.    399.      73.00      16.6        2.1   0.61       3.8    <0.2      576.
                         MBEM- 1           3.74       4.1     10.8     0.72     201.     400.      65.00      17.2        2.3   0.51       3.4      0.4   1090.
                         MBEM-2            3.01       4.2     10.4     0.71     210.     431.      78.00      16.4        2.5   0.53       4.2      0.4   1050.
                         MBEM-3            7.70       3.9     13.1     0.71     243.     370.      105.00     14.6        2.0   0.57       4.3    <0.2    1340.
                         BRCL- 1           2.71       3.9     3.37     0.78     179.     357.      *.68.00    19.1        2.5   0.64       3.7    <0.2    1790.
                         BRCL-2            3.20       6.2     3.44     1.05     220.     573.      49.00      24.7        3.4   0.84       3.7      0.2   1980.
                         BRCL-3            2.16       5.1     2.98     0.60     154.     371.      66.00      20.2        3.0   0.54       3.2    <0.2    1770.
                         BRFS-I            3.88       5.3     4.03     0.86     288.     383.      75.00      17.6        2.1   0.71       4.0      0.4   3920.
                         BRFS-2            3.83       4.2     3.43     1.29     287.     701.      80.00      29.6        2.5   0.86       4.0      0.4   3630.
                         BRFS-3            2.54       6.2     3.00     2.73     284.     259.      84.00      46.3        3.2   1.13       3.4      0.9   4350.
                         GBCR-1            2.95       6.2     3.84     0.62     162.     347.      105.00     16.3        2.1   0.71       3.5      0.4   1790.
                         GBCR-2            4.11       6.1     3.80     0.66     184.     361.      109.00     17.8        1.8   0.76       3.4      0.3   2290.
                         GBCR-3            8.97       6.9     3.99     0.99     187.     472.      117.00     22.3        2.3   0.83       4.0      0.6   2040.
                         GBOB-I            1.18       3.8     1.82     0.34     170.     229.      61.00      46.1        2.0   1.51       3.0      0.2   5460.
                         GBOB-2            0.836      4.7     1.44     0.19     162.     158.      53.00      30.6        1.9   1.49       2.7      0.3   4430.
                         GBOB-3            0.919      3.6     1.53     0.26     154.     163.      46.00      36.5        2.0   1.60       2.8    <0.2    5010.
                         GBTD- 1           2.01       3.8     4.97     0.60     169.     334.      35.00      12.8        2.2   0.62       3.0      0.5   1760.
                         GBTD-2            2.63       3.7     4.95     0.74     205.     442.      45.00      15.4        2.4   0.80       3.3      0.3   1740.
                         GBTD-3            2.16       3.2     4.30     0.72     160.     436.      42.00      16.5        2.2   0.80       3.2      0.3   1550.
                         GBYC- 1           1.43       3.7     4.08     0.48     112.     189.      41.00      20.1        1.6   0.57       3.4      0.4   2820.
                         GBYC-2            1.20       3.2     4.12     0.54     108.     218.      36.00      24.1        1.3   0.61       3.1      0.3   2760.
                         GBYC-3            1.24       2.8     4.32     0.43     119.     184.      46.00      21.1        1.5   0.60       3.5      0.5   2580.
                         GBHR- 1           3.32       5.1     5.74     0.61     162.     287.      45.00      15.8        2.2   0.63       4.6    <0.2    1700.
                         GBHR-2            3.40       5.9     5.87     0.74     169.     306.      44.00      16.2        2.4   0.64       4.9    <0.2    1950.
                         GBHR-3            3.52       6.9     6.09     0.69     178.     345.      53.00      18.1        2.6   0.63       4.7    <0.2    1790.
                         SLBB-1            4.35       5.0     4.84     0.81     234.     445.      67.00      27.2        2.2   0.60       4.9    <0.2    3220.
                         SLBB-2            4.09       5.2     4.69     1.06     204.     541.      80.00      27.1        1.6   0.69       3.7      0.4   2560.
                         SLBB-3            3.07       5.3     5.02     1.60     151.     794.      96.00      32.4        2.1   0.96       4.3      0.5   2250.
                         CLSIJ- 1          3.07       3.9     3.47     0.91     187.     417.      88.00      22.8        2.5   0.60       2.9    <0.2    1750.
                         CLS,J-2           2.54       4.8     4.11     1.17     174.     468.      95.00      24.1        2.7   0.60       3.3      0.6   1870.



                                                                    All concentrations in ppm, gg/g dry wt.






                                                        MUSSEL WATCH YEAR VI - Bivalve Trace Metals Data





                        SAMPLE             Ag      As       Cd       Cr     Cu        Fe         Hg     Mn        Ni       Pb     Se       Sn Zn



                        CLS,J-3        0.801       4.2    3.53    0.55     158.    309.      76.00     20.0       3.3   0.44      3.8      0.2  1470.
                        CLLC- 1        0.715       4.1    2.46    0.37     119.    160.      74.00     10.0       1.5   0.47      2.4    <0.2   2060.
                        CLLC-2         0.686       5.1    2.35    0.26      89.    137.      70.00      7.4       1.2   0.42      3.4    <0.2   1720.
                        CLLC-3         0.883       5.8    2.54    0.66      97.    245.      55.00     18.1       1.4   0,63      3.1      0.3  2230.
                        JHJH-1           2.50      7.5    5.17    0.61     181.    274.      43.00     16.8       1.8   0.48      4.6    <0.2   1310.
                        JHJH-2           1.63      7.1    5.06    0.56     100.    288.      36.00     16.2       2.1   0.45      2.9    <0.2     971.
                        JHJH-3           1.84      6.6    5.20    0.53     120.    300.      55.00     15.4       1.7   0.48      4.5    <0.2   1020.
                        VBSP- 1          5.82      7.4    9.34    0.87     502.    481.      45.00     17.0       2.3   0.75      5.2    <0.2   4200.
                        VBSP-2           6.29      5.3    9.06    0.86     477.    458.      49.00     14.4       2.0   0.71      4.4    <0.2   3680.
                        VBSP-3           4.62      4.7    7.61    0.50     396.    298.      47.00     11.5       2.5   0.51      4.5    <0.2   2570.
                        ABOB-1           2.96      8.7    8.46    0.57     236.    284.      44.00     15.3       1.9   0.67      4.5    <0.2   1980.
                        ABOB-2           2.08     10.0    6.95    0.39     173.    232.      49.00     11.7       1.5   0.60      4.2    <0.2   1880.
                        ABOB-3           3.04      9.1    8.00    1.46     211.    659.      52.00     23.5       2.1   0.84      3.8      0.2  2130.
                        CLCL-I         0.962       6.6    3.40    0.85     112.    436.      31.00     13.2       2.5   0.59      2.3      0.7  1300.
                        CLCL-2           1.11      5.0    3.90    0.85     129.    424.      33.00     15.5       2.4   0.68      2.5    <0.2   1650.
                        CLCL-3           1.07      7.5    3.61    0.83     118.    412.      38.00     14.8       2.8   0.55      3.2    <0.2   1580.
                        TBLB- 1        0.536       4.8    2.06    1.01      76.    494.      60.00     18.1       2.9   0.65      2.8    <0.2   1510.
                        TBLB-2         0.933       5.7    2.79    0.57     116.    345.      64.00     15.7       3.0   0.57      2.6    <0.2   2010.
                        TBLB-3         0.724       4.9    2.81    0.57      97.    309.      43.00     10.1       2.6   0.53      2.3    <0.2   1560.
                        TBLF- 1          1.59      7.1    4.12    0.20     155.    212.      54.00      9.1       2.1   0.34      3.4    <0.2   1660.
                        TBLF-2           1.28      4.9    3.45    0.13     129.    191.      48.00      8.9       2.1   0.31      2.7      0.2  1520.
                        TBLF-3           1.62      5.5    4.21    0.32     162.    228.      96.00      9.0       1.8   0.40      3.0    <0.2   1930.
                        BBSD-1           1.60      4.4    3.36    1.17     157.    245.      34.00     13.3       2.6   0.57      2.5    <0.2   2380.
                        BBSD-2           1.35      5.3    3.19    0.51     129.    257.      40.00     12.8       2.4   0.50      2.6    <0.2   2020.
                        BBSD-3           1.47      5.5    3.17    0.57     134.    311.      40.00     12.0       2.7   0.55      2.4    <0.2   2040.
                        BBMB-1         0.423       8.0    1.38    0.32      40.    276.      64.00      8.6       2.3   0.45      1.9      0.8  1640.
                        BBMB-2         0.489       5.3    1.58    0.42      53.    341.      92.00     10.3       2.1   0.51      2.2      0.9  2020.
                        BBMB-3         0.474       8.2    1.53    0.37      47.    314.      72.00      8.4       2.7   0.51      3.2      1.1  1960.
                        BSSI- 1          2.62      5.1    10.6    0.81     218.    549.      64.00     18.9       4.0   0.70      3.4    <0.2   2170.
                        BSSI-2           1.98      5.7    10.3    0.67     192.    380.      124.00    16.1       3.6   0.56      3.7    <0.2   1990.
                        BSSI-3           2.79      6.1    12.4    0.89     213.    555.      43.00     20.1       4.0   0.70      3.7    <0.2   2200.



                                                                All concentrations in ppm, jig/g dry wt.





                                                        MUSSEL WATCH YEAR VI - Bivalve Trace Metals Data





                        SAMPLE             Ag      As       Cd       Cr     Cu       Fe         Hg      Mn       Ni        Pb      Se     Sn Zn



                        BSBG-1          1.22       3.7   4.99     0.95    129.     601.    126.00      23.3      2.8    0.59     3.5    <0.2    2360.
                        BSBG-2          1.29       3.5   6.30     1.54    134.     780.    191.00      25.8      2.5    0.73     4.1    <0.2    2720.
                        BSBG-3          1.29       4.5   5.33     1.32    142.     752.    170.00      22.7      2.6    0.71     3.5    <0.2    2870.
                        LBMP-1          3.20       5.0   10.0     1.96    332.    1090.    169.00      36.8      3.1    1.07     4.0      0.3   3490.
                        LBMP-2          3.10       3.2   10.5     2.21    382.    1030.    185.00      34.2      3.1    0.46     4.3    <0.2    4170.
                        LBMP-3          2.68       4.6   9.16     1.56    330.     761.    191.00      27.2      2.4    0.82     3.8    <0.2    3660.
                        MSPC-1          3.68       4.6   10.4     0.27    203.     148.    100.00      10.1      1.8    0.60     2.9      0.3   3620.
                        MSPC-2          0.972      3.8   8.30     0.26    164.     134.     92.00       8.2      1.5    0.70     2.9    <0.2    3020.
                        MSPC-3          3.93       2.9   9.73     0.69    218.     147.    121.00       9.6      2.0    0.59     2.8    <0.2    4110.
                        MSBB- 1         2.69       5.5   6.04     0.21    199.     177.    104.00      10.0      1.4    1.69     4.6      0.5   5380.
                        MSBB-2          2.51       8.6   5.62     0.34    193.     180.    103.00      10.9      1.3    1.00     3.6      0.2   4430.
                        MSBB-3          3.06       6.6   5.33     0.16    217.     183.    115.00      10.5      1.2    0.69     4.2    <0.2    5550.
                        MSPB-1          1.99     12.9    2.13     0.25    118.     173.    129.00      11.4      2.3    0.29     4.1    <0.2    3590.
                        MSPB-2          2.16     12.1    2.02     0.29    114.     209.    163.00       9.6      2.0    0.36     2.9      0.3   3400.
                        MSPB-3          2.08     10.2    2.37     0.40    132.     202.    115.00      11.6      2.0    0.30     4.4    <0.2    3470.
                        MBCP-1          2.50       4.7   3.62     0.28      81.    123.     83.00       5.4      2.1    0.31     2.6    <0.2     793.
                        MBCP-2          2.38       5.5   3.38     0.22      83.      91.    62.00       4.4      2.0    0.22     3.6    <0.2     783.
                        MBCP-3          2.57       4.8   3.50     0.24      90.    112.     45.00       5.2      1.4    0.24     2.8    <0.2     860.
                        MBHl- 1         5.77       4.6   5.63     0.51    429.     297.    101.00       8.8      2.3    0.57     2.4      0.3   7870.
                        MBHI-2          4.42       4.5   5.05     0.55    363.     258.     93.00       7.9      2.5    0.40     2.3      0.3   6580.
                        MBHI-3          5.35       4.1   5.18     0.61    451.     280.     84.00       9.9      2.6    0.38     2.3      0.3   8270.
                        PBPH- 1         2.14     12.2    3.13     0.19      56.    123.     82.00       6.3      1.0    0.51     3.5    <0.2    1850.
                        PBPH-2          2.27     13.0    3.20     0.20      53.    118.     74.00       6.2      1.3    0.50     3.4      0.2   1780.
                        PBPH-3          2.31     10.4    3.08     0.45      53.    128.     91.00       7.5      1.4    0.49     3.4    <0.2    1710.
                        PBIB- 1         1.16     12.6    2.77     '0.49     54.    259.     66.00       9.5      1.1    0.28     2.9    <0.2     634.
                        PBIB-2          3.20     16.1    3.40     0.58      63.    276.     68.00      11.2      1.4    0.29     3.6    <0.2     772.
                        PBIB-3          2.51     14.1    3.06     0.78      60.    225.     68.00      10.9      1.5    0.26     2.5    <0.2     612.
                        CRJB- 1         1.21     14.6    1.95     0.69    389.     792.    300.00      12.8      1.0    2.03     5.3      0.8   3780.
                        CBJB-2          1.14     15.6    1.88     0.72    345.     961.    240.00      12.4      1.1    1.45     5.3      0.7   2970.
                        CBJB-3          1.20     14.5    2.19     0.71    381.     742.    225.00      14.7      1.3    1.47     4.8      0.8   4490.
                        CBSR-1          3.64     10.0    3.85     2.37      59.   1350.    168.00      35.7      1.8    0.80     4.8      0.2    733.



                                                                AD concentrations in ppm, gg/g dry wt.






                                                        MUSSEL WATCH YEAR VI - Bivalve Trace Metals Data





                        SAMPLE             Ag      As       Cd      Cr     Cu        Fe         Hg     Mn        Ni       Pb     Se      Sn Zn



                        CBSR-2          2.84      9.4    4.06    1.87      52.    939.     175.00     31.4       1.7   0.58      4.9   <0.2     687.
                        CBSR-3          4.49      9.3    4.61    1.98      50.    1080.    135.00     37.7       1.7   0.74      5.9   <0.2     825.
                        CBSP-1          5.47      9.2    2.97    1.23     128.    607.     374.00     18.6       1.3   7.54      7.2     0.3   4550.
                        CBSP-2          4.01     10.7    2.68    1.37      96.    607.     296.00     19.8       1.4   7.57      6.6   <0.2    3670.
                        CBSP-3          9.70      7.4    2.60    0.86      96.    506.     347.00     11.8       1.2   10.8      5.9     0.4   3720.
                        PCLO-1         0.629      7.2   0.980    0.31      36.    217.     126.00      7.0       0.7   0.71      2.8   <0.2    3810.
                        PCLO-2          1.25     10.0    1.11    0.42      32.    103.      89.00      5.6       0.4   0.43      3.4     0.2   1120.
                        PCLO-3          1.38     10.7    1.17    0.24      39.      88.     88.00      4.4       1.0   0.33      3.9     0.3   1060.
                        SAWB- 1         1.68     14.9   0.751    0.45     194.    136.      49.00     10.2       0.7   1.15      2.0     0.3   2590.
                        SAWB-2          1.10     12.0   0.697    0.34     210.    133.      44.00      7.6       0.7   1.01      2.7   <0.2    2830.
                        SAWB-3         0.864     11.4   0.830    6.46     203.    165.      44.00     10.3       0.7   1.23      2.8     0.3   2700.
                        APDB-1          2.48      6.3    3.93    0.57      63.    279.     108.00     12.4       1.7   0.36      3.0   <0.2     381.
                        APDB-2          2.17      7.3    3.95    0.35      61.    219.     225.00      8.6       1.6   0.27      3.2     0.2    359.
        CIO             APDB-3          2.20      7.3    4.03    0.77      56.    278.     142.00     11.4       1.4   0.23      3.3     0.2    351.
        r-n             APCP- 1         2.11     13.2    1.87    0.95     210.    480.     212.00     17.9       1.4   0.66      2.9   <0.2     940.
                        APCP-2          2.01     14.7    2.29    1.56     185.    472.     159.00     17.8       1.4   0.63      2.8     0.2    831.
                        APCP-3          2.05     18.5    1.97    0.55     232.    290.     183.00     13.2       1.2   0.80      2.7     0.4    986.
                        AESP- 1        0.985     15.5    4.01    0.30      35.    197.     179.00     14.6       1.2   0.47      3.8     0.3    705.
                        AESP-2          1.20     14.5    3.74    0.45      35.    216.     196.00     18.5       1.4   0.47      3.5     0.2    650.
                        AESP-3          1.06     16.9    3.90    0.47      39.    244.     223.00     19.1       1.6   0.45      4.0   <0.2     718.
                        CKBP-1         0.377     24.0    1.71    1.00      12.    354.     126.00     16.6       1.2   0.46      2.2   <0.2     314.
                        CKBP-2         0.411     22.2    2.17    2.14      15.    491.      98.00     18.6       1.4   0.54      2.8   <0.2     338.
                        CKBP-3         0.430     21.6    2.06    1.38      12.    442.     147.00     17.4       1.1   0.44      2.5     0.3    318.
                        TBNP-1          1.72     119.    1.10    0.30      69.    117.     106.00      6.3       1.0   0.76      1.9   <0.2    2660.
                        TBNP-2          1.45     124.    1.10    0.31      64.    104.     112.00      4.0       0.7   0.73      1.6     0.3   2550.
                        TBNP-3          1.68     126.    1.03    0.35      79.    109.      94.00      5.6       1.1   0.78      1.9     0.4   2380.
                        TBMIK-1        0.268     12.8    1.50    0.41      14.    108.     106.00      5.1       0.8   0.29      1.7   <0.2     242.
                        TBMK-2         0.226     15.5    1.91    0.39      13.    105.      91.00      4.7       1.5   0.36      1.3   <0.2     226.
                        TBMK-3         0.240     14.3    1.28    0.36      12.    118.     116.00      4.7       0.9   0.42      1.1   <0.2     341.
                        TBPB-1          1.82      4.5    2.02    0.56      69.    172.     217.00      7.1       1.4   1.01      2.3   <0.2    1910.
                        TBPB-2          1.89      5.0    2.22    0.38      69.    173.     313.00      7.2       1.2   0.96      2.5     0.2   2100.



                                                               All concentrations in ppm, gg/g dry wt.






                                                       MUSSEL WATCH YEAR VI - Bivalve Trace Metals Data





                        SAMPLE             Ag     As       Cd       Cr     Cu        Fe         Hg     Mn       Ni       Pb      Se      Sn Zn



                        TBPB-3          1.15      6.0    2.02    0.39      79.    186.     294.00      6.9      1.2    1.04      2.5     0.3   2680.
                        TBOT-1          3.82      2.4    2.97    1-.42    153.    442.     375.00      9.2      1.9    0.97      3.0     0.3   8400.
                        TBOT-2          2.50      2.4    3.44    1.49     112.    493.     388.00      8.5      2.6    0.98      3.8   <0.2    6330.
                        TBOT-3          1.76      1.6    2.42    1.58     140.    581.     513.00      10.6     2.1    1.09      2.1   <0.2    6810.
                        TBKA-I          4.18      4.4    2.38    1.26     330.    256.     154.00      9.0      1.1    2.12      3.1     0.8   6870.
                        TBKA-2          4.01      4.7    2.40    0.96     683.    247.     367.00      9.1      1.8    1.80      4.4     1.0   8630.
                        TBKA-3          4.12      5.3    2.22    1.05     359.    245.     144.00      8.0      1.3    1.97      3.1     1.1   6640.
                        TBCB-1          1.14      3.7    2.79    0.55     100.    233.     288.00      8.1      1.0    0.40      1.7     0.2   1460.
                        TBCB-2         0.770      2.5    1.98    0.35      77.    193.     126.00      6.4      1.0    0.37      1.7   <0.2    1340.
                        TBCB-3          1.06      3.8    2.14    0.53      85.    213.     175.00      5.5      0.9    0.44      1.5   <0.2    1230.
                        CBBI- 1         1.48     16.3    2.05    0.87      80.    238.     210.00      4.3      0.8    0.45      1.8   <0.2    1050.
                        CBBI-2          1.78     15.6    2.24    0.84      81.    218.     196.00      6.7      0.7    0.40      1.6   <0.2    1080.
                        CBBI-3          3.49     14.0    2.12    0.36      94.    140.     253.00      3.7      0.5    0.32      1.6   <0.2    1350.
                        CBFM- 1         1.75      5.6    2.16    1.22     115.    331.     122.00      11.2     1.1    0.81      3.2     0.2   2390.
                        CBFM-2          2.18      4.7    2.74    1.45     129.    401.     136.00      10.9     1.0    0.99      2.7     0.4   2130.
                        CBFM-3          2.12      6.3    1.97    1.36     160.    472.       90.00     8.4      1.3    1.15      2.2   <0.2    2590.
                        NBNB-1          3.80     12.4    1.31    0.82     379.    223.     109.00      7.2      0.6    0.33      2.3     0.7   2310.
                        NBNB-2          3.28     12.3    1.30    0.98     360.    272.     117.00      6.4      1.0    0.45      2.0     0.7   2580.
                        NBNB-3          3.98     13.8    1.51    1.14     368.    332.     131.00      8.5      0.8    0.48      2.5     0.6   2910.
                        RBHC-1          1.18     10.0    2.53    0.96      36.    226.     122.00      6.4      0.9    0.40      2.1   <0.2     595.
                        RBHC-2         0.800     10.5    2.93    0.78      28.    195.       95.00     6.4      1.1    0.34      2.8   <0.2     492.
                        RBHC-3          1.18     12.0    2.78    0.69      41.    199.     158.00      6.9      0.8    0.42      2.2     0.4   1340.
                        EVFU-1         0.824      4.8    2.05    0.90      43.    256.     183.00      8.2      0.9    0.38      2.0   <0.2     958.
                        EVFU-2         0.777      5.7    2.10    0.58      38.    196.     117.00      7.2      0.8    0.37      1.6   <0.2     772.
                        EVFU-3         0.776      5.0    2.21    0.68      49.    221.     176.00      9.6      1.0    0.29      1.9   <0.2     975.










                                                               All concentrations in pprn, gg/g dry wt.




I
I
I
I
I
I
I
I
I
I            Trace Metal Certified Reference Materials
I
I
I
I
I
I
I
1
                       137
 A






                                                         MUSSEL WATCH YEAR VI - Bivalve Trace Metal Certified Reference Material





                   Date            Sample          Ag ppm As ppm Cd ppm Cr ppm Cu ppm Fe ppm Mn ppm                                  Ni pm     Pb ppm      Se ppm Sn ppm Zn ppm
                 7/9/91          NBS-OYS-129        1.69       10.1        4.13        1.58       56.1        492.       9.53        1.33       0.345       2.21        1.93        852.
                 7/10/91         NBS-OYS-9          1.69       9.58        3.96        1.73       55.1        465.       10.1        1.77       0.373       2.28        1.84        776.
                 7/31/91         NBS-OYS-211        1.65       11.8        4.38        1.35       55.5        471.       9.10        1.45       0.363       1.92        1.74        782.
                 8/3/91          NBS-OYS-10         1.63       11.7        3.79        1.45       53.4        506.       10.6        2.61       0.324       2.11        1.60        773.
                 8/20/91         NBS-OYS-224        1.53       13.5        3.97        1.75       55.1        472.       10.8        2.38       0.355       2.35        1.51        757.
                 8/22/91         NBS-OYS-132        1.54       11.7        3.94        1.42       54.1        480.       10.3        2.18       0.345       2.80        1.97        729.
                 8/23/91         NBS-OYS-221        1.55       12.0        4.09        1.66       59.1        519.       10.8        2.22       0.327       2.41        1.83        764.
                 8/29/91         NBS-OYS-137        1.74       9.92        4.00        1.32       59.2        482.       9.01        2.81       0.330       2.44        2.12        793.
                 9/5/91          NBS-OYS-30         1.81       11.1        4.19        i.80       56.6        456.       9.67        2.77       0.344       2.31        2.17        779.


                                   Average         1.648       11.267      4.050       1.562      56.022      482.556    9.990       2.169      0.345       2.314       1.857     778.333
                                   Std Dev         0.096       1.237       0.171       0.182      2.014       20.100     0.695       0.547      0.017       0.243       0.220     33.136
                                 Certifled Value   1.680       14.000      4.150       1.430      66.300      539.000    12.300      2.250      0.371       2.210                 830.000
                                   Range ï¿½         0.150       1.200       0.380       0.460      4.300       15.000     1.500       0.440      0.014       0.240                 57.000
                                 % Recovery        98.082      80.476    97.590      109.246      84.498      89.528     81.220      96.395     93.022    104.726                 93.775

          00
                 7/9/91          DORM-173          0.175       11.7        0.088       3.52                   62.0       <0.9        1.20       0.549       1.42        0.063       18.7
                 7/10/91         DORM-144          0.194       12.7        0.093       3.25                   60.3       1.47        0.967      0.268       1.37        0.252       20.0
                 8/3/91          DORM-136          0.133       13.8        0.087       3.57                   53.3       1.07        0.914      0.431       1.53        0.069       18.6
                 8/20/91         DORM-26           0.194       14.4        0.087       3.57                   58.9       0.937       1.09       0.420       1.38        <0.03       19.5
                 8/22/91         DORM-173          0.158       15.5        0.084       3.57                   53.3       2.46        1.40       0.468       1.84        0.071       17.2
                 8/29/91         DORM-206          0.179       14.0        0.091       3.93                   59.1       <0.9        1.33       0.444       1.74        0.096       18.0
                 8/30/91         DORM-71           0.184       10.6        0.095       3.60                   53.8       0.960       1.06       0.254       1.73        0.069       16.4
                 9/5/91          DORM-131          0.192       14.9        0.098       4.87                   67.2       1.75        1.26       0.465       1.63        0.111       19.7


                                   Average         0.176       13.450      0.090       3.735                  58.488     1.441       1.153      0.412       1.580       0.104     18.513
                                   Std Dev         0.021       1.664       0.005       0.494                  4.897      0.593       0.173      0.101       0.181       0.067       1.259
                                 Certifled Value               17.700      0.086       3.600                  63.600     1.320       1.200      0.400       1.620                 21.300
                                   Range ï¿½                     2.100       0.012       0.400                  5.300      0.260       0.300      0.120       0.120                   1.000
                                 % Recovery                    75.989    105.087 103.750                      91.961     109.179     96.052     103.094     97.531                86.913




I
I
I
I
I
I
I
I
I
I             Trace Metals QA/QC Data
I
I
I
I
I
I
I
1
                       139
 t---#




I
I
I
I
I
I
I
I
I
I                 Trace Metal Duplicates
I
I
I
I
I
I
I
1
                        140

 "I





                                                                 MUSSEL WATCH YEAR VI - Bivalve Trace Metal Duplicates




                      Date             Sample         Ag ppm As ppm Cd ppm              Cr ppm     Cu ppm. Fe ppm Mn ppm              Ni pm    Pb ppm      Se ppm Sn ppm Zn ppm
                     7/9/91           BBSD-3-A          1.51       5.25       3.14        0.521      135.       304.       11.5       2.89       0.491      2.46        <0.03      2000.
                     7/9/91           BBSD-3-B          1.43       5.83       3.19        0.625      133.       317.       12.6       2.52       0.605      2.41        <0.03      2070.
                                       RPD %            5.44       10.47      1.58        18.15      1.49       4.19       9.13       13.68      20.80      2.05        0.00       3.44


                     7/10/91          APCP-1-A          2.05       12.7       1.90        0.899      210.       477.       18.3       1.38       0.698      2.92        0.138      938.
                     7/10/91          APCP-l-B          2.17       13.6       1.83        0.997      210.       484.       17.4       1.42       0.619      2.97        0.227      943.
                                       RPD %            5.69       6.84       3.75        10.34      0.00       1.46       5.04       2.86       12.00      1.70        48.77      0.53


                     7/31/91          TBMK-3-A          0.237      14.6       1.28        0.361      12.3       117.       4.32       0.862      0.427      1.19        0.213      337.
                     7/31/91          TBMK-3-B          0.243      13.9       1.29        0.351      11.7       119.       5.06       0.844      0.405      1.08        0.131      345.
                                       RPD %            2.50       4.91       0.78        2.81       5.00       1.69       15.78      2.11       5.29       9.69        47.67      2.35


                     7/31/91          MBAR-2-A          0.760      6.80       3.24        0.575      28.0       357.       15.8       1.95       0.511      2.33        0.142      225.
                     7/31/91          MBAR-2-B          0.747      7.61       3.18        0.597      27.3       363.       15.2       2.06       0.495      2.27        0.180      228.
                                       RPD %            1.73       11.24      1.87        3.75       2.53       1.67       3.87       5.49       3.18       2.61        23.60      1.32


                     7/31/91          EVFU-2-A          0.770      5.33       2.09        0.585      37.7       192.       7.08       0.761      0.375      1.58        0.121      789.
                     7/31/91          EVFU-2-B          0.784      6.09       2.11        0.573      38.3       201.       7.27       0.902      0.358      1.67        0.162      755.
                                       RPD %            1.80       13.31      0.95        2.07       1.58       4.58       2.65       16.96      4.64       5.54        28.98      4.40


                     8/3/91           NBNB-1-A          3.91       12.2       1.29        0.807      381.       223.       7.05       0.510      0.324      2.33        0.890      2300.
                     8/3/91           NBNB-1-B          3.70       12.7       1.33        0.831      377.       224.       7.36       0.597      0.336      2.28        0.480      2320.
                                       RPD %            5.52       4.02       3.05        2.93       1.06       0.45       4.30       15.72      3.64       2.17        59.85      0.87


                     8/20/91          TBKA-3-A          3.92       5.56       2.23        1.07       359.       246.       8.36       1.36       1.95       2.93        1.09       6630.
                     8/20/91          TBKA-3-B          4.32       4.98       2.21        1.02       360.       244.       7.61       1.17       1.99       3.22        1.06       6650.
                                       RPD %            9.71       11.01      0.90        4.78       0.28       0.82       9.39       15.02      2.03       9.43        2.79       0.30


                     8/20/91          TBNP-3-A          1.90       124.       1.04        0.367      80.2       ill.       5.28       1.04       0.803      1.93        0.492      2400.
                     8/20/91          TBNP-3-B          1.47       129.       1.01        0.338      77.2       107.       5.85       1.10       0.752      1.79        0.369      2370.
                                       RPD %            25.52      3.95       2.93        8.23       3.81       3.67       10.24      5.61       6.56       7.53        28.57      1.26





                                                                 MUSSEL WATCH YEAR VI - Bivalve Trace Metal Duplicates


                      8/22/91         VBSP-3-A          4.89       4.47       7.64       0.516      397.       299.       11.4       2.46       0.515      4.48      <0.03       2500.
                      8/22/91         VBSP-3-13         4.35       4.94       7.59       0.489      395.       297.       11.6       2.62       0.501      4.58      <0.03       2650.
                                       RPD %            11.69      9.99       0.66       5.37       0.51       0.67       1.74       6.30       2.76       2.21        0.00      5.83


                      8/22/91         MSPB-1-A          1.95       12.3       2.20       0.256      117.       170.       11.3       2.26       0.286      4.21      0.151       3620.
                      8/22/91         MSPB-1-13         2.02       13.4       2.06       0.241      120.       177.       11.4       2.35       0.297      3.93      0.194       3570.
                                       RPD %            3.53       8.56       6.57       6.04       2.53       4.03       0.88       3.90       3.77       6.88      24.93       1.39


                      8/30/91         TBCB-2-A          0.750      2.60       2.00       0.352      77.6       192.       6.47       0.995      0.370      1.75      0.228       1350.
                      8/30/91         TBCB-2-13         0.791      2.49       1.96       0.352      75.9       193.       6.31       0.968      0.360      1.67      0.140       1330.
                                       RPD %            5.32       4.32       2.02       0.00       2.21       0.52       2.50       2.75       2.74       4.68      47.83       1.49


                      9/5/91          CBCR-1-A          4.06       8.23       8.30       0.796      160.       418.       17.7       2.71       1.13       2.90      0.129       1330.
                      9/5/91          CI3CR-l-B         3.78       7.99       8.21       0.783      158.       392.       16.4       2.67       1.08       2.53      0.111       1300.
                                       RPD %            7.14       2.96       1.09       1.65       1.26       6.42       7.62       1.49       4.52       13.63     15.00       2.28


                      9/8/91          Cl3CR-2-A         2.60       7.49       6.82       0.658      ill.       344.       15.8       2.75       0.927      2.67      0.189       936.
                      9/8/91          CBCR-2-13         2.33       7.66       6.83       0.568      ill.       324.       16.9       2.75       0.924      2.78      0.109       953.
                                       RPD %            10.95      2.24       0.15       14.68      0.00       5.99       6.73       0.00       0.32       4.04      53.69       1.80


                      9/8/91          CBSP-l-A          5.62       9.44       2.97       1.19       117.       531.       17.4       1.21       2.29       7.35      0.168       3590.
                      9/8/91          CBSP-1-13         5.87       8.90       2.77       1.22       115.       528.       18.4       1.19       2.26       7.69      0.144       3790.
                                       RPD %            4.35       5.89       6.97       2.49       1.72       0.57       5.59       1.67       1.32       4.52      15.38       5.42


                      Date             Sample         Ag ppm As ppm Cd ppm Cr ppm Cu ppm Fe ppm Mn ppm                               Ni pm    Pb ppm Se ppm         Sn ppm     Zn ppm
                      9/8/91          CBSR-l-A          4.14       9.02       3.86       2.47       60.6       1290.      34.7       1.76       0.786      6.06      0.103       802.
                      9/8/91          CBSR-l-B          3.72       7.59       3.89       2.50       61.3       1290.      35.7       1.83       0.800      5.69      0.065       754.
                                       RPD %            10.69      17.22      0.77       1.21       1.15       0.00       2.84       3.90       1.77       6.30      45.24       6.17


                      9/8/91          LMSB-2-A          0.983      8.90       2.24       1.18       73.9       698.       17.1       1.32       0.775      3.12      0.032       1020.
                      9/8/91          LMSB-2-B          0.978      10.0       2.27       1.18       73.6       710.       16.0       1.31       0.792      3.00      0.075       993.
                                       RPD %            0.51       11.64      1.33       0.00       0.41       1.70       6.65       0.76       2.17       3.92      80.37       2.68


                      9/8/91          ESSP-l-A          1.45       9.66       3.87       0.969      52.1       460.       15.3       1.86       0.618      3.95      0.209       567.
                      9/8/91          ESSP-1-13         1.40       9.08       3.92       0.942      53.8       454.       14.8       1.95       0.625      3.57      0.111       570.





                                                                MUSSEL WATCH YEAR VI - Bivalve Trace Metal Duplicates



                                       RPD %            3.51       6.19      1.28       2.83       3.21       1.31       3,32       4.72       1.13       10.11      61.25      0.53


                     9/8/91           ESSP-3-A          1.57       11.0      4.35       0.587      55.9       306.       11.3       1.81       0.504'     3.70       0.094      593.
                     9/8/91           ESSP-3-13         1.63       10.2      4.34       0.614      59.7       306.       10.8       1.85       0.495      3.87       0.058      587.
                                       RPD %            3.75       7.55      0.23       4.50       6.57       0.00       4.52       2.19       1.80       4.49       47.37      1.02


                     9/8/91           MBTP-1-A          1.49       7.51      4.45       0.460      58.2       261.       12.8       2.56       OA04       4.20       0.074      500.
                     9/8/91           MBTP-1-B          1.33       7.94      4.14       0.561      57.1       259.       11.8       2.85       0.397      4.06       0.082      520.
                                       RPD %            11.35      5.57      7.22       19.78      1.91       0.77       8.13       10.72      1.75       3.39       10.26      3.92


                                   Average RPD          6.99       7.79      2.32       5.87       1.96       2.13       5.84       6.10       4.33       5.52       33.77      2.47




I
I


I
11
I
I
I
I
I             Trace Metal Matrix Spikes and Blanks
I
11
11
11
I
I
I
I
                       144
 JIM





                                                        MUSSEL WATCH YEAR VI - Bivalve Trace Metal Matrix Spikes and Blanks



               MATRIX SPIKES
                      Date        Sample              Ag ppm As ppm Cd ppm Cr pprn Cu ppm Fe ppm Mn pprn                              Ni prn      Pb ppm Se ppm Sn ppm             Zn ppm
                     7/9/91       TBOT-1                3.82       2.38       2.97       1.42        153.       442.       9.16       1.86        0.967      3.03       0.256      8400.
                     7/9/91       TBOT-1+Spike          5.70       7.09       7.03       3.69        352.       841.       102.       6.01        5.96       19.2       9.54       11000.
                                  Theo. Increment       2.07       7.30       4.14       2.31        193.08     387.46     99.47      4.31        5.12       16.96      10.47      2448.55
                                       % Recovery       90.63      64.53      98.02      98.17       103.07     102.98     93.33      96.18       97.51      95.34      88.68      106.19


                     7/9/91       CLSJ-2                2.54       4.81       4.11       1.17        174.       468.       24.1       2.68        0.602      3.32       0.579      1870.
                     7/9/91       CLSJ-2+Spike          4.63       11.5       8.32       3.26        367.       909.       114.       6.97        5.49       18.9       9.04       4520.
                                  Theo. Increment       2.02       7.12       4.04       2.26        188.39     378.05     97.06      4.21        5.00       16.55      10.22      2389.08
                                       % Recovery       103.26     93.94      104.17     92.63       102.45     116.65     92.62      101.90      97.84      94.15      82.83      110.92


                     7/31/91      MSPB-2                2.16       12.1       2.02       0.292       114.       209.       9.60       1.95        0.360      2.87       0.314      3400.
                     7/31/91      MSPB-2+Spike          4.01       19.0       5.76       2.53        301.       605.       100.       5.99        5.80       19.8       8.95       5680.
                                  Theo. Increment       2.07       7.27       4.13       2.30        192.40     386.10     99.13      4.30        5.10       16.90      10.43      2439.94
                                       % Recovery       89.50      94.86      90.61      97.12       97.19      102.56     91.20      93.96       106.61     100.18     82.78      93.44


                     7/31/91      TBCD-3                1.06       3.78       2.14       0.531       84.5       213.       5.48       0.935       0.441      1.50       0.129      1230.
                     7/31/91      TBCB-3+Spike          2.92       10.3       5.74       2.64        269.       589.       98.4       5.12        5.57       17.8       8.57       3780.
                                  Theo. Increment       2.04       7.16       4.07       2.27        189.52     380.33     97.64      4.24        5.03       16.65      10.28      2403.48
                                       % Recovery       91.35      91.00      88.54      92.91       97.35      98.86      95.16      98.81       102.04     97.91      82.14      106.10


                     7/31/91      MBAR-3                0.594      7.09       2.58       0.349       23.1       216.       10.0       1.39        0.473      2.37       0.188      183.
                     7/31/91      MBAR-3+Spike          2.51       14.1       6.34       2.57        211.       578.       98.2       6.18        5.52       19.1       8.92       2540.
                                  Theo. Increment       2.05       7.22       4.10       2.29        190.93     383.15     98.37      4.27        5.06       16.77      10.35      2421.28
                                       % Recovery       93.41      97.12      91.80      97.13       98.41      94.48      89.66      112.26      99.67      99.76      84.34      97.35


                     8/3/91       NBNB-3                3.98       13.8       1.51       1.14        368.       332.       8.49       0.762       0.482      2.47       0.589      2910.
                     8/3/91       NBNB-3+Spike          3.52       20.2       5.37       3.62        570.       693.       99.8       4.86        5.31       18.8       9.47       5410.
                                  Theo. Increment       1.96       6.89       3.91       2.18        182.26     365.75     93.90      4.07        4.83       16.01      9.88       2311.34
                                       % Recovery       -23.49     92.89      98.72      113.62      110.83     98.70      97.24      100.61      99.88      102.00     89.86      108.16


                     8/3/91       MBHI-2                4.42       4.48       5.05       0.548       363.       258.       7.93       2.54        0.399      2.31       0.257      6580.



                                                        M mm@m M w M M.M
                                                        MUSSEL WATCH YEAR VI - Bivalve Trace Metal Matrix Spikes and Blanks


                     8/3/91       MBI-H-2+Spike         3.79       11.7       9.00       2.73       550.       615.        97.6       6.44       5.09        18.0       9.40       8560.
                                  Theo. Increment       1.95       6.85       3.89       2.17       181.19     363.60      93.35      4.05       4.81        15.92      9.82       2297.77
                                       % Recovery       -32.36     105.41     101.62     100.55     103.21     98.18       96.06      96.31      97.62       98.58      93.06      86.17


                         8/20/91 LBMP-1                 3.20       4.98       10.0       1.96       332.       1090.       36.8       3.09       1.07        3.98       0.283      3490.
                         8/20/91  LBMP-1+Spike          4.83       12.8       14.2       4.61       522.       1480.       129.       7.10       5.93        20.2       9.11       5980.
                                  Theo. Increment       1.99       6.99       3.97       2.22       185.01     371.28      95.32      4.13       4.91        16.25      10.03      2346.26
                                       % Recovery       82.01      111.81     105.82     119.60     102.70     105.04      96.73      96.98      99.05       99.81      87.99      106.13


                         8/20/91  AESP-2                1.20       14.5       3.74       0.452      34.6       216.        18.5       1.35       0.468       3.47       0.239      650.
                         8/20/91  AESP-2+Spike          3.08       22.3       7.62       2.74       215.       594.        107.       5.00       5.10        19.33      8.31       2920.
                                  Theo. Increment       1.97       6.95       3.94       2.20       183.80     368.84      94.69      4.11       4.87        16.14      9.97       2330.88
                                       % Recovery       95.21      112.26     98.40      103.94     98.15      102.48      93.46      88.86      95.03       98.24      80.98      97.39


                     8/29/91      SAMP-1                0.828      4.62       2.42       0.316      32.5       213.        11.1       1.98       0.469       3.02       0.275      397.
                     8/29/91      SAMP-1+Spike          2.55       11.0       6.04       2.48       221.       578.        109.       6.04       5.29        19.4       10.94      2710.
                                  Theo. Increment       1.96       6.89       3.91       2.18       182.36     365.96      93.95      4.08       4.84        16.02      9.89       2312.66
                                       % Recovery       87.89      92.54      92.53      99.08      103.37     99.74       104.20     99.62      99.68       102.26     107.85     100.01


                     9/5/91       ABOB-1                2.96       8.66       8.46       0.568      236.       284.        15.3       1.94       0.670       4.51       0.038      1980.
                     9/5/91       ABOB-1+SPIKE          4.97       15.0       12.2       3.05       422.       661.        109.       5.99       5.56        22.0       8.23       4300.
                                  Theo. Increment       2.11       7.44       4.22       2.36       196.71     394.76      101.35     4.40       5.22        17.28      10.67      2494.64
                                       % Recovery       95.11      85.25      88.62      105.35     94.55      95.50       92.45      92.13      93.73       101.22     76.80      93.00


                     9/5/91       CLLC-2                0.686      5.07       2.35       0.256      89.4       137.        7.44       1.17       0.423       3.37       0.166      1720.
                     9/5/91       CLLC-2+SPIKE          2.72       11.0       6.73       2.77       281.       517.        103.       5.69       5.53        21.6       9.67       4320.
                                  Theo. Increment       2.21       7.79       4.42       2.47       206.16     413.72      106.22     4.61       5.47        18.11      11.18      2614.46
                                       % Recovery       91.83      76.09      99.03      101.82     92.94      91.85       89.97      98.11      93.41       100.67     85.02      99.45


                BLANKS
                     Date         Sample              Ag ppm As ppm Cd ppm Cr ppm Cu ppm                       Fe ppm Mn ppm Ni prn Pb ppm Se ppm Sn ppm                           Zn ppm
                     7/9/91       RB-211                0.005      <0.2       <0.003     0.407      <0.09      4.72        <0.9       <0.2       <0.07       <0.4       <0.03      <0.6
                     7/31/91      RB-25                 0.007      <0.2       <0.003     0.081      <0.09      4.89        <0.9       <0.2       <0.07       <0.4       0.065      <0.6





                                                      MUSSEL WATCH YEAR VI - Bivalve Trace Metal Matrix Spikes and Blanks



                    7/31/91      RB-200               <0.005      <0.2      <0.003     0.222      <0.09       4.07       <0.9       <0.2      <0.07       <0.4       0.074      <0.6
                    8/3/91       RB-9                 <0.005      <0.2      <0.003     0.175      <0.09        <4        <0.9       <0.2      <0.07       <0.4       <0.03      <0.6
                    8/3/91       RB-102               <0.005      <0.2      <0.003     <0.05      <0.09        <4        <0.9       <0.2      <0.07       <0.4       0.036      <0.6
                    8/22/91      RB-5                 <0.005      <0.2      <0.003     <0.05      <0.09        <4        <0.9       <0.2      <0.07       <0.4       0.124      <0.6
                    8/23/91      RB-226               0.008       <0.2      <0.003     0.480      <0.09       4.19       <0.9       <0.2      <0.07       <0.4       0.054      <0.6
                    8/23/91      RB-65                0.015       0.218     0.003      0.051      <0.09        <4        <0.9       <0.2      <0.07       <0.4       0.134      <0.6
                    8/29/91      RB-46                <0.005      <0.2      <0.003     0.144      <0.09        <4        <0.9       <0.2      <0.07       <0.4       <0.03      <0.6
                    8/29/91      RB-205               0.007       <0.2      <0.003     <0.05      <0.09       4.90       <0.9       <0.2      <0.07       <0.4       <0.03      <0.6
                    8/30/91      R13-20               0.014       <0.2      0.003      0.053      <0.09       4.19       <0.9       <0.2      0.095       <0.4       <0.03      <0.6
                    8/30/91      RB-101               0.008       <0.2      <0.003     0.063      <0.09       4.55       <0.9       <0.2      <0.07       <0.4       0.072      <0.6
                    9/5/91       RB-221               0.032       <0.2      <0.003     0.071      <0.09       4.90       <0.9       <0.2      <0.07       <0.4       <0.03      <0.6
                    9/8/91       RB-61                <0.005      <0.2      <0.003     0.416      <0.09       5.25       <0.9       <0.2      <0.07       <0.4       <0.03      <0.6




I
I
I
I
I
I
I
I
I
I       Mercury Duplicates, Spikes, Reference Material and Blanks
I
I
I
I
I
I
I
1
                        148






                 MUSSEL WATCH YEAR VI -Bivalve Mercury Duplicates, Spikes, Reference Material and Blanks



            LABORATORY DUPLICATES                                          MATRIX SPIKES
                   Date       Sample                 Hg ppm                      Date        Sample                 Hg ppm
                 10/21/91     ABLR-1-A                 0.072                   10/21/91      AESP-1-B                0.179
                 10/21/91     ABLR-1-B                 0,071                   10/21/91      AESP-l-A                1.095
                                          RPD %        1.50                                  Theo. Increment         0.867
                                                                                                  % Recovery         105.6
                 10/16/91     ABOB-1-A                 0,041
                 10/16/91     ABOB-1-B                 0.043                   10/19/91      APCP-3-B                0.183
                                          RPD %        0.28                    10/19/91      APCP-3-A                1.054
                                                                                             Theo. Increment         0.913
                 10/18/91     AESP-2-A                 0.189                                      % Recovery         95.4
                 10/18/91     AESP-2-B                 0.202
                                          RPD %        6.70                    10/17/91      BRCL-2-B                0.048
                                                                               10/17/91      BRCL-2-A                0.955
                 10/21/91     BBSD-1-A                 0.031                                 Theo. Increment         0.878
                 10/21/91     BBSD-1-B                 0*016                                      % Recovery         103.2
                                          RPD %        13.40
                                                                               10/18/91      CBFM-1-B                0.122
                 10/19/91     BRFS-1-A                 0.074                   10/18/91      CBFM-1-A                1.022
                 10/19/91     BRFS-1-B                 0.076                                 Theo. Increment         0.837
                                          RPD %        1.73                                       % Recovery         107.5


                 10/16/91     BSSI-1-A                 0.063                   10/17/91      CBFM-3-B                0.090
                 10/16/91     BSSI-1-B                 0.064                   10/17/91      CBFM-3-A                0.949
                                          RPD %        1.35                                  Theo. Increment         0.857
                                                                                                  % Recovery         100.2
                 10/14/91     CBCR-2-A                 0.106
                 10/14/91     CBCR-2-B                 0.097                   10/14/91      CCIC-3-B                0.045
                                          RPD %        8.99                    10/14/91      CCIC-3-A-SPK            0.876
                                                                                             Theo. Increment         0.862
                 10/18/91     CBFM-2-A                 0.138                                      % Recovery         96.5
                 10/18/91     CBFM-2-B                 0.133
                                          RPD %        3.64                    10/17/91      EVFU-2-B                0.117
                                                                               10/17/91      EVFU-2-A                1.007
                 10/19/91     CBJB-1-A                 0.296                                 Theo. Increment         0.886
                 10/19/91     CBJB-1-B                 0.305                                      % Recovery         100.3
                                          RPD %        2.84                      Date        Sample                 Hg ppm
                                                                               10/16/91      GBHR-2-B                0.044
                 10/14/91     CBSP-1-A                 0.360                   10/16/91      GBHR-2-A-SPK            0.982
                 10/14/91     CBSP-1-B                 0.387                                 Theo. Increment         0.905
                                          RPD %        7.31                                       % Recovery         103.6


                 10/14/91     CBSR-1-A                 0.171                   10/19/91      MMHI-1-B                0.101
                 10/14/91     CBSR-1-B                 0.165                   10/19/91      MBHI-1-A                0.983
                                          RPD %        3.64                                  Theo. Increment         0.871



                                                                      149






                 MUSSEL WATCH YEAR VI -Bivalve Mercury Duplicates. Spikes, Reference Material and Blanks


                                                                                                 % Recovery          101.2
                 10/18/91     CLCL-3-A                 0.040
                 10/18/91     CLCL-3-B                 0.036                   10/14/91      MBTP-1-B                0.082
                                          RPD %        10.40                   10/14/91      MBTP-1-A+SPK            1.036
                                                                                             Theo. Increment         0.933
                 10/16/91     ESSP-2-A                 0.088                                     % Recovery          102.3
                 10/16/91     ESSP-2-B                 0.092
                                          RPD %        4.39                    10/18/91      PCLO-3-B                0.087
                                                                               10/18/91      PCLO-3-A                1.016
                 10/21/91     EVFU-1-A                 0.188                                 Theo. Increment         0.877
                 10/21/91     EVFU-1-B                 0.177                                     % Recovery          105.7
                                          RPD %        6.13                    10/21/91      RBHC-3-B                0.158
                 10/19/91     G11CR-l-A                0*104                   10/21/91      RBHC-3-A                1.083
                 10/19/91     GBCR-1-B                 0.105                                 Theo. Increment         0.880
                                          RPD %        0.55                                      % Recovery          105.0


                 10/16/91     GBYC-1-A                 0.040                   10/16/91      SAMP-2-B                0.032
                 10/16/91     GBYC-1-B                 0.042                   10/16/91      SAMP-2-A-SPK            0.925
                                          RPD %        6.09                                  Theo. Increment         0.895
                 10/14/91     LMSB-2-A                 0.116                                     % Recovery          99.7
                 10/14/91     LMSB-2-B                 0,116                   10/19/91      SAPP-3-D                0.096
                                          RPD %        0.48                    10/19/91      SAPP-3-A                0.990
                                                                                             Theo. Increment         0.884
                 10/17/91     MBAR-1-A                 0,039                                     % Recovery          101.1
                 10/17/91     MBAR-l-B                 0.042
                                          RPD %        8.36                    10/16/91      VBSP-2-B                0.049
                                                                               10/16/91      VBSP-2-A-SPK            0.920
                 10/14/91     MBGP-3-A                 0.704                                 Theo. Increment         0.865
                 10/14/91     MBGP-3-B                 0.680                                     % Recovery          100.7
                                          RPD %        3.45                    10/18/91      VBSP-3-B                0.047
                 10/19/91     MSPB-2-A                 0.102                   10/18/91      VBSP-3-A                0.926
                 10/19/91     MSPB-2-B                 0.104                                 Theo. Increment         0.840
                                          RPD %        2.39                                      % Recovery          104.7


                 10/18/91     P13113-1-A               0.063
                 10/18/91     PBIB-1-B                 0.067
                                          RPD %        5.51


                 10/18/91     TBKA-3-A                 0.141
                 10/18/91     TBKA-3-B                 0.146
                                          RPD %        3.55               CERTIFIED REFERENCE MATERIALS
                                                                                 Date        Sample                Hg ppm
                 10/19/91     TBPB-3-A                 0*290                   10/14/91      DOLT                    0.207



                                                                     150






                MUSSEL WATCH YEAR VI -Bivalve Mercury Duplicates, Spikes, Reference Material and Blanks



                10/19/91      TBPB-3-B               0.297                    10/16/91     DOLT                    0.219
                                       RPD %          2.30                    10/17/91     DOLT                    0.211
                              Average RPD %           4.56                    10/19/91     DOLT                    0.299
                                                                              10/21/91     DOLT                    0.307
                                                                                                    Average        0.249
             BLANKS                                                                                 Std Dev        0.050
                  Date        Sample                 Hg ppm                                 Certified Value        0.225
                10/14/91      BLANK-A                <0,003                                          Range         0.037
                10/16/91      BLANK-A                <0.003                                     % Recovery         110.5
                10/17/91      BLANK-A                <0.003                    Date        Sample                  Hg ppm
                10/11/91      BLANK-A                <0.003                   10/14/91     DORM                    0.739
                10/19/91      BLANK-A                <0.003                   10/16/91     DORM                    0.758
                10/21/91      BLANK-A                <0.003                   10/17/91     DORM                    0.777
                10/17/91      BLANK-B                <0,003                   10/18/91     DORM                    0.748
                10/18/91      BLANK-13               <0.003                   10/19/91     DORM                    0.759
                10/19/91      BLANK-13               <0.003                                         Average        0.756
                10/21/91      BLANK-13               <0,013                                         Std Dev        0.014
                10/14/91      BLANK-13               <0.003                                 Certified Value        0.798
                10/16/91      BLANK-13               <0.003                                          Range         0.074
                                                                                                % Recovery         94.8


                                                                              10/14/91     NBS OYS                 0.057
                                                                              10/17/91     NBS OYS                 0.060
                                                                              10/18/91     NBS OYS                 0.064
                                                                              10/19/91     NBS OYS                 0.069
                                                                              10/21/91     NBS OYS                 0.065
                                                                                                    Average        0.063
                                                                                                    Std Dev        0.005
                                                                                            Certified Value        0.0642
                                                                                                     Range         0.0067
                                                                                                % Recovery         98.1






















                                                                     151




I
I
I
I
I
I
I
I
I
I              Method Detection Limits
I
I
I
I
I
I
I
I -

I
4-                      152




 I
 I
 I
 I
 I
 I
 I
 I
 I
 I                     Aromatics Method Detection Limits
 I
 I
 I
 I
 I
 I
 I
 1
 '41                                  153







                                          MUSSEL WATCH YEAR VI - Bivalve Aromatics Method Detection Limits




                                 FILE                      >Q 1364                  >Q 1365                                        >Q1355
                             DESCRIPTION        MDL BLANK +SU P530 MDL BLANK +SU P530 AVERAGE BLANK MDL I (SU+CAL P530


                             NAPHTHALENE                   0.99                     3.80                   2.40                    4.57
                             Cl-NAPHTHALENES               1.07                     2.89                   1.98                    7.12
                             C2-NAPHTHALENES               0.00                     0.00                   0.00                    0.00
                             C3-NAPHTHALENES               0.00                     0.00                   0.00                    0.00
                             C4-NAPHTHALENES               0.00                     0.00                   0.00                    0.00
                               BIPHENYL                    0.81                     2.42                   1.62                    4.82
                             ACENAPHTHYLENE                0.06                     0.10                   0.08                    2.78
                             ACENAPHTHENE                  0.07                     0.12                   0.10                    3.05
                               FLUORENE                    0.14                     0.20                   0.17                    3.39
                             Cl-FLUORENES                  0.00                     0.00                   0.00                    0.00
                             C2-FLUORENES                  0.00                     0.00                   0.00                    0.00
                             C3-FLUORENES                  0.00                     0.00                   0.00                    0.00
                             PHENANTHRENE                  0.22                     0.53                   0.38                    3.14
                             ANTHRACENE                    0.05                     0.08                   0.07                    2.72
                             Cl-PHEN-ANTHR                 0.00                     0.00                   0.00                    0.00
                             C2-PHEN-ANTHR                 0.00                     0.00                   0.00                    0.00
                             C3-PHEN-ANTHR                 0.00                     0.00                   0.00                    0.00
                             C4-PHEN@ANTHR                 0.00                     0.00                   0.00                    0.00
                             DIBENZOTHIO                   0.03                     0.10                   0.07                    2.11
                               CI-DIBEN                    0.00                     0.00                   0.00                    0.00
                               C2-DIBEN                    0.00                     0.00                   0.00                    0.00
                               C3-DIBEN                    0.00                     0.00                   0.00                    0.00
                             FLUORANTHENE                  0.09                     0.10                   0.10                    2.44
                                PYRENE                     0.17                     0.25                   0.21                    2.62
                             Cl-FLUORAN-PYR                0.00                     0.00                   0.00                    0.00
                             BENaANTHRACENE                0.04                     0.05                   0.05                    1.37
                               CHRYSENE                    0.04                     0.10                   0.07                    2.72
                             Cl-CHRYSENES                  0.00                     0.00                   0.00                    0.00
                             C2-CHRYSENES                  0.00                     0.00                   0.00                    0.00
                             C3-CHRYSENES                  0.00                     0.00                   0.00                    0.00
                             C4-CHRYSENES                  0.00                     0.00                   0.00                    0.00
                             BENbFLUORAN                   0.02                     0.02                   0.02                    1.87
                             BENkFLIJORAN                  0.01                     0.05                   0.03                    1.95
                             BENePYPENE                    0.03                     0.05                   0.04                    2.12
                             BENaPYRENE                    0.02                     0.01                   0.02                    1.37
                               PERYLENE                    1.60                     0.02                   0.81                    5.11
                             I123cdPYRENE                  0.01                     0.02                   0.02                    1.67
                             DBahANTHRA                    0.02                     0.04                   0.03                    1.26
                             BgiiiPERYLENE                 0.01                     0.03                   0.02                    1.28
                             2-METHYLNAPH                  0.51                     1.58                   1.05                    3.43
                             I-METHYLNAPH                  0.56                     1.31                   0.94                    3.69
                             2,6-DIMETHNAPH                0.19                     0.47                   0.33                    2.98
                         2,3.5-TRIMETHNAPH                 0.14                     0.33                   0.24                    2.80
                             1-METHYLPHEN                  0.05                     0.10                   0.08                    3.00

                        Surrogate Recoveries
                               NAPHD8:                     43.93                    50.97                  47.45                   55.51
                               ACENDIO:                    62.08                    64.54                  63.31                   60.80
                               PHEND 10:                   68.65                    67.31                  67.98                   67.97
                               CHRYD12:                    52.53                    49.02                  50.78                   57.76
                               PERYD12:                    1.11                     60.07                  30.59                   11.38











                                                                                  154







                                        MUSSEL WATCH YEAR VI - Bivalve Aromatics Method Detection Limits





                               FILE                    >Q1356                    >Q1357                >Q1358                  >Q1359
                           DESCRIP'nON         MDL 2 (SU+CAL) P530 MDL 3 (SU+CAL)P530 MDL 4 (SU+CAL) P530 MDL 5 (SU+CAL) P530



                           NAPHTHALENE                   3.85                    3.37                    3.87                    2.90
                           Cl-NAPHTRALENES               6.23                    6.55                    6.15                    5.80
                           C2-NAPHTHALENES               0.00                    0.00                    0.00                    0.00
                           C3-NAPHTHALENES               0.00                    0.00                    0.00                    0.00
                           C4-NAPHTHALENES               0.00                    0.00                    0.00                    0.00
                              BIPHENYL                   3.21                    3.21                    3.80                    2.92
                           ACENAPHTHYLENE                2.54                    2.49                    2.21                    2.32
                           ACENAPITrHENE                 2.68                    2.71                    2.38                    2.49
                              FLUORENE                   2.76                    3.01                    @2.39                   2.58
                           CI-FLUORENES                  0.00                    0.00                    0.00                    0.00
                           C2-FLUORENES                  0.00                    0.00                    0.00                    0.00
                           C3-FLUORENES                  0.00                    0.00                    0.00                    0.00
                           PHENANTHRENE                  2.76                    2.66                    2.54                    2.43
                           ANTHRACENE                    2.56                    2.51                    1.97                    2.08
                           Cl-PHEN-ANTHR                 0.00                    0.00                    0.00                    0.00
                           C2-PHEN-ANTHR                 0.00                    0.00                    0.00                    0.00
                           C3-PHEN-ANTHR                 0.00                    0.00                    0.00                    0.00
                           C4-PHEN-ANMR                  0.00                    0.00                    0.00                    0.00
                           DIBENZOTHIO                   1.94                    1.42                    1.78                    1.43
                              Cl-DIBEN                   0.00                    0.00                    0.00                    0.00
                              C2-DIBEN                   0.00                    0.00                    0.00                    0.00
                              C3-DIBEN                   0.00                    0.00                    0.00                    0.00
                           FLUORANTHENE                  2.34                    2.25                    2.00                    1.95
                              PYRENE                     2.39                    2.27                    2.05                    1.99
                           Cl-FLUORAN-PYR                0.00                    0.00                    0'.00                   0.00
                           BENaANTHRACENE                1.30                    1.23                    1.08                    1.08
                              CHRYSENE                   2.46                    2.50                    2.09                    2.10
                           CI-CHRYSENES                  0.00                    0.00                    0.00                    0.00
                           C2-CHRYSENES                  0.00                    0.00                    0.00                    0.00
                           C3-CHRYSENES                  0.00                    0.00                    0.00                    0.00
                           C4-CHRYSENES                  0.00                    0.00                    0.00                    0.00
                           BENbFLUORAN                   1.62                    1.84                    1.35                    1.34
                           BENkFLUORAN                   1.84                    1.72                    1.57                    1.47
                           BENePYRENE                    1.85                    1.94                    1.59                    1.56
                           BENaPYRENE                    1.03                    0.90                    0.94                    0.87
                              PERYLENE                   3.70                    3.80                    2.23                    3.96
                           1123cdPYRENE                  1.38                    1.43                    1.11                    1.13
                           DBabANTHRA                    1.13                    1.14                    0.88                    0.92
                           BgWPERYLENE                   1.20                    1.11                    0.78                    0.92
                           2-N=HYLNAPH                   3.07                    3.07                    2.99                    2.87
                           1 -METHYLNAPH                 3.16                    3.48                    3.16                    2.93
                           2,6-DD4ETHNAPH                2.57                    2.66                    2.41                    2.49
                           2.3,5-TRIMErtiNAPH            2.35                    2.45                    2.16                    2.36
                           I-METHYLPHEN                  2.69                    2.67                    2.38                    2.29


                           Surrogate Recoveries
                              NAPHD8:                    53.62                   50.24                   54.81                   52.09
                              ACEND10:                   66.68                   62.06                   66.76                   62.30
                              PHEND10:                   72.12                   70.41                   72.20                   73.81
                              CHRYD12:                   62.86                   58.20                   61.10                   61.94
                              PERYD12:                   2.55                    4.16                    6.62                    1.62

















                                                                                 155







                                        MUSSEL WATCH YEAR VI - Bivalve Aromatics Method Detection Limits





                          FILE                  >Q 1360                 >Q 1361                  >Q1362                  >Q 1363             MDL
                     DESCRIPTION        MDL 6 (SU+CAL) P530 MDL 7 (SU+CAL) P530 MDL 8 (SU+CAL) P530 MDL 9 (SU+CAL) P530 TISSUES



                     NAPHTHALENE                  3.41                    4.14                     3.06                    3.53              1.44
                     Ci-NAPHTHALENES              6*64                    7.00                     5.82                    6.25              1.28
                     C2-NAPHTHALENES              0.00                    0.00                     0.00                    0.00              0.00
                     C3-NAPHTHALENES              0.00                    0.00                     0.00                    0.00              0.00
                     C4-NAPHTHALENES              0.00                    0.00                     0.00                    0.00              0.00
                        BIPHENYL                  3.55                    3.86                     3.07                    3.32              1.58
                     ACENAPHTHYLENE               2.24                    2.22                     2.24                    2.21              0.55
                     ACENAPHTHENE                 2.43                    2.38                     2.32                    2.31              0.66
                        FLUORENE                  2.49                    2.53                     2.51                    2.55              0.87
                     CI-FLUORENES                 0.00                    0.00                     0.00                    0.00              0.00
                     C2-FLUORENES                 0.00                    0.00                     0.00                    0.00              0.00
                     M-FLUORENES                  0.00                    0.00                     0.00                    0.00              0.00
                     PHENANTHRENE                 2.43                    2.49                     2.54                    2.55              0.61
                     ANTHRACENE                   1.93                    1.97                     1.72                    2.15              0.92
                     Cl-PHEN  ANTHR               0.00                    0.00                     0.00                    0.00              0.00
                     C2-PHEN  ANTHR               0.00                    0.00                     0.00                    0.00              0.00
                     C3-PHEN  ANTHR               0.00                    0.00                     0.00                    0.00              0.00
                     C4-PHEN  ANTHR               0.00                    0.00                     0.00                    0.00              0.00
                     DIBENZOTHIO                  1.33                    1.36                     1.47                    1.39              0.78
                        Cl-DIBEN                  0.00                    0.00                     0.00                    0.00              0.00
                        C2-DIBEN                  0.00                    0.00                     0.00                    0.00              0.00
                        C3-DIBEN                  0.00                    0.00                     0.00                    0.00              0.00
                     FLUORANTHENE                 1,91                    2.00                     2.00                    1.97              0.53
                        PYPENE                    1.89                    1.99                     1.95                    2.04              0.66
                     Cl-FLUORAN-PYR               0.00                    0.00                     0.00                    0.00              0.00
                     BENaANTHRACENE               0.98                    1.08                     1.03                    1.01              0.37
                        CHRYSENE                  2.05                    2.12                     2.05                    2.09              0.68
                     Cl-CHRYSENES                 0.00                    0.00                     0.00                    0.00              0.00
                     C2-CHRYSENES                 0.00                    0.00                     0.00                    0.00              0.00
                     C3-CHRYSENES                 0.00                    0.00                     0.00                    0.00              0.00
                     C4-CHRYSENES                 0,00                    0.00                     0.00                    0.00              0.00
                     BENbFLUORAN                  1.55                    1.44                     1.27                    1.61              0.59
                     BENkFLUORAN                  1.17                    1.50                     1.49                    1.27              0.69
                     BENePYRENE                   1.50                    1.62                     1.64                    1.60              0.57
                     BENaPYRENE                   0.60                    0.75                     0.47                    0.81              0.70
                        PERYLENE                  6.44                    4.35                     0.00                    4.46              3.21
                     I123cdPYRENE                 1.04                    1.21                     0.98                    1.11              0.61
                     D13ahANTHRA.                 0.84                    0.96                     0.90                    0.98              0.39
                     BgIAPERYLENE                 0.76                    0.89                     0.59                    0.85              0.61
                     2-METHYLNAPH                 3.11                    3.46                     2.80                    2.92              0.63
                     1-ME'rHYLNAPH                3.53                    3.54                     3.02                    3.33              0.71
                     2,6-DIMETHNAPH               2.59                    2.49                     2.49                    2.64              0.46
                     2.3.5-TRRAETHNAPH            2.40                    2.27                     2.24                    2.14              0.54
                     1-METHYLPHEN                 2.37                    2.39                     2.33                    2.40              0.64


                     Surrogate Recoveries
                        NAPHD8:                   50.54                   45.26                    46.72                   49.29           NO DATA
                        ACEND10:                  62.43                   58.63                    59.94                   62.26           NO DATA
                        PHENDIO:                  73.30                   66.79                    66.10                   68.11           NO DATA
                        CHRYD12:                  61.81                   56.49                    55.91                   56.76           NO DATA
                        PERYD12:                  1.62                    3.38                     1.16                    4.29            NO DATA















                                                                                156




 I
 i
 I
 I
 I
 I
 I
 I
 I
 I                Pesticides and PCBs Method Detection Limits
 I
 I
 I
 I
 I
 I
 I
 1
                                      157
 'it





                                                           Mussel Watch Year VI - Bivalve Pesticide and PCB Method Detection Limits




                     RAW         DESIGNATOR           DBOF'B          PCB #103         PCB # 198            ALPHA            HCB               BETA           LINDANE             DEL
                    FILE                               RECOV          % RECOV          % RECOV              BHC                                BHC                                BHC
                                                                                                            (ppb)            (ppb)             (ppb)            (ppb)             (ppb)


                   Q1249P            MDL 2            67.6%             66.7%            68.7%              4.45             0.71              4.19             2.99              2.55
                   Q1250P            MDL 3            67.4%             65.5%            68.6%              4.53             0.87              3.47             3.10              2.91
                   91251P            MDL 4            68.8%             68.6%            71.9%              4.18             0.82              2.98             2.99              2.63
                   Q 1252P           MDL 5            64.0%             66.0%            67.0%              4.14             1.13              4.06             2.84              2.59
                   Q 1253P           MDL 6            67.9%             70.0%            72.2%              4.43             0.74              3.15             2.84              2.26
                   Q 1254P           MDL 7            70.9%             72.0%            72.7%              4.14             0.49              4.07             2.92              2.57
                   Q 1255P           MDL 8            64.3%             65.1%            67.2%              4.06             0.73              3.94             2.75              2.41

                   Average                                                                                  4.277            0.783             3.696            2.919             2.560
                   Variance                                                                                 0.030            0.032             0.206            0.012             0.035
                Std Deviation                                                                               0.174            0.179             0.453            0.111             0.186
               Coef of Variation                                                                            4.1%             22.9%             12.3%            3.8%              7.3%
                     MDL                                                                                    0.522            0.537             1.359            0.331             0.559
                     LCL                                                                                    0.334            0.344             0.870            0.212             0.358
                     UCL                                                                                    1.147            1.182             2.990            0.729             1.229




         00





                                                            Mussel Watch Year VI - Bivalve Pesticide and PCB Method Detection Limits



                      RAW         DESIGNATOR             HEPTA-          ALDRIN             HEPTA             Oxy-           GAMMA-            ALPHA-             TRANS-         DIELDRIN
                     FILE                                CHLOR                           EPOXIDE         CHLORDANE CHLORDANE, CHLORDANE NONACHLOR
                                                         (ppb)             (ppb)                              (ppb)            (ppb)             (ppb)            (ppb)             (ppb)


                    Q 1249P           MDL2               1.87              2.19             0.71              2.97             2.91              1.15             21.51             4.16
                    Q 1250P           MDL3               1.95              2.01             0.71              3.25             3.20              1.34             22.92             4.51
                    Q1251P            MDL4               2.10              2.13             0.61              3.04             2.87              1.19             22.41             4.61
                    91252P            MDL5               2.12              1.89             1.11              2.66             2.91              1.74             20.93             4.24
                    Q 1253P           MDL6               1.88              2.26             0.52              3.41             2.87              1.10             21.77             4.31
                    Q 1254P           MDL7               1.76              1.87             0.91              2.92             3.00              1.45             21.38             4.03
                    Q1255P            MDL8               1.59              1.80             0.91              2.80             2.80              1.74             22.10             3.96

                    Average                              1.898             2.022            0,781             3.008            2.937             1.387            21.860            4.259
                    Variance                             0.030             0.027            0.037             0.056            0.014-            0.063            0.384             0.049
                 Std Deviation                           0.172             0.164            0.191             0.238            0.120             0.251            0.620             0.221
               Coef of Variation                         9.1%              8.1%             24.5%             7.9%             4.1%              18.1%            2.8%              5.2%
                     MDL                                 0.515             0.491            0.573             0.712            0.358             0.752            1.858             0.663
                      LCL                                0.330             0.315            0.367             0.456            0.229             0.481            1.189             0.424
                      UCL                                1.134             1,081            1.262             1.567            0.788             1.653            4.088             1.458






                                                            Mussel Watch Year VI - Bivalve Pesticide and PCB Method Detection Limits




                      RAW         DESIGNATOR            CIS-              MIREX          2ADDE             4,4'DDE          2ADDD              ENDRIN           4,4'DDD           2ADDT
                    FILE                            NONACHLOR                           (O,P'DDE)         (P,P'DDE)         (OX DDD)                           (P,P'DDD)         (0,P'DDT)
                                                        (ppb)             (ppb)             (ppb)            (ppb)             (ppb)             (ppb)            (ppb)             (ppb)


                   Q 1249P            MDL2              3.24              2.21              1.83             11.49             2.30              2.89             3.58              1.12
                   Q 1250P            MDL3              3.26              2.29              1.58             11.98             2.10              2.89             3.59              1.01
                   Q1251P             MDL4              3.40              2.00              1.61             11.82             2.01              2.86             3.77              0.94
                   Q 1252P            MDL 5             3.35              2.37              1.65             11.43             2.02              2.66             3.93              1.39
                   Q 1253P            MDL6              3.19              2.54              1.62             11.38             1.78              2.66             3.62              0.91
                   Q 1254P            MDL7              3.20              2.30              1.49             11.98             1.79              2.69             3.56              1.17
                   Q1255P             MDL 8             3.26              2.00              1.72             11.95             1.62              2.40             3.58              1.20

                   Average                              3.270             2.244             1.644            11.720            1.945             2.722            3.660             1.108
                   Variance                             0.005             0.033             0.010            0.064             0.046             0.027            0.016             0.024
                 Std Deviation                          0.072             0.181             0.098            0.252             0.214             0.163            0.128             0.156
               Coef of Variation                        2.2%              8.1%              6.0%             2.2%              11.0%             6.0%             3.5%              14.1%
                      MDL                               0.217             0.543             0.295            0.756             0.642             0.488            0.384             0.468
                      LCL                               0.139             0.347             0.189            0.484             0.411             0.313            0.246             0.299
                      UCL                               0.477             1.194             0.650            1.662             1.413             1.074            0.845             1.029





                                                             Mussel Watch Year VI - Bivalve Pesticide and PCB Method Detection Limits



                      RAW          DESIGNATOR          4.4'DDT             PC13 #8         PCB # 18          PCB #28          PCB #44           PC13 #52           PCB #66          PCB #101
                     FILE                              (P,P'DDII           (CL2)             (CL3)             (CL3)            (CIA)             (CIA)              (CIA)             (CL5)
                                                         (ppb)             (ppb)             (ppb)             (ppb)            (ppb)             (ppb)              (ppb)             (ppb)


                    Q1249P             MDL 2             2.96               1.9               0.9               2.2              2.4               2.7                2.9              2.7
                    Q1250P             MDL 3             2.98               1.6               0.9               2.2              2.5               3.4                2.5              2.9
                    Q1251P             MDL 4             2.92               1.5               1.0               1.9              2.5               3.4                2.6              2.8
                    Q 1252P            MDL 5             2.93               2.1               1.4               2.0              2.5               3.7                2.5              3.1
                    Q1253P             MDL 6             2.77               1.8               1.1               2.0              2.5               3.1                2.6              2.6
                    9 1254P            MDL 7             2.78               1.5               1.1               2.1              2.5               3.2                2.6              2.9
                    Q 1255P            MDL 8             2.61               1.2               1.1               1.8              2.3               3.4                2.5              3.1

                    Average                              2.848             1.640             1.076             2,039            2.456             3.253              2.597             2.876
                    Variance                             0.016             0.078             0.030             0.014            0.006             0.094              0.017             0.029
                 Std Deviation                           0.126             0.280             0.174             0.118            0.080             0.306              0.129             0.171
               Coef of Variation                         4.4%              17.1%             16.2%             5.80/6           3.3%              9.4%               5.0%              5.9%
                      MDL                                0.379             0.839             0.522             0.354            0.241             0.917              0.386             0.512
                      LCL                                0.242             0.537             0.334             0.227            0.154             0.587              0.247             0.328
                      UCL                                0.833             1.847             1.148             0.779            0.530             2.017              0.850             1.127





                                                            Mussel Watch Year VI - Bivalve Pesticide and PCB Method Detection Limits




                     RAW         DESIGNATOR          PCB # 105       PCB# 110/77        PCB # 118        PCB # 128         PCB # 138         PCB# 126          PCB # 153        PCB # 170
                    FILE                               (CL5)             (CL5/4)           (CL5)            (CL6)              (CL6)            (CL5)            (CL6)              (CL7)
                                                       (ppb)             (ppb)             (ppb)            (ppb)              (ppb)            (ppb)            (ppb)              (ppb)


                    Q 1249P          MDL 2              3.0               3.0               3.5              2.9               8.1               1.9              5.3               INT
                    Q 1250P          MDL 3              3.2               3.6               3.5              3.0               7.8               1.5              5.6               INT
                    Q1251P           MDL 4              3.1               3,7               3.3              2.8               13.6              2.0              5.5               INT
                    Q 1252P          MDL 5              4.0               2.7               3.6              3.0               7.7               2.3              6.8               INT
                    Q 1253P          MDL 6              3.0               2.9               3.2              3.0               9.1               1.8              5.5               INT
                    Q 1254P          MDL 7              3.6               2.8               3.5              3.2               8.1               2.0              6.3               INT
                    Q1255P           MDL 8              3.6               3.4               3.2              2.7               7.9               1.7              6.2               INT

                    Average                            3.347             3.156             3,397            2.957              8.887            1.911            5.896
                    Variance                           0.128             0.138             0.024            0.018              3.871            0.058            0.275
                Std Deviation                          0.358             0.371             0.156            0.133              1.967            0.241            0.524
              Coef of Variation                        10.7%             11.8%             4.60A            4.5%               22.1%            12.6%            8.90/6
                     MDL                               1.074             1.213             0.467            0.400              5.898            0.722            1.572
                     LCL                               0.688             0.712             0.299            0,256              3.775            0.462            1.006
                     UCL                               2.363             2.449             1.028            0.880              12.976           1.589            3.458






                                                             Mussel Watch Year VI - Bivalve Pesticide and PCB Method Detection Limits




                      RAW         DESIGNATOR          PCB # 180         PC13 # 187        PCB # 195         PC13 #206         PCB #209
                     FILE                                (CL7)             (CL7)             (CL8)             (CL9)             (CLIO)
                                                         (ppb)             (ppb)             (ppb)             (ppb)             (ppb)



                    Q 1249P           MDL 2               4.2               6.1               2.6               1.2              10.0
                    Q 1250P           MDL 3               4.3               6.0               2.7               1.7              10.5
                    Q1251P            MDL 4               4.1               5.4               2.3               1.7              10.5
                    Q1252P            MDL 5               4.4               5.8               2.8               1.5              10.5
                    Q 1253P           MDL 6               4.4               6.0               1.9               1.4              10.4
                    Q1254P            MDL 7               4.4               5.6               2.5               1.4              10.0
                    Q 1255P           MDL 8               4.4               5.8               2.8               1.1              10.5

                    Average                              4.312             5.805             2.516             1.436             10.327
                    Variance                             0.014             0.056             0.087             0.039             0.038
                 Std Deviation                           0.119             0.238             0.296             0.197             0.196
               Coef of Variation                         2.8%              4.1%              11.7%             13.7%             1.90A
                      MDL                                0.358             0.712             0.886             0.591             0.587
                      LCL                                0.229             0.456             0.567             0.378             0.376
                      UCL                                0.788             1.567             1.949             1.301             1.292




I
I
I
I
I
I
I
I
I
I            Trace Metals Method Detection Limits
I
I
I
I
I
I
I
I
 ,-J,                   164





                                                           MUSSEL WATCH YEAR VI - Bivalve Trace Metals Method Detection Limits










                                           Ag (ppb)   As (ppb)   Cd (ppb) Cr (ppb)     Cu (ppb)  Fe (pprn) Hg (ppb) Mn (pprn)       Pb (ppb)   Se (ppb)   Sn (ppb) Zn (pprn)

                             OYSTER          3.220    722.63        23.3      46.6     485.55      17.21      29.71       2.65      121.04     128.16     39.78      3.96
                                             4.16     752.02        24.18     52.71    497.21      17.73      31.6        3.42      131.03     198.69     40.31      3.98
                                             4.29     811.74        24.64     62.34    506.28      18.83      31.8        3.53      134.93     201.64     44.77      4.06
                                             5.04     831.17        24.8      63.22    514.92      18.89      32.61       3.59      135.57     223.44     49.4         4.2
                                             5.36     839.53        24.99     69.08    537.12      18.97      33.85       3.64      148.8      225.12     49.61      4.27
                                             5.39     878.92        25.38     69.77    538.99      18.99      33.94       3.64      148.95     235.74     51.73      4.32
                                             5.39     889.42        25.77     78.59    546.66      20.67      34.61       3.65      171.83     267.47     56.13      4.33


                             Average         4.693    817.919       24.723    63.187   518.104     18.756     32,589      3.446     141.736    211.466    47.390     4.160
                            Variance         0.593    3276.713      0,562     100.133  465.649     1.033      2.484       0.111     233.554    1607.879   31.299     0.022
                          Std Deviation      0.770    57.243        0.749     10.007   21.579      1.016      1.576       0.334     15.282 40.098         5.595      0.147
                        Coef of Variation    16.4%     7.0%         3.0%      15.8%     4.2%       5.40A      4.8%        9.7%      10.8%      19.0%      11.8%      3.5%
                              MDL            2.309    171.613       2.247     30.000   64.694      3.047      4.725       1.000     45.817     120.215    16.773     0.440
                               LCL           1.478    109.832       1,438     19.200   41.404      1.950      3.024       0.640     29.323     76.938     10.734     0.281
                               UCL           5.080    377.549       4.943     66.000   142.326     6.703      10.396      2.200     100.797    264.473    36.900     0.967
          Cil




I
I
I
I
I
I


I
I
I           Organotin TBT18 Method Detection Limits
I
II
I
I
I
I
I
1
                       166





                                     $12 MUSSEL WATCH YEAR VI - Bivalve Organotin TBT18 Method Detection Limits



                    File Number   Description                     Tetrabutyltin     Tributyltin   Dibutyltin     Monobutyltin      O/6TPT Rec.

                                                                        ng Sn           ng Sn       ng Sn            ng Sn             %

                    T0261         SpikedTissue MDL                      68.8            146.7         68.5            5.5              66
                    T0262         SpikedTissue MDL                      70.8            154.9         72.9            5.0              67
                    T0263         Spiked TIssue MDL                     64.8            146.9         74.1            6.3              97
                    T0264         SpikedTissue MDL                      73.0            146.8         82.8            7.6              44
                    T0265         SpikedTissue MDL                      68.3            151.8         94.7            6.7              43
                    T0266         SpIkedTissue MDL                      70.5            165.8         73.7            5.3              56
                    T0267         SpikedTissue MDL                      70.5            150.5         70.6            3.5              63
                    T0268         SpikedTissue MDL                      70.3            164.3         76.0            2.9              19

                    T0269         BlankTissue                           ND              73             5              ND               45
                    T0270         BlankTissue                           ND              75            ND              ND               53
                    T0271         Blanknssue                            ND              76             3              ND               62
                    T,0272        BlankTissue                           ND              73             5               2               58

                    T0273         Blank                                 ND              ND             4              ND               65
                    T0274         Blank                                 ND               1             3              ND               61

                    T0275         Spike Blank                           70.9            74.9          73.5            6.7              67
                    T0276         Spike Blank                           65.3            67.0          68.6            5.8              73

                    SpikeTissue                  Average Value          69.6            153.5         76.7            5.4
                                            Standard Deviation          2.4             7.7           8.4             1.6

                    BlankTissue                  Average Value          ND              74.3          3.3             0.5
                                            Standard Deviation                          1.5           2.4             1.0

                    Spike Blank                  Average Value          68.0            71.0          71.5            6.5
                                            Standard Deviation          4.2             5.7           3.5             0.7

                    Average %     AygTis - Avg Blk'ns/ .60 ng           116%            132%          122%            8%

                                                            MDL         7.2             23.1          25.2            4.8
                                                     MDL (LCL)          5.0             15.9          17.4            3.3
                                                     MDL (UCL)          13.8            44.4          48.4            9.2




I
I
I
I
I
I
I
I
I
I         Percent Lipids and Dry Weight Data
I
I
I
I
I
I
I
1
                        168
 A






                             MUSSEL WATCH YEAR V1 - Bivalve Percent Lipids and Dry Weight Data



                           SITE               STATION          % DRY WEIGHT % WET WEIGHT                    % LIPIDS



                           LMSB                    1                15.58                84.42                 4.04
                           LMSB                    2                16.67                83.33                 4.41
                           LMSB                    3                14.47                85.53                 3.24
                           ccic                    1                16.67                83.33                 4.73
                           ccic                    2                17.50                82.50                 6.11
                           ccic                    3                17.27                82.73                 5.19
                           ABLR                    1                23.75                76.25                 6.17
                           ABLR                    2                22.61                77.39                 ND
                           ABLR                    3                23.20                76.80                 7.00
                           CBCR                    1                15.94                84.06                 3.77
                           CBCR                    2                18.75                81.25                 3.49
                           CBCR                    3                19.75                80.25                 4.06
                           MBAR                    1                20.16                79.84                 7.03
                           MBAR                    2                23.26                76.74                 7.50
                           MBAR                    3                22.54                77.46                 8.47
                           SAPP                    1                16.83                83.17                 7.00
                           SAPP                    2                19.40                80.60                 7.40
                           SAPP                    3                17.72                82.28                 6.61
                           SAMP                    1                24.04                75.96                 9.16
                           SAMP                    2                22.52                77.48                 6.22
                           SAMP                    3                23.89                76.11                 8.22
                           ESSP                    1                18.68                81.32                 6.09
                           ESSP                    2                18.18                81.82                 5.88
                           ESSP                    3                17.86                82.14                 7.19
                           MBLR                    1                16.48                83.52                 5.38
                           MBLR                    2                12.50                87.50                 4.38
                           MBLR                    3                14.58                85.42                 4.69
                           MBGP                    1                21.24                78.76                 6.90
                           MBGP                    2                20.00                80.00                 6.40
                           MBGP                    3                23.38                76.62                 6.91
                           MBTP                    1                17.W                 82.03                 6.22
                           MBTP                    2                18.39                81.61                 5.49
                           MBTP                    3                19.54                80.46                 6.15
                           MBEM                    2                14.56                85.44                 3.95
                           MBEM                    3                16.85                83.15                 4.07
                           MBEM                    1                14.29                85.71                 3.39
                           BRCL                    1                16.83                83.17                 4.23
                           BRCL                    2                12.96                87.04                 3.39
                           BRCL                    3                15.00                85.00                 3.46
                           BRFS                    1                15.00                85.00                 4.08
                           BRFS                    2                13.04                86.96                 3.93
                           BRFS                    3                9.17                 90.83                 2.64
                           GBCR                    1                15.89                84.11                 5.21
                           GBCR                    2                15.53                84.47                 4.64
                           GBCR                    3                15.49                84.51                 4.45
                           GBOB                    1                16.85                83.15                 6.33
                           GBOB                    2                15.79                84.21                 6.28
                           GBOB                    3                15.73                84.27                 8.09
                           GBTD                    1                21.37                78.63                 8.62
                           GBTD                    2                Rm                   75.00                 8.40






                            MUSSEL WATCH YEAR V1 - Bivalve Percent Lipids and Dry Weight Data




                          SITE              STATION          % DRY WEIGHT % WET WEIGHT                   % LrPIDS



                          GBTD                   3                 22.44               77.56                 8.11
                          GBYC                   1                 19.72               80.28                 10.90
                          GBYC                   2                 17.86               82.14                 14.15
                          GBYC                   3                 19.61               80.39                 11.50
                          GBSC                   1                 14.87               85.13                 12.70
                          GBSC                   2                 15.47               84.53                 11.70
                          GBSC                   3                 14.13               85.87                 13.30
                          GBHR                   1                 20.51               79.49                 ND
                          GBHR                   2                 21.74               78.26                 8.39
                          GBHR                   3                 19.12               80.88                 8.89
                          SLBB                   1                 12.12               87.88                 7.55
                          SLBB                   2                 13.33               86.67                 10.50
                          SLBB                   3                 13.13               86.87                 5.68
                          CL&J                   1                 20.99               79.01                 6.02
                          CLSJ                   2                 15.50               84.50                 4.09
                          CLSIJ                  3                 16.67               83.33                 4.19
                          CLLC                   1                 22.34               77.66                 9.52
                          CLLC                   2                 22.22               77.78                 5.58
                          CLLC                   3                 22.67               77.33                 7.98
                          JHJH                   1                 19.72               80.28                 6.97
                          JHJH                   2                 17.86               82.14                 9.23
                          JHJH                   3                 17.20               82.80                 8.66
                          VBSP                   1                 17.86               82.14                 9.51
                          VBSP                   2                 17.33               82.67                 8.63
                          VBSP                   3                 18.42               81.58                 9.94
                          ABOB                   1                 17.83               82.17                 10.50
                          ABOB                   2                 16.67               83.33                 10.20
                          ABOB                   3                 21.38               78.62                 9.94
                          CLCL                   1                 18.75               81.25                 8.76
                          CLCL                   2                 20.78               79.22                 9.38
                          CLCL                   3                 21.05               78.95                 9.41
                          TBLB                   1                 16.92               83.08                 5.58
                          TBLB                   2                 14.75               85.25                 6.91
                          TBLB                   3                 16.09               83.91                 4.59
                          TBLF                   1                 22.50               77.50                 6.73
                          TBLF                   2                 23.53               76.47                 7.24
                          TBLF                   3                 23.53               76.47                 7.45
                          BBSD                   1                 15.49               84.51                 8.53
                          BBSD                   2                 16.90               83.10                 8.31
                          BBSD                   3                 18.57               81.43                 8.34
                          BBMB                   1                 18.10               81.90                 6.29
                          BBMB                   2                 14.73               85.27                 5.29
                          BBMB                   3                 15.63               84.37                 5.72
                          MRTP                   1                 16.07               83.93                 8.62
                          MRTP                   2                 20.37               79.63                 9.36
                          MRT?                   3                 18.03               81.97                 6.09
                          BSSI                   1                 15.73               84.27                 8.88
                          BSSI                   2                 15.32               84.68                 9.73
                          BSSI                   3                 18.75               81.25                 7.81
                          BSBG                   1                 J7-M                82.02                 4.52






                            MUSSEL WATCH YEAR VI - Bivalve Percent Lipids and Dry                  Weight Data




                           SITE              STATION          % DRY WEIGHT o/o WET WEIGHT                  % LEPIDS



                           BSBG                   2                 17.86               82.14                 11.90
                           BSBG                   3                 17.05               82.95                 4.01
                           LBMP                   1                 13.70               86.30                 5.32
                           LBMP                   2                 12.32               87.68                 11.10
                           LBMP                   3                 15.28               84.72                 5.38

                           LPGO                   1                 13.36               86.64                 10.30
                           LPGO                   2                 12.44               87.56                 8.13
                           LPGO                   3                 13.43               86.57                 8.05

                           mspc                   1                 14.09               85.91                 9.42

                           mspc                   2                 18.18               81.82                 11.00
                           mspc                   3                 18.18               81.82                 8.71
                           MSBB                   1                 14.87               85.13                 8.52
                           MSBB                   2                 13.64               86.36                 15.10
                           MSBB                   3                 13.24               86.76                 7.09
                           MSPB                   1                 13.75               86.25                 4.83
                           MSPB                   2                 13.89               86.11                 6.35

                           MSPB                   3                 13.33               86.67                 3.81
                           MBCP                   1                 20.25               79.75                 12.30
                           MBCP                   2                 23.33               76.67                 10.80
                           MBCP                   3                 20.31               79.69                 10.80
                           MBHI                   1                 10.53               89.47                 8.34
                           MBHI                   2                 13.12               86.88                 7.72

                           MBH1                   3                 8.82                91.18                 6.95
                           PBPH                   1                 20.29               79.71                 11.50

                           PBPH                   2                 13.66               86.34                 LOST
                           PBPH                   3                 14.25               85.75                 15.50
                           PBIB                   1                 24.52               75.48                 12.70
                           P13113                 2                 19.20               80.80                 14.90
                           PBIB                   3                 18.07               81.93                 16.20
                           CBJB                   1                 13.45               86.55                 6.36
                           CBJB                   2                 13.59               86.41                 6.54
                           CBJB                   3                 12.54               87.46                 6.38
                           CBSR                   1                  ND                   ND                  ND
                           CBSR                   2                 13.69               86.31                 9.12
                           CBSR                   3                 14.60               85.40                 7.87
                           CBSP                   1                                     87.77                 6.32
                           CBSP                   2                 14.91               85.09                 6.64
                           CBSP                   3                 12.57               87.43                 6.26
                           PCLO                   1                 14.64               85.36                 9.11
                           PCLO                   2                 10.48               89.52                 22.70
                           PCLO                   3                 14.66               85.34                 14.90
                           SAWB                   1                 16.58               83.42                 10.60
                           SAVvrB                 2                 10.59               89.41                 14.90
                           SAVvTB                 3                 11.75               88.25                 13.30
                           APDB                   1                 10.86               89.14                 11.80
                           APDB                   2                 11.38               88.62                 8.29
                           APDB                   3                 10.56               89.44                 11.60
                           APCP                   1                 13.97               86.03                 8.67
                           APCP                   2                 13.85               86.15                 7.21
                           APCP                   3                 1&m                 83.74                 8.28






                            MUSSEL WATCH YEAR VI - Bivalve Percent Lipids and Dry Weight Data



                           SITE              STATION          % DRY WEIGHT % WET WEIGHT                   % LIPIDS


                           AESP                    2                 11.22               88.78                5.54
                           AESP                    3                 10.02               89.98                6.03
                           AESP                    1                 10.04               89.96                7.65
                           CKBP                    1                 12.02               87.98                4.65
                           CKBP                    2                 13.40               86.60                4.72
                           CKBP                    3                 14.30               85.70                3.81
                           TBNP                    1                 19.39               80.61                8.31
                           TBNP                    2                 17.86               82.14                8.46
                           TBNP                    3                 17.56               82.44                7.43
                           TBMK                    1                 21.02               78.98                9.06
                           T13MK                   2                 10.81               89.19                18.40
                           TBMK                    3                 12.04               87.96                18.80
                           TBPB                    1                 15.39               84.61                6.99
                           TBPB                    2                 11.40               88.60                10.90
                           TBPB                    3                 16.86               83.14                6.59
                           TBOT                    1                 9.07                90.93                7.24
                           TBOT                    2                 9.09                90.91                6.08
                           TBOT                    3                 9.18                90.82                6.21
                           TBKA                    1                 13.52               86.48                7.47
                           TBKA                    2                 13.92               86.08                5.80
                           TBKA                    3                 10.20               89.80                9.53
                           TBCB                    1                 16.42               83.58                8.44
                           TBCB                    2                 10.41               89.59                16.70
                           TBCB                    3                 16.41               83.59                10.90
                           CBBI                    1                 15.28               84.72                9.23
                           CBBI                    2                 13.84               86.16                7.09
                           CBBI                    3                 16.85               83.15                5.01
                           CBFM                    1                 15.46               84.54                8.14
                           CBFM                    2                 12.17               87.83                8.25
                           CBFM                    3                 12.04               87.96                5.67
                           NBNB                    1                 14.65               85.35                8.20
                           NBNB                    2                 15.61               84.39                6.17
                           NBNB                    3                 16.02               83.98                7.42
                           RBHC                    1                 15.74               84.26                8.11
                           RBHC                    2                 15.76               84.24                8.86
                           RBHC                    3                 16.09               83.91                8.11
                           EVFU                    1                 8.99                91.01                5.03
                           EVFU                    2                 15.88               84.12                3.22
                           EVFU                    3                 15.48               84.52                4.01
                           BHKF                    1                 19.61               80.39                4.62
                           BHKF                    2                 18.06               81.94                5.49
                           BHKF                    3                 16.39               83.61                4.85










                                                                     172




 I
 i
 I
 I
 I
 I
 I
 I
 I
                        Percent Lipids - Duplicates and Spikes
 I
 I
 I
 I
 I
 I
 I
 I
 1
                                         173

1
 A






                               MUSSEL WATCH YEAR VI - Bivalve Percent Lipids - Duplicates and Spikes




                          SITE AND STATION          TYPE        % DRY WEIGHT % WET WEIGHT                    % LEPIDS



                                 SAMP-2             QAQC               22.52              77.48                 7.09
                                 SAMP-2              SPK               22.52              77.48                 7.67


                                 SAMP-3             QAQC               23.89              76.11                 10.20
                                 SAMP-3              SPK               23.89              76.11                 9.79


                                 GBYC-2             QAQC               17.86              82.14                 10.80
                                 GBYC-2              SPK               17.86              82.14                 14.20


                                 GBYC-3             QAQC               19.61              80.39                 11.00
                                 GBYC-3              SPK               19.61              80.39                 11.10


                                 GBHR-1             QAQC               20.51              79.49                 8.28
                                 GBHR- I             SPK               20.51              79.49                 9.40


                                 GBHR-2             QAQC               21.74              78.26                 8.37
                                 GBHR-2              SPK               21.74              78.26                 9.11


                                 VBSP-i             QAQC               17.86              82.14                 11.00
                                 VBSP-1              SPK               17.86              82.14                 9.82


                                 BBSD-3             QAQC               18.57              81.43                 10.60
                                 BBSD-3              SPK               18.57              81.43                 9.67


                                 BSSI-2             QAQC               15.32              84.68                 8.31
                                 BSSI-2              SPK               15.32              84.68                 8.17


                                 LPGO- I            QAQC               13.34              86.66                 12.00
                                 LPGO-2             QAQC               12.44              87.56                 8.12


                                 MSPC-l             QAQC               14.09              85.91                 8.82
                                 MSPC-l              SPK               14.09              85.91                 8.30


                                 MBHI-3             gAQC               8.82               91.18                 7.47
                                 MBF11-3             SPK               8.82               91.18                 7.80


                                 PBIB-1             QAQC               24.44              75.56                 12.90


                                 PBIB-3             QAQC               18.07              81.93                 15.40


                                 SAVM-2             QAQC               10.59              89.41                 13.30


                                 TBMK-1             QAQC               20.42              79.58                 8.36


                                 TBCB-2             QAQC               10.41              89.59                 16.33


                                 TBCB-3             QAQC               16.41              83.59                 9.47


                                 BHKF-3             QAQC               16.81              83.19                 4.12
                                 BHKF-3              SPK               19.83              80.17                 2.39
















                                                                       174




 I
 I
 I
 i
 I
 I
 I
 I
 I
 I                    Butyltin Concentrations
 I
 I
 I
 I
 I
 I
 I
 1
                                    175
t, @



                                        we m mm m m mm                                       m m @ m @
                                    MUSSELL WATCH YEAR VI - Bivalve Butyltin Concentrations




                             TETRABUTYLTIN     TRIBUTYLTIN       DIBUTYLTIN      MONOBUTYLTIN     TOTAL BUTYLTIN
                   SITE         ng Sn/g          ng Sn/g           ng Sn/g          ng Sn/g          ng Sn/g


                   LMSB            0                42                12               0                54
                   CCIC            1                267               79               29               375
                   ABLR            0                1                 1                1                3
                   CBCR            1                0                 3                5                8
                   SAPP            1                6                 0                4                10
                   SAMP            3                2                 7                3                12
                   MBAR            0                1                 7                8                16
                   ESSP            2                7                 0                0                7
                   MBLR            0                117               11               5                133
                   MBGP            0                62                8                1                71
                   MBTP            0                12                0                0                12
                   MBEM            2                7                 7                7                22
                   BRCL            9                40                17               7                63
                   BRFS            7                578               103              22               702
                   GBCR            1                197               31               8                236
                   GBOB            3                ill               27               11               149
                   GBTD            5                280               23               6                309
                   GBYC            5                544               45               10               599
                   GBHR            2                42                14               2                58
                   SLBB            2                135               17               3                155
                   CLSJ            1                59                3                3                66
                   CLLC            1                208               15               4                228
                   JHJH            0                9                 8                1                19
                   VBSP            4                4                 7                0                10
                   ABOB            0                4                 1                2                7
                   CLCL            1                3                 2                1                6
                   TBLB            1                10                0                0                10
                   TBLF            0                3                 0                0                3
                   BBSD            0                12                4                5                21
                   BBMB           38                1165              114              21               1300
                   MRTP            0                79                5                0                83



                        mmm @@ M@ go mm m
                                       MUSSELL WATCH YEAR VI - Bivalve Butyltin Concentrations




                               TETRABUTYLTIN        TRIBUTYLTIN        DIBUTYLnN        MONOBUTYLTIN       TOTAL BUTYLTIN
                     SITE          ng Sn/g            ng Sn/g            ng Sn/g            ng Sn/g            ng Sn/g



                     BSSI              0                 64                 8                  0                  72
                     BSBG              1                 6                  2                  3                  11
                     LBMP              0                 13                 0                  3                  16
                     LPGO              0                 484                61                 24                 568
                     MSPC              1                 19                 4                  10                 34
                     MSBB              0                 193                21                 0                  214
                     MSPB              4                 260                29                 9                  298
                     MBCP              1                 35                 0                  3                  38
                     MBHI              1                 179                30                 0                  208
                     PBPH              1                 28                 2                  1                  31
                     PBIB              1                 4                  1                  0                  5
                     CBJB              3                 700                71                 7                  778
                     CBSP              4                 58                 23                 0                  82
                     CBSR              0                 4                  0                  0                  4
                     PCLO              3                 16                 8                  0                  24
                     SAVVrB            1                 199                39                 5                  243
                     APDB              1                 7                  1                  0                  8
                     APCP              0                 35                 9                  7                  51
                     AESP              1                 22                 3                  1                  26
                     CKBP              4                 0                  6                  9                  15
                     TBMK              0                 5                  1                  0                  6
                     TBPB              2                 85                 15                 0                  100
                     TBOT              2                 19                 5                  0                  25
                     TBNP              0                 61                 16                 3                  80
                     TBCB              1                 2                  2                  0                  3
                     TBKA              1                 785                196                42                 1022
                     CBBI              0                 78'                22                 0                  100
                     CBFM              0                 270                66                 6                  342
                     NBNB              0                 845                146                6                  996
                     RBHC              1                 50                 16                 2                  67
                     EVFU              1                 39                 5                  7                  51





                                    MUSSELL WATCH YEAR VI - Bivalve Butyltin Concentrations




                             TETRABUTIfLTIN     TRIBUTYLTIN      DIBUTYLMN       MONOBUTYLIIN     TOTAL BUTYLTIN
                   SITE          ng Sn/g          ng Sn/g          ng Sn/g           ng Sn/g          ng Sn/g



                   BHKF            0                58               23                52               133


















      00




I
I
I
I
I
I
I
I
I
I       Infection, Condition and Gonadal Data
I
I
I
I
I
I
I
I
I
                       179

1
1,



                                        m lilt m m m m m m m m m mm
                                             MUSSEL WATCH YEAR VI - Bivalve Infection, Condition and Gonadal Data





              SITE NUMBER SITE         % INFECTION        MEDIAN             5%              95%            MEAN                STD       MEDIAN              5%
                                                        INFECTION        CONF LIM        CONF LIM           LENGTH                       CONDition      CONF LIM




                     I         LMSB          100            1.67             1.67            1.67           6.66            1.5364           5                4
                     3         CCIC          100              2              1.67             2             6.515           1.2407           4                4
                     4         ABLR          70             0.5              0.33            0.67           4.96            0.77003          4                3
                     5         CBCR          100            2.165             2              2.5            5.235           0.80356          4                4
                     8         MBAR          100            1.67             1.67             2             6.0733          1.078            4                4
                     6         SAPP          50               0               0              .0.33          5.7933          1.1836           4                4
                     7         SAMP          80             0.67             0.33            0.67           7.775           0.9568           3                3
                     9         ESSP        98.333           1.67             1.67             2             7.1567          1.0823           4                4
                     11        MBLR          100            1.33             1.33            1.67           6.9033          1.1668           4                4
                     12        MBGP        48.333             0               0              0.33           5.3883          0.9939           4                3
                     13        MBfP        98.333           1.33             1.33            1.67           7.01            1.3637           3                3
                     14        MBEM          100            2.33              2              2.33           7.9667          1.0903           4                4
                     15        BRCL        98.333           1.67             1.67            1.835          7.4267          0.9277           5                4
                     16        BRFS        98.333           1.835            1.67             2             8.37            1.8835           5                4
         00          17        GBCR          100            1.835            1.67             2             6.9633          0.94581          4                4
         0           18        GBOB          100            1.67             1.67             2             6.7233          0.82654          4                4
                     19        GBTD          35               0               0               0             7.4833          1.3177           2                2
                     20        GBYC        63.333           0.33             0.33            0.67           8.8367          1.3164           3                2
                     59        GBSC        6.6667             0               0               0             5.935           0.94829          4                4
                     22        GBHR        21.667             0               0               0             7.765           0.84107          2                2
                     23        SLBB          80             0.5              0.33            0.67           8.75            1.8312           3                2
                     24        CLSJ          100            1.67             1.33            1.67           8.1917          1.5104           3                3
                     25        CLLC        93.333             1              0.67            1.33           7.645           1.5433          2.5               2
                     26        JHJH          100            2.33              2              2.67           7.8617          1.5581           2                2
                     27        VBSP          10               0               0               0             8.205           1.1482           3                3
                     28        ABOB          85             1.67             1.33            1.67           8.3033          1.6524           3                2
                     29        CLCL        33.333             0               0               0             7.0333          1.5593           3                3
                     30        TBLB        96.667           1.67             1.33            1.67           7.6367          1.1056           3                3
                     31        TBLF        98.333           1.33             1.165           1.5            6.3333          0.58242          3                3
                     @32       BBSD        53.333           0.33              0              0.67           8.0367          1.0559           3                2
                     33        BBMB          100            1.67             1.67            1.67           8.5517          1.4547           3                3
                     34        MR`I?       3.3333             0               0               0             4.9733          0.8658           3                3
                     35        BSSI        96.667           1.67             1.67            1.67           8.865           1.3714           2                2
                     36        BSBG        96.667           1.67             1.33             2             5.8633          0.78632          3                3





                                             MUSSEL WATCH YEAR VI - Bivalve Infection, Condition and Gonadal Data




             SITE NUMBER SITE % INFECTION                 MEDLAN             5%             95%             MEAN               STD       MEDIAN               5%
                                                        INFECTION        CONF LIM        CONF LIM           LENGTH                      CONDition       CONF LIM


                    37         LBMP       48.333              0               0             0.33            6.1667         1.0864            3                3
                    38         LPGO       47.458              0               0             0.33            6.3881           1.174           4                3
                    39         MSPC          45               0               0             0.33            7.6867         1.3503            3                3
                    40         MSBB       98.333            1.67             1.67           1.67            7.6083         1.2828            3                3
                    41         MSP13         100            1.67             1.33           1.67            7.6067         1.0431            3                3
                    42         MBCP       31.667              0               0               0             6.1333         0.98405           4                3
                    43         MBHI          10               0               0               0             7.8583         0.90222           3                3
                    44         PBPH       6.6667              0               0               0             5.8283         0.94314           3                3
                    46         PBIB          0                0               0               0             6.545          0.61076           3                3
                    47         CBJB          35               0               0               0             5.775          0.92875           7                7
                    49         CBSR          100            1.67             1.33           1.67            6.485          1.0588            5                4
                    48         CBSP          20               0               0               0             7.01           1.4946            7                7
                    51         PCLO       93.333            1.67             1.33           1.67            7.2967         1.3958            3                3
                    52         SAWB          95               1              0.835          1.33            5.4033         0.9074            3                3
        00          53         APD13      91.667              1              0.67             1             6.675          0.90397           3                3
          d         54         APCP          90             1.33              1             1.33            6.345          0.87864           4                4
                    55         AESP          90               1              0.67             1             7.05           0.92489           4                4
                    56         CKBP       98.333            1.33              1             1.33            5.6417         0.93306           7                6
                    60         TBNP       91.667              1              0.67             1               5.9            1.523           5                5
                    57         TBMK          70             0.33             0.33           0.67            6.4317         0.9155            4                4
                    58         TBPB          90               1              0.67           1.67            4.5733         0.73735           5                5
                    59         TBOT       78.333              1              0.67             1             6.6917         1.0785            5                5
                    62         TBKA       98.333              1               1             1.165           6@01           0.88273           5                5
                    61         TBCB       91.667            0.67             0.67           0.67            6.5017         0.93437           5                4
                    63         CBBI       96.667            0.67             0.67           0.67            5.7017         0.88614           4                4
                    64         CBFM          75             0.67             0.33           0.67            6.27           1.3299            4                4
                    65         NBNB       78.333            0.67             0.67           0.67            5.66           0.99834           5                4
                    66         RBHC       66.667            0.33             0.33           0.67            5.4367         0.84672           4                4
                    67         EVFU          75             0.67             0.33           0.67            6.8633         0.92626           4                4
                    68         BHKF



                                            m mm mm mm m mm m
                                          MUSSEL WATCH YEAR VI - Bivalve Infection, Condition and Gonadal Data





            SITE NUMBER SITE            95%          COND        % FEMALE       % MALE       % STAGE I % STAGE 2 % STAGE 3 % STAGE 4
                                     CONF LIM         INDEX



                    I       LMSB          5          0.06764        53.333        6.667          0             0             0             100
                    3       CCIC          4          0.10182        53.333        26.667       33.333          0             0           66.667
                    4       ABLR          4          0.14406        53.333        13.333         40            0             0             60
                    5       CBCR          4          0.098683       6.667           0          6.667           0             0           93.333
                    8       MBAR          4          0.08475         80           6.667        73.333          0             0           26.667
                    6       SAPP          4          0.07615        26.667        6.667          40            0             0             60
                    7       SAMP          3          0.12548        73.333          20         73.333          0             0           26.667
                    9       ESSP          4          0.090744       33.333          0          46.667          0             0           53.333
                    11      MBLR          4          0.067844       26.667          0          6.667           0             0           93.333
                    12      MBGP          4          0.10351        86.667        13.333       93.333          0             0           6.667
                    13      MBIP          4          0.078672       93.333        6.667        6.667         6.667           0           86.667
                    14      MBEM          4          0.062163       6.667         13.333       46.667          0             0           53.333
                    15      BRCL          5          0.099323       13.333        6.667          0             0             0             100
                    16      BRFS          5          0.062089       6.667         6.667        13.333          0             0           86.667
        00          17      GBCR          4          0.072324       33.333        6.667          0             0             0             100
        tQ          18      GBOB          4          0.071259       46.667          20           20            0             0             80
                    19      GBTD          2          0.11222        33.333        33.333       13.333          0             0           86.667
                    20      GBYC          3          0.11519         80             0          53.333          0             0           46.667
                    59      GBSC          4          0.094219       73.333        13.333       73.333          0             0           26.667
                    22      GBHR          2          0.10047        66.667        13.333       6.667           0             0           93.333
                    23      SLBB          3          0.071603        60             0            60            0             0             40
                    24      CL&J          4          0.086005        20           6.667        6.667           0             0           93.333
                    25      CLLC          3          0.11406        66.667        26.667       13.333          0             0           86.667
                    26      JHJH         2.5         0.095791       46.667        6.667        46.667        6.667           0           46.667
                    27      VBSP          3          0.11008        33.333        26.667       73.333          0             0           26.667
                    28      ABOB          3          0.11558        86.667          0          93.333          0             0           6.667
                    29      CLCL          3          0.11249        66.667          0            60            0             0             40
                    30      TBLB          3          0.10555        7.143         7.143        42.857          0             0           57.714
                    31      TBLF          3          0.099063       66.667        33.333       66.667        26.667          0           6.667
                    32      BBSD          3          0.12911         80             20         93.333        6.667           0             0
                    33      BBMB          3          0.079458        40           6.667        13.333          0             0           86.667
                    34      MRTP          3          0.11354        46.667        33.333         0             0             0             100
                    35      BSSI          2          0.10581        73.333        6.667          20            0             0             80
                    36      BSBG          3          0.075475       66.667        13.333         60            0             0             40



   Imimmmmm mm m m m m m m m M@m@
                                         MUSSEL WATCH YEAR VI - Bivalve Infection, Condition and Gonadal Data





            SITE NUMBER     SITE        95%          COND        % FEMALE       % MALE      % STAGE 1 % STAGE 2 % STAGE 3 % STAGE 4
                                     CONF LIM        INDEX



                  37        LBMP         3           0.10077       57.143          0           21.429          0             0           78.571
                  38        LPGO         4           0.076832      66.667          20          13.333          0             0           86.667
                  39        MSPC         3           0.11905       86.667        6.667         66.667          0             0           26.667
                  40        MSBB         3           0.13022       53.333        13.333        86.667          0             0           6.667
                  41        MSPB         4           0.10622       46.667        6.667           60            0             0            40
                  42        MBCP         4           0.09497       86.667        6.667         53.333        13.333          0           33.333
                  43        MBHI         3           0.12596       66.667          0           53.333          0             0           46.667
                  44        PBPH         4           0.078475      66.667        33.333          40            20            0            40
                  46        PBIB         4           0,10908       33.333        66.667        6.667           0             0           93.333
                  47        CBJB         8           0.080021      66.667        6.667           40          6.667           0           53.333
                  49        CBSR         5           0.09606       73.333        6.667           40            0             0            60
                  48        CBSP         7.5         0.066471      86.667          0           73.333          0             0           26.667
                  51        PCLO         4           0.12779       33.333        26.667        66.667          0             0           33.333
                  52        SAWB         3           0.12335       66.667        26.667        86.667        6.667           0           6.667
        00        53        APDB         3           0.10194       86.667        6.667         86.667          0             0           13.333
                  54        APCP         4           0.11096         60          6.667           60            0             0            40
                  55        AESP         5           0.10523       93.333        6.667         66.667          0             0           33.333
                  56        CKBP         7           0.073857      46.667        6.667           20            0             0            80
                  60        TBNP         5           0.13512       46.667          20          26.667          0             0           73.333
                  57        TBMK         4           0.18815       33.333        33.333        46.667        6.667           0           46.667
                  58        TBPB         6            0.112          20          26.667        26.667        13.333          0            60
                  59        TBOT         5           0.06721         40            0             0             0             0            100
                  62        TBKA         5           0.091896        40            0             20            0             0            80
                  61        TBCB         5           0.12483       26.667        6.667           40          6.667           0           53.333
                  63        CBBI         4           0.09219         40            20          73.333          0             0           26.667
                  64        CBFM         5           0.069618        80          13.333          40            20            0            40
                  65        NBNB         5           0.10202       46.667        33.333        6.667           0             0           93.333
                  66        RBHC         4           0.12179       46.667        26.667        46.667        13.333          0            40
                  67        EVFU         5           0.076869      53.333        26.667        13.333        13.333        6.667         66.667
                  68        BHKF































                                                                                                                                                        DATE DUE

























                                                                                                                            GAYLORD No. 2333                                                          PRI7171D 1% 'J S A

























                                                                                                                                                        3 6668 14106 7381