[From the U.S. Government Printing Office, www.gpo.gov]
NOAA NATIONAL STATUS AND TRENDS Musse Watc Project Year 10 Dioxin & Furan Data Report The Geochemical & Environmental Research Group h"IM, R M 0, S, 10 Asof+, "ng a z@M@ R K, n R w f7t P,- i@@ 2`5 R A, 1, k "-,im g g'@ ""ggg lli"J M" "V" - Rill n HIM ............... 'I'MRwE R "4 M-m w t . ........ WEST EAST COAST OAST QH U 541.5 U L C65 -M@ GRg@ N3 u",@""Hk --; Ll 1: 1K Ll 1995 ST---@ SEPTEMBER 1995 PCDD/PCDF Analysis Page 1 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Samples LAB SAMPLE ID K9431 CLIENT SAMPLE ID AESP INSTRUMENT DATA FILE 50705LCA04-S8 WET WEIGHT 10.00 DRY WEIGHT 0.79 PERCENT SOLIDS 7.9 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX0202 EXTRACTION DATE 4-6-75 ANALYSIS DATE 7-5-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 1.81 12.7 ND 1,2,3,7,8-PeCDF 2.80 63.6 ND 2,3,4,7,8-PeCDF 3.56 63.6 ND 1,2,3,4,7,8-HxCDF 2.13 63.6 ND 1,2,3,6,7,8-HxCDF 2.04 63.6 ND 2,3,4,6,7,8-HxCDF 2.49 63.6 ND 1,2,3,7,8,9-HxCD .F 7.44 3.42 63.6-- J 1,2,3,4,6,718-HpCDF 2.77 63.6' ND 1,2,3,4,7,8,9-HpCDF 3.21 63.6 ND OCDF 8.49 127 ND 2,3,7,8-TCDD 2.49 12.7 ND 1,2,3,7,8-PeCDD 4.23 63.6 ND 1,2,3,4,7,8-HxCDD 5.33 63.6 ND 1,2,3,6,7,8-HxCDD 5.07 63.6 ND 1,2,3,7,8,9-HxCDD 5.23 63.6 ND 1,2,3,4,6,7,8-HpCDD 6.08 3.95 63.6 1 OCDD 16.3 5.29 127 1 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 54 13C-1,2,3,7,8-PeCDF 64 13C-2,3,4,7,8-PeCDF 62 13C-1,2,3,4,7,8-HxCDF 58 13C-1,2,3,6,7,8-HxCDF 60 13C-2,3,4,6,7,8-HxCDF 58 13C-1,2,3,7,8,9-HxCDF 57 13C-1,2,3,4,6,7,8-HpCDF 59 13C-1,2,3,4,7,8,9-HpCDF 61 13C-2,3,7,8-TCDD 54 13C-1,2,3,7,8-PeCDD 61 13C-1,2,3,4,7,8-HxCDD 58 13C-1,2,3,6,7,8-HxCDD 59 3C-1,2,3,4,6,7,8-HpCDD 59 13C-OCDD 50 GERG/TAMU Date: 7/24/95 PCDD/PCDF Analysis Page 2 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Samples LAB SAMPLE ID K9433 CLIENT SAMPLE ID APCP INSTRUMENT DATA FILE 50705LCA04-S9 WET WEIGHT 10.19 DRY WEIGHT 0.91 PERCENT SOLIDS 9.0 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX0202 EXTRACTION DATE 4-6-75 ANALYSIS DATE 7-5-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 2.13 1.25 11.0 1 1,2,3,7,8-PeCDF 2.22 .2.21 54.8 1 2,3,4,7,8-PeCDF 3.08 54.8 ND 1,2,3,4,7,8-HxCDF 1.39 54.8 ND 1,2,3,6,7,8-HxCDF 2.50 1.32 54.8 1 2,3,4,6,7,8-HxCDF. 2.47 1.61 54.8 .-82 4 54.8 1 1,2,3,7,8,9-@Hxcb.F -.6 .2.2 1 2,3,4-6,7@8-HpCDF' 2.57 54.-B ND 1:2,3,4:7,8:9-HpCDF 2.43 54.8 ND OCDF 6.22 110 ND 2,3,7,8-TCDD 2.48 11.0 ND 1,2,3,7,8-PeCDD 4.20 2.99 54.8 1 1,2,3,4,7,8-HxCDD 3.51 54.8 ND 1,2,3,6,7,8-HxCDD 3.54 54.8 ND 1,2,3,7,8,9-HxCDD 3.56 54.8 ND 1,2,3,4,6,7,8-HpCDD 12.1 2.84 54.8 1 OCDD 80.8 4.83 110 1 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 63 13C-1,2,3,7,8-PeCDF 74 13C-2,3,4,7,8-PeCDF 74 13C-1,2,3,4,7,8-HxCDF 64 13C-1,2,3,6,7,8-HxCDF 68 13C-2,3,4,6,7,8-HxCDF 66 13C-1,2,3,7,8,9-HxCDF 64 13C-1,2,3,4,6,7,8-HpCDF 68 13C-1,2,3,4,7,8,9-HpCDF 74 13C-2,3,7,8-TCDD 7.1 13C-1,2,3,7,8-PeCDD 73 13C-1,2,3,4,7,8-HxCDD 67 13C-1,2,3,6,7,8-HxCDD 68 3C-1,2,3,4,6,7,8-HpCD'D 68 13C-OCDD 61 GERGITAMU Date: 7/24/95 PCDD/PCDF Analysis Page 3 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Samples LAB SAMPLE ID K9435 CLIENT SAMPLE ID APDB INSTRUMENT DATA FILE 50705LCA04-SlO WET WEIGHT 10.05 DRY WEIGHT 1.45 PERCENT SOLIDS 14.5 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX0202 EXTRACTION DATE 4-6-75 ANALYSIS DATE 7-5-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,87TCDF 2.91 1.03 6.89 1 1,2,3,7,8-PeCDF 1.85 34.5 ND 2,3,4,7,8-PeCDF 2.26 34.5 ND 1,2,3,4,7,8-HxCDF 1.03 34.5 ND 1,2,3,6,7,8-HxCDF 1.01 34.5 ND 2,3,4,6,7,8-HxCDF 1.46 1.24 34.5 1 xCDF 2.10 34.5. ND 112,3"4,6,7,8-:HOCDF V.49 34.5 ND 1,2,3,4,7,8,9-HpCbF 1.71 34 ' 5 ND OCDF 4.54 68.9 ND 2,3,7,8-TCDD 2.13 6.89 ND 1,2,3,7,8-PeCDD 3.61 2.64 34.5 1 1,2,3,4,7,8-HxCDD 2.80 34.5 ND 1,2,3,6,7,8-HxCDD 2.84 34.5 ND 1,2,3,7,8,9-HxCDD 2.84 34.5 ND 1,2,3,4,6,7,8-HpCDD 6.65 1.72 34.5 1 OCDD 40.2 1.61 68.9 1 Internal Standard % Recov D13 Qual % Recoveries 13C-2,3,7,8-TCDF 65 13C-1,2,3,7,8-PeCDF 77 13C-2,3,4,7,8-PeCDF 76 13C-1,2,3,4,7,8-HxCDF 71 13C-1,2,3,6,7,8-HxCDF 77 13C-2,3,4,6,7,8-HxCDF 72 13C-1,2,3,7,8,9-HxCDF 71 13C-1,2,3,4,6,7,8-HpCDF 73 13C-1,2,3,4,7,8,9-HpCDF 76 13C-2,3,7,8-TCDD 13C-1,2,3,7,8-PeCDD 75 13C-1,2,3,4,7,8-HxCDD 71 13C-1,2,3,6,7,8-HxCDD 76 3C-1,2,3,4,6,7,8-HpCDD 73 13C-OCDD 63 GERG/TAMU Date: 7/24/95 PCDD/PCDF Analysis Page 4 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Samples LAB SAMPLE ID K9437 CLIENT SAMPLE ID CKBP INSTRUMENT DATA FILE 50705LCA04-Sl 1 WET WEIGHT 10.09 DRY WEIGHT 1.33 PERCENT SOLIDS 13.1 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX0202 EXTRACTION DATE, 4-6-75 ANALYSIS DATE 7-5-95 Conc EDL LMCL DBQual Compound Name (pg/9) (pg/g) (pg/g) 2,3,7,8-TCDF 1.83 7.54 ND 1,2,3,7,8-PeCDF 1.22 37.7 ND 2,3,4,7,8-PeCDF 1.54 37.7 ND 1,2,3,4,7,8-HxCDF 1.31 37.7 ND 1,2,3,6,7,8-HxCDF 1.28 37.7 ND 2,.3,4,6,7,8-HxCDF 1.55 37.7 ND 1-,"2,3,7,8,9-HxCDF. 4-28. 1.98 37.7 J .1,2-,3j4,6,71'8-HpCDF .1.38 37.1 Nb 1,2,3,4,7,8,9-HpCDF 1.59 37.7 ND OCDF 2.44 75.4 ND 2,3,7,8-TCDD 2.15 7.54 ND 1,2,3,7,8-PeCDD 1.23 37.7 ND 1,2,3,4,7,8-HxCDD 2.87 37.7 ND 1,2,3,6,7,8-HxCDD 2.90 37.7 ND 1,2,3,7,8,9-HxCDD 2.91 37.7 ND 1,2,3,4,6,7,8-HpCDD 2.08 37.7 ND OCDD 7.18 75.4 ND Internal Standard % Recov DB Qual .% Recoveries 13C-2,3,7,8-TCDF 62 13C-1,2,3,7,8-PeCDF 82 13C-2,3,4,7,8-PeCDF 82 13C-1,2,3,4,7,8-HxCDF 65 13C-1,2,3,6,7,8-HxCDF 67 13C-2,3,4,6,7,8-HxCDF 66 13C-1,2,3,7,8,9-HxCDF 67 13C-1,2,3,4,6,7,8-HpCDF 70 13C-1,2,3,4,7,8,9-HpCDF 75 13C-21-3,7,8-TCDD 70 13C-1,2,3,7,8-PeCDD 83 13C-1,2,3,4,7,8-HxCDD 67 13C-1,2,3,6,7,8-HxCDD 70 3C-1,2,3,4,6,7,8-HpCDD 71 13C-OCDD 62 GERG/TAMU Date: 7/24/95 PCDD/PCDF Analysis Page 5 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Samples LAB SAMPLE ID K9445 CLIENT SAMPLE ID FBFO INSTRUMENT DATA FILE 50705LCA04-Sl 2 WET WEIGHT 10.83 DRY WEIGHT 1.28 PERCENT SOLIDS 11.8 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX0202 EXTRACTION DATE 4-6-75 ANALYSIS DATE 7-5-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 2.02 0.92 7.84 1 1,2,3,7,8-PeCDF 1.81 39.2 ND 2,3,4,7,8-PeCDF 2.26 39.2 ND 1,2,3,4,7,8-HxCDF 1.12 39.2 ND 1,2,3,6,7,8-HxCDF 1.09 39.2 ND 2,3,4,6,7,8-HxCDF 1.76 1.36 39.2 1 4.48 1.93 39.2 'J 1,2,3,7.,8,9-HxCDF -1,2,3,4,61718-HpCDF 1.43 39.2 ND 1,2,3,4,7,8,9-HpQDF 1.75 39.2 ND OCDF 2.94 78.4 ND 2,3,7,8-TCDD 1.84 7.84 ND 1,2,3,7,8-PeCDD 2.36 2.56 39.2 1 1,2,3,4,7,8-HxCDD 1.84 39.2 ND 1,2,3,6,7,8-HxCDD 1.72 39.2 ND 1,2,3,7,8,9-HxCDD 1.79 39.2 ND 1,2,3,4,6,7,8-HpCDD 3.80 1.20 39.2 1 OCDD 6.28 78.4 ND Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 60 13C-1,2,3,7,8-PeCDF 76 13C-2,3,4,7,8-PeCDF 74 13C-1,2,3,4,7,8-HxCDF 67 13C-1,2,3,6,7,8-HxCDF 68 13C-2,3,4,6,7,8-HxCDF 66 13C-1,2,3,7,8,9-HxCDF 63 13C-1,2,3,4,6,7,8-HpCDF 69 13C-1,2,3,4,7,8,9-HpCDF 68 13C-2,3,7,8-TCDD 67- 13C-1,2,3,7,8-PeCDD 76 13C-1,2,3,4,7,8-HxCDD 65 13C-1,2,3,6,7,8-HxCDD 68 3C-1,2,3,4,6,7,8-HpCDD 66 13C-OCDD 57 GERG/TAMU Date: 7/24/95 PCDD/PCDF Analysis Page 6 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Samples LAB SAMPLE ID K9447 CLIENT SAMPLE ID EVFU INSTRUMENT DATA FILE 50705LCA04-S13 WET WEIGHT 10.51 DRY WEIGHT 0.41 PERCENT SOLIDS 3.9 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX0202 EXTRACTION DATE 4-6-75 ANALYSIS DATE 7-5-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pgg) (pg/g) 2,3,7,8-TCDF 1.86 24.4 ND 1,2,3,7,8-PeCDF 4.69 122 ND 2,3,4,7,8-PeCDF 5.86 122 ND 1,2,3,4,7,8-HxCDF 2.58 122 ND 1,2,3,6,7,8-HxCDF 2.53 122 ND 2,3,4,6,7,8-HxCDF 3.02 122 ND 1,2,3,7,8j9-HxCDF -122 4.20 ND. 1,2,3,4,6,7,8;.HpCDF 5-.02 122 ND 1,2,3,4,7,8,9-HpCDF 5.67 122 ND OCDF 8.11 244 ND 2,3,7,8-TCDD 3.03 24.4 ND 1,2,3,7,8-PeCDD 4.19 122 ND 1,2,3,4,7,8-HxCDD 7.44 122 ND 1,2,3,6,7,8-HxCDD 6.52 122 ND 1,2,3,7,8,9-HxCDD 6.99 122 ND 1,2,3,4,6,7,8-HpCDD 5.03 122 ND OCDD 28.6 244 ND Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 56 13C-1,2,3,7,8-PeCDF 76 13C-2,3,4,7,8-PeCDF 72 13C-1,2,3,4,7,8-HxCDF 62 13C-1,2,3,6,7,8-HxCDF 62 13C-2,3,4,6,7,8-HxCDF 61 13C-1,2,3,7,8,9-HxCDF 61 13C-1,2,3,4,6,7,8-HpCDF 60 13C-1,2,3,4,7,8,9-HpCDF 64 13C-2,3,7,8-TCDD 71 13C-1,2,3,7,8-PeCDD 75 13C-1,2,3,4,7,8-HxCDD 60 13C-1,2,3,6,7,8-HxCDD 63 3C-1,2,3,4,6,7,8-HpCDD 60 13C-OCDD 50 GERG/TAMU Date: 7/24/95 PCDD/PCDF Analysis Page 7 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Samples LAB SAMPLE ID K9474 CLIENT SAMPLE ID CBSR INSTRUMENT DATA FILE 50705LCA04-S14 WET WEIGHT 10.44 DRY WEIGHT 0.78 PERCENT SOLIDS 7.5 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX0202 EXTRACTION DATE 4-6-75 ANALYSIS DATE 7-5-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 1.58 12.8 ND 1,2,3,7,8-PeCDF 2.86 63.8 ND 2,3,4,7,8-PeCDF 3.71 63.8 ND 1,2,3,4,7,8-HxCDF 1.22 63.8 ND 1,2,3,6,7,8-HxCDF 1.13 63.8 ND 2,3,4,6,7,8-HxCDF 1.43 63.'8 ND 8,9@HxCDF.. .1 63.8 ..99 ND 1,2,3,4,6,7-,8-HpCDF '3.b4 63.81 ND 1,2,3,4,7,8,9-HpCDF 4.65 63.8 ND OCDF 3.58 128 ND 2,3,7,8-TCDD 2.43 12.8 ND 1,2,3,7,8-PeCDD 3.68 63.8 ND 1,2,3,4,7,8-HxCDD 4.42 63.8 ND 1,2,3,6,7,8-HxCDD 4.27 63.8 ND 1,2,3,7,8,9-HxCDD 4.38 63.8 ND 1,2,3,4,6,7,8-HpCDD 11.6 3.34 63.8 1 OCDD 135 3.68 128 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 59 13C-1,2,3,7,8-PeCDF 71 13C-2,3,4,7,8-PeCDF 68 13C-1,2,3,4,7,8-HxCDF 65 13C-1,2,3,6,7,8-HxCDF 67 13C-2,3,4,6,7,8-HxCDF 64 13C-1,2,3,7,8,9-HxCDF 63 13C-1,2,3,4,6,7,8-HpCDF 63 13C-1,2,3,4,7,8,9-HpCDF 63 13C-2,3,7,8-TCDD 63 13C-1,2@3,7,8-PeCDD 70 13C-1,2,3,4,7,8-HxCDD 64 13C-1,2,3,6,7,8-HxCDD 65 3C-1,2,3,4,6,7,8-HpCDD 63 13C-OCDD 50 GERG/TAMU Date: 7/24/95 PCDD/PCDF Analysis Page 8 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Samples LAB SAMPLE ID K9476 CLIENT SAMPLE ID PCLO INSTRUMENT DATA FILE 50705LCA04-S15 WET WEIGHT 10.27 DRY WEIGHT 1.08 PERCENTSOLIDS 10.5 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX0202 EXTRACTION DATE 4-6-75 ANALYSIS DATE 7-5-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 5.53 0.82 9.30 1,2,3,7,8-PeCDF 1.59 46.5 ND 2,3,4,7,8-PeCDF 3.71 46.5 ND 1,2,3,4,7,8-HxCDF 0.60 46.5 ND 1,2,3,6,7,8-HxCDF 2.65 46.5 ND 2,3,4,6,7,8-HxCD@ 0.72 46.5 ND 1,2,3,7,8j9-HxCDF 5.21 0.9.7. 46.'5 J 1,2,3,4,6,7i8-HpCDF .0 * J0 46.5 ND 1,2.,3,4,7,8,9-HpCDF 0.78 46.5 ND OCDF 2.22 93.0 ND 2,3,7,8-TCDD 1.83 9.30 ND 1,2,3,7,8-PeCDD 2.99 3.46 46.5 1 1,2,3,4,7,8-HxCDD 1.74 46.5 ND 1,2,3,6,7,8-HxCDD 1.70 46.5 ND 1,2,3,7,8,9-HxCDD 1.73 46.5 ND 1,2,3,4,6,7,8-HpCDD 8.47 1.24 46.5 1 OCDD 44.9 1.10 93.0 1 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 66 13C-1,2,3,7,8-PeCDF 90 13C-2,3,4,7,8-PeCDF 88 13C-1,2,3,4,7,8-HxCDF 71 13C-1,2,3,6,7,8-HxCDF 72 13C-2,3,4,6,7,8-HxCDF 70 13C-1,2,3,7,8,9-HxCDF 68 13C-1,2,3,4,6,7,8-HpCDF 64 13C-1,2,3,4,7,8,9-HpCDF 68 13C-2,3,7,8-TCDD 77 13C-1,2,3,7,8-PeCDD 88 13C-1,2,3,4,7,8-HxCDD 70 13C-1,2,3,6,7,8-HxCDD 73 3C-1,2,3,4,6,7,8-HpCDD 64 13C-OCDD 45 GERGITAMU Date: 7/24/95 PCDD/PCDF Analysis Page 9 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Samples LAB SAMPLE ID K9478 CLIENT SAMPLE ID PCMP INSTRUMENT DATA FILE 50705LCA04-Sl 6 WET WEIGHT 10.21 DRY WEIGHT 1.70 PERCENT SOLIDS 10.1 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX0202 EXTRACTION DATE 4-6-75 ANALYSIS DATE 7-5-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg1g) 2,3,7,8-TCDF 11.8 0.53 5.87 DB225 1,2,3,7,8-PeCDF 0.68 29.4 ND 2,3,4,7,8-PeCDF 0.86 29.4 ND 1,2,3,4,7,8-HxCDF 0.85 29.4 ND 1,2,3,6,7-18-HxCDF 0.80 29.4 ND 2,3,4,6,7,8-HxCDF 0.97 29.4 ND .29;4: 1,2,3,7,8,9-HxCDF -3.57 ND 1,2.,3,4,6,71-8-HpCDP 1.82 29.4 ND 1,2,3,4,7,8,9-HpCDF 0.42 29.4 ND OCDF 0.82 58.7 ND 2,3,7,8-TCDD 0.57 5.87 ND 1,2,3,7,8-PeCDD 2.38 29.4 ND 1,2,3,4,7,8-HxCDD 1.05 29.4 ND 1,2,3,6,7,8-HxCDD 4.29 0.97 29.4 1 1,2,3,7,8,9-HxCDD 1.02 29.4 ND 1,2,3,4,6,7,8-HpCDD 18.6 0.46 29.4 OCDD 122 0.47 58.7 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 66 13C-1,2,3,7,8-PeCDF 92 13C-2,3,4,7,8-PeCDF 88 13C-1,2,3,4,7,8-HxCDF 70 13C-1,2,3,6,7,8-HxCDF 71 13C-2,3,4,6,7,8-HxCDF 70 13C-1,2,3,7,8,9-HxCDF 70 13C-1,2,3,4,6,7,8-HpCDF 71 13C-1,2,3,4,7,8,9-HpCDF 76 13C-2,3,7,8-TCDD 72 13C-1,2,3,7,8-PeCDD 87 13C-1,2,3,4,7,8-HxCDD 71 13C-1,2,3,6,7,8-HxCDD 73 3C-1,2,3,4,6,7,8-HpCDD 73 13C-OCDD 66 GERG[TAMU Date: 818/95 PCDD/PCDF Analysis Page 10 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Samples LAB SAMPLE ID K9480 CLIENT SAMPLE ID SAWB INSTRUMENT DATA FILE 50706LCA02-S28 WET WEIGHT 10.16 DRY WEIGHT 1.52 PERCENT SOLIDS 14.9 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX0202 EXTRACTION DATE 4-6-75 ANALYSIS DATE 7-6-95 Conc EDL LMCL DBQuaI Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 17.3 0.38 6.58 DB225 1,2,3,7,8-PeCDF 2.03 32.9 ND 2,3,4,7,8-PeCDF 6.49 32.9 ND 1,2,3,4,7,8-HxCDF 1.59 32.9 ND 1,2,3,6,7,8-HxCDF 2.12 32.9 ND 2,3,4,6,7,8-HxCDF 2.52 1.30 32.9 1 .1,2,3,7,8,9-HxCDF.@. i4.62 1.71 32@9 i 1,2,3 ' 4'6,7,8-HpCDF. 3.95- 0.53 32.9 1 1,2,3,4,7,8,9-HpCE)F 1.62 0.70 32.9 1 OCDF 6.47 65.8 ND 2,3,7,8-TCDD 1.53 0.55 6.58 1 1,2,3,7,8-PeCDD 4.10 1.98 32.9 1 1,2,3,4,7,8-HxCDD 2.80 32.9 ND 1,2,3,6,7,8-HxCDD 3.42 1.26 32.9 1 1,2,3,7,8,9-HxCDD 3.63 1.28 32.9 1 1,2,3,4,6,7,8-HpCDD 15.8 0.63 32.9 1 OCDD 76.2 0.55 65.8 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 73 13C-1,2,3,7,8-PeCDF 61 13C-2,3,4,7,8-PeCDF 58 13C-1,2,3,4,7,8-HxCDF 67 13C-1,2,3,6,7,8-HxCDF 69 13C-2,3,4,6,7,8-HxCDF 70 13C-1,2,3,7,8,9-HxCDF 71 13C-1,2,3,4,6,7,8-HpCDF 82 13C-1,2,3,4,7,8,9-HpCDF 81 13C-2,3,7,8-TCDD- 76 13C-1,2,3,7,8-PeCDD 64 13C-1,2,3,4,7,8-HxCDD 72 13C-1,2,3,6,7,8-HxCDD 74 3C-1,2,3,4,6,7,8-HpCDD 83 13C-OCDD 62 GERG/TAMU Date: 8/8/95 PCDD/PCDF Analysis Page 11 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Samples LAB SAMPLE ID Q10381 CLIENT SAMPLE ID INSTRUMENT DATA FILE 50705LCA04-S7 WET WEIGHT 1.00 DRY WEIGHT 1.00 PERCENT SOLIDS 100.0 CALCULATION BASIS DRY SAMPLE TYPE BLANK MATRIX QC BATCH DX0202 EXTRACTION DATE 4-6-75 ANALYSIS DATE 7-5-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 2.16 10.0 ND 1,2,3,7,8-PeCDF 3.32 50.0 ND 2,3,4,7,8-PeCDF 4.05 50.0 ND 1,2,3,4,7,8-HxCDF 2.60 50.0 ND 1,2,3,6,7,8-HxCDF 2.52 50.0 ND 2,3,4,6,7,8-HxCDF 3.17 50.0 ND. 1,2,3,,7,8,9-HxCDF. 6.93 50.0 ND 1 2 3,4,6,7,8-HpCDF'@ 4.35 50.0 ND 1:2:3,4,7,8,9-HpCDF 4.90 50.0 ND OCDF 10.7 100 ND 2,3,7,8-TCDD 3.80 10.0 ND 1,2,3,7,8-PeCDD 3.77 4.41 50.0 1 1,2,3,4,7,8-HxCDD 4.96 50.0 ND 1,2,3,6,7,8-HxCDD 4.52 50.0 ND 1,2,3,7,8,9-HxCDD 4.76 50.0 ND 1,2,3,4,6,7,8-HpCDD 4.26 50.0 ND OCDD 10.2 4.80 100 1 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 61 13C-1,2,3,7,8-PeCDF 74 13C-2,3,4,7,8-PeCDF 72 13C-1,2,3,4,7,8-HxCDF 70 13C-1,2,3,6,7,8-HxCDF 71 13C-2,3,4,6,7,8-HxCDF 67 13C-1,2,3,7,8,9-HxCDF 67 13C-1,2,3,4,6,7,8-HpCDF 65 13C-1,2,3,4 7,8,9-HpCDF 66 13C-2,3,7,8-TCDD @66 13C-1,2,3,7,8-PeCDD 72 13C-1,2,3,4,7,8-HxCDD 67 13C-1,2,3,6,7,8-HxCDD 70 3C-1,2,3,4,6,7,8-HpCDD 64 13C-OCDD 53 GERG/TAMU Date: 8/8/95 PCDD/PCDF Analysis Page 12 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Samples LAB SAMPLE ID Q10382 CLIENT SAMPLE ID APCP INSTRUMENT DATA FILE 50705LCA04-S19 WET WEIGHT 10.33 DRY WEIGHT 0.99 PERCENT SOLIDS 9.6 CALCULATION BASIS DRY SAMPLE TYPE DUP MATRIX TISSUE QC BATCH DX0202 EXTRACTION DATE 4-6-75 ANALYSIS DATE 7-5-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 4.22 10.1 ND 1,2,3,7,8-PeCDF 50.3 ND 2,3,4,7,8-PeCDF 2.34 50.3 ND 1,2,3,4,7,8-HxCDF 0.63 50.3 ND 1,2,3,6,7,8-HxCDF 0.62 50.3 ND 2,3,4,6,7,8-HxCDF 0.77 50.3 ND. 1,2,3,7,8,9-HxC.DF 5.21 1.05 .50.3 1,2,3,4,6,7,8-HpCDF 1.73 50.3 ND 1,2,3,4,7,8,0-HpCDF 1.81 50.3 ND OCDF 2.10 101 ND 2,3,7,8-TCDD 1.35 10.1 ND 1,2,3,7,8-PeCDD 2.56 50.3 ND 1,2,3,4,7,8-HxCDD 1.28 50.3 NID 1,2,3,6,7,8-HxCDD 1.25 50.3 ND 1,2,3,7,8,9-HxCDD 1.27 50.3 ND 1,,2,3,4,6,7,8-HpCDD 8.28 1.89 50.3 OCDD 79.3 2.93 101 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 63 13C-1,2,3,7,8-PeCDF 74 13C-2,3,4,7,8-PeCDF 76 13C-1,2,3,4,7,8-HxCDF 74 13C-1,2,3,6,7,8-HxCDF 75 13C-2,3,4,6,7,8-HxCDF 73 13C-1,2,3,7,8,9-HxCDF 71 13C-1,2,3,4,6,7,8-HpCDF 64 13C-1,2,3,4,7,8,9-HpCDF 67 13C-2,3,7,8-TCDD 72 13C-1,2,3,7,8-PeCDD 77 13C-1,2,3,4,7,8-HxCDD 73 13C-1,2,3,6,7,8-HxCDD 73 3C-1,2,3,4,6,7,8-HpCDD 64 13C-OCDD 49 GERG/TAMU Date: 8/8/95 PCDD/PCDF Analysis Page 13 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Samples LAB SAMPLE ID K9433 Q10382 CLIENT SAMPLE 10 APCP APCP INSTRUMENT DATA FILE 50705LCA04-S9 50705LCA04-S19 WET WEIGHT 10.19 10.33 DRY WEIGHT 0.91 0.99 PERCENT SOLIDS 9.0 9.6 CALCULATION BASIS DRY DRY SAMPLE TYPE SAMP DUP MATRIX TISSUE TISSUE QC BATCH DX0202 DX0202 EXTRACTION DATE 4-6-75 4-6-75 ANALYSIS DATE 7-5-95 7-5-95 Conc Conc RPD DB Compound Name (pg/g) (pg/g) 6/0) Qual 2,3,7,8-TCDF 2.13 1,2,3,7,8-PeCDF 2.22 2,3,4,7,8-PeCDF 1,2,3,4,7,8-HxCDF 1,2,3,6,7,8-HxCDF 2.50- 2,3,4,6,7,8-HxCDF 2.47 1,2,3,7,\8,9-HxCDF 6.82 5.21 27 1,2,3,4,6,7,8-HpCDF 1,2,3,4,7,8,9-HpCDF OCDF 2,3,7,8-TCDD 1,2,3,7,8-PeCDD 4.20 1,2,3,4,7,8-HxCDD 1,2,3,6,7,8-HxCDD 1,2,3,7,8,9-HxCDD 1,2,3,4,6,7,8-HpCDD 12.1 8.28 38 OCDD 80.8 79.3 2 Internal Standard % Recoveries 13C-2,3,7,8-TCDF 13C-1,2,3,7,8-PeCDF 13C-2,3,4,7,8-PeCDF 13C-1,2,3,4,7,8-HxCDF 13C-1,2,3,6,7,8-HxCDF 13C-2,3,4,6,7,8-HxCDF 13C-1,2,3,7,8,9-HxCDF 13C-1,2,3,4,6,7,8-HpCDF 13C-1,2,3,4,7,8,9-HpCDF 13C-2,3,7,8-TCDD 13C-1,2,3,7,8-PeCDD 13C-1,2,3,4,7,8-HxCDD 13C-1,2,3,6,7,8-HxCDD 3C-1,2,3,4,6,7,8-HpCDD 13C-OCDD GERG/TAMU Date: 8/8/95 PCDD/PCDF Analysis Page 14 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Samples LAB SAMPLE ID Q10384 CLIENT SAMPLE ID APCP INSTRUMENT DATA FILE 50705LCA04-S21 WET WEIGHT 10.28 DRY WEIGHT 1.02 PERCENT SOLIDS 9.9 CALCULATION BASIS DRY SAMPLE TYPE MS MATRIX TISSUE QC BATCH DX0202 EXTRACTION DATE 4-6-75 ANALYSIS DATE 7-5-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 3996 0.69 9.80 1,2,3,7,8-PeCDF 16654 10.1 49.0 2,3,4,7,8-PeCDF 18396 11.8 49.0 1,2,3,4,7,8-HxCDF 15548 3.21 49.0 1,2,3,6,7,8-HxCDF 15877 2.93 49.0 2,3,4,6,7,8-HxCDF 15760 3.68 49.0 1,2,3,7,8,9-HxCDF 15255 4.71 49.0 1,2,3,4,6,7,8-HpCDF 167 73 1.04 49.0 1,2,3,4,7,8,9-HpCDF 16154 1.19 49.0 OCDF 35996 2.35 98.0 2,3,7,8-TCDO 3039 1.73 9.80 1,2,3,7,8-PeCDD 16672 1.37 49.0 1,2,3,4,7,8-HxCDD 17928 1.68 49.0 1,2,3,6,7,8-HxCDO 18320 1.44 49.0 1,2,3,7,8,9-HxCDD 18912 1.56 49.0 1,2,3,4,6,7,8-HpCDD 16667 1.24 49.0 OCDD 31890 1.68 98.0 Internal Standard % Recov D13 Qual % Recoveries 13C-2,3,7,8-TCDF 57 13C-1,2,3,7,8-PeCDF 73 13C-2,3,4,7,8-PeCDF 79 13C-1,2,3,4,7,8-HxCDF 83 13C-1,2,3,6,7,8-HxCDF 83 13C-2,3,4,6,7,8-HxCDF 81 13C-1,2,3,7,8,9-HxCDF 80 13C-1,2,3,4,6,7,8-HpCDF 77 13C-1,2,3,4,7,8,9-HpCDF 78 13C-2,3,7,8-TCDD 65 13C-1,2,3,7,8-PeCDD 77 13C-1,2,3,4,7,8-.HxCDD 70 13C-1,2,3,6,7,8-HxCDD 73 3C-1,2,3,4,6,7,8-HpCDD 78 13C-OCDD 59 GERG/TAMU Date: 8/8/95 PCDD/PCDF. Analysis Page 15 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Samples LAB SAMPLE ID K9433 Q10384 CLIENT SAMPLE ID APCP APCP INSTRUMENT DATA FILE 50705LCA04-S9 50705LCA04,-p2l WET WEIGHT 10.19 10.28 DRY WEIGHT 0.91 1.02 PERCENT SOLIDS 9.0 9.9 CALCULATION BASIS DRY DRY SAMPLE TYPE SAMP IVIS MATRIX TISSUE TISSUE QC BATCH DX0202 DX0202 EXTRACTION DATE 4-6-75 4-6-75 ANALYSIS DATE 7-5-95 7-5-95 Conc Spike Amnt Conc Recov DB Compound Name (pg/g) (pg/g) (pg/g) d/0) Qual 2,3,7,8-TCDF 2.13 3137 3996 127 1,2,3,7,8-PeCDF 2.22 15686 16654 106 2,3,4,7,8-PeCDF 15686 18396 117 1,2,3,4,7,8-HxCDF 15686 15548 99 1,2,3,6,7,8-HxCDF 2.50 15686 15877 101 2,3,4,6,7,8-HxCDF 2.47 15686 15760 100 1,2,3,7,8,9-HxCDF 6.82 15686 15255 97 1,2,3,4,6,7,8-HpCDF 15686 16773 107 1,2,3,4,7,8,9-HpCDF 15686 16154 103 OCDF 31373 35996 115 2,3,7,8-TCDD 3137 3039 97 1,2,3,7,8-PeCDD 4.20 15686 16672 106 1,2,3,4,7,8-HxCDD 15686 17928 114 1,2,3,6,7,8-HxCDD 15686 18320 117 1,2,3,7,8,9-HxCDD 15686 18912 121 1,2,3,4,6,7,8-HpCDD 12.1 15686 16667 106 -OCDD 80.8 31373 31890 101 Internal Standard % Recoveries 13C-2,3,7,8-TCDF 13C-1,2,3,7,8-PeCDF 13C-2,3,4,7,8-PeCDF 13C-1,2,3,4,7,8-HxCDF 13C-1,2,3,6,7,11-HxCDF 13C-2,3,4,6,7,8-HxCDF 13C-1,2,3,7,8,9-HxCDF 13C-1,2,3,4,6,7,8-HpCDF 13C-1,2,3,4,7,8,9-HpCDF 13C-2,3,7,8-TCDD 13C-1,2,3,7,8-PeCDD 13C-1,2,3,4,7,8-HxCDD 13C-1,2,3,6,7,8-HxCDD 3C-1,2,3,4,6,7,8-HpCDD 13C-OCDD GERG/TAMU Date: 8/8/95 PCDD/PCDF Analysis Page 16 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Samples LAB SAMPLE ID Q10385 CLIENT SAMPLE ID APCP INSTRUMENT DATA FILE 50705LCA04-S22 WET WEIGHT 10.13 DRY WEIGHT 1.05 PERCENT SOLIDS 10.4 CALCULATION BASIS DRY SAMPLE TYPE MSD MATRIX TISSUE QC BATCH DX0202 EXTRACTION DATE 4-6-75 ANALYSIS DATE 7-5-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 3600 0.86 9.51 1,2,3,7,8-PeCDF 15469 12.4 47.6 2,3,4,7,8-PeCDF 17801 15.9 47.6 1,2,3,4,7,8-HxCDF 15533 3.11 47.6 1,2,3,6,7,8-HxCDF 15150 2.97 47.6 2,3,4,6,7,8-HxCDF 14566 4.09 47.6 1,2,3,7,8,9-HxCDF 14663 5.13 47.6 1,2,3,4,6,7,8-HpCDF 15971 1.74 47.6 1,2,3,4,7,8,9-HpCDF 14160 2.00 47.6 OCDF 34513 1.55 95.1 2,3,7,8-TCDD 3048 0.88 9.51 1,2,3,7,8-PeCDD 15537 2.38 47.6 1,2,3,4,7,8-HxCDD 16616 3.34 47.6 1,2,3,6,7,8-HxCDD 17809 3.18 47.6 1,2,3,7,8,9-HxCDD 17589 3.30 47.6 1,2,3,4,6,7,8-HpCDD 15752 1.45 47.6 OCDD 31386 1.30 95.1 Internal Standard % Recov D13 Qual % Recoveries 13C-2,3,7,8-TCDF 59 13C-1,2,3,7,8-PeCDF 77 13C-2,3,4,7,8-PeCDF 73 13C-1,2,3,4,7,8-HxCDF 78 13C-1,2,3,6,7,8-HxCDF 78 13C-2,3,4,6,7,8-HxCDF 73 13C-1,2,3,7,8,9-HxCDF 72 13C-1,2,3,4,6,7,8-HpCDF 74 13C-1,2,3,4,7,8,9-HpCDF 73 13C-2,3,7,8-TCDD 71 13C-1,2,3,7,8-PeCDD 74 13C-1,2,3,4,7,8-HxCDD 72 13C-1,2,3,6,7,8-HxCDD 68 3C-1,2,3,4,6,7,8-HpCDD 70 13C-OCDD 54 GERG/TAMU Date: 8/8/95 PCDD/PCDF Analysis Page 17 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Samples LAB SAMPLE ID K9433 Q1 0385 CLIENT SAMPLE ID APCP APCP INSTRUMENT DATA FILE 50705LCA04-S9 50705LCA04-@22 WET WEIGHT 10.19 10.13 DRY WEIGHT 0.91 1.05 PERCENT SOLIDS 9.0 10.4 CALCULATION BASIS DRY DRY SAMPLE TYPE SAMP MSD MATRIX TISSUE TISSUE QC BATCH DX0202 DX0202 EXTRACTION DATE 4-6-75 4-6-75 ANALYSIS DATE 7-5-95 7-5-95 Conc Spike Amnt Conc Recov D13 Compound Name (pg/g) (pg/g) (pg/g) (6/.) Qual 2,3,7,8-TCDF 2.13 3045 3600 118 1,2,3,7,8-PeCDF 2.22 15224 15469 102 2,3,4,7,8-PeCDF 15224 17801 117 1,2,3,4,7,8-HxCDF 15224 15533 102 1,2,3,6,7,8-HxCDF 2.50 15224 15150 100 2,3,4,6,7,8-HxCDF 2.47 15224 14566 96 1,2,3,7,8,9-HxCDF 6.82 15224 14663 96 1,2,3,4,6,7,8-HpCDF 15224 15971 105 1,2,3,4,7,8,9-HpCDF 15224 14160 93 OCDF 30447 34513 113 2,3,7,8-TCDD 3045 3048 100 1,2,3,7,8-PeCDD 4.20 15224 15537 102 1,2,3,4,7,8-HxCDD 15224 16616 109 1,2,3,6,7,8-HxCDD 15224 17809 117 1,2,3,7,8,9-HxCDD 15224 17589 116 1,2,3,4,6,7,8-HpCDD 12.1 15224 15752 103 OCDD 80.8 30447 31386 103 Internal Standard % Recoveries 13C-2,3,7,8-TCDF 13C-1,2,3,7,8-PeCDF 13C-2,3,4,7,8-PeCDF 13C-1,2,3,4,7,8-HxCDF 13C-1,2,3,6,7,8-HxCDF 13C-2,3,4,6,7,8-HxCDF 13C-1,2,3,7,8,9-HxCDF 13C-1,2,3,4,6,7,8-HpCDF 13C-1,2,3,4,7,8,9-HpCDF 13C-2,3,7,8-TCDD 13C-1,2,3,7,8-PeCDD 13C-1,2,3,4,7,8-HxCDD 13C- 1,2,3,6,7,8-HxCDD 3C-1,2,3,4,6,7,8-HpCDD 13C-OCDD GERG/TAMU Date: 8/8/95 PCDD/PCDF Analysis Page 18 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Samples LAB SAMPLE ID Q1 0384 Q10385 CLIENT SAMPLE ID APCP APCP INSTRUMENT DATA FILE 50705LCA04-S21 50705LCA04-,S22 WET WEIGHT 10.28 10.13 DRY WEIGHT 1.02 1.05 PERCENT SOLIDS 9.9 10.4 CALCULATION BASIS DRY DRY SAMPLE TYPE MS MSD MATRIX TISSUE TISSUE QC BATCH DX0202 DX0202 EXTRACTION DATE 4-6-75 4-6-75 ANALYSIS DATE 7-5-95 7-5-95 Conc Conc RPD DI3 Compound Name (pg/g) (pg/g) M Qual 2,3,7,8-TCDF 3996 3600 10 1,2,3,7,8-PeCDF 16654 15469 7 2,3,4,7,8-PeCDF 18396 17801 3 1,2,3,4,7,8-HxCDF 15548 15533 0 1,2,3,6,7,8-HxCDF 15877 15150 5 2,3,4,6,7,8-HxCDF 15760 14566 8 1,2,3,7,8,9-HxCDF 15255 14663 4 1,2,3,4,6,7,8-HpCDF 16773 15971 5 1 2,3,4,7,8,9-HpCDF 16154 14160 13 OCDF 35996 34513 4 2,3,7,8-TCDD 3039 3048 0 1,2,3,7,8-PeC-DD 16672 15537 7 1,2,3,4,7,8-HxCDD 17928 16616 8 1,2,3,6,7,8-HxCDD 18320 17809 3 1,2,3,7,8,9-HxCDD 18912 17589 7 1,2,3,4,6,7,8-HpCDD 16667 15752 6 OCDD 31890 31386 2 Internal Standard % Recoveries 13C-2,3,7,8-TCDF 13C-1,2,3,7,8-PeCDF 13C-2,3,4,7,8-PeCDF 13C-1,2,3,4,7,8-HxCDF 13C-1,2,3,6,7,8-HxCDF 13C-2,3,4,6,7,8-HxCDF 13C-1,2,3,7,8,9-HxCDF 13C-1,2,3,4,6,7,8-HpCDF 13C-1,2,3,4,7,8,9-HpCDF 13C-2,3,7,8-TCDD 13C-1,2,3,7,8-PeCDD 13C-1,2,3,4,7,8-HxCDD 13C-1,2,3,6,7,8-HxCDD 3C-1,2,3,4,6,7,8-HpCDD 13C-OCDD GERG/TAMU Date: 8/8/95 PCDD/PCDF Analysis Page 19 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Samples LAB SAMPLE ID 010383 CLIENT SAMPLE ID INSTRUMENT DATA FILE 50705LCA04-S20 WET WEIGHT 10.00 DRY WEIGHT PERCENT SOLIDS CALCULATION BASIS WET SAMPLE TYPE SRM MATRIX TISSUE QC BATCH DX0202 EXTRACTION DATE 4-6-75 ANALYSIS DATE 7-5-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 22.5 0.47 1.00 D132@-5 1,2,3,7,8-PeCDF 42.2 3.2 5.00 2,3,4,7,8-PeCDF 46.3 4.2 5.00 1,2,3,4,7,8-HxCDF 89.0 0.61 5.00 1,2,3,6,7,8-HxCDF 65.1 0.63 5.00 2,3,4,6,7,8-HxCDF 63.0 0.81 5.00 1,2,3,7,8,9-HxCDF 60.1 1.00 5.00 1,2,3,4,6,7,8-HpCDF 93.4 0.75 5.00 1,2,3,4,7,8,9-HpCDF 79.8 0.92 5.00 OCDF 229 2.03 10.0 2,3,7,8-TCDD 24.9 1.38 1.00 1,2,3,7,8-PeCDD 54.7 1.04 5.00 1,2,3,4,7,8-HxCDD 68.7 1.25 5.00 1,2,3,6,7,8-HxCDD 69.6 1.29 5.00 1,2,3,7,8,9-HxCDD 73.9 1.28 5.00 1,2,3,4,6,7,8-HpCDD 86.9 1.35 5.00 OCDD 210 1.85 10.0 Internal Standard % Recov D13 Qual % Recoveries 13C-2,3,7,8-TCDF 59 13C-1,2,3,7,8-PeCDF 82 13C-2,3,4,7,8-PeCDF 79 13C-1,2,3,4,7,8-HxCDF 73 13C-1,2,3,6,7,8-HxCDF 74 13C-2,3,4,6,7,8-HxCDF 69 13C-1,2,3,7,8,9-HxCDF 70 13C-1,2,3,4,6,7,8-HpCDF 64 13C-1,2,3,4,7,8,9-HpCDF 65 13C-2,3,7,8-TCDD 72 13C-1,2,3,7,8-PeCDD 80 13C-1,2,3,4,7,8-HxCDD 66 13C-1,2,3,6,7,8-HxCDD 64 3C-1,2,3,4,6,7,8-HpCDD 61 13C-OCDD 49 GERG/TAMU Date: 8/8/95 PCDDIPCDF Analysis Page 20 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 -PURCHASE ORDER NO. Gulf Coast Samples LAB SAMPLE ID Ql 0383 EDF-2526 CLIENT SAMPLE ID INSTRUMENT DATA FILE 50705LCA04-S20 WET WEIGHT 10.00 DRY WEIGHT PERCENT SOLIDS CALCULATION BASIS WET SAMPLE TYPE SRM SRM MATRIX TISSUE TISSUE QC BATCH DX0202 EXTRACTION DATE 4-6-75 ANALYSIS DATE 7-5-95 Conc Conc Recy,. Compound Name (pg/g) (pg/g) M 2,3,7,8-TCDF 22.5 17 132 1,2,3,7,8-PeCDF 42.2 40 106 2,3,4,7,8-PeCDF 46.3 38 122 1,2,3,4,7,8-HxCDF 89.0 80 ill 1,2,3,6,7,8-HxCDF 65.1 63 103 2,3,4,6,7,8-HxCDF 63.0 60 105 1,2,3,7,8,9-HxCDF 60.1 58 104 1,2,3,4,6,7,8-HpCDF 93.4 83 113 1,2,3,4,7,8,9-HpCDF 79.8 73 109 OCDF 229 190 121 2,3,7,8-TCDD 24.9 19 131 1,2,3,7,8-PeCDD 54.7 40 137 1,2,3,4,7,8-HxCDD 68.7 60 115 1,2,3,6,7,8-HxCDD 69.6 56 124 1,2,3,7,8,9-HxCDD 73.9 60 123 1,2,3,4,6,7,8-HpCDD 86.9 76 114 OCDD 210 192 109 Internal Standard % Recoveries 13C-2,3,7,8-TCDF 13C-1,2,3,7,8-PeCDF 13C-2,3,4,7,8-PeCOF 13C-1,2,3,4,7,8-HxCDF 13C-1,2,3,6,7,8-HxCDF 13C-2,3,4,6,7,8-HxCDF 13C-1,2,3,7,8,9-HxCDF 13C-1,2,3,4,6,7,8-HpCDF 13C-1,2,3,4,7,8,9-HpCDF 13C-2,3,7,8-TCDD 13C-1,2,3,7,8-PeCDD 13C-1,2,3,4,7,8-HxCDD 13C-1,2,3,6,7,8-HxCDD 3C-1,2,3,4,6,7,8-HpCDD 13C-OCDD GERG/TAMU Date: 8/8/95 PCDD/PCDF Analysis Page 1 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID K9351 CLIENT SAMPLE ID NYSH INSTRUMENT DATA FILE 50718LCA01-S4 WET WEIGHT 10.04 DRY WEIGHT 0.85 PERCENT SOLIDS 8.50 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX0204 EXTRACTION DATE 4-21-95 ANALYSIS DATE 7-18-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF MI 11.7 ND- 1,2,3,7,8-PeCDF 12.7 58.5 ND 2,3,4,7,8-PeCDF 10.9 58.5 ND 1,2,3,4,7,8-HxCDF 7.18 58.5 ND 1,2,3,6,7,8-HxCDF 6.34 58.5 ND 2,3,4,6,7,8-HxCDF 8.22 58.5 ND t12,3,.7.,8,.9-HxCDF- .1 2@2 58.5 N D 112,3,4,6,7,8-HpCDF 6.24 58.5 ND 1,2,3,4,7,8,9-HpCDF 7.77 58.5 ND OCDF 14.8 117 ND 2,3,7,8-TCDD MI 11.7 ND 1,2,3,7,8-PeCDD 12.3 58.5 ND 1,2,3,4,7,8-HxCDD 9.72 58.5 ND 1,2,3,6,7,8-HxCDD 9.25 58.5 ND 1,2,3,7,8,9-HxCDD 9.69 58.5 ND 1,2,3,4,6,7,8-HpCDD 16.1 8.05 58.5 1 OCDD 82.9 9.42 117 1 Internal Standard % Recov D13 Qual % Recoveries 13C-2,3,7,8-TCDF 62 13C-1,2,3,7,8-PeCDF MI 13C-2,3,4,7,8-PeCDF MI 13C-1,2,3,4,7,8-HxCDF 63 13C-1,2,3,6,7,8-HxCDF 76 13C-2,3,4,6,7,8-HxCDF 69 13C-1,2,3,7,8,9-HxCDF 66 13C-1,2,3,4,6,7,8-HpCDF 86 13C-1,2,3,4,7,8,9-HpCDF 92 13C-2,*3,7,8-TCDD 134 13C-1,2,3,7,8-PeCDD MI 13C-1,2,3,4,7,8-HxCDD 69 13C-1,2,3,6,7,8-HxCDD 80 3C-1,2,3,4,6,7,8-HpCDD 79 13C-OCDD 88 GERG/TAMU Date: 8/25/95 PCDDIPCDF Analysis- Page 2 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID K9353 CLIENT SAMPLE ID HRUB INSTRUMENT DATA FILE 50718LCA01 -S5 WET WEIGHT 10.06 DRY WEIGHT 0.74 PERCENT SOLIDS 7.32 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX0204 EXTRACTION DATE 4-21-95 ANALYSIS DATE 7-18-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF Ml 13.6 ND 1,2,3,7,8-PeCDF 14.3 20.8 67.9 2,3,4,7,8-PeCDF 25.6 19.7 67.9 1 1,2,3,4,7,8-HxCDF 7.57 67.9 ND 1,2,3,6,7,8-HxCDF 6.88 67.9 ND 2,3,4,6,7,8-HxCDF 8.33 8.37 67.9 1 1,2,3,7,8,9-:HxCOF-' -"8.@22--' 12.0. -..67,9 1 1,2,3,4;6,7',8-HpCbF 17.6 6.55 67.9 @j 1,2,3,4,7,8,9-HpCDF 8.16 67.9 ND OCDF 23'.0 11.3 136 1 2,3,7,8-TCDD Ml 13.6 ND 1,2,3,7,8-PeCDD 18.9 67.9 ND 1,2,3,4,7,8-HxCDD 11.6 67.9 ND 1,2,3,6,7,8-HxCDD 11.5 67.9 ND 1,2,3,7,8,9-HxCDD 11.8 67.9 ND 1,2,3,4,6,7,8-HpCDD 68.0 7.39 67.9 OCDD, 324 6.40 136 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 56 13C-1,2,3,7,8-PeCDF MI 13C-2,3,4,7,8-PeCDF MI 13C-1,2,3,4,7,8-HxCDF 59 13C-1,2,3,6,7,8-HxCDF 66 13C-2,3,4,6,7,8-HxCDF 66 13C-1,2,3,7,8,9-HxCDF 69 13C-1,2,3,4,6,7,8-HpCDF 84 13C-1,2,3,4,7,8,9-HpCDF 95 13C-2,3,7,8-TCDD 153 Q 13C-1,2,3,7,8-PeCDD MI 13C-1,2,3,4,7,8-HxCDD 63 13C-1,2,3,6,7,8-HxCDD 77 3C-1,2,3,4,6,7,8-HpCDD 85 13C-OCDD 99 GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 3 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID K9355 CLIENT SAMPLE ID HRJB INSTRUMENT DATA FILE 50706LCA01-SlO WET WEIGHT 10.01 DRY WEIGHT 1.09 PERCENT SOLIDS 10.90 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX0204 EXTRACTION DATE 4-21-95 ANALYSIS DATE 7-6-95 Conc EDL LMCL DBQual Compound Name (pg1g) (pg/g) (pg/g) 2,3,7,8-TCDF 20.2 1.09 9.16 1,2,3,7,8-PeCDF 4.13 2.21 45.8 1 2,3,4,7,8-PeCDF 5.37 2.55 45.8 1,2,3,4,7,8-HxCDF 1.50 45.8 ND 1,2,3,6,7,8-HxCDF 1.38 45.8 ND 2,3,4,6,7,8-HxCDF 2.28 1.67 45.8 458 .1,2,3,7,8,9:-HxCDF. 5.16 2.28 J 1,2,3,4,6,7,8-HpCDF 3.92 1.29 45.8 1 1,2,3,4,7,8,9-HpCDF 1.44 45.8 ND OCDF 4.11 2.01 91.6 1 2,3,7,8-TCDD 2.92 1.36 9.16 1,2,3,7,8-PeCDD 1.70 45.8 ND 1,2,3,4,7,8-HxCDD 1.58 45.8 ND 1,2,3,6,7,8-HxCDD 1.50 45.8 ND 1,2,3,7,8,9-HxCDD 1.53 45.8 ND 1,2,3,4,6,7,8-HpCDD 15.2 1.26 45.8 1 OCDD 68.9 1.32 91.6 Internal Standard % Recov D13 Qual % Recoveries 13C-2,3,7,8-TCDF 77 13C-1,2,3,7,8-PeCDF 104 13C-2,3,4,7,8-PeCDF 115 13C-1,2,3,4,7,8-HxCDF 68 13C-1,2,3,6,7,8-HxCDF 73 13C-2,3,4,6,7,8-HxCDF 75 13C-1,2,3,7,8,9-HxCDF 79 13C-1,2,3,4,6,7,8-HpCDF 101 13C-1,2,3,4,7,8,9-HpCDF 114 13C-2,3,7,8-TCDD 96 13C-1,2,3,7,8-PeCDD 125 13C-1,2,3,4,7,8-HxCDD 77 13C-1,2,3,6,7,8-HxCDD 82 3C-1,2,3,4,6,7,8-HpCDD 114 13C-OCDD 113 GERG/TAMIJ Date: 8/25/95 PCDD/PCDF Analysis Page 4 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID K9357 CLIENT SAMPLE ID HRRB INSTRUMENT DATA FILE 50706LCA01-Sl 1 WET WEIGHT 10.14 DRY WEIGHT 1.04 PERCENT SOLIDS 10.21 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE OC BATCH DX0204 EXTRACTION DATE 4-21-95 ANALYSIS DATE 7-6-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg1g) 2,3,7,8-TCDF 33.5 0.54 9.66 DB225 1,2,3,7,8-PeCDF 5.36 1.56 48.3 1 2,3,4,7,8-PeCDF 8.23 1.87 48.3 1 1,2,3,4,7,8-HxCDF 2.98 0.94 48.3 1 1,2,3,6,7,8-HxCDF 2.41 0.89 48.3 1 2,3,4,6,7,8-HxCDF 3.00 48.3 ND -26 .1.42 J. T,.2,3,7,.8,9-HxCDF.- 4. .48.3 l,2,3,'4,6,7,8-HpCDF 13.2 1.14 48.3 1 1,2,3,4,7,8,9-HpCDF 1.21 48.3 ND OCDF 14.5 1.05 96.6 1 2,3,7,8-TCDD 5.54 0.72 9.66 1 1,2,3,7,8-PeCDD 1.61 48.3 ND 1,2,3,4,7,8-HxCDD 1.62 48.3 ND 1,2,3,6,7,8-HxCDD 1.49 48.3 ND 1,2,3,7,8,9-HxCDD 1.55 48.3 ND 1,2,3,4,6,7,8-HpCDD 45.8 0.41 48.3 1 OCDD 483 0.86 96.6 Internal Standard % Recov DB, Qual % Recoveries 13C-2,3,7,8-TCDF 75 13C-1,2,3,7,8-PeCDF 86 13C-2,3,4,7,8-PeCDF 88 13C-1,2,3,4,7,8-HxCDF 72 13C-1,2,3,6,7,8-HxCDF 73 13C-2,3,4,6,7,8-HxCDF 76 13C-1,2,3,7,8,9-HxCDF 82 13C-1,2,3,4,6,7,8-HpCDF 93 13C-1,2,3,4,7,8,9-HpCDF 113 13C-2,3,7,8-TCDD 89- 13C-1,2,3,7,8-PeCDD 94 13C-1,2,3,4,7,8-HxCDD 80 13C-1,2,3,6,7,8-HxCDD 81 3C-1,2,3,4,6,7,8-HpCDD 112 13C-OCDD 113 GERGfTAMU Date: 8125/95 PCDDIPCDF Analysis Page 5 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID K9359 CLIENT SAMPLE ID HRLB INSTRUMENT DATA FILE 50706LCA01-S12 WET WEIGHT 10.12 DRY WEIGHT 0.74 PERCENT SOLIDS 7.30 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX0204 EXTRACTION DATE 4-21-95 ANALYSIS DATE 7-6-95 Conc EDL LMCL DBOual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 48.2 0.89 13.5 DB225 1,2,3,7,8-PeCDF 5.76 67.7 ND 2,3,4,7,8-PeCDF 8.53 5.47 67.7 1 1,2,3,4,7,8-HxCDF 1.39 67.7 ND 1,2,3,6,7,8-HxCDF 2.96 67.7 ND 2,3,4,6,7,8-HxCDF 2.60 1.59 67.7 1,2,3;7,8,9-HxCDF.'- 6..-119 2.19.- .67.7 1.60. 1,2 3 4,6,7,8-HPCDF, 6.14 67.7 1,2,3,4,7,8,9-HpCDF 1.84 67.7 ND OCDF 8.29 1.55 135 2,3,7,8-TCDD 11.1 1.66 13.5 J 1,2,3,7,8-PeCDD 4.24 67.7 ND 1,2,3,4,7,8-HxCDD 2.66 67.7 ND 1,2,3,6,7,8-HxCDD 2.60 67.7 ND 1,2,3,7,8,9-HxCDD 2.63 67.7 ND 1,2,3,4,6,7,8-HpCDD 18.3 1.56 67.7 OCDD 88.4 1.73 135 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 69 13C-1,2,3,7,8-PeCDF 77 13C-2,3,4,7,8-PeCDF 82 13C-1,2,3,4,7,8-HxCDF 63 13C-1,2,3,6,7,8-HxCDF 68 13C-2,3,4,6,7,8-HxCDF 68 13C-1,2,3,7,8,9-HxCDF 69 13C-1,2,3,4,6,7,8-HpCDF 85 13C-1,2,3,4,7,8,9-HpCDF 96 13C-2,3,7,8-TCDD 82 13C-1,2,3,7,8-PedDD 87 1 3C-1,2,3,4,7,8-HxCOD 71' 13C-1,2,3,6,7,8-HxCDD 74 3C-1,2,3,4,6,7,8-HpCDD 94 13C-OCDD 85 GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 6 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID K9361 CLIENT SAMPLE ID NYSR. INSTRUMENT DATA FILE 50706LCA01-S13 WET WEIGHT 10.20 DRY WEIGHT 0.75 PERCENT SOLIDS 7.37 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX0204 EXTRACTION DATE 4-21-95 ANALYSIS DATE 7-6-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/gy (pg/g) 2,3,7,8-TCDF 38.8 0.86 13.3 1)1322@@- 1,2,3,7,8-PeCDF 6.43 4.24 66.5 1 2,3,4,7,8-PeCDF 10.7 5.10 66.5 1 1,2,3,4,7,8-HxCDF 3.69 0.98 66.5 1,2,3,6,7,8-HxCDF 3.47 0.90 66.5 1 2,3,4,6,7,8-HxCDF 4.46 1.11 66.5 1 q -HxCD -7.97: 1.47 1,2,37,8,9 F .66@5. 1,2,314,6,7,8-HpCDF 13.2 1.47 '66.5 1 1,2,3,4,7,8,9-HpCDF 1.53 66.5 N D OCDF 17.2 2.27 133 1 2,3,7,8-TCDD 10.2 1.68 13.3 1 1,2,3,7,8-PeCDD 2.76 66.5 N D 1,2,3,4,7,8-HxCDD 1.95 66.5 N D 1,2,3,6,7,8-HxCDD 1.82 66.5 N D 1,2,3,7,8,9-HxCDD 1.88 66.5 N D 1,2,3,4,6,7,8-HpCDD 47.9 1.55 66.5 1 OCDD 288 1.24 133 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 71 13C-1,2,3,7,8-PeCDF 79 13C-2,3,4,7,8-PeCDF 82 13C-1,2,3,4,7,8-HxCDF 65 13C-1,2,3,6,7,8-HxCDF 69 13C-2,3,4,6,7,8-HxCDF 70 13C-1,2,3,7,8,9-HxCDF 73 13C-1,2,3,4,6,7,8-HpCDF 83 13C-1,2,3,4,7,8,9-HpCDF 99 13C-2,3,7,8-TCDD 84 13C-1,2,3,7,8-PeCDD 87 -1 3C-1,2,3,4,7,8-HxCDD 74 13C-1,2,3,6,7,8-HxCDD 74 3C-1,2,3,4,6,7,8-HpCDD 101 13C-OCDD 94 GERG/TAMU Date: 8125/95 PCDD/PCDF Analysis Page 7 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID K9365 CLIENT SAMPLE ID NYLB INSTRUMENT DATA FILE 50706LCA01-S14 WET WEIGHT 10.19 DRY WEIGHT 0.75 PERCENT SOLIDS 7.39 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX0204 EXTRACTION DATE 4-21-95 ANALYSIS DATE 7-6-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 31.3 0.71 13.3 DB225 1,2,3,7,8-PeCDF 6.10 66.4 ND 2,3,4,7,8-PeCDF, 11.9 5.02 66.4 1 1,2,3,4,7,8-HxCDF 3.61 2.18 66.4 1 1,2,3,6,7,8-HxC DF 3.82 2.09 66.4 1 2,3,4,6,7,8-HxCDF 3.82 66.4 ND 1 12,3,7,.8,9@HxCDF..- 7.68 3.42 66.4 1 1,213;4,6,7,8-HpCDF 14.9 2.25 66.4 J 1,2,3,4,7,8,9-HpCDF 2.44 66.4 ND OCDF 18.5 1.66 133 1 2,3,7,8-TCDD 10.2 0.93 13.3 j 1,2,3,7,8-PeCDD 3.70 66.4 ND 1,2,3,4,7,8-HxCDD 2.34 66.4 ND 1,2,3,6,7,8-HxCDD 2.30 66.4 ND 1,2,3,7,8,9-HxCDD 2.33 66.4 ND 1,2,3,4,6,7,8-HpCDD 54.7 1.00 66.4 1 OCDD 315 1.67 133 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 67 13C-1,2,3,7,8-PeCDF 77 13C-2,3,4,7,8-PeCDF 79 13C-1,2,3,4,7,8-HxCDF 63 13C-1,2,3,6,7,8-HxCDF 66 13C-2,3,4,6,7,8-HxCDF 68 13C-1,2,3,7,8,9-HxCDF 71 13C-1,2,3,4,6,7,8-HpCDF 78 13C-1,2,3,4,7,8,9-HpCDF 93 13C-2,3,7,8-TCDD 80 13C-1,2,3,7,8-PeCDD 83 13C-1,2,3,4,7,8-HxCDD 71 13C-1,2,3,6,7,8-HxCDD 71 3C-1,2,3,4,6,7,8-HpCDD 92 GERG/TAMU 13C-OCDD 85 Date: 8/25/95 PCDD/PCDF Analysis Page 8 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID K9542 CLIENT SAMPLE ID DBCI INSTRUMENT DATA FILE 50718LCA01-S6 WET WEIGHT 10.20 DRY WEIGHT 2.17 PERCENT SOLIDS 21.25 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX0204 EXTRACTION DATE 4-21-95 ANALYSIS DATE 7-18-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF MI 4.61 ND 1,2,3,7,8-PeCDF 5.55 23.1 ND 2,3,4,7,8-PeCDF 4.60 23.1 ND 1,2,3,4,7,8-HxCDF 2.27 23.1 ND 1,2,3,6,7,8-HxCDF 2.12 23.1 ND 2,3,4,6,7,8-HxCDF 2.46 23.1 ND j,2,3-,7,%9-HxCDF 3.5 7 .23.1 ND. .1,2,3,4,6,7,8-HpC.DF. 1.56 23.1 ND 1,2,3,4,7,8,9-HpCDF 1.90 23.1 ND OCDF 3.54 46.1 ND 2,3,7,8-TCDD MI 4.61 ND 1,2,3,7,8-PeCDD 4.99 23.1 ND 1,2,3,4,7,8-HxCDD 2.58 23.1 ND 1,2,3,6,7,8-HxCDD 2.49 23.1 ND 1,2,3,7,8,9-HxCDD 2.59 23.1 ND 1,2,3,4,6,7,8-HpCDD 7.66 2.08 23.1 1 OCDD 33.6 2.41 46.1 1 Internal Standard % Recov D13 Qual % Recoveries 13C-2,3,7,8-TCDF 56 13C-1,2,3,7,8-PeCDF ml 13C-2,3,4,7,8-PeCDF ml 13C-1,2,3,4,7,8-HxCDF 61 13C-1,2,3,6,7,8-HxCDF 69 13C-2,3,4,6,7,8-HxCDF 73 13C-1,2,3,7,8,9-HxCDF 73 13C-1,2,3,4,6,7,8-HpCDF 96 13C-1,2,3,4,7,8,9-HpCDF 104 13C-2,3,7,8-TCDD .128 13C-1,2,3,7,8-PeCDD ml 13C-1,2,;3,4,7,8-HxCDD 70 13C-1,2,3,6,7,8-HxCDD 82 3C-1,2,3,4,6,7,8-HpCDD 100 13C-OCDD 105 GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 9 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID K9544 CLIENT SAMPLE ID CCNH INSTRUMENT DATA FILE 50718LCA01-S7 WET WEIGHT 10.42 DRY WEIGHT 2.16 PERCENT SOLIDS 20.76 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX0204 EXTRACTION DATE 4-21-95 ANALYSIS DATE 7-18-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 3.42 1.29 4.62 1 1,2,3,7,8-PeCDF 1.31 23.1 ND 2,3,4,7,8-PeCDF 1.46 23.1 ND 1,2,3,4,7,8-HxCDF 0.78 23.1 ND 1,2,3,6,7,8-HxCDF 0.53 0.73. 23.1 1 2,3,4,6,'1,8-HxCDF 0*91 .23*1 ND 1,2 3,7'8,9-HxCDF 2.13 .-.23.1 ND 0.89 -23.1 ND -7' 1,2,3,-4,6,' 8-HpCDF 1,2,3,4,7,8,9-HpCDF. 1.03 23.1 ND OCDF 2.16 46.2 ND 2,3,7,8-TCDD 1.30 4.62 ND 1,2,3,7,8-PeCDD 1.62 23.1 ND 1,2,3,4,7,8-HxCDD 1.12 23.1 ND 1,2,3,6,7,8-HxCDD 1.15 23.1 ND 1,2,3,7,8,9-HxCDD 1.17 23.1 ND 1,2,3,4,6,7,8-HpCDD 3.07 1.38 23.1 1 OCDD 18.7 1.12 46.2 1 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 58 13C-1,2,3,7,8-PeCDF Ml 13C-2,3,4,7,8-PeCDF MI 13C-1,2,3,4,7,8-HxCDF 69 13C-1,2,3,6,7,8-HxCDF 75 13C-2,3,4,6,7,8-HxCDF 73 13C-1,2,3,7,8,9-HxCDF 75 13C-1,2,3,4,6,7,8-HpCDF 80 13C-1,2,3,4,7,8,9-HpCDF 87 13C-2,3,7,8-TCDD- 98 13C-1,2,8,7,8-PeCDD Ml 13C-1,2,3,4 7,8-HxCDD '73 13*C-1,2,3,6,'7,8-HxCDD 77 3C-1,2,3,4,6,7,8-HpCDD 79 GERG/TAMU 13C-OCDD 84 Date: 8/25195 PCDD/PCDF Analysis Page 10 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID K9546 CLIENT SAMPLE ID SHFP INSTRUMENT DATA FILE 50706LCA01-S18 WET WEIGHT 10.27 DRY WEIGHT 1.47 PERCENT SOLIDS 14.30 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX0204 EXTRACTION DATE 4-21-95 ANALYSIS DATE 7-06-95 Conc EDL LMCL DBQuaI Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 6.82 0.51 6.81 1,2,3,7,8-PeCDF 3.36 34.0 ND 2,3,4,7,8-PeCDF 1.58 34.0 ND 1,2,3,4,7,8-HxCDF 1.72 34.0 ND 1,2,3,6,7,8-HxCD-F 1.66 34.0 ND 2,3,4,6,7,8-HxCDF 1.-96 34.0 ND - -HxCQF 34.0 J* 1,2,3,7,8,9 4.08 2:38 1,2,3,4,6,7' 8-HpdbF 8.90 0.91 34.0' J OCDF 10.2 0.33 68.1 1 1,2',3,4,7,8,9-HpCDF 1.10 34.0 ND 2,3,7,8-TCDD 1.17 6.81 ND 1,2,3,7,8-PeCDD 2.98 1.27 34.0 1 1,2,3,4,7,8-HxCDD 0.99 34.0 ND 1,2,3,6,7,8-HxCDD 0.91 34.0 ND 1,2,3,7,8,9-HxCDD 0.94 34.0 ND 1,2,3,4,6,7,8-HpCDD 38.1 0.42 34.0 OCDD 185 0.35 68.1 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 53 13C-1,2,3,7,8-PeCDF 72 13C-2,3,4,7,8-PeCDF 80 13C-1,2,3,4,7,8-HxCDF 51 13C-1,2,3,6,7,8-HxCDF 51 13C-2,3,4,6,7,8-HxCDF 55 13C-1,2,3,7,8,9-HxCDF 53 13C-1,2,3,4,6,7,8-HpCDF 66 13C-1,2,3,4,7,8,9-HpCDF 72 13C-2,3,7,8-TCDD 70- 13C-1,2,3,7,8-PeCDD 87 13C-1,2,3,4,7,8-HxCDD 54 13C-1,2,3,6,7,8-HxCDD 57 3C-1,2,3,4,6,7,8-HpCDD 73 13C-OCDD 66 GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 11 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID K9548 CLIENT SAMPLE ID MBNB INSTRUMENT DATA FILE 50706LCA01-S19 WET WEIGHT 10.03 DRY WEIGHT 1.61 PERCENT SOLIDS 16.05 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX0204 EXTRACTION DATE 4-21-95 ANALYSIS DATE 7-06-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg1g) (pg/g) 2,3,7,8-TCDF 8.00 0.23 ...6.21 DB225 1,2,3,7,8-PeCDF 1.16 0.46 31.1 1 2,3,4,7,8-PeCDF 1.41 0.52 31.1 1 1,2,3,4,7,8-HxCDF 0.57 31.1 ND 1,2,3,6,7,8-HxCDF 0.53 31.1 ND 2,3,4,6,7,8-HxCDF 1.23 31.1 ND .1,2,3,7,8,9-HxCDF 2.95 31.1 ND 1,-2,3,4,6,7,8-HpCDF 4.26 0.49 31.1 1 1,2,3,4,7,8,9-HpCDF 0.52 31.1 ND OCDF 4.28 62.1 ND 2,3,7,8-TCDD 0.88 6.21 ND 1,2,3,7,8-PeCDD 1.20 31.1 ND 1,2,3,4,7,8-HxCDD 0.58 31.1 ND 1,2,3,6,7,8-HxCDD 0.55 31.1 ND 1,2,3,7,8,9-HxCDD 0.57 31.1 ND 1,2,3,4,6,7,8-HpCDD 19.9 0.36 31.1 1 OCDD 83.7 0.28 62.1 Internal Standard % Recov DI3 Qual % Recoveries 13C-2,3,7,8-TCDF 67 13C-1,2,3,7,8-PeCDF 65 13C-2,3,4,7,8-PeCDF 71 13C-1,2,3,4,7,8-HxCDF 62 13C-1,2,3,6,7,8-HxCDF 62 13C-2,3,4,6,7,8-HxCDF 65 13C-1,2,3,7,8,9-HxCDF 66 13C-1,2,3,4,6,7,8-HpCDF 73 13C-1,2,3,4,7,8,9-HpCDF 86 13C-2,3,7,8-TCDD 76 13C-1,2,3,7,8-PeCDD 72 1 3C- 1 - 2,3,4,7,8-HxCD D 65 13C-1:2,3,6,7,8-HxCDD 67 3C-1,2,3,4,6,7,8-HpCDD 88 GERG/TAMU 13C-OCDD 81 Date: 8/25/95 PCDD/PCDF Analysis Page 12 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID K9550 CLIENT SAMPLE ID CAKP INSTRUMENT DATA FILE 50706LCA01-S20 WET WEIGHT 10.39 DRY WEIGHT 2.03 PERCENT SOLIDS 19.49 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX0204 EXTRACTION DATE 4-21-95 ANALYSIS DATE 7-06-95 Compound Name Conc EDL LMCL DBQuaI (pg/g) (pg1g) (pg/g) 2,3,7,8-TCDF 2.58 0.19 4.94 1,2,3,7,8-PeCDF 0.94 24.7 ND 2,3,4,7,8-PeCDF 0.99 24.7 ND 1,2,3,4,7,8-HxCDF 0.37 24.7 ND 1,2,3,6,7,8-HxCDF 0.86 0.35 24.7 2,3,4,6,7,8-HxCDF 0.77 0.43 24.7 1,2,3-'7,-$,'9-HxCDF 12.'29 58. ...24.7 1 .1.99, 0.23 24.7 J 1,2,3,4,7,8,9-HpCDF 0.25 24.7 ND OCDF 2.04 0.37 49.4 2,3,7,8-TCDD 0.27 4.94 ND 1,2,3,7,8-PeCDD 1.19 0.81 24.7 1 1,2,3,4,7,8-HxCDD 0.57 24.7 ND 1,2,3,6,7,8-HxCDD 0.56 24.7 ND 1,2,3,7,8,9-HxCDD 0.57 24.7 ND 1,2,3,4,6,7,8-HpCDD 6.06 0.24 24.7 1 OCDD 23.7 0.42 49.4 -J Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 61 13C-1,2,3,7,8-PeCDF 65 13C-2,3,4,7,8-PeCDF 66 13C-1,2,3,4,7,8-HxCDF 63 13C-1,2,3,6,7,8-HxCDF 64 13C-2,3,4,6,7,8-HxCDF 66 13C-1,2,3,7,8,9-HxCDF 67 13C-1,2,3,4,6,7,8-HpCDF 73 13C-1,2,3,4,7,8,9-HpCDF 81 13C-2,3,7,8-TCDD 74 13C-1,2,3,7,8-PeCDD 68 13C-1,2,3,4,7,8-HxCDD 67 13C-1,2,3,6,7,8-HxCDD 68 3C-1,2,3,4,6,7,8-HpCDD 84 13C-OCDD 74 GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 13 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID K9552 CLIENT SAMPLE ID CAGH INSTRUMENT DATA FILE 50706LCA01-S21 WET WEIGHT 10.07 DRY WEIGHT 1.63 PERCENT SOLIDS 16.22 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE OC BATCH DX0204 EXTRACTION DATE 4-21-95 ANALYSIS DATE 7-06-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 3.10 0.19 6.12 1,2,3,7,8-PeCDF 0.94 30.6 ND 2,3,4,7,8-PeCDF 0.99 30.6 ND 1,2,3,4,7,8-HxCDF 0.37 30.6 ND 1,2,3,6,7,8-HxCDF 0.94 0.35 30.6 1 2,3,4,6,7,8-HxCDF 1.15 0.43 30.6 1 .0.58 30.6 -J 1,2,3,7,8,9-HxCDF .2.93 023 30.6 1 1,2,3,4,6,7 8-HOCDF 1.74 1,2,3,4,7,8:9-HpCDF 0,25 30.6 ND OCDF 2.59 0.37 61.2 1 2,3,7,8-TCDD 1.08 0.27 6.12 1 1,2,3,7,8-PeCDD 0.81 30.6 ND 1,2,3,4,7,8-HxCDD 0.57 30.6 ND 1,2,3,6,7,8-HxCDD 0.56 30.6 ND 1,2,3,7,8,9-HxCDD 0.57 30.6 ND 1,2,3,4,6,7,8-HpCDD 9.50 0.24 30.6 1 OCDD 36.7 0.42 61.2 1 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 58 13C-1,2,3,7,8-PeCDF 58 13C-2,3,4,7,8-PeCDF 58 3C-1,2,3,4,7,8-HxCDF 56 13C-1,2,3,6,7,8-HxCDF 58 13C-2,3,4,6,7,8-HxCDF 59 13C-1,2,3,7,8,9-HxCDF 60 13C-1,2,3,4,6,7,8-HpCDF 62 13C-1,2,3,4,7,8,9-HpCDF 77 13C-2,3,7,8-TCDD 67 13C-1,2,3,7,8-PeCDD 59 1 3C-1,2,3,4,7,8-HxCDD 60 13C-1,2,3,6,7,8-HxCDD 60 3C-1,2,3,4,6,7,8-HpCDD 77 GERG/TAMU 13C-OCDD 66 Date: 8/25/95 PCDD/PCDF Analysis Page 14 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID K9554 CLIENT SAMPLE ID MSSP INSTRUMENT DATA FILE 50706LCA01-S22 WET WEIGHT 10.06 DRY WEIGHT 1.66 PERCENT SOLIDS 16.46 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX0204 EXTRACTION DATE 4-21-95 ANALYSIS DATE 7-06-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 3.15 0.21 6.04 1 1,2,3,7,8-PeCDF 1.27 0.58 30.2 2,3,4,7,8-PeCDF 1.09 0.66 30.2 1 1,2,3,4,7,8-HxCDF 0.81 30.2 ND 1,2,3,6,7,8-HxCDF 1.34 0.55 30.2 1 2,3,4,6,7,8-HxCDF 0.73 0.66 30.2 1 .1, 2,3' 7,8,9-HxC,DF 3.04 -0.90 30.2 ..J 1,2,3,4,6,7 ' 8-HpCDF 2.10 0.38 30.2 1 1,2,3,4,7,8,9-HpCDF 0.43 30.2 ND OCDF 2.45 0.31 60.4 1 2,3,7,8-TCDD 0.61 0.24 6.04 1 1,2,3,7,8-PeCDD 2.13 0.54 30.2 1 1,2,3,4,7,8-HxCDD 0.28 30.2 ND 1,2,3,6,7,8-HxCDD 0.27 30.2 ND 1,2,3,7,8,9-HxCDD 0.27 30.2 ND 1,2,3,4,6,7,8-HpCDD 6.07 0.35 30.2 1 OCDD 24.5 0.47 60.4 1 Internal Standard % Recov D13 Qual % Recoveries 13C-2,3,7,8-TCDF 58 13C-1,2,3,7,8-PeCDF 58 13C-2,3,4,7,8-PeCDF 62 13C-1,2,3,4,7,8-HxCDF 56 13C-1,2,3,6,7,8-HxCDF 59 13C-2,3,4,6,7,8-HxCDF 61 13C-1,2,3,7,8,9-HxCDF 60 13C-1,2,3,4,6,7,8-HpCDF 72 13C-1,2,3,4,7,8,9-HpCDF 79 13C-2,3,7,8-TCDD 68 13C-1,2,3,7,8-PeCDD 59 13C-1,2,3,4,7,8-HxCDD 61 13C-1,2,3,6,7,8-HxCDD 63 3C-1,2,3,4,6,7,8-HpCDD 82 13C-OCDD 70 GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 15 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID K9556 CLIENT SAMPLE ID PBSI INSTRUMENT DATA FILE 50706LCA01-S23 WET WEIGHT 10.14 DRY WEIGHT 1.50 PERCENT SOLIDS 14.78 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX0204 EXTRACTION DATE 4-21-95 ANALYSIS DATE 7-06-95 Conc EDL LMCL DBQuaf Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 5.14 0.26 6.67 1 1,2,3,7,8-PeCDF 0.85 0.73 33.4 1 2,3,4,7,11-PeCDF 1,15 33*4 ND 1,2,3,4,7,8-HxCDF 0.71 33.4 ND 1,2,3,6,7,8-HxCDF 1.03 0.66 33.4 2,3,4,6,7,8-HxCDF 1.00 0.79 33.4 - 3,7,8,9-HkCDF 3.43 1.12 33.4 2 1,2,3j4,6,7,8-HbCDF 3.09 33.4 ND 1,2,3,4,7,8,9-HpCDF 0.55 33.4 ND OCDF 3.06 66.7 ND 2,3,7,8-TCDD 0.66 0.29 6.67 1,2,3,7,8-PeCDD 1.93 1.44 33.4 1,2,3,4,7,8-HxCDD 1.76 0.64 33.4 1,2,3,6,7,8-HxCDD 1.38 0.60 33.4 1,2,3,7,8,9-HxCDD 0.62 33.4 ND 1,2,3,4,6,7,8-HpCDD 11.2 0.16 33.4 OCDD 42.4 0.57 66.7 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 61 13C-1,2,3,7,8-PeCDF 60 13C-2,3,4,7,8-PeCDF 61 13C-1,2,3,4,7,8-HxCDF 61 13C-1,2,3,6,7,8-HxCDF 63 13C-2,3,4,6,7,8-HxCDF 65 13C-1,2,3,7,8,9-HxCDF 65 13C-1,2,3,4,6,7,8-HpCDF 74 13C-1,2,3,4,7,8,9-HpCDF 84 13C-2,3,7,8-TCDD 72 13C-1,2,3,7,8-PeCDD 65 13C-1,2,3,4,7,8-HxCDD 65 13C-1,2,3,6,7,8-HxCDD 67 3C-1,2,3,4,6,7,8-HpCDD 84 GERG/TAMU 13C-OCDD 71 Date: 8/25/95 PCDD/PCDF Analysis Page 16 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID Q1 1920 CLIENT SAMPLE ID INSTRUMENT DATA FILE 50706LCA01-S7 WET WEIGHT 1.00 DRY WEIGHT 1.00 PERCENT SOLIDS CALCULATION BASIS DRY SAMPLE TYPE BLANK MATRIX QC BATCH DX0204 EXTRACTION DATE 4-21-95 ANALYSIS DATE 7-06-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 1.66 10.0 ND 1,2,3,7,8-PeCDF 2.71 1.65 50.0 1 2,3,4,7,8-PeCDF 2.24 1.92 50.0 1 1,2,3,4,7,8-HxCDF 1.93 1.66 50.0 1 1,2,3,6,7,8-HxCDF 3.06 50.0 ND 2,3,4,6,7,8-HxCDF 2.44 1.94 50.0 1 1,2,3,7,8,9-14xCDF -5.99'- -2.87. 50.0.. 1 1,2,3"4,617,87HpCDF'' 3.11' 50.0 ND 1,2,3,4,7,8,9-HpCDF 2.13 50.0 ND OCDF 3.63 100 ND 2,3,7,8-TCDD 1.58 10.0 ND 1,2,3,7,8-PeCDD 3.82 2.46 50.0 1 1,2,3,4,7,8-HxCDD 2.52 50.0 ND 1,2,3,6,7,8-HxCDD 2.40 50.0 ND 1,2,3,7,8,9-HxCDD 2.44 50.0 ND 1,2,3,4,6,7,8-HpCDD 2.92 50.0 1 OCDD 5.06 2.50 100 1 Internal Standard % Recov DI3 Qual % Recoveries 13C-2,3,7,8-TCDF 69 13C-1,2,3,7,8-PeCDF 89 13C-2,3,4,7,8-PeCOF 97 13C-1,2,3,4,7,8-HxCDF 71 13C-1,2,3,6,7,8-HxCDF 81 13C-2,3,4,6,7,8-HxCDF 78 13C-1,2,3,7,8,9-HxCDF 76 13C-1,2,3,4,6,7,8-HpCDF 78 13C-1,2,3,4,7,8,9-HpCDF 84 13C-2,3,7,8-TCDD 8i 13C-1,2,3,7,8-PeCDD 97 13C-1,2,3,4,7,8-HxCDD 74 13C-1,2,3,6,7,8-HxCDD 81 3C-1,2,3,4,6,7,8-HpCDD 80 13C-OCDD 73 GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 17 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID 011924 CLIENT SAMPLE ID HRRI3 INSTRUMENT DATA FILE 50706LCA01-S24 WET WEIGHT 10.13 DRY WEIGHT 1.11 PERCENT SOLIDS 10.93 CALCULATION BASIS DRY SAMPLE TYPE DUP MATRIX TISSUE QC BATCH DX0204 EXTRACTION DATE 4-21-95 ANALYSIS DATE 7-06-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 32.1 0.46 9.03 DB225 1,2,3,7,8-PeCDF 4.50 3.30 45.2 1 2,3,4,7,8-PeCDF 6.13 4.14 45.2 1 1,2,3,4,7,8-HxCDF 2.47 1.29 45.2 1 1,2,3,6,7,8-HxCDF 2.07 1.17 45.2 2,3,4,6,7,8-HxCDF 2.15 1.44 45.2 1.,2,3,7,8,9-HxCDF 4..52 1.94 45.2 J. 1,2,3,4,617,8-HOCDF 12.1 1.25 45.2 1,2,3,4,7,8,9-HpCDF 1.41 45.2 ND OCDF 15.4 90.3 ND 2,3,7,8-TCDD 5.27 9.03 ND 1,2,3,7,8-PeCDD 3.15 1.93 45.2 1,2,3,4,7,8-HxCDD 2.44 2.81 45.2 1,2,3,6,7,8-HxCDD 4.79 2.74 45.2 1,2,3,7,8,9-HxCDD 2.78 45.2 ND 1,2,3,4,6,7,8-HpCDD 46.8 0.81 45.2 OCDD 472 0.41 90.3 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 63 13C-1,2,3,7,8-PeCDF 64 13C-2,3,4,7,8-PeCDF 64 13C-1,2,3,4,7,8-HxCDF 64 13C-1,2,3,6,7,8-HxCDF 66 13C-2,3,4,6,7,8-HxCDF 68 13C-1,2,3,7,8,9-HxCDF 71 13C-1,2,3,4,6,7,8-HpCDF 80 13C-1,2,3,4,7,8,9-HpCDF 86 13C-2,3,7,8-TCDD 77 13C-1,2,3,7,8-PeCDD 67 13,C-1,2,3,4,7,8-HxCDD 68 13C-1,2,3,6,7,8-HxCDD 69 3C-1,2,3,4,6,7,8-HpCDD 89 GERG/TAMU 13C-OCDD 75 Date: 8/25/95 PCDD/PCDF Analysis Page 18 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID K9357 Q1 1924 CLIENT SAMPLE ID HRRB HRRB INSTRUMENT DATA FILE 50706LCA01-Sl 1 50706LCAOJ@S24 WET WEIGHT 10.14 10.13 DRY WEIGHT 1.04 1.11 PERCENT SOLIDS 10.21 10.93 CALCULATION BASIS DRY DRY SAMPLE TYPE SAMP DUP MATRIX TISSUE TISSUE QC BATCH DX0204 DX0204 EXTRACTION DATE 4-21-95 4-21-95 ANALYSIS DATE 7-6-95 7-06-95 Conc Conc f3pD DI3 Compound Name (pg/g) (pg/g) (%) Qual 2,3,7,8-TCDF 33.5 32.1 4 1,2,3,7,8-PeCDF 5.36 4.50 17 2,3,4,7,8-PeCDF 8.23 6.13 29 1,2,3,4,7,8-HxCDF 2.98 2.47 19 1,2,3,6,7,8-HxCDF 2.41 2.07 15 2,3,4,6,7,8-HxCDF 2.15 1,2,3,7,8,9-HxCDF 4.26 .4.52 .6 1,2,3,4,6,7,8-HpCDF 13.2 12.1 9 1,2,3,4,7,8,9-HpCDF OCDF 14.5 2,3,7,8-TCDD 5.54 1,2,3,7,8-PeCDD 3.15 1,2,3,4,7,8-HxCDD 2.44 1,2,3,6,7,8-HxCDD 4.79 1,2,3,7,8,9-HxCDD 1,2,3,4,6,7,8-HpCDD 45.8 46.8 2 OCDD 483 472 -2 Internal Standard % Recoveries 13C-2,3,7,8-TCDF 13C-1,2,3,7,8-PeCDF 13C-2,3,4,7,8-PeCDF 13C-1,2,3,4,7,8-HxCDF 13C-1,2,3,6,7,8-HxCDF 13C-2,3,4,6,7,8-HxCDF 13C-1,2,3,7,8,9-HxCDF 13C-1,2,3,4,6,7,8-HpCDF 13C-1,2,3,4,7,8,9-HpCDF 13C-2,3,7,8-TCDD 13C-1,2,3,7,8-PeCDD 13C-1,2,3,4,7,8-HxCDD 13C-1,2,3,6,7,8-HxCDD 3C-1,2,3,4,6,7,8-HpCDD 13C-OCDD GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 19 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID Q1 1922 CLIENT SAMPLE ID HRRB INSTRUMENT DATA FILE 50706LCA01-S26 WET WEIGHT 10.12 DRY WEIGHT 1.10 PERCENT SOLIDS 10.90 CALCULATION BASIS DRY SAMPLE TYPE MS MATRIX TISSUE OC BATCH DX0204 EXTRACTION DATE 4-21-95 ANALYSIS DATE 7-06-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 852 0.41 9.07 1,2,3,7,8-PeCDF 3335 5.48 45.3 2,3,4,7,8-PeCDF 3485 6.62 45.3 1,2,3,4,7,8-HxCDF 3547 2.09 45.3 1,2,3,6,7,8-HxCDF 3456 1.94 45.3 2,3,4,6,7,8-HxCDF 3383 2.41 45.3 1,2,3 '7,8,9-HxCDF 3306 3.24 45.3 1,2,3,4,6,7,8-HpCDF 3466 0.97 45.3 1,2,3,4,7,8,9-HpCDF 3382 1.06 45.3 OCDF 6521 1.08 90.7 2,3,7,8-TCDD 679 0.71 9.07 1,2,3,7,8-PeCDD 3441 2.20 45.3 1,2,3,4,7,8-HxCDD 3468 1.69 45.3 1,2,3,6,7,8-HxCDD 3616 1.59 45.3 1,2,3,7,8,9-HxCDD 3661 1.64 45.3 1,2,3,4,6,7,8-HpCDD 3469 0.83 45.3 OCDD 7102 0.53 90.7 Internal Standard % Recov DI3 Qua[ % Recoveries 13C-2,3,7,8-TCDF 66 13C-1,2,3,7,8-PeCDF 60 13C-2,3,4,7,8-PeCDF 59 13C-1,2,3,4,7,8-HxCDF 70 13C-1,2,3,6,7,8-HxCDF 71 13C-2,3,4,6,7,8-HxCDF 73 13C-1,2,3,7,8,9-HxCDF 77 13C-1,2,3,4,6,7,8-HpCDF 79 13C-1,2,3,4,7,8,9-HpCDF 89 13C-2,3,7,8-TCDD 84 13C-1,2,3,7,8-PeCDD 69 13C-1,2,3,4,7,8-HxCDD 75 13C-1,2,3,6,7,8-HxCDD 73 3C-1,2,3,4,6,7,8-HpCDD 91 GERG/TAMU 13C-OCDD 86 Date: 8/25/95 PCDD/PCDF Analysis Page 20 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID K9357 Q1 1922 CLIENT SAMPLE ID HRRB HRRB INSTRUMENT DATA FILE 50706LCA01-Sl 1 50706LCAOI-.S26 WET WEIGHT 10.14 10.12 DRY WEIGHT 1.04 1.10 PERCENT SOLIDS 10.21 10.90 CALCULATION BASIS DRY DRY SAMPLE TYPE SAMP IVIS MATRIX TISSUE TISSUE QC BATCH DX0204 DX0204 EXTRACTION DATE 4-21-95 4-21-95 ANALYSIS DATE 7-6-95 7-06-95 Conc Spike Amnt Conc Repov DB Compound Name (pg/g) (pg/g) (pg/g) (%) Qual 2,3,7,8-TCDF 33.5 725 852 113 1,2,3,7,8-PeCDF 5.36 3626 3335 92 2,3,4,7,8-PeCDF 8.23 3626 3485 96 1,2,3,4,7,8-HxCDF 2.98 3626 3547 98 1,2,3,6,7,8-HxCDF 2.41 3626 3456 95 2,3,4,6,7,8-HxCDF 3626 3383 93 1,2,3,7,8,9-HxCDF 4.26 3626 3306 91 1,2,3,4,6,7,8-HpCDF 13.2 3626 3466 95 1,2,3,4,7,8,9-HpCDF 3626 3382 93 OCDF 14.5 7253 6521 90 2,3,7,8-TCDD 5.54 725 679 93 1,2,3,7,8-PeCDD 3626 3441 95 1,2,3,4,7,8-HxCDD 3626 3468 96 1,2,3,6,7,8-HxCDD 3626 3616 100 1,2,3,7,8,9-HxCDD 3626 3661 101 1,2,3,4,6,7,8-HpCDD 45.8 3626 3469 94 OCDD 483 7253 7102 91 Internal Standard % Recoveries 13C-2,3,7,8-TCDF 13C-1,2,3,7,8-PeCDF 13C-2,3,4,7,8-PeCDF 13C-1,2,3,4,7,8-HxCDF 13C-1,2,3,6,7,8-HxCDF 13C-2,3,4,6,7,8-HxCDF 13C-1,2,3,7,8,9-HxCDF 13C-1,2,3,4,6,7,8-HpCDF 13C-1,2,3,4,7,8,9-HpCDF 13C-2,3,7,8-TCDD 13C-1,2,3,7,8-PeCDD 13C-1,2,3,4,7,8-HxCDD 13C-1,2,3,6,7,8-HxCDD 3C-1,2,3,4,6,7,8-HpCDD 13C-OCDD GERG/TAMU Date: 8/25/95 PCDDIPCDF Analysis Page 21 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID Q1 1923 CLIENT SAMPLE ID HRRB INSTRUMENT DATA FILE 50706LCA01-S27 WET WEIGHT 10.18 DRY WEIGHT 1.09 PERCENT SOLIDS 10.71 CALCULATION BASIS DRY SAMPLE TYPE MSD MATRIX TISSUE QC BATCH DX0204 EXTRACTION DATE 4-21-95 ANALYSIS DATE 7-06-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 832 0.25 9.17 1,2,3,7,8-PeCDF 3077 3.60 45.9 2,3,4,7,8-PeCDF 3452 4.57 45.9 1,2,3,4,7,8-HxCDF 3395 0.67 45.9 1,2,3,6,7,8-HxCDF 3151 0.64 45.9 2,3,4,6,7,8-HxCDF 3213 0.75 45.9 1,2,3,7,8,9-HxCDF 3299 0.96 45.9 1,2,3,4,6,7,8-HpCDF 3352 0.85 45.9 1,2,3,4,7,8,9-HpCDF 2965 1.08 45.9 OCDF 6421 0.69 91.7 2,3,7,8-TCDD 723 0.45 9 " 17 1,2,3,7,8-PeCDD 3414 0.59 45.9 1,2,3,4,7,8-HxCDD 3441 1.12 45.9 1,2,3,6,7,8-HxCDD 3433 1.01 45.9 1,2,3,7,8,9-HxCDD 3571 1.06 45.9 1,2,3,4,6,7,8-HpCDD 3357 0.48 45.9 OCDD 6798 0.82 91.7 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 64 13C-1,2,3,7,8-PeCDF 53 13C-2,3,4,7,8-PeCDF 51 13C-1,2,3,4,7,8-HxCDF 57 13C-1,2,3,6,7,8-HxCDF 55 13C-2,3,4,6,7,8-HxCDF 60 13C-1,2,3,7,8,9-HxCDF 65 13C-1,2,3,4,6,7,8-HpCDF 63 13C-1,2,3,4,7,8,9-HpCDF 63 13C-2,3,7,8-TCDD 71 13C-1,2,3,7,8-PeCDD 57 13C-1,2,3,4,7,8-HxCDD 63 13C-1,2,3,6,7,8-HxCDD 63 3C-1,2,3,4,6,7,8-HpCDD 69 GERG/TAMU 13C-OCDD 62 Date: 8/25/95 PCDD/PCDF Analysis Page 22 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID K9357 Q1 1923 CLIENT SAMPLE ID HRRB HRRB INSTRUMENT DATA FILE 50706LCA01-Sl 1 50706LCA01-,S27 WET WEIGHT 10.14 10.18 DRY WEIGHT 1.04 1.09 PERCENT SOLIDS 10.21 10.71 CALCULATION BASIS DRY DRY SAMPLE TYPE SAMP MSD MATRIX TISSUE TISSUE QC BATCH DX0204 DX0204 EXTRACTION DATE 4-21-95 4-21-95 ANALYSIS DATE 7-6-95 7-06-95 Conc Spike Amnt Conc Rqipov DB Compound Name (pg/g) (pg/g) (pg/g) (6/.) Qual 2,3,7,8-TCDF 33.5 734 832 109 1,2,3,7,8-PeCDF 5.36 36.70 3077 84 2,3,4,7,8-PeCDF 8.23 3670 3452 94 1,2,3,4,7,8-HxCDF 2.98 3670 3395 92 1,2,3,6,7,8-HxCDF 2.41 3670 3151 86 2,3,4,6,7,8-HxCDF 3670 3213 88 1,2,3,7,8,9-HxCDF 4.26 3670 3299 90 1,2,3,4,6,7,8-HpCDF 13.2 3670 3352 91 1,2,3,4,7,8,9-HpCDF 3670 2965 81 OCDF 14.5 7339 6421 87 2,3,7,8-TCDD 5.54 734 723 98 1,2,3,7,8-PeCDD 3670 3414 93 1,2,3,4,7,8-HxCDD 3670 3441 94 1,2,3,6,7,8-HxCDD 3670 3433 94 1,2,3,7,8,9-HxCDD 3670 3571 97 1,2,3,4,6,7,8-HpCDD 45.8 3670 3357 90 OCDD 483 7339 6798 86 Internal Standard % Recoveries 13C-2,3,7,8-TCDF 13C-1,2,3,7,8-PeCDF 13C-2,3,4,7,8-PeCDF 13C-1,2,3,4,7,8-HxCDF 13C-1,2,3,6,7,8-HxCDF 13C-2,3,4,6,7,8-HxCDF 13C-1,2,3,7,8,9-HxCDF 13C-1,2,3,4,6,7,8-HpCDF 13C-1,2,3,4,7,8,9-HpCDF 13C-2,3,7,8-TCDD 13C-1,2,3,7,8-PeCDD 13C-1,2,3,4,7,8-HxCDD 13C-1,2,3,6,7,8-HxCDD 3C-1,2,3,4,6,7,8-HpCDD 13C-OCDD GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 23 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID Q1 1922 Q1 1923 CLIENT SAMPLE ID HRRB HRRB INSTRUMENT DATA FILE 50706LCA01-S26 50706LCAOI-.S27 WET WEIGHT 10.12 10.18 DRY WEIGHT 1.10 1.09 PERCENT SOLIDS 10.90 10.71 CALCULATION BASIS DRY DRY SAMPLE TYPE MS MSD MATRIX TISSUE TISSUE QC BATCH DX0204 DX0204 EXTRACTION DATE 4-21-95 4-21-95 ANALYSIS DATE 7-06-95 7-06-95 Conc Conc RPD DB Compound Name (pg/g) (pg/g) Qual 2,3,7,8-TCDF 852 832 2 1,2,3,7,8-PeCDF 3335 3077 8 2,3,4,7,8-PeCDF 3485 3452 1 1,2,3,4,7,8-HxCDF 3547 3395 4 1,2,3,6,7,8-HxCDF 3456 3151 9 2,3,4,6,7,8-HxCDF 3383 3213 5 1,2,3,7,8,9-HxCDF 3306 3299 0 1,2,3,4,6,7,8-HpCDF 3466 3352 3 1,2,3,4,7,8,9-HpCDF 3382 2965 13 OCDF 6521 6421 2 2,3,7,8-TCDD 679 723 6 1,2,3,7,8-PeCDD 3441 3414 1 1,2,3,4,7,8-HxCDD 3468 3441 1 1,2,3,6,7,8-HxCDD 3616 3433 5 1,2,3,7,8,9-HxCDD 3661 3571 2 1,2,3,4,6,7,8-HpCDD 3469 3357 3 OCDD 7102 6798 4 Internal Standard % Recoveries 13C-2,3,7,8-TCDF 13C-1,2,3,7,8-PeCDF 13C-2,3,4,7,8-PeCDF 13C-1,2,3,4,7,8-HxCDF 13C-1,2,3,6,7,8-HxCDF 13C-2,3,4,6,7,8-HxCDF 13C-1,2,3,7,8,9-HxCDF 13C-1,2,3,4,6,7,8-HpCDF 13C-1,2,3,4,7,8,9-HpCDF 13C-2,3,7,8-TCDD 13C-1,2,3,7,8-PeCDD 13C-1,2,3,4,7,8-HxCDD 13C-1,2,3,6,7,8-HxCDD 3C-1,2,3,4,6,7,8-HpCDD GERG/TAMU 13C-OCDD Date: 8/25/95 PCDDIPCDF Analysis Page 24 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID Q1 1921 CLIENT SAMPLE ID INSTRUMENT DATA FILE 50706LCA01-S25 WET WEIGHT 8.48 DRY WEIGHT PERCENT SOLIDS CALCULATION BASIS WET SAMPLE TYPE SRM CARP-1 MATRIX TISSUE OC BATCH DX0204 EXTRACTION DATE 4-21-95 ANALYSIS DATE 7-06-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 14.6 0.05 1.18 DB225 1,2,3,7,8-PeCDF 31.4 0.25 5.90 2,3,4,7,8-PeCDF 14.7 0.35 5.90 1,2,3,4,7,8-HxCDF 12.2 0.22 5.90 1,2,3,6,7,8-HxCDF 2.03 0.21 5.90 1 2,3,4,6,7,8-HxCDF 1.41 0.26 5.90 1 1,2,3,7,8,9-HxCDF 0.66 0.34 5.90 1 1,2,3,4,6,7,8-HpCDF 5.63 0.33 5.90 1 1,2,3,4,7,8,9-HpCDF 0.39 5.90 ND OCDF 0.31 11.8 ND 2,3,7,8-TCDD 6.90 0.10 1.18 1,2,3,7,8-PeCDD 4.60 0.36 5.90 1 1,2,3,4,7,8-HxCDD 4.64 0.51 5.90 1 1,2,3,6,7,8-HxCDD 5.81 0.49 5.90 1 1,2,3,7,8,9-HxCDD 0.50 5.90 ND 1,2,3,4,6,7,8-HpCDD 6.34 0.41 5.90 OCDD 4.78 0.37 11.8 1 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 65 13C-1,2,3,7,8-PeCDF 62 13C-2,3,4,7,8-PeCDF 56 13C-1,2,3,4,7,8-HxCDF 63 13C-1,2,3,6,7,8-HxCDF 64 13C-2,3,4,6,7,8-HxCDF 67 13C-1,2,3,7,8,9-HxCDF 68 13C-1,2,3,4,6,7,8-HpCDF 70 13C-1,2,3,4,7,8,9-HpCDF 73 13C-2,3,7,8-TCDD 77 13C-1,2,3,7,8-PeCDD 59 13C-1,2,3,4,7,8-HxCDD 69 13C-1,2,3,6,7,8-HxCDD 69 3C-1,2,3,4,6,7,8-HpCDD 76 13C-OCDD 66 GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 25 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID Q1 1921 CARP-1 CLIENT SAMPLE ID INSTRUMENT DATA FILE 50706LCA01-S25 WET WEIGHT 8.48 DRY WEIGHT PERCENT SOLIDS CALCULATION BASIS WET SAMPLE TYPE SRM CARP-1 SRM MATRIX TISSUE TISSUE QC BATCH DX0204 EXTRACTION DATE 4-21-95 ANALYSIS DATE 7-06-95 Conc Concensus Conc. .Recy -Compound Name (pg/g) (pg/g) M 2,3,7,8-TCDF 14.6 11.9 123 1,2,3,7,8-PeCDF 31.4 5.0 628 2,3,4,7,8-PeCDF 14.7 1,2,3,4,7,8-HxCDF 12.2 1,2,3,6,7,8-HxCDF 2.03 2,3,4,6,7,8-HxCDF 1.41 1,2,3,7,8,9-HxCDF 0.66 1,2,3,4,6,7,8-HpCDF 5.63 1,2,3,4,7,8,9-HpCDF OCDF 2,3,7,8-TCDD 6.90 6.6 105 1,2,3,7,8-PeCDD 4.60 4.4 105 1,2,3,4,7,8-HxCDD 4.64 1.9 244 1,2,3,6,7,8-HxCDD 5.81 5.6 104 1,2,3,7,8,9-HxCDD 0.7 1,2,3,4,6,7,8-HpCDD 6.34 6.5 98 OCDD 4.78 6.3 76 Internal Standard % Recoveries 13C-2,3,7,8-TCDF 13C-1,2,3,7,8-PeCDF 13C-2,3,4,7,8-PeCDF 13C-1,2,3,4,7,8-HxCDF 13C-1,2,3,6,7,8-HxCDF 13C-2,3,4,6,7,8-HxCDF 13C-1,2,3,7,8,9-HxCDF 13C-1,2,3,4,6,7,8-HpCDF 13C-1,2,3,4,7,8,9-HpCDF 13C-2,3,7,8-TCDD 13C-1,2,3,7,8-PeCDD 13C-1,2,3,4,7,8-HxCDD 13C-1,2,3,6,7,8-HxCDD 3C-1,2,3,4,6,7,8-HpCDD 13C-OCDD GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 1 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID K9534 CLIENT SAMPLE ID MBNR INSTRUMENT DATA FILE 50713LCA02-S8 WET WEIGHT 10.07 DRY WEIGHT 1.38 PERCENT SOLIDS 13.71 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX0205 EXTRACTION DATE 4-25-95 ANALYSIS DATE 7-13-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 14.8 0.99 7.24 1,2,3,7,8-PeCDF 3.27 36.2 ND 2,3,4,7,8-PeCDF 4.24 2.18 36.2 1,2,3,4,7,8-HxCDF 2.11 1.54 36.2 1 1,2,3,6,7,8-HxCDF 2.60 1.47 36.2 1 2,3,4,6,7,8-HxCDF 3.34 1.98 36.2 1,21. 3,-7.8,9-HxCDF 4;67 36.2 ND 1,2,3,416,7,8-HPCDF. 1.66 36.2 ND 1,2,3,4,7,8,9-HpCDF 1.89 36.2 ND OCDF 2.19 72.4 ND 2,3,7,8-TCDD 1.23 7.24 ND 1,2,3,7,8-PeCDD 3.90 36.2 ND 1,2,3,4,7,8-HxCDD 2.35 36.2 ND 1,2,3,6,7,8-HxCDD 2.20 36.2 ND 1,2,3,7,8,9-HxCDD 2.33 36.2 ND 1,2,3,4,6,7,8-HpCDD 11.8 1.65 36.2 1 OCDD 42.8 1.71 72.4 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 67 13C-1,2,3,7,8-PeCDF 74 13C-2,3,4,7,8-PeCDF 74 13C-1,2,3,4,7,8-HxCDF 71 13C-1,2,3,6,7,8-HxCDF 76 13C-2,3,4,6,7,8-HxCDF 72 13C-1,2,3,7,8,9-HxCDF 73 13C-1,2,3,4,6,7,8-HpCDF 73 13C-1,2,3,4,7,11,9-HpCDF 86 13C-2,3,7,8-TCDD 78 13C-1,2,3,7,8-PeCDD 73 13C'-1,2,3,4,'7,8-HxCDb 71 13C-1,2,3,6,7,8-HxCDD 78 3C-1,2,3,4,6,7,8-HpCDD 75 GERG/TAMU 13C-OCDD 70 Date: 8/25/95 PCDD/PCDF Analysis Page 2 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID K9536 CLIENT SAMPLE ID BHHB INSTRUMENT DATA FILE 50713LCA02-S9 WET WEIGHT 10.17 DRY WEIGHT 1.53 PERCENT SOLIDS 15.08 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX0205 EXTRACTION DATE 4-25-95 ANALYSIS DATE 7-13-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 28.2 0.48 6.52 DB22@7- 1,2,3,7,8-PeCDF 2.68 0.90 32.6 1 2,3,4,7,8-PeCDF 4.05 1.10 32.6 1 1,2,3,4,7,8-HxCDF 0.82 32.6 ND 1,2,3,6,7,8-HxCDF 2.09 32.6 ND 2,3,4,6,7,8-HxCDF 2.4.2 32.6 ND ..1;2,'3 7,8,9-HiCDF 3'68 3@2.6 14D 1,2,3,4A7,8-HpCDF 3.84- 1 16 32.6 1 1,2,3,4,7,8,9-HpCDF 1.38 32.6 ND OCDF 4.72 1.96 65.2 1 2,3,7,8-TCDD 0.55 6.52 ND 1,2,3,7,8-PeCDD 1.76 32.6 ND 1,2,3,4,7,8-HxCDD 1.17 1.35 32.6 1 1,2,3,6,7,8-HxCDD 1.41 32.6 ND 1,2,3,7,8,9-HxCDD 1.44 32.6 ND 1,2,3,4,6,7,8-HpCDD 20.8 1.36 32.6 OCDD 85.8 0.29 65.2 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 68 13C-1,2,3,7,8-PeCDF 76 13C-2,3,4,7,8-PeCDF 76 13C-1,2,3,4,7,8-HxCDF 68 13C-1,2,3,6,7,8-HxCDF 67 13C-2,3,4,6,7,8-HxCDF 67 13C-1,2,3,7,8,9-HxCDF 66 13C-1,2,3,4,6,7,8-HpCDF 70 13C-1,2,3,4,7,8,-9-HpCDF 75 13C-2,3,7,8-TCDD 74 13C-1,2,3,7,8-PeCDD 72 13C-1,2,3,4,7,8-HxCDD 72- 13C-1,2,3,6,7,8-HxCDD 70 3C-1,2,3,4,6,7,8-HpCDD 67 13C-OCDD 62 GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 3 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID K9538 CLIENT SAMPLE ID BHDB INSTRUMENT DATA FILE 50713LCA02-SlO WET WEIGHT 10.28 DRY WEIGHT 1.49 PERCENT SOLIDS 14.47 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX0205 EXTRACTION DATE 4-25-95 ANALYSIS DATE 7-13-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 36.8 0.58 6.72 DB225 1,2,3,7,8-PeCDF 2.07 33.6 ND 2,3,4,7,8-PeCDF 6.62 33.6 ND 1,2,3,4,7,8-HxCDF 2.08 ND 1,2,3,6,7,8-HxCDF 1.85 33.6 ND 2,3,4,6,7,8-HxCDF 2.24 33.6 ND 1.,2-,3,7,819-Hx'CDF. 3..46. 3M 'ND 1,2,3,4,6 7,8-HOCDF- 9.46 @3.6 ND 1,2:3,4,7:8,9-HpCDF 2.32 33.6 ND OCDF 8.31 67.2 ND 2,3,7,8-TCDD 1.44 6.72 ND 1,2,3,7,8-PeCDD 1.93 33.6 ND 1,2,3,4,7,8-HxCDD 4.39 33.6 ND 1,2,3,6,7,8-HxCDD 4.35 33.6 ND 1,2,3,7,8,9-HxCDD 4.50 33.6 ND 1,2,3,4,6,7,8-HpCDD 30.2 1.70 33.6 1 OCDD 110.3 0.72 67.2 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 71 13C-1,2,3,7,8-PeCDF 77 13C-2,3,4,7,8-PeCDF 75 13C-1,2,3,4,7,8-HxCDF 63 13C-1,2,3,6,7,8-HxCDF 72 13C-2,3,4,6,7,8-HxCDF 72 13C-1,2,3,7,8,9-HxCDF 66 13C-1,2,3,4,6,7,8-HpCDF 73 13C-1,2,3,4,7,8,9-HpCDF 81 13C-2,3,7,8-TCDD 83 13C-1,2,3,7,8-PeCDD 75 13,C-1,2,3,4,7,8-HxCDD 71 13C-1,2,3,6,7,8-HxCDD 75 3C-1,2,3,4,6,7,8-HpCDD 72 GERG/TAMU 13C-OCDD 71 Date: 8/25/95 PCDD/PCDF Analysis Page 4 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID K9540 CLIENT SAMPLE ID BHDI INSTRUMENT DATA FILE 50713LCA02-Sl 1 WET WEIGHT 10.08 DRY WEIGHT 1.76 PERCENT SOLIDS 17.48 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX0205 EXTRACTION DATE 4-25-95 ANALYSIS DATE 7-13-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 24.5 0.54 5.68 131322@@-- 1,2,3,7,8-PeCDF 1.75 1.24 28.4 1 2,3,4,7,8-PeCDF 3.90 1.67 28.4 1 1,2,3,4,7,8-HxCDF 1.74 28.4 ND 1,2,3,6,7,8-HxCDF 1.61 28.4 ND 2,3,4,6,7,8-HxCDF 2.11 2.18 28.4 1 1,2,3,7,8,9-HxCDF. 3.18 2@'A ND 1,2,3,4k6,7,8-HpCDF 3.85 @.04 28.4 1 1,2,3,4,7,8,9-HpCDF 2.50 28.4 N D OCDF 1.54 56.8 N D 2,3,7,8-TCDD 0.71 5.68 N D 1,2,3,7,8-PeCDD 2.52 28.4 N D 1,2,3,4,7,8-HxCDD 1.02 28.4 ND 1,2,3,6,7,8-HxCDD 1.06 28.4 N D 1,2,3,7,8,9-HxCDD 1.08 28.4 ND 1,2,3,4,6,7,8-HpCDD 14.30 28.4 N D OCDD 69.0 0.62 56.8 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 69 13C-1,2,3,7,8-PeCDF 73 13C-2,3,4,7,8-PeCDF 69 13C-1,2,3,4,7,8-HxCDF 70 13C-1,2,3,6,7,8-HxCDF 74 13C-2,3,4,6,7,8-HxCDF 70 13C-1,2,3,7,8,9-HxCDF 71 13C-1,2,3,4,6,7,8-HpCDF 73 13C-1,2,3,4,7,8,9-HpCDF 75 13C-2,3,7,8-TCDD 81 13C-1,2,3,7,8-PeCDD 75 13C-1,2,3,4,7,8-HxCDD 72 13C-1,2,3,6,7,8-HxCDD 75 3C-1,2,3,4,6,7,8-HpCDD 70 13C-OCDD 63 GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 5 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID K9565 CLIENT SAMPLE ID BHBI INSTRUMENT DATA FILE 50713LCA02-Sl 2 WET WEIGHT 10.29 DRY WEIGHT 1.59 PERCENT SOLIDS 15.48 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE OC BATCH DX0205 EXTRACTION DATE 4-25-95 ANALYSIS DATE 7-13-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 16.1 0.59 6.28 DB225 1,2,3,7,8-PeCDF 3.42 31.4 ND 2,3,4,7,8-PeCDF 3.55 31.4 ND 1,2,3,4,7,8-HxCDF 1.59 31.4 ND 1,2,3,6,7,8-HxCDF 1.53 31.4 ND 2,3,4,6,7,8-HxCDF 1.97 31.4 ND .1,2,3,7;8,9-:HxCDF 4.1.1 2.611 31.4 1,2,3,4,6,7,8-Hp@CDF 4.19 31.4 ND 1,2,3,4,7,8,9-HpCDF 1.81 31.4 ND OCDF 0.59 62.8 ND 2,3,7,8-TCDD 0.62 6.28 ND 1,2,3,7,8-PeCDD 2.45 31.4 ND 1,2,3,4,7,8-HxCDD 1.86 31.4 ND 1,2,3,6,7,8-HxCDD 1.85 31.4 ND 1,2,3,7,8,9-HxCDD 1.92 31.4. ND 1,2,3,4,6,7,8-HpCDD 15.1 0.56 31.4 1 OCDD 72.4 0.76 62.8 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 73 13C-1,2,3,7,8-PeCDF 78 13C-2,3,4,7,8-PeCDF 77 13C-1,2,3,4,7,8-HxCDF 67 13C-1,2,3,6,7,8-HxCDF 69 13C-2,3,4,6,7,8-HxCDF 68 13C-1,2,3,7,8,9-HxCDF 72 13C-1,2,3,4,6,7,8-HpCDF 70 13C-1,2,3,4,7,8,9-HpCDF 80 13C-2,3,7,8-TCDD 83 13C-1,2,3,7,8-PeCDD 79 13C-1,2,3,4,7,8-HxCDD 72 13C-1,2,3,6,7,8-HxCDD 73 3C-1,2,3,4,6,7,8-HpCDD 72 GERG/TAMU 13C-OCDD 72 Date: 8/25/95 PCOD/PCDF Analysis Page 6 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID K9569 CLIENT SAMPLE ID NBDI INSTRUMENT DATA FILE 50713LCA02-S 14 WET WEIGHT 10.13 DRY WEIGHT 1.69 PERCENT SOLIDS 16.69 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX0205 EXTRACTION DATE 4-25-95 ANALYSIS DATE 7-13-95 qqnc EDL LMCL DBQual Compound Name (P,g/g) (pg/g) (pg/g) 2,3,7,8-TCDF 23.3 0.35 5.91 DB225 1,2,3,7,8-PeCDF 2.06 29.6 ND 2,3,4,7,8-PeCDF 4.35 1.70 29.6 1 1,2,3,4,7,8-HxCDF 0.98 29.6 ND 1,2,3,6,7,8-HxCDF 0.95 29.6 ND 2,3,4,6,7,8-HxCDF .1.21 29.6 ND 112,3,7,8,9-HxCDF. 2.95@ 1.62 .29.6- 1 4@ 11 - 29.6 1,2,3@4.6,7,8-1-10CDF 0.58 1,2,3,4,7,8,9-HpCDF 0.63 29.6 ND OCDF 3.57 0.31 59.1 1 2,3,7,8-TCDD 2.04 0.18 5.91 1,2,3,7,8-PeCDD 1.71 1.76 29.6 1 1,2,3,4,7,8-HxCDD 0.95 29.6 ND 1,2,3,6,7,8-HxCDD 1.00 29.6 ND 1,2,3,7,8,9-HxCDD 1.01 29.6 ND 1,2,3,4,6,7,8-HpCDD 14.3 o.41 29.6 OCDD 52.8 0.32 59.1 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 78 13C-1,2,3,7,8-PeCDF 83 13C-2,3,4,7,8-PeCDF 85 13C-1,2,3,4,7,8-HxCDF 73 13C-1,2,3,6,7,8-HxCDF 75 13C-2,3,4,6,7,8-HxCDF 74 13C-1,2,3,7,8,9-HxCDF 75 13C-1,2,3,4,6,7,8-HpCDF 75 13C-1,2,3,4,7,8,9-HpCDF 87 13C-2,3 ''7,8-TCDD 88 13C-1,2,3,7,8-PeCDD 84 1.3C-l,2,3,4,7,8-HxCDD 81 13C-1,2,3,6,7,8-HxCDD 77 3C-1,2,3,4,6,7,8-HpCDD 79 13C-OCDD 79 GERG/TAMU Date: 8/25/95 PCDDIPCDF Analysis Page 7 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID K9571 CLIENT SAMPLE ID NBPI INSTRUMENT DATA FILE 50713LCA02-S15 WET WEIGHT 10.21 DRY WEIGHT 1.90 PERCENT SOLIDS 18.64 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX0205 EXTRACTION DATE 4-25-95 ANALYSIS DATE 7-13-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 26.2 0.09 5.26 DB225 1,2,3,7,8-PeCDF 2.50 1.12 26.3 1 2,3,4,7,8-PeCDF 5.14 26.3 ND 1,2,3,4,7,8-HxCDF 0.74 26.3 ND 1,2,3,6,7,8-HxCDF 0.66 26.3 ND 2,3,4,6,7,8-HxCDF - 2.08 26.3 ' ND li2,3,7,8,9-HxCDF 3.21 OJ7 26.3.. J. 1,2,3,4,6,7,8-HpCDF 4.33 26.3 ND 1,2,3,4,7,8,9-HpCDF 0.37 26.3 ND OCDF 3.56 52.6 ND 2,3,7,8-TCDD 1.56 0.17 5.26 1 1,2,3,7,8-PeCDD 1.75 26.3 ND 1,2,3,4,7,8-HxCDD 1.00 26.3 ND 1,2,3,6,7,8-HxCDD 0.92 26.3 ND 1,2,3,7,8,9-HxCDD 0.99 26.3 ND 1,2,3,4,6,7,8-HpCDD 11.9 0.37 26.3 1 OCDD 51.3 0.38 52.6 1 Internal Standard % Recov D13 Qual % Recoveries 13C-2,3,7,8-TCDF 70 13C-1,2,3,7,8-PeCDF 63 13C-2,3,4,7,8-PeCDF 43 13C-1,2,3,4,7,8-HxCDF 42 13C-1,2,3,6,7,8-HxCDF 45 13C-2,3,4,6,7,8-HxCDF 68 13C-1,2,3,7,8,9-HxCDF 69 13C-1,2,3,4,6,7,8-HpCDF 62 13C-1,2,3,4,7,8,9-HpCDF 77 13C-2,3,7,8-TCDD 81 13C-1,2,3,7;8-PeCDD 64 1 3C-1,2,3,4,7,8-HxCDD 50 13C-1,2,3,6,7,8-HxCDD 52 3C-1,2,3,4,6,7,8-HpCDD 70 GERG[TAMU 13C-OCDD 58 Date: 8/25/95 PCDD/PCDF Analysis Page 8 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID Q1 1925 CLIENT SAMPLE ID INSTRUMENT DATA FILE 50713LCA02-S7 WET WEIGHT 1.00 DRY WEIGHT 1.00 PERCENT SOLIDS CALCULATION BASIS DRY SAMPLE TYPE BLANK MATRIX QC BATCH DX0205 EXTRACTION DATE 4-215-95 ANALYSIS DATE 7-13-95 Conc EDL LMCL DBQual Compound Name lpg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 8.13 10.0 ND 1,2,3,7,8-PeCDF 6.49 2.49 50.0 1 2,3,4,7,8-PeCDF 10.5 3.08 50.0 1 1,2,3,4,7,8-HxCDF 7.17 3.05 50.0 1 1,2,3,6,7,8-HxCDF 8.20 2.86 50.0 2,.3,4,6,7,8-HxCDF 6.11 4.01 .50.0 1 1.2,3,7,8,9.HxCDF 8.68 -5.68 50.0 1 1,2,8,4,6,7,8-HpCDF 4.79 50.0 ND 1,2,3,4,7,8,9-HpCDF 5.53 50.0 ND OCDF 21.7 19.1 100 1 2,3,7,8-TCDD 2.66 10.0 ND 1,2,3,7,8-PeCDD 7.38 4.10 50.0 1 1,2,3,4,7,8-HxCDD 4.86 50.0 ND 1,2,3,6,7,8-HxCDD 4.84 50.0 ND 1,2,3,7,8,9-HxCDD 4.99 50.0 ND 1,2,3,4,6,7,8-HpCDD 6.15 50.0 ND OCDD 27.2 4.91 100 1 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 68 13C-1,2,3,7,8-PeCDF 77 13C-2,3,4,7,8-PeCDF 77 13C-1,2,3,4,7,8-HxCDF 71 13C-1,2,3,6,7,8-HxCDF 76 13C-2,3,4,6,7,8-HxCDF 69 13C-1,2,3,7,8,9-HxCDF 69 13C-1,2,3,4,6,7,8-HpCDF 66 13C-1,2,3,4,7,8,9-HpCDF 76 3C-2,3,7,8-TCDD 79 13C-1,2,3,7,8-PeCDD 72 13C-1,2,3,4,7,8-HxCDD 67 13C-1,2,3,6,7,8-HxCDD 74 3C-1,2,3,4,6,7,8-HpCDD 62 13C-OCDD 33 GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 9 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID Q1 1927 CLIENT SAMPLE ID BHDI INSTRUMENT DATA FILE 50713LCA02-S16 WET WEIGHT 10.15 DRY WEIGHT 1.79 PERCENT SOLIDS 17.60 CALCULATION BASIS DRY SAMPLE TYPE DUP MATRIX TISSUE QC BATCH DX0205 EXTRACTION DATE 4-25-95 ANALYSIS DATE 7-13-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 19.9 0.24 5.60 DB225 1,2,3,7,8-PeCDF 1.07 28.0 ND 2,3,4,7,8-PeCDF 1.31 28.0 ND 1,2,3,4,7,8-HxCDF 0.34 28.0 ND 1,2,3,6,7,8-HxCDF 0.34 28.0 ND 2,3,4,6,7,8-HxCDF 0.43 28.0 ND 1,2,-3,7,8,9-HxCDF' 0.52 28 .0 ND 1,2,3,4,6,7,8-HpCDF 1.26 28.0 ND 1,2,3,4,7,8,9-HpCDF 1.32 28.0 ND OCDF 0.7 56.0 ND 2,3,7,8-TCDD 4.29 5.60 ND 1,2,3,7,8-PeCDD 1.76 28.0 NO 1,2,3,4,7,8-HxCDD 0.71 28.0 ND 1,2,3,6,7,8-HxCDD 0.68 28.0 ND 1,2,3,7,8,9-HxCDD 0.72 28.0 ND 1,2,3,4,6,7,8-HpCDD 12.0 1.01 28.0 1 OCDD 48.7 0.81 56.0 1 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 67 13C-1,2,3,7,8-PeCDF 74 13C-2,3,4,7,8-PeCDF 75 13C-1,2,3,4,7,8-HxCDF 62 13C-1,2,3,6,7,8-HxCDF 62 13C-2,3,4,6,7,8-HxCDF 61 13C-1,2,3,7,8,9-HxCDF 66 13C-1,2,3,4,6,7,8-HpCDF 68 13C-1,2,3,4,7,8,9-HpCDF 79 13C-2,317,8-TCDD 78 13C-1,2,3,7,8-PeCDD 74 13.C-1,2,3,4,7,8-HxCDD 70 13C-1,2,3,6,7,8-HxCDD 67 3C-1,2,3,4,6,7,8-HpCDD 71 GERG/TAMU 13C-OCDD 69 Date: 8/25/95 PCDD/PCDF Analysis Page 10 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID K9540 Q1 1927 CLIENT SAMPLE ID BHDI BHDI INSTRUMENT DATA FILE 50713LCA02-Sl 1 50713LCA02;-S16 WET WEIGHT 10.08 10.15 DRY WEIGHT 1.76 1.79 PERCENT SOLIDS 17.48 17.60 CALCULATION BASIS DRY DRY SAMPLE TYPE SAMP DUP MATRIX TISSUE TISSUE QC BATCH DX0205 -DX0205 EXTRACTION DATE 4-25-95 4-25-95 ANALYSIS DATE 7-13-95 7-13-95 Conc Conc RPD DB Compound Name (pg/g) (pg/g) M Qual 2,3,7,8-TCDF 24.5 19.9 21 1,2,3,7,8-PeCDF 1.75 2,3,4,7,8-PeCDF 3.90 1,2,3,4,7,8-HxCDF 1,2,3,6,7,8-HxCDF 2,3,4,6,7,8-HxCDF 2.11 .1,2,3,7,8,9-Hx.C.DF. .. .* 1,2,314,6,7,8-HpCDF 3.85 1,2;3,4,7,8,9-HpCDF OCDF 2,3,7,8-TCDD 1,2,3,7,8-PeCDD 1,2,3,4,7,8-HxCDD 1,2,3,6,7,8-HxCDD 1,2,3,7,8,9-HxCDD 1,2,3,4,6,7,8-HpCDD 12.0 OCDD 69.0 48.7 34 Internal Standard % Recoveries 13C-2,3,7,8-TCDF 13C-1,2,3,7,8-PeCDF 13C-2,3,4,7,8-PeCDF 13C-1,2,3,4,7,8-HxCDF 13C-1,2,3,6,7,8-HxCDF 13C-2,3,4,6,7,8-HxCDF 13C-1,2,3,7,8,9-HxCDF 13C-1,2,3,4,6,7,8-HpCDF 13C-1,2,3,4,7,8,9-HpCDF 13C-2,3,7,8-TCDD 13C-1,2,3,7,8-PeCDD 13C-1,2,3,4,7,8-H'XCDD 13C-1,2,3,6,7,8-HxCDD 3C-1,2,3,4,6,7,8-HpCDD 13C-OCDD GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 11 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID Q1 1928 CLIENT SAMPLE ID BHDI INSTRUMENT DATA FILE 50713LCA02-Sl 8 WET WEIGHT 10.08 DRY WEIGHT 1.75 PERCENT SOLIDS 17.31 CALCULATION BASIS DRY SAMPLE TYPE MS MATRIX TISSUE QC BATCH DX0205 EXTRACTION DATE 4-25-95 ANALYSIS DATE 7-13-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 602 0.32 5.73 DB225 1,2,3,7,8-PeCDF 2432 3.54 28.7 2,3,4,7,8-PeCDF 2649 4.42 28.7 1,2,3,4,7,8-HxCDF 2319 0.52 28.7 1,2,3,6,7,8-HxCDF 2311 0.50 28.7 2,3,4,6,7,8-HxCDF 2176 0.61 28.7 1,2,3,7,8,9-HxCDF 2233 0.82 28.7 1,2,3,4,6,7,8-HpCDF 2449 0.96 28.7 1,2,3,4,7,8,9-HpCDF 2302 1.06 28.7 OCDF 4766 0.7 57.3 2,3,7,8-TCDD 439 0.24 5.73 1,2,3,7,8-PeCDD 2393 3.19 28.7 1,2,3,4,7,8-HxCDD 2277 1.24 28.7 1,2,3,6,7,8-HxCDD 2302 1.28 28.7 1,2,3,7,8,9-HxCDD 2371 1.30 28.7 1,2,3,4,6,7,8-HpCDD 2265 0.60 28.7 OCDD 4306 0.63 57.3 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 73 13C-1,2,3,7,8-PeCDF 78 13C-2,3,4,7,8-PeCDF 81 13C-1,2,3,4,7,8-HxCDF 68 13C-1,2,3,6,7,8-HxCDF 69 13C-2,3,4,6,7,8-HxCDF 71 13C-1,2,3,7,8,9-HxCDF 73 13C-1,2,3,4,6,7,8-HpCDF 71 13C-1,2,3,4,7,8,9-HpCDF 81 13C-2,3,7,8-TCDD 84 13C-1,2,3,7,8-PeCDD 75 13C-1,2,3,4,7,8-HxCDD 73 13C-1,2,3,6,7,8-HxCDD 74 3C-1,2,3,4,6,7,8-HpCDD 75 GERG/TAMU 13C-OCDD 75 Date: 8/25/95 PCDD/PCOF Analysis Page 12 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID K9540 Q1 1928 CLIENT SAMPLE ID BHDI BHDI INSTRUMENT DATA FILE 50713LCA02-S 11 50713LCA02-S18 WET WEIGHT 10.08 10.08 DRY WEIGHT 1.76 1.75 PERCENT SOLIDS 17.48 17.31 CALCULATION BASIS DRY DRY SAMPLE TYPE SAMP IVIS MATRIX TISSUE TISSUE QC BATCH DX0205 DX0205 EXTRACTION DATE 4-25-95 4-25-95 ANALYSIS DATE 7-13-95 7-13-95 Conc Spike Amnt Conc Recov DS Qual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 24.5 458 602 126 1,2,3,7,8-PeCDF 1.75 2292 2432 106 2,3,4,7,8-PeCDF 3.90 2292 2649 115 1,2,3,4,7,8-HxCDF 2292 2319 101 1,2,3,6,7,8-HxCDF 2292 2311 101 2,3,4,6,7,8-HxCDF 2.11 2292 2176 95 1,2,3,7,8,9-HxCDF 2292 2233 97 1,2,3,4,6,7,8-HpCDF 3.85 2292 2449 107 1,2,3,4,7,8,9-HpCDF 2292 2302 100 OCDF 4585 4766 104 2,3,7,8-TCDD 458 439 96 1,2,3,7,8-PeCDD 2292 2393 104 1,2,3,4,7,8-HxCDD 2292 2277 99 1,2,3,6,7,8-HxCDD 2292 2302 100 1,2,3,7,8,9-HxCDD 2292 2371 103 1,2,3,4,6,7,8-HpCDD 2292 2265 99 OCDD 69.0 4585 4306 92 Internal Standard % Recoveries 13C-2,3,7,8-TCDF 13C-1,2,3,7,8-PeCDF 13C-2,3,4,7,8-PeCDF 13C-1,2,3,4,7,8-HxCDF 13C-1,2,3,6,7,8-HxCDF 13C-2,3,4,6,7,8-HxCDF 13C-1,2,3,7,8,9-HxCDF 13C-1,2,3,4,6,7,8-HpCDF 13C-1,2,3,4,7,8,9-HpCDF .13C-2,3,7,8-TCDD 13C-1,2,3,7,8-PeCDD 13C-1,2,3,4,7,8-HxCDD 13C-1,2,3,6,7,8-HxCDD 3C-1,2,3,4,6,7,8-HpCDD 13C-OCDD GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 13 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID Q1 1929 CLIENT SAMPLE ID BHDI INSTRUMENT DATA FILE 50713LCA02-S19 WET WEIGHT 10.15 DRY WEIGHT 1.83 PERCENT SOLIDS 18.03 CALCULATION BASIS DRY SAMPLE TYPE IVISD MATRIX TISSUE OC BATCH DX0205 EXTRACTION DATE 4-25-95 ANALYSIS DATE 7-13-95 Conc EDL LMCL DBO.ual Compound Name (pg1g) (pg/g) (pg/g) 2,3,7,8-TCDF 543 0.33 5.46 DB225 1,2,3,7,8-PeCDF 2127 2.03 27.3 2,3,4,7,8-PeCDF 2395 2.40 27.3 1,2,3,4,7,8-HxCDF 2006 0.98 27.3 1,2,3,6,7,8-HxCDF 2056 0.99 27.3 2,3,4,6,7,8-HxCDF 2034 1.12 27.3 1,2,3,7,8,9-HxCDF 1990 1.65 27.3 1,2,3,4,6,7,8-HpCDF 2109 0.91 27.3 1,2,3,4,7,8,9-HpCDF 2021 1.05 27.3 OCDF 4041 0.5 54.6 2,3,7,8-TCDD 370 0.14 5.46 1,2,3,7,8-PeCDD 2058 2.62 27.3 1,2,3,4,7,8-HxCDD 1871 0.47 27.3 1,2,3,6,7,8-HxCDD 2036 0.50 27.3 1,2,3,7,8,9-HxCDD 2034 0.51 27.3 1,2,3,4,6,7,8-HpCDD 1954 0.36 27.3 OCDD 3680 0.57 54.6 Internal Standard % Recov D13 Qual % Recoveries 13C-2,3,7,8-TCDF 71 13C-1,2,3,7,8-PeCDF 76 13C-2,3,4,7,8-PeCDF 79 13C-1,2,3,4,7,8-HxCDF 67 13C-1,2,3,6,7,8-HxCDF 65 13C-2,3,4,6,7,8-HxCDF 67 13C-1,2,3,7,8,9-HxCDF 67 13C-1,2,3,4,6,7,8-HpCDF 71 13C-1,2,3,4,7,8,9-HpCDF 78 13C-2,3,7,8-TCDD 84 13C-1,2,3,7,8-PeCDD 79 13C-1,2,3,4,7,8-HxCDD 76 13C-1,2,3,6,7,8-HxCDD 72 3C-1,2,3,4,6,7,8-HpCDD 75 GERG/TAMU 13C-OCDD 75 Date: 8/25/95 PCDDIPCDF Analysis Page 14 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID K9540 0.11929 CLIENT SAMPLE ID BHDI BHDI INSTRUMENT DATA FILE 50713LCA02-Sl 1 50713LCA02.-Sl 9 WET WEIGHT 10.08 10.15 DRY WEIGHT 1.76 1.83 PERCENT SOLIDS 17.48 18.03 CALCULATION BASIS DRY DRY SAMPLE TYPE SAMP MSD MATRIX TISSUE TISSUE QC BATCH DX0205 DX0205 EXTRACTION DATE 4-25-95 4-25-95 ANALYSIS DATE 7-13-95 7-13-95 Conc Spike Amnt Conc Recov DB Compound Name (pg/g) (pg/g) (pg/g) (%) Qual 2,3,7,8-TCDF 24.5 437 543 119 1,2,3,7,8-PeCDF 1.75 2186 2127 97 2,3,4,7.,8-PeCDF 3.90 2186 2395 109 1,2,3,4,7,8-HxCDF 2186 2006 92 1,2,3,6,7,8-HxCDF 2186 2056 94 2,3,4,6,7,8-HxCDF 2.11 2186 2034 93 1,2,3,7,8,9-HxCDF 2186 1990 91 1,2,3,4,6,7,8-HpCDF 3.85 2186 2109 96 1,2,3,4,7,8,9-HpCDF 2186 2021 92 OCDF 4372 4041 92 2,3,7,8-TCDD 437 370 85 1,2,3,7,8-PeCDD 2186 2058 94 1,2,3,4,7,8-HxCDD 2186 1871 86 1,2,3,6,7,8-HxCDD 2186 2036 93 1,2,3,7,8,9-HxCDD 2186 2034 93 1,2,3,4,6,7,8-HpCDD 2186 1954 89 OCDD 69.0 4372 3680 83 Internal Standard % Recoveries 13C-2,3,7,8-TCDF 13C-1,2,3,7,8-PeCDF 13C-2,3,4,7,8-PeCDF 13C-1,2,3,4,7,8-HxCDF 13C-1,2,3,6,7,8-HxCDF 13C-2,3,4,6,7,8-HxCDF 13C-1,2,3,7,8,9-HxCDF 13C-1,2,3,4,6,7,8-HpCDF 13C-1,2,3,4,7,8,9-HpCDF 13C-2,3,7,8-TCDD 13C-1,2,3,7,8-PeCDD 13C-1,2,3,4,7,8-HxCDD 13C-1,2,3,6,7,8-HxCDD 3C-1,2,3,4,6,7,8-HpCDD 13C-OCDD GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 15 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID Q1 1928 Q1 1929 CLIENT SAMPLE ID BHD1 BHDI INSTRUMENT DATA FILE 50713LCA02-S18 507113LCAOg-@S`19 WET WEIGHT 10.08 10. 15 DRY WEIGHT 1.75 1.83 PERCENT SOLIDS 17.31 18.03 CALCULATION BASIS DRY DRY SAMPLE TYPE MS MSD MATRIX TISSUE TISSUE QC BATCH DX0205 DX0205 EXTRACTION DATE 4-25-95 4-25-95 ANALYSIS DATE 7-13-95 7-13-95 Conc Conc RPD DS Compound Name (pg/g) (pg/g) M Qual 2,3,7,8-TCDF 602 543 10 1,2,3,7,8-PeCDF 2432 2127 13 2,3,4,7,8-PeCDF 2649 2395 10 1,2,3,4,7,8-HxCDF 2319 2006 14 1,2,3,6,7,8-HxCDF 2311 2056 12 2,3,4,6,7,8-HxCDF 2176 2034 7 1,2,3,7,8,9-HxCDF 2233 1990 12 1,2,3,4,6,7,8-HpCDF 2449 2109 15 1,2,3,4,7,8,9-HpCDF 2302 2021 13 OCDF 4766 4041 16 2,3,7,8-TCDD 439 370 17 1,2,3,7,8-PeCDD 2393 2058 15 1,2,3,4,7,8-HxCDD 2277 1871 20 1,2,3,6,7,8-HxCDD 2302 2036 12 1,2,3,7,8,9-HxCDD 2371 2034 15 1,2,3,4,6,7,8-HpCDD 2265 1954 15 OCDD 4306 3680 16 Internal Standard % Recoveries 13C-2,3,7,8-TCDF .1 3C-1,2,3,7,8-PeCDF 13C-2,3,4,7,8-PeCDF 13C-1,2,3,4,7,8-HxCDF 13C-1,2,3,6,7,8-HxCDF 13C-2,3,4,6,7,8-HxCDF 13C-1,2,3,7,8,9-HxCDF 13C-1,2,3,4,6,7,8-HpCDF 13C-1,2,3,4,7,8,9-HpCDI 13C-2,3,7,8-TCDD 13C-1,2,3,7,8-PeCDD 13C-1,2,3,4,7,8-HxCDD 13C-1,2,3,6,7,8-HxCDD 3C-1,2,3,4,6,7,8-HpCDD GERGITAMU 13C-OCDD Date: 8/25/95 PCDD/PCDF Analysis Page 16 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAB SAMPLE ID Q1 1926 CLIENT SAMPLE ID INSTRUMENT DATA FILE 50713LCA02-Sl 7 WET WEIGHT 8.80 DRY WEIGHT PERCENT SOLIDS CALCULATION BASIS WET SAMPLE TYPE SRM CARP-1 MATRIX TISSUE QC BATCH DX0205 EXTRACTION DATE 4-25-95 ANALYSIS DATE 7-13-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 15.4 0.11 1.14 DB225 1,2,3,7,8-PeCDF 4.53 0.38 5.68 2,3,4,7,8-PeCDF 14.1 0.44 5.68 1,2,3,4,7,8-HxCDF 3.82 0.28 5.68 1,2,3,6,7,8-HxCDF 2.46 0.26 5.68 2,3,4,6,7,8-HxCDF 1.93 5.68 ND 1,2,3,7,8,9-HxCDF 0.45 5.68 ND 1,2,3,4,6,7,8-HpCDF 4.83 0.07 5.68 1 1,2,3,4,7,8,9-HpCDF 0.10 5.68 ND OCDF 0.2 11.4 ND 2,3,7,8-TCDD 7.18 0.06 1.14 1,2,3,7,8-PeCDD 5.29 0.33 5.68 1,2,3,4,7,8-HxCDD 1.87 0.45 5.68 1,2,3,6,7,8-HxCDD 6.11 5.68 ND 1,2,3,7,8,9-HxCDD 0.47 5.68 ND 1,2,3,4,6,7,8-HpCDD 6.75 0.13 5.68 OCDD 5.01 0.41 11.4 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 70 13C-1,2,3,7,8-PeCDF 78 13C-2,3,4,7,8-PeCDF 79 13C-1,2,3,4,7,8-HxCDF 64 13C-1,2,3,6,7,8-HxCDF 67 13C-2,3,4,6,7,8-HxCDF 69 13C-1,2,3,7,8,9-HxCDF 66 13C-1,2,3,4,6,7,8-HpCDF 72 13C-1,2,3,4,7,8,9-HpCDF 76 13C-2,3,7,8-TCDD 82 13C-1,2,3,7,8-PeCDD 75 13C-1,2,3,4,7,8-HxCDD 75 13C-1,2,3,6,7,8-HxCDD 73 3C-1,2,3,4,6,7,8-HpCDD 73 13C-OCDD 62 GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Pa.ge.1 7 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Samples LAS SAMPLE ID Q1 1926 CARP-1 CLIENT SAMPLE ID INSTRUMENT DATA FILE 50713LCA02-S 17 WET WEIGHT 8.80 DRY WEIGHT PERCENT SOLIDS CALCULATION BASIS WET SAMPLE TYPE SRM CARP-1 SRM MATRIX TISSUE TISSUE QC BATCH DX0205 EXTRACTION DATE 4-25-95 ANALYSIS DATE 7-13-95 Conc Concensus Conc. Recy Compound Name (pg/g) (pg/g) M 2,3,7,8-TCDF 15.4 11.9 129 1,2,3,7,8-PeCDF 4.53 5.0 91 2,3,4,7,8-PeCDF 14.1 1,2,3,4,7,8-HxCDF 3.82 1,2,3,6,7,8-HxCDF 2.46 2,3,4,6,7,8-HxCDF 1,2,3,7,8,9-HxCDF 1,2,3,4,6,7,8-HpCDF 4.83 1,2,3,4,7,8,9-HpCDF OCDF 2,3,7,8-TCDD 7.18 6.6 109 1,2,3,7,8-PeCDD 5.29 4.4 120 1,2,3,4,7,8-HxCDD 1.87 1.9 98 1,2,3,6,7,8-HxCDD 5.6 1,2,3,7,8,9-HxCDD 0.7 1,2,3,4,6,7,8-HpCDD 6.75 6.5 104 OCDD 5.01 6.3 80 Internal Standard % Recoveries 13C-2,3,7,8-TCDF 13C-1,2,3,7,8-PeCDF 13C-2,3,4,7,8-PeCDF 13C-1,2,3,4,7,8-HxCDF 13C-1,2,3,6,7,8-HxCDF 13C-2,3,4,6,7,8-HxCDF 13C-1,2,3,7,8,9-HxCDF 13C-1,2,3,4,6,7,8-HpCDF 13C-1,2,3,4,7,8,9-HpCDF 13C-2,3,7,8-TCDD 13C-1,2,3,7,8-PeCDD 13C-1,2,3,4,7,8-HxCDD 13C-1,2,3,6,7,8-HxCDD 3C-1,2,3,4,6,7,8-HpCDD GERG/TAMU 13C-OCDD Date: 8/25/95 PCDD/PCDF Analysis Page 1 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Sediment Samples LAB SAMPLE ID K9608 CLIENT SAMPLE ID GBCR INSTRUMENT DATA FILE 50721LCA03-S9 WET WEIGHT 40.46 DRY WEIGHT 31.56 PERCENT SOLIDS 78.00 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX SEDIMENT QC BATCH DX0209 EXTRACTION DATE 7-7-95 ANALYSIS DATE 7-21-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 0.42 0.08 0.32 1,2,3,7,8-PeCDF 1.80 0.26 1.58 2,3,4,7,8-PeCDF 1.80 0.32 1.58 1,2,3,4,7,8-HxCDF 1.90 0.44 1.58 1,2,3,6,7,8-HxCDF 2.78 0.41 1.58 2,a,4,6,7,8-Hx,.CD.F 2.01 0.51 1.58 1,,2,3,7,8,9-MxCDF '.2 01 0479 1..58 1,2,3,4,6,7,8-HpCDF 3.43 0.30 1.58 1,2,3,4,7,8,9-HpCDF 2.39 0.36 1.58 OCDF 6.23 0.34 3.17 2,3,7,8-TCDD 0.35 0.16 0.32 1,2,3,7,8-PeCDD 1.85 0.70 1.58 1,2,3,4,7,8-HxCDD 1.84 0.37 1.58 1,2,3,6,7,8-HxCDD 2.24 0.36 1.58 1,2,3,7,8,9-HxCDD 3.60 0.39 1.58 1,2,3,4,6,7,8-HpCDD 17.7 0.30 1.58 OCDD 204 0.28 3.17 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 56 13C-1,2,3,7,8-PeCDF 65 13C-2,3,4,7,8-PeCDF 67 13C-1,2,3,4,7,8-HxCDF 62 13C-1,2,3,6,7,8-HxCDF 13C-2,3,4,6,7,8-HxCDF 63 13C-1,2,3,7,8,9-HxCDF 64 13C-1,2,3,4,6,7,8-HpCDF 70 13C-1,2,3,4,7,8,9-HpCDF 74 13C-2,3,7,8-TCDD 68 13C-1,2,3,7,8-PeCDD 65 13C-1 2,3,4,7,8-HxCDD 60 13C-1,2,3,6,7,8-HxCDD 62 3C-1,2,3,4,6,7,8-HpCDD 70 GERG/TAMU 13C-OCDD 76 Date: 8/25/95 PCDD/PCDF Analysis Page 2 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Sediment Samples LAB SAMPLE ID K9609 CLIENT SAMPLE ID GBOB INSTRUMENT DATA FILE 50721 LCA03-S 10 WET WEIGHT 42.99 DRY WEIGHT 9.89 PERCENT SOLIDS 23.00 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX SEDIMENT QC BATCH DX0209 EXTRACTION DATE 7-7-95 ANALYSIS DATE 7-21-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 1.65 0.19 1.01 DB225 1,2,3,7,8-PeCDF 2.71 1.28 5.06 1 2,3,4,7,8-PeCDF 3.53 1.48 5.06 1 1,2,3,4,7,8-HxCDF 3.65 1.28 5.06 1 1,2,3,6,7,8-HxCDF 4.13 1.21 5.06 1 2,3,4,6,7,8-HxCDF 4.28 1.42 5.06 1 1,2,3,7 1819 HxCDF 2.97 2.05 .5.06 1,2,3,4,6,7,8-HpCDF 21.9 0.68 5.06- 1,2,3,4,7,8,9-HpCDF 3.95 0.80 5.06 1 OCDF 46.0 0.61 10.1 2,3,7,8-TCDD 0.71 0.24 1.01 1,2,3,7,8-PeCDD 4.07 0.93 5.06 1 1,2,3,4,7,8-HxCDD 73.0 0.69 5.06 1,2,3,6,7,8-HxCDD 20.0 0.69 5.06 1,2,3,7,8,9-HxCDD 9.77 0.73 5.06 1,2,3,4,6,7,8-HpCDD 132 0.69 5.06 OCDD 1300 0.68 10.1 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 75 13C-1,2,3,7,8-PeCDF 89 13C-2,3,4,7,8-PeCDF 98 13C-1,2,3,4,7,8-HxCDF 75 13C-1,2,3,6,7,8-HxCDF 72 13C-2,3,4,6,7,8-HxCDF 79 13C-1,2,3,7,8,9-HxCDF 85 13C-1,2,3,4,6,7-,8-HpCDF 86 13C-1,2,3,4,7,8,9-HpCDF 91 3C-2,:@,7,'8-TCDD 96 13C-1,2,3,7,8-PeCDD 95 13C-1,2,3,4,7,&HxCD-D 80 13C-1,2,3,6,7,8-HxCDD 74 3C-1,2,3,4,6,7,8-HpCDD 87 13C-OCDD 103 GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 3 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Sediment Samples LAB SAMPLE ID - K9610 CLIENT SAMPLE ID BRCL INSTRUMENT DATA FILE 5 07 21 LCA03-S 11 WET WEIGHT 41.65 DRY WEIGHT 21.86 PERCENT SOLIDS 52.48 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX SEDIMENT OC BATCH DX0209 EXTRACTION DATE 7-7-95 ANALYSIS DATE 7-21-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 1.52 0.07 0.46 DB225 1,2,3,7,8-PeCDF 2.45 2.42 2.29 2,3,4,7,8-PeCDF 2.33 2.91 2.29 1,2,3,4,7,8-HxCDF 13.6 1.0b 2.29 1,2,3,6,7,8-HxCDF 7.'88 1.03 2.29 2,3,4,6,7,8-HxCDF 5.13 -1.23 2.29 2,3'7,8,9MxCDF 3.77- Z 19 . I .. j.f)1 . ! I .. . .I ... 1,2,3,4,6,7,8-HpCDF '5 1'6 1.24 2.29 1,2,3,4,7,8,9-HpCDF 18.2 0.27 2.29 OCDF 296 0.14 4.57 2,3,7,8-TCDD 0.31 0.10 0.46 1,2,3,7,8-PeCDD 1.39 0.71 2.29 1 1,2,3,4,7,8-HxCDD 1.83 0.36 2.29 1 1,2,3,6,7,8-HxCDD 2.25, 0.34 2.29 1 1,2,3,7,8,9-HxCDD 0.37 2.29 N D 1,2,3,4,6,7,8-HpCDD 27.5 0.24 2.29 OCDD 281 0.37 4.57 Internal Standard % Recov D13 Qual % Recoveries 13C-2,3,7,8-TCDF 82 13C-1,2,3,7,8-PeCDF 103 13C-2,3,4,7,8-PeCDF 107 13C-1,2,3,4,7,8-HxCDF 150 Q 13C-1,2,3,6,7,8-HxCDF 146 13C-2,3,4,6,7,8-HxCDF 155 Q 13C-1,2,3,7,8,9-HxCDF 171 Q 13C-1,2,3,4,6,7,8-HpCDF 166 Q 13C-1,2,3,4,7,8,9-HpCDF 194 a 13C-213,7,8-TCDD lob 13C-1,2,3,7,8-PeCDD 105 13C-1,2,3,4,7,8-HxCDD 152 Q 13C-1,2,3,6,7,8-HxCDD 157 Q 3C-1,2,3,4,6,7,8-HpCDD 162 Q 13C-OCDD 205 Q GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 4 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Sediment Samples LAB SAMPLE ID K961 1 CLIENT SAMPLE ID BRFS INSTRUMENT DATA FILE 507 21 LCA03-S 12 WET WEIGHT 42.42 DRY WEIGHT 21.59 PERCENT SOLIDS 50.89 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX SEDIMENT QC BATCH DX0209 EXTRACTION DATE 7-7-95 ANALYSIS DATE 7-21-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 1.85 0.07 0.46 DB225 1,2,3,7,8-PeCDF 1.80 0.57 2.32 1 2,3,4,7,8-PeCDF 1.37 0.66 2.32 1 1,2,3,4,7,8-HxCDF 3.50 0.37 2.32 1,2,3,6,7,8-HxCDF 2.*26 0.37 2.32 a 2,3,4,6,7,8-HxCDF .1.80. 0.41 2.32 .1 9-HxCDF 1m.74' 0.55 2.32 J .,2,3,.7 8, 1,2,8,4,6,7,'8-HpCDF 10.3- '0. 16 2.32 1,2,3,4,7,8,9-HpCDF 3.43 0.19 2.32 OCDF 54.8 0.21 4.63 2,3,7,8-TCDD 0.21 0.08 0.46 J 1,2,3,7,8-PeCDD 0.95 0.31 2.32 1,2,3,4,7,8-HxCDD 1.26 0.29 2.32 1,2,3,6,7,8-HxCDD 1.22 2.32 ND 1,2,3,7,8,9-HxCDD 1.42 0.30 2.32 1,2,3,4,6,7,8-HpCDD 14.0 0.21 2.32 OCDD 141 0.28 4.63 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 83 13C-1,2,3,7,8-PeCDF 101 13C-2,3,4,7,8-PeCDF 107 13C-1,2,3,4,7,8-HxCDF 76 13C-1,2,3,6,7,8-HxCDF 72 13C-2,3,4,6,7,8-HxCDF 80 13C-1,2,3,7,8,9-HxCDF 91 13C-1,2,3,4,6,7,8-HpCDF 89 13C-1,2,3,4,7,8,9-HpCDF 97 13C-2,3,7,8-TCDD 13C-1,2,3,7,8-PeCDD 107 13C-1,2,3,4,7,8-HxtDD 83 13C-1,2,3,6,7,8-HxCDD 80 3C-1,2,3,4,6,7,8-HpCDD 92 13C-OCDD 107 GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 5 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Sediment Samples LAB SAMPLE ID K9612 CLIENT SAMPLE ID GBTD INSTRUMENT DATA FILE 50721 LCA03-S 13 WET WEIGHT 40.50 DRY WEIGHT 25.92 PERCENT SOLIDS 64.00 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX SEDIMENT aC BATCH DX0209 EXTRACTION DATE 7-7-95 ANALYSIS DATE 7-21-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 2.06 0.04 0.39 DB225 1,2,:a,7,8-PeCDF 0.44 0.23 1.93 1 2,3,4,7,8-PeCDF 0.69 0.26 1.93 1 1,2,3,4,7,8-HxCDF 0.77 0.26 1.93 1 1,2,3,6,7,8-HxCDF 0.78 0.24 1.93 1 2,3,4,6,7,8-HxCDF, 0.77 0.29 1.93 1 ND 1,2,2I,7,8,9-HxCDF 0. 7!5 1.93 1,2,3,4,6,7,8-HpCDF 4.14 0.16 1.93' 1,2,3,4,7,8,9-HpCDF 0.71 0.20 1.93 OCDF 18.0 0.12 3.86 2,3,7,8-TCDD 0.67 0.06 0.39 1,2,3,7,8-PeCDD 0.97 0.29 1.93 1,2,3,4,7,8-HxCDD 1.05 1.93 N D 1,2,3,6,7,8-HxCDD 1.23 1.93 ND 1,2,3,7,8,9-HxCDD 2.46 1.93 ND 1,2,3,4,6,7,8-HpCDD 40.6 0.17 1.93 OCDD 841 0.26 3.86 Internal Standard % Recov DI3 Qual % Recoveries 13C-2,3,7,8-TCDF 75 13C-1,2,3,7,8-PeCDF 88 13C-2,3,4,7,8-Pe CDF 94 13C-1,2,3,4,7,8-HxCDF 70 13C-1,2,3,6,7,8-HxCDF 68 13C-2,3,4,6,7,8-HxCDF 74 13C-1,2,3,7,8,9-HxCDF 82 13C-1,2,3,4,6,7,8-HpCDF 84 13C-1,2,3,4,7,8,9-HpCDF 90 13C-2,3,7,8-TCDD 87 13C-1,2,3,7,8-PeCDD 93 13C-1,2,3,4,7',8-HxCDD 73 1 jC-1,2,3,6,7,8-HxCDD 74 3C-1,2,3,4,6,7,8-HpCDD 82 GERG/TAMU 13C-OCDD 94 Date: 8/25/95 PCDD/PCDF Analysis Page 6 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Sediment Samples LAB SAMPLE ID K9613 CLIENT SAMPLE ID GBHR INSTRUMENT DATA FILE 50721LCA03-S14 WET WEIGHT 40.65 DRY WEIGHT 11.38 PERCENT SOLIDS 28.00 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX SEDIMENT QC BATCH DX0209 EXTRACTION DATE 7-7-95 ANALYSIS DATE 7-21-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 1.85 0.09 0.88 DB225 1,2,3,7,8-PeCDF 0.91 0.71 4.39 1 2,3,4,7,8-PeCDF 1.42 4.39 ND 1,2,3,4,7,8-HxCDF 1.26 4.39 ND 1,2,3,6,7,8-HxCDF 1.15 4.39 ND 2,3,4,6,7,8-Hx CDF 1.32 4.39 ND :..1,2,3,7,8."9-HXCDF 1.17 0.86 4.39 1,2,3,4,6,7,8-HpCDF 5.16 0.25 4.39 1,2,3,4,7,8,9-HpCDF 0.89 4.39 ND OCDF 13.5 0.19 8.79 2,3,7,8-TCDD 0.85 0.88 ND 1,2,3,7,8-PeCDD 1.49 1.06 4.39 1,2,3,4,7,8-HxCDD 3.39 0.42 4.39 1,2,3,6,7,8-HxCDD 3.97 0.40 4.39 1,2,3,7,8,9-HxCDD 6.81 0.44 4.39 112,3,4,6,7,8-HpCDD 108 0.37 4.39 OCDD 2098 0.61 8.79 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 81 13C-1,2,3,7,8-PeCDF 99 13C-2,3,4,7,8-PeCDF 103 13C-1,2,3,4,7,8-HxCDF 69 13C-1,2,3,6,7,8-HxCDF 67 13C-2,3,4,6,7,8-HxCDF 72 13C-1,2,3,7,8,9-HxCDF 82 13C-1,2,3,4,6,7,8-HpCDF 81 13C-1,2,3,4,7,8,9-HpCDF 91 *1 3C-2,3,7,8-TCDD 96 13C-1,2,3,7,8-PeCDD 101 13C-1,2,3,4,7,8-HxCDD 71 13C-1,2,3,6,7,8-HxCDD 71 3C-1,2,3,4,6,7,8-HpCDD 82 13C-OCDD 98 GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 7 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Sediment Samples LAB SAMPLE ID K9614 CLIENT SAMPLE ID GBYC INSTRUMENT DATA FILE 50721LCA03-S15 WET WEIGHT 41.47 DRY WEIGHT 20.74 PERCENT SOLIDS 50.00 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX SEDIMENT QC BATCH DX0209 EXTRACTION DATE 7-7-95 ANALYSIS DATE 7-21-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 9.06 0.06 0.48 DB225 1,2,3,7,8-PeCDF 0.72 0.45 2.41 1 2,3,4,7,8-PeCDF 0.85 0.53 2.41 1 1,2,3,4,7,8-HxCDF 1.03 0.32 2.41 1 1,2,3,6,7,8-HxCDF 0.76 2.41 ND 2,3,4,6,7,8-HxCDF 0.82 2.41 ND 1,2,3,7,8,9-HxCDF., 0.64 2.41 @ND 1@,2'3,4,6,7-8-HpCDF 5.47 0.06 2.41 1,213,4,7,8:9-HpCDF 0.73 2.41 ND OCDF 35.4 0.06 4.82 2,3,7,8-TCDD 2.59 0.10 0.48 1,2,3,7,8-PeCDD 0.61 2.41 ND 1,2,3,4,7,8-HxCDD 1.35 0.26 2.41 1 1,2,3,6,7,8-HxCDD 2.43 2.41 ND 1,2,3,7,8,9-HxCDD 4.16 0.26 2.41 1,2,3,4,6,7,8-HpCDD 66.8 0.09 2.41 OCDD 2839 0.18 4.82 Internal Standard % Recov D13 Qual % Recoveries 13C-2,3,7,8-TCDF 80 13C-1,2,3,7,8-PeCDF 98 13C-2,3,4,7,8-PeCDF 107 13C-1,2,3,4,7,8-HxCDF 79 13C-1,2,3,6,7,8-HxCDF 45 13C-2,3,4,6,7,8-HxCDF 82 13C-1,2,3,7,8,9-HxCDF 94 13C-1,2,3,4,6,7,8-HpCDF 94 13C-1,2,3,4,7,8,9-HpCD F 110 13C-2,3,7 ' 8-TCDD --93 13C-1,2,3,7,8-PeCDD 103 13C-1,2,3,4,7,8-HxCDD 74 13C-1,2,3,6,7,8-HxCDD 73 3C-1,2,3,4,6,7,8-HpCDD 98 GERG/TAMU 13C-OCDD 131 Date: 8/25/95 PCDD/PCDF Analysis Page 8 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Sediment Samples LAB SAMPLE ID Q10569 CLIENT SAMPLE ID INSTRUMENT DATA FILE 50721 LCA03-S8 WET WEIGHT 20.00 DRY WEIGHT 20.00 PERCENT SOLIDS CALCULATION BASIS DRY SAMPLE TYPE BLANK MATRIX QC BATCH DX0209 EXTRACTION DATE 7-7-95 ANALYSIS DATE 7-21-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 0.42 0.15 0.50 1,2,3,7,8-PeCDF 2.28 0.35 2.50 2,3,4,7,8-PeCDF 1.81 0.41 2.50 1,2,3,4,7,8-HxCDF 2.16 0.26 2.50 1,2,3,6,7,8-HxCDF 2.60 0.32 2.50 2,3,4,6,7,8-HxCDF 2.19 0.47 2.50 1,2,3,7,8,9-HxCDF. '2;69.'.' ..0.24 2.50' 1,2,3,4,6,7,8LHpCDF 2.78 0.29 2.50 1,2,3,4,7,8,9-HpCDF 2.06 0.29 2.50 OCDF 3.33 0.06 5.00 2,3,7,8-TCDD 0.12 0.50 ND 1,2,3,7,8-PeCDD 2.67 0.27 2.50 1,2,3,4,7,8-HxCDD 1.65 2.50 ND 1,2,3,6,7,8-HxCDD 2.78 0.30 2.50 1,2,3,7,8,9-HxCDD 2.54 2.50 ND 1,2,3,4,6,7,8-HpCDD 2.94 2.50 ND OCDD 4.87 0.31 5.00 Internal Standard % Recov DB Oual % Recoveries 13C-2,3,7,8-TCDF 46 13C-1,2,3,7,8-PeCDF 94 13C-2,3,4,7,8-PeCDF 96 13C-1,2,3,4,7,8-HxCDF 83 13C-1,2,3,6,7,8-HxCDF 77 13C-2,3,4,6,7,8-HxCDF 77 13C-1,2,3,7,8,9-HxCDF 81 13C-1,2,3,4,6,7,8-HpCDF 84 13C-1,2,3,4,7,8,9-HpCDF 91 13C-2,3,7,8-TCDD 74 13C-1,2,3,7,8-PeCDD 96 13C-1,2,3,4,7,8-HxCDD 82 13C-1,2,3,6,7,8-HxCDD 78 3C-1,2,3,4,6,7,8-HpCDD 86 13C-OCDD 90 GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 9 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Sediment Samples LAB SAMPLE ID Q10570 CLIENT SAMOLE ID GBYC INSTRUMENT DATA FILE 50721LCA03-S16 WET WEIGHT 41.74 DRY WEIGHT 20.87 PERCENT SOLIDS 50.00 CALCULATION BASIS DRY SAMPLE TYPE DUP MATRIX SEDIMENT QC BATCH DX0209 EXTRACTION DATE 7-7-95 ANALYSIS DATE 7-21-95 Conc EDL LMCL DBQuaI Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 8.42 0.05 0.48 DB225 1,2,3,7,8-PeCDF 0.62 0.38 2.40 1 2,3,4,7,8-PeCDF 1.03 0.44 2.40 1 1,2,3,4,7,8-HxCDF 0.91 2.40 ND 1,2,3,6,7,8-HxCDF 0.68 2.40 ND 2,3,4,6,7,8-HxCDF 0.70 0.25 2.40 1 1,2,3,7,8,9-HxCDF 0.61 0.35 2.40 1 1,2,3,4,6,7,8-HpCDF 4.41 0.10 2.40 1,2,3,4,7,8,9-HpCDF 0.54 0.11 2.40 1 OCDF 32.5 0.12 4.79 2,3,7,8-TCDD 2.46 0.10 0.48 1,2,3,7,8-PeCDD 0.82 2.40 ND 1,2,3,4,7,8-HxCDD 1.01 2.40 ND 1,2,3,6,7,8-HxCDD 1.84 2.40 ND 1,2,3,7,8,9-HxCDD 2.78 2.40 ND 1,2,3,4,6,7,8-HpCDD 55.9 0.14 2.40 OCDD 2316 0.23 4.79 Internal Standard % Recov D13 Qua[ % Recoveries 13C-2,3,7,8-TCDF 80 13C-1,2,3,7,8-PeCDF 97 13C-2,3,4,7,8-PeCDF 102 13C-1,2,3,4,7,8-HxCDF 78 13C-1,2,3,6,7,8-HxCDF 70 13C-2,3,4,6,7,8-HxCDF 81 13C-1,2,3,7,8,9-HxCDF 88 13C-1,2,3,4,6,7,8-HpCDF 89 13C-1,2,3,4,7,8,9-HpCDF 112 13C-2,3,7,8-TCDD 96 13C-1,2,3,7,8-PeCDD 98 13C-1,2,3,4,7,8-HxCDD 66 13C-1,2,3,6,7,8-HxCDD 74 3C-1,2,3,4,6,7,8-HpCDD 96 GERGfTAMU 13C-OCDD 117 Date: 8/25/95 PCDDIPCDF Analysis Page 10 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Sediment Samples LAB SAMPLE ID K9614 Q10570 CLIENT SAMPLE ID GBYC GBYC INSTRUMENT DATA FILE 50721 LCA03-S 15 50721 LCAO@-,S 16 WET WEIGHT 41.47 41.74 DRY WEIGHT 20.74 20.87 PERCENT SOLIDS 50.00 50.00 CALCULATION BASIS DRY DRY SAMPLE TYPE SAMP DUP MATRIX SEDIMENT SEDIMENT QC BATCH DX0209 DX0209 EXTRACTION DATE 7-7-95 7-7-95 ANALYSIS DATE 7-21-95 7-21-95 Conc Conc RPD DB Compound Name (pg/g) (pg1g) Qual 2,3,7,8-TCDF 9.06 8.42 7 1,2,3,7,8-PeCDF 0.72 0.62 15 2,3,4,7,8-PeCDF 0.85 1.03 19 1,2,3,4,7,8-HxCDF 1.03 1,2,3,6,7,8-HxCDF 2,3,4,6,7,8-HxCDF 0.70 1,2,3,7,8,9-HxCDF 0.61 1,2,3,4,6,7,8'HpCDF 5.47 4.41 21 1,2,3,4,7,8,9-HpCDF 0.54 OCDF 35.4 32.5 9 2,3,7,8-TCDD 2.59 2.46 5 1,2,3,7,8-PeCDD 1,2,3,4,7,8-HxCDD 1.35 1,2,3,6,7,8-HxCDD 1,2,3,7,8,9-HxCDD 4.16 1,2,3,4,6,7,8-HpCDD 66.8 55.9 18 OCDD 2839 2316 20 Internal Standard % Recoveries 13C-:2,3,7,8-TCDF 13C-1,2,3,7,8-PeCDF 13C-2,3,4,7,8-PeCDF 13C-1,2,3,4,7,8-HxCDF 13C-1,2,3,6,7,8-HxCDF 13C-2,3,4,6,7,8-HxCDF 13C-1,2,3,7,8,9-HxCDF 13C-1,2,3,4,6,7,8-HpCDF 13C-1,2,3,4,7,8,9-HpCDF 13C-2,3,7,87-TCDD 13C-1,2,3,7,8-PeCDD 13C-1,2,3,4,7,8-HxCDD 13C-1,2,3,6,7,8-HxCDD 3C-1,2,3,4,6,7,8-HpCDD 13C-OCDD GERG/TAMU Date: 8/26/95 PCDD/PCDF Analysis Page 11 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Sediment Samples LAB SAMPLE ID G10572 CLIENT SAMPLE ID GBTD INSTRUMENT DATA FILE 5 07 21 LCA03-S 18 WET WEIGHT 40.82 DRY WEIGHT 26.12 PERCENT SOLIDS 64.00 CALCULATION BASIS DRY SAMPLE TYPE MS MATRIX SEDIMENT QC BATCH DX0209 EXTRACTION DATE 7-7-95 ANALYSIS DATE 7-21-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 213,7,8-TCDF 45.1 0.03 0.38 DB225 1,2,3,7,8-PeCDF 168 0.21 1.91 2,3,4,7,8-PeCDF 191 0.25 1.91 1,2,3,4,7,8-HxCDF 165 0.22 1.91 1,2,3,6,7,8-HxCDF 166 0.20 1.91 2,3,4,6,7,8-HxCDF 157 0.23 1.91 1,2,3,7,8,9-HxCDF 162 0.29 1.91 1,2,3,4,6,7 8-HpCDF 172 0.02 1.91 1,2,3,4,7,8:0-HpCDF 165 0.03 1.91 OCDF 410 0.05 3.83 2,3,7,8-TCDD 28.3 0.03 0.38 1,2,3,7,8-PeCDD 175 0.22 1.91 1,2,3,4,7,8-HxCDD 175 0.47 1.91 1,2,3,6,7,8-HxCDD 181 0.36 1.91 1,2,3,7,8,9-HxCDD 197 0.44 1.91 1,2,3,4,6,7,8-HpCDD 218 0.12 1.91 OCDD 1153 0.08 3.83 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 85 13C-1,2,3,7,8-PeCDF 103 13C-2,3,4,7,8-PeCDF 105 13C-1,2,3,4,7,8-HxCDF 83 13C-1,2,3,6,7,8-HxCDF 73 13C-2,3,4,6,7,8-HxCDF 87 13C-1,2,3,7,8,9-HxCDF 97 13C-1,2,3,4,6,7,8-HpCDF 117 13C-1,2,3,4,7,11,9-HpCDF 142 13C-2,3,7,8-TCDD 97 13C-1,2,3,7,8-PeCDD 100 13C-1,2,3,4,7,8-HxCDD 82 13C-1,2,3,6,7,8-HxCDD 75 3C-1,2,3,4,6,7,8-HpCDD 123 GERG/TAMU 13C-OCDD 139 Date: 8/25/95 PCDD/PCDF Analysis Page'l 2 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Sediment Samples LAB SAMPLE ID K9612 Ql 0572 CLIENT SAMPLE ID GBTD GBTD INSTRUMENT DATA FILE 50721LCA03-S13 50721LCA03-.Sl8 WET WEIGHT 40.50 40.82 DRY WEIGHT 25.92 26.12 PERCENT SOLIDS 64.00 64.00 CALCULATION BASIS DRY DRY SAMPLE TYPE SAMP IVIS MATRIX SEDIMENT SEDIMENT QC BATCH DX0209 DX0209 EXTRACTION DATE 7-7-95 7-7-95 ANALYSIS DATE 7-21-95 7-21-95 Conc Spike Arnnt Conc Rq90V DB Compound Name (pg/g) (pg/g) (pg/g) (6/-) Qual 2,3,7,8-TCDF 2.06 30.6 45.1 141 Q 1,2,3,7,8-PeCDF 0.44 153 168 log 2,3,4,7,8-PeCDF 0.69- 153 191 124 1,2,3,4,7,8-HxCDF 0.77 153 165 107 1,2,3,6,7,8-HxCDF 0.78 153 166 108 2,3,4,6,7,8-HxCDF 0.77 153 157 102 1,2,3,7,8,9-HxCDF 153 162 106 1,2,3,4,6,7,8-HpCDF 4.14 153 172 110 1,2,3,4,7,8,9-HpCDF 0.71 153 165 107 OCDF 18.0 306 410 128 2,3,7,8-TCDD 0.67 31 28.3 90 1,2,3,7,8-PeCDD 0.97 153 175 114 1,2,3,4,7,8-HxCDD 153 175 114 1,2,3,6,7,8-HxCDD 153 181 118 1,2,3,7,8,9-HxCDD 153 197 129 1,2,3,4,6,7,8-HpCDD 40.6 153 218 116 OCDD 841 306 1153 102 Internal Standard % Recoveries 13C-2,3,7,8-TCDF 13C-1,2,3,7,8-PeCDF 13C-2,3,4,7,8-PeCDF 13C-1,2,3,4,7,8-HxCDF 13C-1,2,3,6,7,8-HxCDF 13C-2,3,4,6,7,8-HxCDF 13C-1,2,3,7,8,9-HxCDF 13C-1,2,3,4,6,7,8-HpCDF 13C-1,2,3,4,7,8,9-HpCDF 13C-2,3,7,8-TCDD 13C-1,2,3,7,8-PeCDD 13C-1,2,3,4,7,8-HxCDD 13C-1,2,3,6,7,8-HxCDD 3C-1,2,3,4,6,7,8-HpCDD 13C-OCDD GERG[TAMU Date: 8/25/95 PCDD/pCDF Analysis Page 13 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Sediment Samples LAB SAMPLE ID G10573 CLIENT SAMPLE ID GBTD INSTRUMENT DATA FILE 50721 LCA03-S 19 WET WEIGHT 41.63 DRY WEIGHT 26.64 PERCENT SOLIDS 64.00 CALCULATION BASIS DRY SAMPLE TYPE MSD MATRIX SEDIMENT QC BATCH DX0209 EXTRACTION DATE 7-7-95. ANALYSIS DATE 7-21-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 44.5 0.02 0.38 DB225 1,2,3,7,8-PeCDF 166 0.11 1.88 2,3,4,7,8-PeCDF 186 0.13 1.88 1,2,3,4,7,8-HxCDF 159 0.11 1.88 1,2,3,6,7,8-HxCDF 162 0.13 1.88 2,3,4,6,7,8-HxCDF 160 0.13 1.88 1,2,3,7,8,9-HxCDF 154 0.15 1.88 1,2,3,4,6,7,8-HpCDF 175 0.03 1.88 1,2,3,4,7,8,9-HpCDF 160 0.03 1.88 OCDF 398 0.04 3.75 2,3,7,8-TCDD 28.7 0.04 0.38 1,2,3,7,8-PeCDD 175 0.11 1.88 1,2,3,4,7,8-HxCDD 167 0.04 1.88 1,2,3,6,7,8-HxCDD 192 0.04 1.88 1,2,3,7,8,9-HxCDD 210 0.04 1.88 1,2,3,4,6,7,8-HpCDD 212 0.01 1.88 OCDD 1089 0.05 3.75 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 87 13C-1,2,3,7,8-PeCDF 109 13C-2,3,4,7,8-PeCDF 113 13C-1,2,3,4,7,8-HxCDF 86 13C-1,2,3,6,7,8-HxCDF 66 13C-2,3,4,6,7,8-HxCDF 85 13C-1,2,3,7,8,9-HxCDF 100 13C-1,2,3,4,6,7,8-HpCDF 112 13C-1,2,3,4,7,8,9-HpCDF 147 13C-2,3,7,8-TCDD 97 13C-1,2,3,7,8-PeCDD 102 13C-1,2,3,4,7,8-HxCDD 86 13C-1,2,3,6,7,8-HxCDD 66 3C-1,2,3,4,6,7,8-HpCDD 129 GERG/TAMU 13C-OCDD 134 Date: 8/25/95 PCDD/PCDF Analysis Page 14 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Sediment Samples LAB SAMPLE ID K9612 Q10573 CLIENT SAMPLE ID GBTD GBTD INSTRUMENT DATA FILE 50721 LCA03-Sl 3 50721LCA03@-819 WET WEIGHT 40.50 41.63 DRY WEIGHT 25.92 26.64 PERCENT SOLIDS 64.00 64.00 CALCULATION BASIS DRY DRY SAMPLE TYPE SAMP MSD MATRIX SEDIMENT SEDIMENT QC BATCH DX0209 DX0209 EXTRACTION DATE 7-7-95 7-7-95 ANALYSIS DATE 7-21-95 7-21-95 Conc Spike Amnt Conc Rec.ov DI3 Compound Name (pg/g) (pg/g) (pg/g) N.) Qual 2,3,7,8-TCDF 2.06 30 44.5 141 a 1,2,3,7,8-PeCDF 0.44 150 166 lio 2,3,4,7,8-PeCDF 0.69 150 186 123 1,2,3,4,7,8-HxCDF 0.77 150 159 105 1,2,3,6,7,8-HxCDF 0.78 150 162 107 2,3,4,6,7,8-HxCDF 0.77 150 160 106 1,2,3,7,8,9-HxCDF 150 154 103 1,2,3,4,6,7,8-HpCDF 4.14 150 175 113 1,2,3,4,7,8,9-HpCDF 0.71 150 160 106 OCDF 18.0 300 398 126 2,3,7,8-TCDD 0.67 30 28.7 93 1,2,3,7,8-PeCDD 0.97 150 175 116 1,2,3,4,7,8-HxCDD 150 167 ill 1,2,3,6,7,8-HxCDD 150 192 128 1,2,3,7,8,9-HxCDD 150 210 140 Q 1,2,3,4,6,7,8-HpCDD 40.6 150 212 114 OCDD 841 300 1089 82 Internal Standard % Recoveries 13C-2,3,7,8-TCDF 13C-1,2,3,7,8-PeCDF 13C-2,3,4,7,8-PeCDF 1 W-1,2,3,4,7,8-HxCDF 13C-1,2,3,6,7,8-HxCDF 13C-2,3,4,6,7,8-HxCDF 13C-1,2,3,7,8,9-HxCDF 13C-1,2,3,4,6,7,8-HpCDF 13C-1,2,3,4,7,8,9-HpCDF 13C-2,3,7,8-TCDD 13C-1,2,3,7,8-PeCDD 13C-1,2,3,4,7,8-HxCDD 13C-1,2,3,6,7,8-HxCDD 3C-1,2,3,4,6,7,8-HpCDD 13C-OCDD GERGITAMU Date: 8/25/95 PCDD/PCDF Analysis Page 15 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Sediment Samples LAB SAMPLE ID Q1 0572 Q10573 CLIENT SAMPLE ID GBTD GBTD, INSTRUMENT DATA FILE 50721 LCA03-Sl 8 50721LCA03-.S19 WET WEIGHT 40.82 41.63 DRY WEIGHT 26.12 26.64 PERCENT SOLIDS 64.00 64.00 CALCULATION BASIS DRY DRY SAMPLE TYPE MS MSD MATRIX SEDIMENT SEDIMENT QC BATCH DX0209 DX0209 EXTRACTION DATE 7-7-95 7-7-95 ANALYSIS DATE 7-21-95 7-21-95 Conc Conc RPD DB Compound Name (pg/g) (pg/g) 6m Qual 2,3,7,8-TCDF 45.1 44.5 1 1,2,3,7,8-PeCDF 168 166 1 2,3,4,7,8-PeCDF 191 186 3 1,2,3,4,7,8-HxCDF 165 159 4 1,2,3,6,7,8-HxCDF 166 162 2 2,3,4,6,7,8-HxCDF 157 160 2 1,2,3,7,8,9-HxCDF 162 154 5 1,2,3,4,6,7,8-HpCDF 172 175 1 1,2,3,4,7,8,9-HpCDF 165 160 3 OCDF 410 398 3 2,3,7,8-TCDD 28.3 28.7 2 1,2,3,7,8-PeCDD 175 175 0 1,2,3,4,7,8-HxCDD 175 167 5 1,2,3,6,7,8-HxCDD 181 192 6 1,2,3,7,8,9-HxCDD 197 210 7 1,2,3,4,6,7,8-HpCDD 218 212 3 OCDD 1153 1089 6 Internal Standard % Recoveries 13C-2,3,7,8-TCDF 13C-1,2,3,7,8-PeCDF 13C-2,3,4,7,8-PeCDF 13C-1,2,3,4,7,8-HxCDF 13C-1,2,3,6,7,8-HxCDF 13C-2,3,4,6,7,8-HxCDF 13C-1,2,3,7,8,9-HxCDF 13C-1,2,3,4,6,7,8-HpCDF 13C-1,2,3,4,7,8,9-HpCDF 13C-2,3,7,8-TCDD 13C-1,2,3,7,8-PeCDD 13C-1,2,3,4,7,8-HxCDD 13C-1,2,3,6,7,8-HxCDD 3C-1,2,3,4,6,7,8-HpCDD 13C-OCDD GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 16 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Sediment Samples LAB SAMPLE ID Q10571 CLIENT SAMPLE ID INSTRUMENT DATA FILE 50721 LCA03-S 17 WET WEIGHT 5.15 DRY WEIGHT 5.15 PERCENT SOLIDS 100.00 CALCULATION BASIS DRY SAMPLE TYPE SRM 1941A MATRIX SEDIMENT QC BATCH DX0209 EXTRACTION DATE 7-7-95 ANALYSIS DATE 7-21-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF - 115 0.57 1.94 DB225 1,2,3,7,8-PeCDF 150 12.4 9.71 2,3,4,7,8-PeCDF 56.5 14.9 9.71 1,2,3,4,7,8-HxCDF 334 5.60 9.71 1,2,3,6,7,8-HxCDF 94.6 5.44 9.71 2,3,4,6,7,8-HxCDF 44.7 6.09 9.71 1,2,3,7,8,9-HxCDF 60.9 7.53 9.71 1,2,3,4,6,7,8-HpCDF 433 1.14 9.71 1,2,3,4,7,8,9-HpCDF 268 1.16 9.71 OCDF 6983 2.19 19.4 2,3,7,8-TCDD 2.89 1.94 ND 1,2,3,7,8-PeCDD 8.78 9.71 ND 1,2,3,4,7,8-HxCDD 13.6 9.71 ND 1,2,3,6,7,8-HxCDD 27.8 2.95 9.71 1,2,3,7,8,9-HxCDD 23.5 3.42 9.71 1,2,3,4,6,7,8-HpCDD 555 0.99 9.71 OCDD 7192 1.16 19.4 Internal Standard % Recov D13 Qual % Recoveries 13C-2,3,7,8-TCDF 74 13C-1,2,3,7,8-PeCDF 81 13C-2,3,4,7,8-PeCDF 86 13C-1,2,3,4,7,8-HxCDF 71 13C-1,2,3,6,7,8-HxCDF 65 13C-2,3,4,6,7,8-HxCDF 77 13C-1,2,3,7,8,9-HxCDF 83 13C-1,2,3,4,6,7,8-HpCDF 85 13C-1,2,3,4,7,8,9-HpCDF 103 13C-2,3,7,8-TCDD 85 13C-1,2,3,7,8-PeCDD 81 13C-1,2,3,4,7,8-HxCDD 69 13C-1,2,3,6,7,8-HxCDD 66 3C-1,2,3,4,6,7,8-HpCDD 84 13C-OCDD ill GERGITAMU Date: 8/25/95 PCDD/PCDF Analysis Page 17 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Gulf Coast Sediment Samples LAB SAMPLE ID Q10571 NIST 1941 a CLIENT SAMPLE ID INSTRUMENT DATA FILE 50721 LCA03-Sl 7 WET WEIGHT 5.15 DRY WEIGHT 5.15 PERCENT SOLIDS 100.00 CALCULATION BASIS DRY SAMPLE TYPE SRIVI 1941 A SRM MATRIX -SEDIMENT SEDIMENT QC BATCH DX0209 EXTRACTION DATE 7-7-95 ANALYSIS DATE 7-21-95 Conc Lab Average Con. .,Recy Compound Name (pg/g) (pg/g) M 2,3,7,8-TCDF 115 69.7 165 1,2,3,7,8-PeCDF 150 124 121 2,3,4,7,8-PeCDF 56.5 47.0 120 1,2,3,4,7,8-HxCDF 334 291 115' 1,2,3,6,7,8-HxCDF 94.6 72.7 130 2,3,4,6,7,8-HxCDF 44.7 39.1 114 1,2,3,7,8,9-HxCDF 60.9 29.3 208 1,2,3,4,6,7,8-HpCDF 433 374 116 1,2,3,4,7,8,9-HpCDF 268 231 116 OCDF 6983 3455 202 2,3,7,8-TCDD 1.33 1,2,3,7,8-PeCDD 6.29 1,2,3,4,7,8-HxCDD 9.88 1,2,3,6,7,8-HxCDD 27.8 23.2 120 1,2,3,7,8,9-HxCDD 23.5 23.3 101 1,2,3,4,6,7,8-HpCDD 555 418 133 OCDD 7192 5288 136 Internal Standard % Recoveries 13C-2,3,7,8-TCDF 13C-1,2,3,7,8-PeCDF 13C-2,3,4,7,8-PeCDF 13C-1,2,3,4,7,8-HxCDF 13C-1,2,3,6,7,8-HxCDF 13C-2,3,4,6,7,8-HxCDF 13C-1,2,3,7,8,9-HxCDF 13C-1,2,3,4,6,7,8-HpCDF 13C-1,2,3,4,7,8,9-HpCDF 13C-2,3,7,8-TCDD 13C-1,2,3,7,8-PeCDD 13C-1,2,3,4,7,8-HxCDD 13C-1,2,3,6,7,8-HxCDD 3C-1,2,3,4,6,7,8-HpCDD GERG/TAMU 13C-OCDD Date: 8/25/95 PCDD/PCDF Analysis Page 1 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Texas Coast Samples LAB SAMPLE ID K9145 CLIENT SAMPLE ID GBTD Station 1 INSTRUMENT DATA FILE 50718LCA03-S5 WET WEIGHT 10.02 DRY WEIGHT 0.77 PERCENT SOLIDS 7.66 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX021 0 EXTRACTION DATE 6-5-95 ANALYSIS DATE 7-18-95 Conc EDL LMCL DBEual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 131.0 5.78 13.0 DB2T5- 1,2,3,7,8-PeCDF 9.16 65.1 ND 2,3,4,7,8-PeCDF 11.5 65.1 ND 1,2,3,4,7,8-HxCDF 8.44 65.1 ND* 1,2,3,6,7,8-HxCDF 8.26 65.1 ND 2,3,4,6,7,8-HxCDF 10.8 65.1 ND 1.,2j3,7,8,9-HiCDF 16.2.' @65.11 ND. 1,2,3,4,-6,7i8-HpCDF' 16.3 65.1 ND 1,2,3,4,7,8,9-HpCDF 20.8 65.1 ND .OCDF 70.6 130 ND 2,3,7,8-TCDD 25.3 5.36 13.0 1,2,3,7,8-PeCDD 25.9 65.1 ND 1,2,3,4,7,8-HxCDD 15.0 65.1 ND 1,2,3,6,7,8-HxCDD 15.3 65.1 ND 1,2,3,7,8,9-HxCDD 15.6 65.1 ND 1,2,3,4,6,7,8-HpCDD 30.4 17.7 65.1 OCDD 401 34.8 130 Internal Standard % Recov D13 Qual % Recoveries 13C-2,3,7,8-TCDF 57 13C-1,2,3,7,8-PeCDF 60 13C-2,3,4,7,8-PeCDF 59 13C-1,2,3,4,7,8-HxCDF 59 13C-1,2,3,6,7,8-HxCDF 59 13C-2,3,4,6,7,8-HxCDF 59 13C-1,2,3,7,8,9-HxCDF 55 13C-1,2,3,4,6,7,8-HpCDF 61 13C-1,2,3,4,7,8,9-HpCDF 65 . 13C-2,3,7,8-TCDD 71 13C-1,2,3,7,8-PeCDD 60 13C-1,2,3,4,7,8-HxCDD 66 13C-1,2,3,6,7,8-HxCDD 70 3C-1,2,3,4,6,7,8-HpCDD 52 13C-OCDD 27 GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 2 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Texas Coast Samples LAB SAMPLE ID K9146 CLIENT SAMPLE ID GBTD Station 2 INSTRUMENT DATA FILE 50718LCA03-S6 WET WEIGHT 10.04 DRY WEIGHT 1.20 PERCENT SOLIDS 11.96 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX021 0 EXTRACTION DATE 6-5-95 ANALYSIS DATE 7-18-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 70.3 2.89 8.33 DB225 1,2,3,7,8-PeCDF 5.79 41.6 ND 2,3,4,7,8-PeCDF 7.5 41.6 ND 1,2,3,4,7,8-HxCDF 8.50 41.6 ND 1,2,3,6,7,8-HxCDF 7.68 41.6 ND 2,3,4,6,7,8-HxCDF 10.6 41.6 ND 4 -ND'. 1,2,.3,7-,8,9-HxCDF 14.3 71,6 1,2,3,4,6,7,8-HpCDF 10.2 41.6 ND 1,2,3,4,7,8,0-HpCDF 14.7 41.6 ND OCDF 52.3 83.3 ND 2,3,7,8-TCDD 11.4 8.33 ND 1,2,3,7,8-PeCDD 9.54 41.6 ND 1,2,3,4,7,8-HxCDD 13.6 41.6 ND 1,2,3,6,7,8-HxCDD 13.3 41.6 ND 1,2,3,7,8,9-HxCDD 13.9 41.6 ND 1,2,3,4,6,7,8-HpCDD 8.19 41.6 ND OCDD 216 15.3 83.3 Internal Standard % Recov DI3 Qual % Recoveries 13C-2,3,7,8-TCDF 59 13C-1,2,3,7,8-PeCDF 60 13C-2,3,4,7,8-PeCDF 61 13C-1,2,3,4,7,8-HxCDF 60 13C-1,2,3,6,7,8-HxCDF 61 13C-2,3,4,6,7,8-HxCDF 55 13C-1,2,3,7,8,9-HxCDF 58 13C-1,2,3,4,6,7,8-HpCDF 57 13C-1,2,3,4,7,8,9-HpCDF 57 .1 3C-2,3,7,8-TCDD 74 13C-1,2,3,7,8-PeC DD 64 13C-1,2,3,4,7,8-HxCDD 65 13C-1,2,3,6,7,8-HxCDD 71 3C-1,2,3,4,6,7,8-HpCDD 50 13C-OCDD 24 Q GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 3. CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Texas Coast Samples LAB SAMPLE ID K9147 CLIENT SAMPLE ID GBTD Station 3 INSTRUMENT DATA FILE 50718LCA03-S7 WET WEIGHT 10.05 DRY WEIGHT 1.32 PERCENT SOLIDS 13.16 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX021 0 EXTRACTION DATE 6-5-95 ANALYSIS DATE 7-18-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 67.6 2.44 7.56 DB225 1,2,3,7,8-PeCDF 5.89 37.8 ND 2,3,4,7,8-PeCDF 7.33 37.8 ND 1,2,3,4,7,8-HxCDF 2.25 37.8 ND 1,2,3,6,7,8-HxCDF 2.14 37.8 ND 2,3,4,6,7,8-HxCDF 2.59 37.8 ND -,1,2,3,7 8,9@HxcbF 4J7 37.8- ND. 1,2,3,4,6 -7,8-HpCDF .9101 37.8 ND 1,2,3,4,7:8,9-HpCDF 12'.1 37.8 ND OCDF 47.9 75.6 ND 2,3,7,8-TCDD 14.8 4.52 7.56 1,2,3,7,8-PeCDD 12.5 37.8 ND 1,2,3,4,7,8-HxCDD 5.69 37.8 ND 1,2,3,6,7,8-HxCDD 5.97 37.8 ND 1,2,3,7,8,9-HxCDD 6.04 37.8 ND 1,2,3,4,6,7,8-HpCDD 16.5 37.8 ND OCDD, 185 23.3 75.6 Internal Standard % Recov D13 Qual % Recoveries 13C-2,3,7,8-TCDF 68 13C-1,2,3,7,8-PeCDF 71 13C-2,3,4,7,8-PeCDF 71 13C-1,2,3,4,7,8-HxCDF 67 13C-1,2,3,6,7,8-HxCDF 70 13C-2,3,4,6,7,8-HxCDF 69 13C-1,2,3,7,8,9-HxCDF 64 13C-1,2,3,4,6,7,8-HpCDF 75 13C-1,2,3,4,7,8,9-HpCDF 77 13C-2,3,7*8-TCDD 87 13C-1,2,3,7,;-PeCDD 78 13C-1,2,3,4,7,8-HxCDD 80 13C-1,2,3,6,7,8-HxCDD 81 3C-1,2,3,4,6,7,8-HpCDD 69 13C-OCDD 35 GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 4 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Texas Coast Samples LAB SAMPLE ID K9599 CLIENT SAMPLE ID GBCR INSTRUMENT DATA FILE 50718LCA03-S8 WET WEIGHT 10.03 DRY WEIGHT 1.24 PERCENT SOLIDS 12.34 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX021 0 EXTRACTION DATE 6-5-95 ANALYSIS DATE 7-18-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 13.2 5.28 8.08 DB225 1,2,3,7,8-PeCDF 6.10 40.4 ND 2,3,4,7,8-PeCDF 7.67 40.4 ND 1,2,3,4,7,8-HxCDF 4.46 40.4 ND 1,2,3,6,7,8-HxCDF 4.11 40.4 ND 2,3,4"6,7,8-HxCDF .5.46 40.4 ND 1 j2,31-7,8,9-HxCDF 8.51: 40.4, ND* 1,2,3,4,6,7,8-.HpCDF 26.3 40.4 Nb OCDF 33.8 80.8 ND 1,2,3@4,7,8,9-HpCDF 22.5 40.4 ND 2,3,7,8-TCDD 3.57 8.08 ND 1,2,3,7,8-PeCDD 10.1 40.4 ND 1,2,3,4,7,8-HxCDD 6.81 40.4 ND 1,2,3,6,7,8-HxCDD 6.69 40.4 ND 1,2,3,7,8,9-HxCDD 6.95 40.4 ND 1,2,3,4,6,7,8-HpCDD 16.8 40.4 ND OCDD 105 80.8 ND- Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 46 13C-1,2,3,7,8-PeCDF 50 13C-2,3,4,7,8-PeCDF 53 13C-1,2,3,4,7,8-HxCDF 54 13C-1,2,3,6,7,8-HxCDF 55 13C-2,3,4,6,7,8-HxCDF 52 13C-1,2,3,7,8,9-HxCDF 46 13C-1,2,3,4,6,7,8-HpCDF 53 13C-1,2,3 4,7,8,9-HpCDF 54 13C-2,3,7,8-TCDD 61 13C-1,2,3,7,8-PeCDD 55 13C-1,2,3,4,7,8-'HxCDD 58 13C-1,2,3,6,7,8-HxCDD 63 3C-1,2,3,4,6,7,8-HpCDD 50 13C-OCDD 32 GERG/TAMU Date: 8/25/95 PCDDIPCDF Analysis Page 5 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Texas Coast Samples LAB SAMPLE ID K9600 CLIENT SAMPLE ID GBOB INSTRUMENT DATA FILE 50718LCA03-S9 WET WEIGHT 10.21 DRY WEIGHT 1.73 PERCENT SOLIDS 16.96 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX021 0 EXTRACTION DATE 6-5-95 ANALYSIS DATE 7-18-95 Conc EDL LMCL DBQuW1- Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 2.60 .5.77 ND 1,2,3,7,8-PeCDF 5.85 28.9 ND 2,3,4,7,8-PeCDF 6.45 28.9 ND 1,2,3,4,7,8-HxCDF 5.18 28.9 ND 1,2,3,6,7,8-HxCDF 5.19 28.9 ND 2,3,4,6,7,8-Hx,CDF 6.24- 28.9 ND 1,2j3,7,8,9-HxCDF.- 9.59. .-:@8..9 ND 1,2,3,4,6,7 8-HpCDF 3.09 28.9 ND 1,2,:3,4,7,8:9-HpCDF 4.15 28.9 ND OCDF 23.4 57.7 ND 2,3,7,8-TCDD 2.13 5.77 ND 1,2,3,7,8-PeCDD 7.73 28.9 ND 1,2,3,4,7,8-HxCDD 10.4 28.9 ND 1,2,3,6,7,8-HxCDD 9.63 28.9 ND 1,2,3,7,8,9-HxCDD 10.4 28.9 ND 1,2,3,4,6,7,8-HpCDD 7.49 28.9 ND OCDD 15.6 57.7 ND Internal Standard % Recov DB Qua[ % Recoveries 13C-2,3,7,8-TCDF 61 13C-1,2,3,7,8-PeCDF 67 13C-2,3,4,7,8-PeCDF 73 13C-1,2,3,4,7,8-HxCDF 62 13C-1,2,3,6,7,8-HxCDF 63 13C-2,3,4,6,7,8-HxCDF 61 13C-1,2,3,7,8,9-HxCDF 55 13C-1,2,3,4,6,7,8-HpCDF 67 13C-1,2,3,4,7,8,9-HpCDF 66 13C-2,3,7,8-TCDD 75 13C-1,2,3,7,8-PeCDD 73 13t-1,2,3,4,7,8-HxCDD 76 13C-1,2,3,6,7,8-HxCDD 74 3C-1,2,3,4,6,7,8-HpCDD 62 GERG/TAMU 13C-OCDD 51 Date: 8/25/95 PCDD/PCDF Analysis Page 6 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Texas Coast Samples LAB SAMPLE ID K9601 CLIENT SAMPLE ID BRCL INSTRUMENT DATA FILE 50718LCA03-SlO WET WEIGHT 10.07 DRY WEIGHT 0.72 PERCENT SOLIDS 7.14 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX021 0 EXTRACTION DATE 6-5-95 ANALYSIS DATE 7-18-95 Compound Name Conc EDL LMCL DBQual (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 4.98 13.9 ND 1,2,3,7,8-PeCDF 26.1 69.5 ND 2,3,4,7,8-PeCDF 35.6 69.5 ND 1,2,3,4,7,8-HxCDF 23.4 69.5 ND 1,2,3,6,7,8-'HxCDF 24.1 69.5 'ND 2,3,4,6,7,8-HxCDF 28.0 '69.5 ND -,li2,3,7,8,9-HxCDF .48.9: .69.6 AD 1,2,314,6,7,8-HpCDF 17.0 69.5 ND 1,2,3,4,7,8,9-HpCDF 22.8 69.5 ND OCDF 100 139 ND 2,3,7,8-TCDD 6.47 13.9 ND 1,2,3,7,8-PeCDD 36.3 69.5 ND 1,2,3,4,7,8-HxCDD 41.2 .69.5 ND 1,2,3,6,7,8-HxCDD 45.5 69.5 ND 1,2,3,7,8,9-HxCDD 45.1 69.5 ND 1,2,3,4,6,7,8-HpCDD 19.3 69.5 ND OCIDD 72.3 139 ND Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 55 13C-1,2,3,7,8-PeCDF 58 13C-2,3,4,7,8-PeCDF 55 13C-1,2,3,4,7,8-HxCDF 57 13C-1,2,3,6,7,8-HxCDF 63 13C-2,3,4,6,7,8-HxCDF 59 13C-1,2,3,7,8,9-HxCDF 53 13C-1,2,3,4,6,7,8-HpCDF 59 13C-1,2,3,4,7,8,9-HpCDF 62 13C-2,3,7,8-TCDD 75 13C-1,2,3,7,8-PeCDD. 65 13C-1,2,3,4,7,8-HxCDD 68 13C-1,2,3,6,7,8-HxCDD 67 3C-1,2,3,4,6,7,8-HpCDD 55 13C-OCDD 41 GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 7 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Texas Coast Samples LAB SAMPLE ID K9602 CLIENT SAMPLE ID BRFS INSTRUMENT DATA FILE 50718LCA03-Sl 1 WET WEIGHT 10.04 DRY WEIGHT 0.85 PERCENT SOLIDS 8.43 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX021 0 EXTRACTION DATE 6-5-95 ANALYSIS DATE 7-18-95 Conc EDL LMCL DBQuaI Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 7.29 11.8 ND 1,2,3,7,8-PeCDF 22.8 59.1 ND 2,3,4,7,8-PeCDF 27.8 59.1 ND 1,2,3,4,7,8-HxCDF 33.1 59.1 ND 1,2,3,6,7,8-HxCDF 28.4 59.1 ND 2,3,4,6,7,8-HxCDF 38.5 59.1 ND .1 1'2,3j,8,9-HxCbF. 64.6 59.1 ND 1,2,3,4i6,7,8-HpCDF. 17.8 69.1 ND 1,2,3,4,7,'8,9-HpCDF 22.1. 59.1 ND OCDF 21.6 118 ND 2,3,7,8-TCDD 4.97 11.8 ND 1,2,3,7,8-PeCDD 36.8 59.1 ND 1,2,3,4,7,8-HxCDD 36.5 59.1 ND 1,2,3,6,7,8-HxCDD 34.0 59.1 ND 1,2,3,7,8,9-HxCDD 36.3 59.1 ND 1,2,3,4,6,7,8-HpCDD 16.0 59.1 ND OCDD 35.6 118 ND Internal Standard % Recov DB Qua] % Recoveries 13C-2,3,7,8-TCDF 61 13C-1,2,3,7,8-PeCDF 66 13C-2,3,4,7,8-PeCDF 66 13C-1,2,3,4,7,8-HxCDF 59 13C-1,2,3,6,7,8-HxCDF 64 13C-2,3,4,6,7,8-HxCDF 58 13C-1,2,3,7,8,9-HxCDF 55 13C-1,2,3,4,6,7,8-HpCDF 61 13C-1,2,3,4,7,8,9-HpCDF 73 13C-2,3,7,8-TCDD- 84 13C-1,2,3,7,8-PeCDD 72 13C-1,2,3,4,7,8-HxCDD 65 13C-1,2,3,6,7,8-HxCDD 69 3C-1,2,3,4,6,7,8-HpCDD 65 13C-OCDD 46 GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 8 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Texas Coast Samples LAB SAMPLE ID K9606 CLIENT SAMPLE ID GBHR INSTRUMENT DATA FILE 50718LCA03-S 12 WET WEIGHT 10.29 DRY WEIGHT 1.07 PERCENT SOLIDS 10.38 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX021 0 EXTRACTION DATE 6-5-95 ANALYSIS DATE 7-18-95 Conc EDL LMCL DBQual Compound Name' (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 1.86 9.36 ND 1,2,3,7,8-PeCDF 3.40 46.8 ND 2,3,4,7,8-PeCDF 4.73 46.8 ND 1,2,3,4,7,8-HxCDF 3.74 46.8 ND 1,2,3,6,7,8-HxCDF. 3.72 46.8 ND 2,3,4,6,7,8-HxCDF 4.65 4:6.8. ND -46'.8 ND .1,2,3,7,8,9-HxCDF 7.14. 112,3,4,6,7,8-HpCDF 8.70 - 46.8 1`41) 1,2,3,4,7,8,9-HpCDF 9.30 46.8 ND OCDF 11.2 93.6 ND 2,3,7,8-TCDD 2.52 9.36 ND 1,2,3,7,8-PeCDD 16.7 46.8 ND 1,2,3,4,7,8-HxCDD 10.1 46.8 ND 1,2,3,6,7,8-HxCDD 9.93 46.8 ND 1,2,3,7,8,9-HxCDD 10.3 46.8 ND 112,3,4,6,7,8-HpCDD 15.0 46.8 ND OCDD 15.0 93.6 ND Internal Standard % Recov D13 Qual % Recoveries 13C-2,3,7,8-TCDF 58 13C-1,2,3,7,8-PeCDF 69 13C-2,3,4,7,8-PeCDF 63 13C-1,2,3,4,7,8-HxCDF 61 13C-1,2,3,6,7,8-HxCDF 64 13C-2,3,4,6,7,8-HxCDF 65 13C-1,2,3,7,8,9-HxCDF 55 13C-1,2,3,4,6,7,8-HpCDF 72 13C-1,2,3,4,7,8,9-HpCDF 85 13C-2,3,7,8-TCDD 17 13C-1,2,3,7,8-PeCDD 76 13C-1*,2,3,4,7,8-HxcbD 67 13C-1,2,3,6,7,8-HxCDD 73 3C-1,2,3,4,6,7,8-HpCDD 72 13C-OCDD 56 GERG/TAMU Date: 8/25/95 PCDDIPCDF Analysis Page 9 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. Texas Coast Samples LAB SAMPLE ID K9607 CLIENT SAMPLE ID GBYC INSTRUMENT DATA FILE 5071 8LCA03-S 13 WET WEIGHT 10.07 DRY WEIGHT 1.27 PERCENT SOLIDS 12.59 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX021 0 EXTRACTION DATE 6-5-95 ANALYSIS DATE 7-18-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 140 3.80 7.89 DB225 1,2,3,7,8-PeCDF 2.15 39.4 ND 2,3,4,7,8-PeCDF 3.00 39.4 ND 1,2,3,4,7,8-HxCDF 9.99 39.4 ND 1,2,3,6,7,8-HxCDF 8.31 39.4 ND 2,3,4,6,7,8-HxCDF 10.4 39.4 ND 1 i2,3,7i8,9-H-xCDF 14.3 39.4 ND 1,2,34,6,7 ' 8-HpCDF 9.03 39.4 ND 1,2,3:4,7,8,9-HpCDF 9.14 39.4 ND OCDF 14.7 78.9 ND 2,3,7,8-TCDD 50.8 50.8 ND 1,2,3,7,8-PeCDD 15.2 39.4 ND 1,2,3,4,7,8-HxCDD 8.03 39.4 ND 1,2,3,6,7,8-HxCDD 8.46 39.4 ND 1,2,3,7,8,9-HxCDD 8.59 39.4 ND 1,2,3,4,6,7,8-HpCDD 10.8 39.4 ND OCDD 18.1 78.9 ND Internal Standard % Recov D13 Qual % Recoveries 13C-2,3,7,8-TCDF 52 13C-1,2,3,7,8-PeCDF 58 13C-2,3,4,7,8-PeCDF 55 13C-1,2,3,4,7,8-HxCDF 56 13C-1,2,3,6,7,8-HxCDF 65 13C-2,3,4,6,7,8-HxCDF 58 13C-1,2,3,7,8,9-HxCDF 56 13C-1,2,3,4,6,7,8-HpCDF 61 13C-1,2,3,4,7,8,9-HpCDF 74 1:3C-2,3,7,8-TCDD 64 13C-1,2,3,7,8-PeCDD 55 13C@1,2,3,4,7,8-HxCDD 76 13C-1,2,3,6,7,8-HxCDD 72 3C-1,2,3,4,6,7,8-HpCDD 68 13C-OCDD 56 GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 10 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Sample LAB SAMPLE ID K9563 CLIENT SAMPLE ID PBPI INSTRUMENT DATA FILE 50718LCA03-S14 WET WEIGHT 10.17 DRY WEIGHT 2.23 PERCENT SOLIDS 21.94 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX021 0 EXTRACTION DATE 6-5-95 ANALYSIS DATE 7-18-95 Compound Name Conc EDL LMCL DBQual (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 1.48 4.48 ND 1,2,3,7,8-PeCDF 1.82 22.4 ND 2,3,4,7,8-PeCDF 2.21 22.4 ND 1,2,3,4,7,8-HxCDF 3.28 22.4 ND 1,2,3,6,7,8-HxCDF 3.57 22.4 ND 2,3,4,6-17.,8-HxCDF 4.79 22.4 ND. 1,2-3,7,8,9-HXCDF .5.6.9. 22.4 ND 1,2,3,4,6,7,8-HpCDF 4.98 22.4 ND 1,2,3,4,7,8,9-HpCDF 6.38 22.4 ND OCDF 7.77 44.8 ND 2,3,7,8-TCDD 1.31 4.48 ND 1,2,3,7,8-PeCDD 3.50 22.4 ND 1,2,3,4,7,8-HxCDD 4.16 22.4 ND 1,2,3,6,7,8-HxCDD 4.52 22.4 ND 1,2,3,7,8,9-HxCDD 4.50 22.4 ND 1,2,3,4,6,7,8-HpCDD 3.51 22.4 ND OCDD 6.06 44.8 ND Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 62 13C-1,2,3,7,8-PeCDF 64 13C-2,3,4,7,8-PeCDF 64 13C-1,2,3,4,7,8-HxCDF 64 13C-1,2,3,6,7,8-HxCDF 64 13C-2,3,4,6,7,8-HxCDF 61 13C-1,2,3,7,8,9-HxCDF 62 13C-1,2,3,4,6,7,8-HpCDF 72 13C-1,2,3,4,7,8,9-HpCDF 76 13C-2,3,7,8-TCDD 74 13C-1,2,3,7,8-PeCDD 72 13C-1,2,3,4,7,8-HxCDD 77 13C-1,2,3,6,7,8-HxCDD 79 3C-1,2,3,4,6,7,8-HpCDD 74 13C-OCDD 64 GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 11 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Sample LAB SAMPLE ID K9573 CLIENT SAMPLE ID BIBI INSTRUMENT DATA FILE 50718LCA03-S15 WET WEIGHT 10.09 DRY WEIGHT 1.14 PERCENT SOLIDS 11.29 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX021 0 EXTRACTION DATE 6-5-95 ANALYSIS DATE 7-18-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 4.34. 8.78 ND 1,2,3,7,8-PeCDF 9.29 43.9 ND 2,3,4,7,8-PeCDF 12.1 43.9 ND 1,2,3,4,7,8-HxCDF 5.61 43.9 ND 1,2,3,6,7,8-HxCDF 5.47 43.9 ND 2,3,4,6,7,8-HxCDF .6.92 43.9 ND 1,2,-3,7,8,9@-HxCDF 9.83 43;9 ND.. 1,2,3,4,6,7,8-HOCDF -8.08 43 * 9 ND 1,2,3,4,7,8,9-HpCDF 10.1 43.9 ND OCDF 12.7 87.8 ND 2,3,7,8-TCDD 3.30 8.78 ND 1,2,3,7,8-PeCDD 9.10 43.9 ND 1,2,3,4,7,8-HxCDD 8.56 43.9 ND 1,2,3,6,7,8-HxCDD 8.98 43.9 ND 1,2,3,7,8,9-HxCDD 9.08 43.9 ND 1,2,3,4,6,7,8-HpCDD 14.5 43.9 ND OCDD 14.4 87.8 ND Internal Standard Recov D13 Qual % Recoveries 13C-2,3,7,8-TCDF 61 13C-1,2,3,7,8-PeCDF 65 13C-2,3,4,7,8-PeCDF 62 13C-1,2,3,4,7,8-HxCDF 68 13C-1,2,3,6,7,8-HxCDF 68 13C-2,3,4,6,7,8-HxCDF 64 13C-1,2,3,7,8,9-HxCDF 65 13C-1,2,3,4,6,7,8-HpCDF 72 13C-1,2,3,4,7,8,9-HpCDF 78 13C-2,3,7,8-TCDD 70 13C-1,2,3,7,8-PeCDD 66 13C-1,2,3,4,7,8-HxCDD 77 13C-1 12,3,6,7,8-HxCDD 81 3C-1,2,3,4,6,7,8-HpCDD 70 13C-OCDD 63 GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 12 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Sample LAB SAMPLE ID K9567 CLIENT SAMPLE ID NBDU INSTRUMENT DATA FILE 50718LCA03-S 18 WET WEIGHT 10.18 DRY WEIGHT 1.95 PERCENT SOLIDS 19.17 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX021 0 EXTRACTION DATE 6-5-95 ANALYSIS DATE 7-18-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 1.36 5.1 ND 1,2,3,7,8-PeCDF 2.43 25.6 ND 2,3,4,7,8-PeCDF :3.09 25.6 ND i,2,3,4,7,8-HxCDF 11.0 25.6 ND 1,2,3,6,7,8-HxCDF 9.14 25.6 NO 2,3,4,6,7,8-HxCDF 12.3 25.6 ND 1,2,3,7,8,9;@HxCDF. 15.8 25.6 ND 1,2,3,4,6,7,8-HpCDF 6.02 25.6 ND 1,2,3,4,7,8,9-HpCDF 8.84 25.6 NO OCDF 3.84 51.2 ND 2,3,7,8-TCDD 1.33 5.1 ND 1,2,3,7,8-PeCDD 4.90 25.6 ND 1,2,3,4,7,8-HxCDD 5.08 25.6 ND 1,2,3,6,7,8-HxCDD 5.37 25.6 ND 1,2,3,7,8,9-HxCDD 5.44 25.6 NO 1,2,3,4,6,7,8-HpCDD 4.91 25.6 ND OCDD 7.08 51.2 NO, Internal Standard % Recov DI3 Qual % Recoveries 13C-2,3,7,8-TCDF 63 13C-1,2,3,7,8-PeCDF 73 13C-2,3,4,7,8-PeCDF 70 13C-1,2,3,4,7,8-HxCDF 64 13C-1,2,3,6,7,8-HxCDF 68 13C-2,3,4,6,7,8-HxCDF 63 13C-1,2,3,7,8,9-HxCDF 62 13C-1,2,3,4,6,7,8-HpCDF 72 13C-1,2,3,4,7,8,9-HpCDF 76 13C-2,3,7,8-TCDD 87 13C-1,2,3,7,8-PeCDD 78 13C-1,2,3,4,7,8-HxCDD 79 13C-1,2,3,6,7,8-HxCDD 75 3C-1,2,3,4,6,7,8-HpCDD 81 13C-OCDD 71 GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 13 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Sample LAB SAMPLE ID Q1 0597 CLIENT SAMPLE ID INSTRUMENT DATA FILE 50718LCA03-S4 WET WEIGHT 1.00 DRY WEIGHT 1.00 PERCENT SOLIDS CALCULATION BASIS DRY SAMPLE TYPE BLANK MATRIX QC BATCH DX021 0 EXTRACTION DATE 6-5-95 ANALYSIS DATE 7-18-95 Conc EDL LMCL DBQuaI Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 3.20 10.0 ND 1,2,3,7,8-PeCDF 2.90 50.0 ND 2,3,4,7,8-PeCDF 3.70 50.0 ND 1,2,3,4,7,8-HxCDF 5.93 50.0 ND 1,2,3,6,7,8-HxCDF 4.27 50.0 ND 2,3,4,6,7,8-HxCDF 5.54 50.0 ND 1,2,3,7,8,9-HxCDF 8.73 -50.0 ND 1,2,3,4,6,7,8-HpCDF 6.86 50.0 ND 1,2,3,4,7,8,9-HpCDF 8.39 50.0 ND OCDF 36.2 100 ND 2,3,7,8-TCDD 3.26 10.0 ND 1,2,3,7,8-PeCDD 5.34 50.0 ND 1,2,3,4,7,8-HxCDD 7.47 50.0 ND 1,2,3,6,7,8-HxCDD 7.47 50.0 ND 1,2,3,7,8,9-HxCDD 7.69 50.0 ND 1,2,3,4,6,7,8-HpCDD 8.66 50.0 ND OCDD 14.2 100 ND. Internal Standard % Recov D13 Qual % Recoveries 13C-2,3,7,8-TCDF 64 13C-1,2,3,7,8-PeCDF 62 13C-2,3,4,7,8-PeCDF 65 13C-1,2,3,4,7,8-HxCDF 64 13C-1,2,3,6,7,8-HxCDF 69 13C-2,3,4,6,7,8-HxCDF 64 13C-1,2,3,7,8,9-HxCDF 60 13C-1,2,3,4,6,7,8-HpCDF 66 13C-1,2,3,4,7,8, 9-HpCDF 68 13C-2,3,7,8-TCDD 13C-1,2,3,7,8-PeCDD 67 13C-1,2,3,4,7,8-HxCDD 69 13C-1,2,3,6,7,8-HxCDD 75 3C-1,2,3,4,6,7,8-HpCDD 56 13C-OCDD 30 GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 14 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Sample LAB SAMPLE ID Q10599 CLIENT SAMPLE ID PBPI , INSTRUMENT DATA FILE 50718LCA03-S19 WET WEIGHT 10.40 DRY WEIGHT 2.21 PERCENT SOLIDS 21.25 CALCULATION BASIS DRY SAMPLE TYPE DUP MATRIX TISSUE QC BATCH DX021 0 EXTRACTION DATE 6-5-95 ANALYSIS DATE 7-18-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 0.48 4.52 ND 1,2,3,7,8-PeCDF 1.40 22.6 ND 2,3,4,7,8-PeCDF 1.83 22.6 ND 1,2,3,4,7,8-HxCDF 1.24 22.6 ND 1,2,3,6,7,8-HxCDF 1.16 22.6 ND 2,3,4,6,7,8-HxCDF 1.49 22.6 ND 1,2,3,7,8,9-HxCDF' 2.26 22.6 ND 112,3,4,6,7,8-HpCDF 4.23 22.6 ND 1,2,3,4,7,8,9-HpCDF 4.51 22.6 ND OCDF 5.63 45.2 ND 2,3,7,8-TCDD 0.45 4.52 ND 1,2,3,7,8-PeCDD 1.40 22.6 ND 1,2,3,4,7,8-HxCDD 2.18 22.6 ND 1,2,3,6,7,8-HxCDD 2.03 22.6 ND 1,2,3,7,8,9-HxCDD 2.17 22.6 ND 1,2,3,4,6,7,8-HpCDD 1.78 22.6 ND OCDD 2.84 45.2 ND Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 72 13C-1,2,3,7,8-PeCDF 74 13C-2,3,4,7,8-PeCDF 71 13C-1,2,3,4,7,8-HxCDF 75 13C-1,2,3,6,7,8-HxCDF 73 13C-2,3,4,6,7,8-HxCDF 70 13C-1,2,3,7,8,9-HxCDF 69 13C-1,2,3,4,6,7,8-HpCDF 78 13C-1,2,3,4, 7,8,9-HpCDF 87 13C-2,3,7,8-TCDD 91 13C-1,2,3,7,8-PeCDD 80 13C-1,2,3,4,7,8-HxCDD 81 13C-1,2,3,6,7,8-HxCDD 86 3C-1,2,3,4,6,7,8-HpCDD 80 13C-OCDD 71 GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 15 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Sample LAB SAMPLE ID K9563 Q10599 CLIENT SAMPLE ID PBPI PBPI INSTRUMENT DATA FILE 50718LCA03-S14 50718LCA03-.S19 WET WEIGHT 10.17 10.40 DRY WEIGHT 2.23 2.21 PERCENT SOLIDS 21.94 21.25 CALCULATION BASIS DRY DRY SAMPLE TYPE SAMP DUP MATRIX TISSUE TISSUE QC BATCH DX021 0 DX021 0 EXTRACTION DATE 6-5-95 6-5-95 ANALYSIS DATE 7-18-95 7-18-95 Conc Conc RPD DB Compound Name (pg/g) (pg/g) Qual 2,3,7,8-TCDF 1,2,3,7,8-PeCDF 2,3,4,7,8-PeCDF 1,2,3,4,7,8-HxCDF 1,2,3,6,7,8-HxCDF 2,3,4,6,7,8-HxCDF 1,2,3,7,8,9-HxCDF 1,2,3,4,6,7,8-HpCDF 1,2,3,4,7,8,9-HpCDF OCDF 2,3,7,8-TCDD 1,2,3,7,8-PeCDD 1,2,3,4,7,8-HxCDD 1,2,3,6,7,8-HxCDD 1,2,3,7,8,9-HxCDD 1,2,3,4,6,7,8-HpCDD OCDD Internal Standard % Recoveries 13C-2,3,7,8-TCDF 13C-1,2,3,7,8-PeCOF 13C-2,3,4,7,8-PeCDF 13C-1,2,3,4,7,8-HxCDF 13C-1,2,3,6,7,8-HxCDF 13C-2,3,4,6,7,8-HxCDF 13C-1,2,3,7,8,9-HxCDF 13C-1,2,3,4,6,7,8-HpCDF 13C-1,2,3,4,7,8,9-HpCDF 13C-2,3,7,8-TCDD 13C-1,2,3,7,11-PeCDD 13C-1,2,3,4,7,8-HxCDD 13C-1,2,3,6,7,8-HxCDD 3C-1,2,3,4,6,7,8-HpCDD 13C-OCDD GERG[TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 16 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Sample LAB SAMPLE ID Q1 0600 CLIENT SAMPLE ID PBPl INSTRUMENT DATA FILE 50718LCA03-S21 WET WEIGHT 10.24 DRY WEIGHT 2.08 PERCENT SOLIDS 20.35 CALCULATION BASIS DRY SAMPLE TYPE MS MATRIX TISSUE QC BATCH DX021 0 EXTRACTION DATE 6-5-95 ANALYSIS DATE 7-18-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 475 3.69 4.80 1,2,3,7,8-PeCDF 2163 25.4 24.0 2,3,4,7,8-PeCDF 2180 29.4 24.0 1,2,3,4,7,8-HxCDF 2137 7.15 24.0 1,2,3,6,7,8-HxCDF 2238 7.22 24.0 2,3,4,6,7,8-HxCDF 2218 8.80 24.0 1,2,3,7,8,9-HxCDF 2119 13.1 24.0 1,2,3,4,6,7,8-HpCDF 2180 9.17 24.0 1,2,3,4,7,8,9-HpCDF 2471 11.1 24.0 OCDF 4112 18.3 48.0 2,3,7,8-TCDD 361 8.14 4.80 1,2,3,7,8-PeCDD 1832 9.07 24.0 1,2,3,4,7,8-HxCDD 1807 6.90 24.0 1,2,3,6,7,8-HxCDD 1748 7.14 24.0 1,2,3,7,8,9-HxCDD 1737 7.26 24.0 1,2,3,4,6,7,8-HpCDD 2021 10.2 24.0 OCDD 3671 5.83 48.0. Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 68 13C-1,2,3,7,8-PeCDF 68 13C-2,3,4,7,8-PeCDF 74 13C-1,2,3,4,7,8-HxCDF 68 13C-1,2,3,6,7,8-HxCDF 70 13C-2,3,4,6,7,8-HxCDF 66 13C-1,2,3,7,8,9-HxCDF 62 13C-1,2,3,4,6,7,8-HpCDF 81 13C-1,2,3,4,7,8,9-HpCDF 73 13C-2,3,7,8-TCDD 80 13C-1,2,3,7,8-PeCOD so 13C-1,2,3,4,7,8-HxCDD 85 13C-1,2,3,6,7,8-HxCDD 89 3C-1,2,3,4,6,7,8-HpCDD 78 13C-OCDD 76 GERGITAMU Date: 8/25/95 PCDD/PCDF Analysis Page 17 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Sample LAB SAMPLE ID K9563 Ql 0600 CLIENT SAMPLE ID PBPI PBPI INSTRUMENT DATA FILE 50718LCA03-S14 50718LCAO3-S21 WET WEIGHT 10.17 10.24 DRY WEIGHT 2.23 2.08 PERCENT SOLIDS 21.94 20.35 CALCULATION BASIS DRY DRY SAMPLE TYPE SAMP IVIS MATRIX TISSUE TISSUE QC BATCH DX021 0 DX021 0 EXTRACTION DATE 6-5-95 6-5-95 ANALYSIS DATE 7-18-95 7-18-95 Conc Spike Arnnt Conc Recov DB Compound Name (pg/g) (pg/g) (pg/g) Qua[ 2,3,7,8-TCDF 384 475 124 1,2,3,7,8-PeCDF 1919 2163 113 2,3,4,7,8-PeCDF 1919 2180 114 1,2,3,4,7,8-HxCDF 1919 2137 ill 1,2,3,6,7,8-HxCDF 1919 2238 117 2,3,4,6,7,8-HxCDF 1919 2218 116 1,2,3,7,8,9-HxCDF 1919 2119 110 1,2,3,4,6,7,8-HpCDF 1919 2180 114 1,2,3,4,7,8,9-HpCDF 1919 2471 129 OCDF 3839 4112 107 2,3,7,8-TCDD 384 361 94 1,2,3,7,8-PeCDD 1919 1832 95 1,2,3,4,7,8-HxCDD 1919 1807 94 1,2,3,6,7,8-HxCDD 1919 1748 91 1,2,3,7,8,9-HxCDD 1919 1737 90 1,2,3,4,6,7,8-HpCDD 1919 2021 105 OCDD 3839 3671 96 Internal Standard % Recoveries 13C-2,3,7,8-TCDF 13C-1,2,3,7,8-PeCDF 13C-2,3,4,7,8-PeCDF 13C-1,2,3,4,7,8-HxCDF 13C-1,2,3,6,7,8-HxCDF 13C-2,3,4,6,7,8-HxCDF 13C-1,2,3,7,8,9-HxCDF 13C-1,2,3,4,6,7,8-HpCDF 13C-1,2,3,4,7,8,9-HpCDF 13C-2,3,7,8-TCDD 13C-1,2,3,7,8-PeCDD 13C-1,2,3,4,7,8-HxCDD 13C-1,2,3,6,7,8-HxCDD 3C-1,2,3,4,6,7,8-HpCDD 13C-OCDD GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 18 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Sample LAB SAMPLE ID Q1 0601 CLIENT SAMPLE ID PBPI INSTRUMENT DATA FILE 50718LCA03-S22 WET WEIGHT 10.08 DRY WEIGHT 2.05 PERCENT SOLIDS 20.32 CALCULATION BASIS DRY SAMPLE TYPE MSD MATRIX TISSUE QC BATCH DX021 0 EXTRACTION DATE 6-5-95 ANALYSIS DATE 7-18-95 Compound Name Conc EDL LMCL DBQual (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 513 2.42 4.88 1,2,3,7,8-PeCDF 2266 15.1 24.4 2,3,4,7,8-PeCDF 2444 19.0 24.4 1,2,3,4,7,8-HxCDF 1978 2.59 24.4 1,2,3,6,7,8-HxCDF 2222 2.73 24.4 2,3,4,6,7,8-HxCDF 2042 3.42 24.4 1,2,3,7,8,9-HxCDF 1978 4.66 24.4 1,2,3,4,6,7,8-HpCDF 2376 4.55 24.4 1,2,3,4,7,8,9-HpCDF 2199 5.03 24.4 OCDF 4691 27.6 48.8 2,3,7,8-TCDD 405 4.48 4.88 1,2,3,7,8-PeCDD 1855 3.78 24.4 1,2,3,4,7,8-HxCDD 1752 8.33 24.4 1,2,3,6,7,8-HxCDD 1882 7.98 24.4 1,2,3,7,8,9-HxCDD 1945 8.51 24.4 1,2,3,4,6,7,8-HpCDD 1717 5.87 24.4 OCDD 4109 5.21 48.8 Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 65 13C-1,2,3,7,8-PeCDF 62 13C-2,3,4,7,8-PeCDF 66 13C-1,2,3,4,7,8-HxCDF 70 13C-1,2,3,6,7,8-HxCDF 68 13C-2,3,4,6,7,8-HxCDF 70 13C-1,2,3,7,8,9-HxCDF 66 13C-1,2,3,4,6,7,8-HpCDF 75 13C-1,2,3,4,7,8,9-HpCDF 80 13C-2,3,7,8-TCDD 72 13C-1,2,3,7,8-PeCDD 76 13C-1,2,3,4,7,8-HxCDD 81 13C-1,2,3,6,7,8-HxCDD 74 3C-1,2,3,4,6,7,8-HpCDD 86 13C-OCDD 68 GERG[TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 19 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Sample LAB SAMPLE ID K9563 Q10601 CLIENT SAMPLE ID PBPI PBPI INSTRUMENT DATA FILE 50718LCA03-S14 50718LCA03-.S22 WET WEIGHT 10.17 10.08 DRY WEIGHT 2.23 2.05 PERCENT SOLIDS 21.94 20.32 CALCULATION BASIS DRY DRY SAMPLE TYPE SAMP MSD MATRIX TISSUE TISSUE QC BATCH DX021 0 DX021 0 EXTRACTION DATE 6-5-95 6-5-95 ANALYSIS DATE 7-18-95 7-18-95 Conc Spike Amnt Conc Recov DI3 Compound Name (pg/g) (pg/g) (pg/g) M Qual 2,3,7,8-TCDF 391 513 131 Q 1,2,3,7,8-PeCDF 1953 2266 116 2,3,4,7,8-PeCDF 1953 2444 125 1,2,3,4,7,8-HxCDF 1953 1978 101 1,2,3,6,7,8-HxCDF 1953 2222 114 2,3,4,6,7,8-HxCDF 1953 2042 105 1,2,3,7,8,9-HxCDF 1953 1978 101 1,2,3,4,6,7,8-HpCDF 1953 2376 122 1,2,3,4,7,8,9-HpCDF 1953 2199 113 OCDF 3906 4691 120 2,3,7,8-TCDD 391 405 104 1,2,3,7,8-PeCDD 1953 1855 95 1,2,3,4,7,8-HxCDD 1953 1752 90 1,2,3,6,7,8-HxCDD 1953 1882 96 1,2,3,7,8,9-HxCDD 1953 1945 100 1,2,3,4,6,7,8-HpCDD 1953 1717 88 OCDD 3906 4109 105 Internal Standard % Recoveries 13C-2,3,7,8-TCDF 13C-1,2,3,7,8-PeCDF 13C-2,3,4,7,8-PeCDF 13C-1,2,3,4,7,8-HxCDF 13C-1,2,3,6,7,8-HxCDF 13C-2,3,4,6,7,8-HxCDF 13C-1,2,3,7,8,9-HxCDF 13C-1,2,3,4,6,7,8-HpCDF 13C-1,2,3,4,7,8,9-HpCDF 13C-2,3,7,8-TCDD 13C-1,2,3,7,8-PeCDD 13C-1,2,3,4,7,8-HxCDD 13C-1,2,3,6,7,8-HxCDD 3C- 1, 2,3,4,6,7,8-HpCDD 13C-OCDD GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 20 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Sample LAB SAMPLE ID Q10600 Q10601 CLIENT SAMPLE ID PBPI PBPI INSTRUMENT DATA FILE 50718LCA03-S21 50718LCA03-@S22 WET WEIGHT 10.24 10.08 DRY WEIGHT 2.08 2.05 PERCENT SOLIDS 20.35 20.32 CALCULATION BASIS DRY DRY SAMPLE TYPE MS MSD MATRIX TISSUE TISSUE QC BATCH DX021 0 DX021 0 EXTRACTION DATE 6-5-95 6-5-95 ANALYSIS DATE 7-18-95 7-18-95 Conc Conc RPD DB Compound Name (pg/g) (pg/9) M Qual 2,3,7,8-TCDF 475 513 8 1,2,3,7,8-PeCDF 2163 2266 5 2,3,4,7,8-PeCDF 2180 2444 11 1,2,3,4,7,8-HxCDF 2137 1978 8 1,2,3,6,7,8-HxCDF 2238 2222 1 2,3,4,6,7,8-HxCDF 2218 2042 8 1,2,3,7,8,9-HxCDF 2119 1978 7 1,2,3,4,6,7,8-HpCDF 2180 2376 9 1,2,3,4,7,8,9-HpCDF 2471 2199 12 OCDF 4112 4691 13 2,3,7,8-TCDD 361 405 12 1,2,3,7,8-PeCDD 1832 1855 1 1,2,3,4,7,8-HxCDD 1807 1752 3 1,2,3,6,7,8-HxCDD 1748 1882 7 1,2,3,7,8,9-HxCDD 1737 1945 11 1,2,3,4,6,7,8-HpCDD 2021 1717 16 OCDD 3671 4109 11 Internal Standard % Recoveries 13C-2,3,7,8-TCDF 13C-1,2,3,7,8-PeCDF 13C-2,3,4,7,8-PeCDF 13C-1,2,3,4,7,8-HxCDF 13C-1,2,3,6,7,8-HxCDF 13C-2,3,4,6,7,8-HxCDF 13C-1,2,3,7,8,9-HxCDF 13C-1,2,3,4,6,7,8-HpCDF 13C-1,2,3,4,7,8,9-HpCDF 13C-2,3,7,8-TCDD 13C-1,2,3,7,8-PeCDD 13C-1,2,3,4,7,8-HxCDD 13C-1,2,3,6,7,8-HxCDD 3C-1,2,3,4,6,7,8-HpCDD 13C-OCDD GERG/TAMU Date: 8/25/95 PCDD/PCDF Analysis Page 21 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Sample LAB SAMPLE ID Q10532 CLIENT SAMPLE ID INSTRUMENT DATA FILE 50718LCA03-S20 WET WEIGHT 8.86 DRY WEIGHT PERCENT SOLIDS CALCULATION BASIS WET SAMPLE TYPE SRM CARP-1 MATRIX TISSUE QC BATCH DX021 0 EXTRACTION DATE 6-5-95 ANALYSIS DATE 7-18-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 17.7 1.13 1.13 DB225 1,2,3,7,8-PeCDF 14.0 2.84 5.65 2,3,4,7,8-PeCDF 14.0 3.30 5.65 1,2,3,4,7,8-HxCDF 1.94 5.65 ND 1,2,3,6,7,8-HxCDF 1.64 5.65 ND 2,3,4,6,7,8-HxCDF 2.10 5.65 ND 1,2,3,7,8,9-HxCDF 3.45 5.65 ND 1,2,3,4,6,7,8-HpCDF 1.25 5.65 ND 1,2,3,4,7,8,9-HpCDF 1.82 5.65 ND OCDF 6.99 11.3 ND 2,3,7,8-TCDD 8.65 0.52 1.13 1,2,3,7,8-PeCDD 2.08 5.65 ND 1,2,3,4,7,8-HxCDD 1.13 5.65 ND 1,2,3,6,7,8-HxCDD 1.28 5.65 ND 1,2,3,7,8,9-HxCDD 1.26 5.65 ND 1,2,3,4,6,7,8-HpCDD 4.56 5.65 ND OCDD 2.50 11.3 ND Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 81 13C-1,2,3,7,8-PeCDF 80 13C-2,3,4,7,8-PeCDF 80 13C-1,2,3,4,7,8-HxCDF 73 13C-1,2,3,6,7,8-HxCDF 79 13C-2,3,4,6,7,8-HxCDF 74 13C-1,2,3,7,8,9-HxCDF 65 13C-1,2,3,4,6,7,8-HpCDF 85 13C-1,2,3,4,7,8,9-HpCDF 84 13C-2,3,7,8-TCDD 95 13C-1,2,3,7,8-PeCDD 83 13C-1,2,3,4,7,8-HxCDD 91 13C-1,2,3,6,7,8-HxCDD 85 3C-1,2,3,4,6,7,8-HpCDD 83 GERG/TAMU 13C-OCDD 59 Date: 8/25/95 PCDD/PCDF Analysis Page 22 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. East Coast Sample LAB SAMPLE ID Q1 0532 CARP-1 CLIENT SAMPLE ID INSTRUMENT DATA FILE 50718LCA03-S20 WET WEIGHT 8.86 DRY WEIGHT PERCENT SOLIDS CALCULATION BASIS WET SAMPLE TYPE SRM CARP-1 SRM MATRIX TISSUE TISSUE QC BATCH DX021 0 EXTRACTION DATE 6-5-95 ANALYSIS DATE 7-18-95 Conc Concensus Conc. .Recy Compound Name (pg/g) -(Pg/g) (%) 2,3,7,8-TCDF 17.7 11.9 149 112,3,7,8-PeCDF 14.0 5.0 279 2,3,4,7,8-PeCDF 14.0 1,2,3,4,7,8-HxCDF 1,2,3,6,7,8-HxCDF 2,3,4,6,7,8-HxCDF 1,2,3,7,8,9-HxCDF 1,2,3,4,6,7,8-HpCDF 1,2,3,4,7,8,9-HpCDF OCDF 2,3,7,8-TCDD 8.65 6.6 131 1,2,3,7,8-PeCDD 4.4 1,2,3,4,7,8-HxCDD 1.9 1,2,3,6,7,8-HxCDD 5.6 1,2,3,7,8,9-HxCDD 0.7 1,2,3,4,6,7,8-HpCDD 6.5 OCDD 6.3 Internal Standard % Recoveries 13C-2,3,7,8-TCDF 13C-1,2,3,7,8-PeCDF 13C-2,3,4,7,8-PeCDF 13C-1,2,3,4,7,8-HxCDF 13C-1,2,3,6,7,8-HxCDF 13C-2,3,4,6,7,8-HxCDF 13C-1,2,3,7,8,9-HxCDF 13C-1,2,3,4,6,7,8-HpCDF 13C-1,2,3,4,7,8,9-HpCDF 13C-2,3,7,8-TCDD 13C-1,2,3,7,8-PeCDD 13C-1,2,3,4,7,8-HxCDD 13C-1,2,3,6,7,8-HxCDD 3C-1,2,3,4,6,7,8-HpCDD 13C-OCDD GERG/TAMU Date: 8/25195 PCDD/PCDF Analysis Page 1 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. West Coast Samples LAB SAMPLE ID K9379 CLIENT SAMPLE ID IBNJ INSTRUMENT DATA FILE 50719LCA01-S5 WET WEIGHT 10.30 DRY WEIGHT 1.83 PERCENT SOLIDS 1739 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX021 1 EXTRACTION DATE 6-7-95 ANALYSIS DATE 7-19-95 Conc EDL LMCL DBQual Compound Name (pg/9) (pg/g) (pg/g) 2,3,7,8-TCDF 4.00 0.95 5.46 1 1,2,3,7,8-PeCDF 1.15 27.3 ND 2,3j4,7,8-PeCDF 1.40 27.3 ND 1,2,3,4,7,8-HxCDF 0.98 27.3 ND 1,2,3,6,7,8-HxCDF 0.89 27.3 ND 2,3,4,6,7,8-HxCDF 1.08 27.3 ND 1,2,3,7,8,9-HxCDF 2.66 1.66 27.3 1 1,2,3,4,6,7,8-HpCDF 1.79 27.3 ND 1,2,3,4,7,8,9-HpCDF 2.37 27.3 ND OCDF 4.17 54.6 ND 2 - 3,7,8-TCDD 1.12. 1.5.46 ND 1 1,2,3,7,8-PeCDD 2.08 27.3 ND 1,2,3,4,7,8-HxCDD 2.20 27.3 ND 1 @, 2,3,6,7,8-H xC D D 2.20 27.3 N D 1,2,3,7,8,9-HxCDD 2.27 27.3 N D 1,2,3,4,6,7,8-HpCDD 2.39 27.3 N D OCDD 10.8 2.92 54.6 Internal Standard % Recov DB Qual 1@ Recoveries 13C-2,3,7,8-TCDF 71 13C-1,2,3,7,8-PeCDF 80 13C-2,3,4,7,8-PeCDF 83 13C-1,2,3,4,7,8-HxCDF 63 13C-1,2,3,6,7,8-HxCDF 73 13C-2,3,4,6,7,8-HxCDF 71 13C-1,2,3,7,8,9-HxCDF 67 13C-1,2,3,4,6,7,8-HpCDF 73 13C-1,2,3,4,7,8,%-HpCDF 80 13C-2,3,7,8-TCDD 87 13C-1,2,3,7,8-PeCDD 83 13C-1,2,3,4,7,8-HxCDD 76 13C-1,2,3,6,7,8-HxCDD 82 3C-1,2,3,4,6,7,8-HpCDD 74 13C-OCDD 62 GERG/TAMU Date: 8/9/95 PCDD/PCDF Analysis Page 2 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. West Coast Samples LAB SAMPLE* ID K9381 CLIENT SAMPLE ID SDHI INSTRUMENT DATA FILE 50719LCA01-S6 WET WEIGHT 10.08 DRY WEIGHT 0.95 PERCENT SOLIDS 9.4.1 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX021 1 EXTRACTION DATE 6-7-95 ANALYSIS DATE 7-19-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 73.5 5.33 10.5 DB225 1,2,3,7,8-PeCDF 5.22 52.7 ND 2,3,4,7,8-PeCDF 10.7 52.7 ND 1,2,3,4,7,8-HxCDF 2.11 52.7 ND 1,2,3,6,7,8-HxCDF 1.95 52.7 ND 2,3,4,6,7,8-HxCDF 2.48 52.7 ND 1,2,3,7,8,9-HxCDF 5.48 52.7 ND 1,2,3,4,6,7,8-HpCDF 4.87 52.7 ND 1,2,3,4,7,8,9-HpCDF 2.22 52.7 ND OCDF 8.97 5.52 105 4.79 10.5 ND-- 2,3,7,8-TCDD i.,2,3,7,8-PeCDD 6.63 52.7 ND 1,2,3,4,7,8-HxCDD 3.84 52.7 ND 1,,2,3,6,7,8-HxCDD 3.64 52.7 ND 1,2,3,7,8,9-HxCDD 3.84 52.7 ND 1,2,3,4,6,7,8-HpCDD 29.8 2.66 52.7 1 OCDD 172 3.11 105 Internal Standard % Recov DB Qual @/o Recoveries 13C-2,3,7,8-TCDF 73 13C-1,2,3,7,8-PeCDF MI 13C-2,3,4,7-18-PeCDF M1 13C-1,2,3,4,7,8-HxCDF 59 13C-1,2,3,6,7,8-HxCDF 65 13C-2,3,4,6,7,8-HxCDF 64 13C-1,2,3,7,8,9-HxCDF 66 13C-1,2,3,4,6,7,8-HpCDF 80 13C-1,2,3,4,7,8,9zHpCDF 93 13C-2,3,7,8-TCDD 120 13C-1,2,3,7,8-PeCDD MI 13C-1,2,3,4,7,8-HxCDD 75 13C-1,2,3,6,7,8-HxCDD 81 3C-1,2,3,4,6,7,8-HpCDD 85 13C-OCDD 7.2 GERG/TAMU Date: 8/9/95 PCDD/PCDF Analysis Page 3 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. West Coast Samples LAB SAMPLE ID K9383 CLIENT SAMPLE ID SDCB INSTRUMENT DATA FILE 50719LCA01-S7 WET WEIGHT 10.43 DRY WEIGHT 1.56 PERCENT SOLIDS 14.93 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX021 1 EXTRACTION DATE 6-7-95 ANALYSIS DATE 7-19-95 Cone EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 83.8 0.52 6.42 DB225 1,2,3,7,8-PeCDF 5.64 1.16 32.1 1 2,3,4,7,8-PeCDF 11.3 32.1 ND 1,2,3,4,7,8-HxCDF 0.73 1.10 32.1 1,2,3,6,7,8-HxCDF 1.09 1.07 32.1 2,3,4,6,7,8-HxCDF 2.31 32.1 ND 1,2,3,7,8,9-HxCDF 2.84 1.83 32.1 1,2,3,4,6,7,8-HpCDF 5.36 0.64 32.1 1,2,3,4,7,8,9-HpCDF 0.72 32.1 ND OCDF 7.40 1.28 64.2 2,3,7,8-TCDD 0.96 0.43. 6.42 -.J 1,2,3,7,8-PeCDD 3.73 0.85 32.1 1,2,3,4,7,8-HxCDD 1.15 32.1 ND 1)2,3,6,7,8-HxCDD 1.18 32.1 ND 1,2,3,7,8,9-HxCDD 1.21 32.1 ND 1,2,1,4,6,7,8-HpCDD 29.7 0.70 32.1 OCDD 165 0,76 64*2 Intern,al Standard % Recov DB Qual @/o Recoveries 13C-2,3,7,8-TCDF 67 13C-1,2,3,7,8-PeCDF 88 13C-2,3,4,7-18-PeCDF 89 13C-1,2,3,4,7,8-HxCDF 69 13C-1,2,3,6,7,8-HxCDF 71 13C-2,3,4,6,7,8-HxCDF 68 13C-1,2,3,7,8,9-HxCDF 73 13C-1,2,3,4,6,7,8-HpCDF 82 13C-1,2,3,4,7,8,.9,;HpCDF 95 13C-2,3,7,8-TCDD 92 13C-1,2,3,7,8-PeCDD 93 13C-1,2,3,4,7,8-HxCDD 84 13C-1,2,3,6,7,8-HxCDD 81 3C-1,2,3,4,6,7,8-HpCDD 87 13C-OCDD 79 GERGITAMU Date: 8/9/95 PCDD/PCDF Analysis Page 4 CLIENT NAME NOAA PROJECTNAME NS&TYear10 PURCHASE ORDER NO. West Coast Samples LAB SAMPLE ID K9385 CLIENT -SAMPLE ID 'MBVB IN STRUMENT DATA FILE 50719LCA01-S8 WET WEIGHT 10.14 DRY WEIGHT 1.59 PERCENT SOLIDS 15,63 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX021 1 EXTRACTION DATE 6-7-95 ANALYSIS DATE 7-19-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 3.91 0.53 6.31 1,2,3,7,8-PeCDF 1.06 31.5 ND 2,3,4,7,8-PeCDF 1.23 31.5 ND 1,2,3,4,7,8-HxCDF 0.63 31.5 ND 1,2,3,6,7,8-HxCDF 0.59 31.5 ND 2,3,4,6,7,8-HxCDF 0.77 31.5 ND 1,2,3,7,8,9-HxCDF 3.38 1.13 31.5 1 1,2,3,4,6,7,8-HpCDF 0.94 31.5 ND 1,2,3,4,7,8,9-HpCDF 1.05 31.5 ND OCDF 2.56 63.1 ND 6.81 ND 2f21,7j8-TCDP. 0'. 6 8 1,2,3,7,8-PeCDD 1.71 31.5 ND 1,2,3,4,7,8@HxCDD 1.53 31.5 ND 152,3,6,7,8-HxCDD 1.49 31.5 ND 1,2,3,7,8,9-HxCDD 1.55 31.5 ND 1,2,1,4,6,7,8-HpCDD 4.42 0.58 31.5 1 OCDD 12.9 2.04 63.1 1 internal Standard % Recov DB Qual 61o Recoveries 13C-2,3,7,8-TCDF 64 13C-1,2,3,7,8-PeCDF 75 13C-2,3,4,7-,8-PeCDF 80 13C-1,2,3,4,7,8-HxCDF 64 13C-1,2,3,6,7,8-HxCDF 66 13C-2,3,4,6,7,8-HxCDF 63 13C-1,2,3,7,8,9-HxCDF 65 13C-1,2,3,4,6,7,8-HpCDF 68 13C-1,2,3,4,7,8a-HpCDF 78 13C-2,3,7,8-TCDD 82 13C-1,2,3,7,8-PeCDD 82 13C-1,2,3,4,7,8-HxCDD 71 13C-1,2,3,6,7,8-HxCDD 77 3C-1,2,3,4,6,7,8-HpCDD 67 13C-OCDD 53 GERG/TAMU Date: 8/9/95 PCDD/PCDF Analysis Page 5 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO.. West Coast Samples LAB SAMPLE ID K9387 CLIENT. SAMPLE ID ABWJ INSTRUMENT DATA FILE 50719LCA01 -S9 WET WEIGHT 10.60 DRY WEIGHT 2.42 PERCENT SOLIDS 22.' 81 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX021 1 EXTRACTION DATE 6-7-95 ANALYSIS DATE 7-19-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 7.97 0.21 4.14 DB225 1,2,3,7,8-PeCDF 0.78 20.7 ND 2,3,4,7,8-PeCDF 1.87 0.56 20.7 1 1,2,3,4,7,8-HxCDF 0.62 20.7 ND 1,2,3,6,7,8-HxCDF 0.60 20.7 ND 2,3,4,6,7,8-HxCDF 0.76 20.7 ND 1,2,3,7,8,9-HxCDF 1.77 1.10 20.7 1,2,3,4,6,7,8-HpCDF 1.63 20.7 ND 1,2,3,4,7,8,9-HpCDF 0.50 20.7 ND OCDF 3.13 0.80 41.4 1 2,3,7,8-TCDD 0.63 0.29 1,2,3' 7,8-PeCDD 1.15 20.7 ND 1,2,3,4,7,8-HxCDD 0.51 20.7 ND 1,,2,3,6,7,8-HxCDD 0.52 20.7 ND 1,2,3,7,8,9-HxCDD 0.54 20.7 ND 1,2,3,4,6,7,8-HpCDD 9.36 0.65 20.7 1 OCDD 43.9 0.40 41.4 Internal Standard % Recov DB Qual @/o Recoveries 13C-2,3,7,8-TCDF 67 13C-1,2,3,7,8-PeCDF 80 13C-2,3,4,7,8-PeCDF 80 13C-1,2,3,4,7,8-HxCDF 67 13C-1,2,3,6,7,8-HxCDF 67 13C-2,3,4,6,7,8-HxCDF 64 13C-1,2,3,7,8,9-HxCDF 68 13C-1,2,3,4,6,7,8-HpCDF 69 13C-1,2,3,4,7,8,9 ,@-HpCDF 84 13C-2,3,7,8-TCDD 83 13C-1,2,3,7,8-PeCDD 81 13C-1,2,3,4,7,8-HxCDD 72 13C-1,2,3,6,7,8-HxCDD 71 3C-1,2,3,4,6,7,8-HpCDD 72 13C-OCDD 62 GERGITAMU Date: 8/9/95 PCDDIPCDF Analysis Page 6 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 .PURCHASE ORDER NO. West Coast Samples LAB SAMPLE ID K9397 CLIENT SAMPLE'ID QSBJ- INSTRUMENT DATA FILE 50719LCA01-SlO WET WEIGHT 10.20 DRY WEIGHT 2.10 PERCENT SOLIDS 20.56 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX021 1 EXTRACTION DATE 6-7-95 ANALYSIS DATE 7-19-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg1g) 2,3,7,8-TCDF 1.05 0.23 4.77 T- 1,2,3,7,8-PeCDF 0.69 23.8 ND 2,3,4,7,8-PeCDF 0.55 23.8 ND 1,2,3,4,7,8-HxCDF 0.47 23.8 ND 1,2,3,6,7,8-HxCDF 0.47 23.8 ND 2,3,4,6,7,8-HxCDF 0.60 23.8 ND 1,2,3,7,8,9-HxCDF 2.77 23.8 ND 1,2,3,4,6,7,8-HpCDF 1.99 23.8 ND 1,2,3,4,7,8,9-HpCDF 0.49 23.8 ND OCDF 4.10 1.99 47.7 1 2,3,1.,8-TCDD 01.48 4.77 ND 1,2,3,7,8-PeCDD 0.80 23.8 ND 1,2,3,4,7,8-HxCDD 0.59 23.8 ND 1@2,3,6,7,8-HxCDD 0.60 23.8 ND 1,2,3,7,8,9-HxCDD 0.62 23.8 ND 1,2,@,4,6,7,8-HpCDD 7.99 23.8 ND OCDD 32.8 0.50 47.7 1 Internal Standard % Recov DB Qual @/o Recoveries 13C-2,3,7,8-TCDF 58 13C-1,2,3,7,8-PeCDF 67 13C-2,3,4,7-,8-PeCDF 69 13C-1,2,3,4,7,8-HxCDF 53 13C-1,2,3,6,7,8-HxCDF 53 13C-2,3,4,6,7,8-HxCDF 51 13C-1,2,3,7,8,9-HxCDF 54 13C-1,2,3,4,6,7,8-HpCDF 54 13C-1,2,3,4,7,8,9:HpCDF 65 13C-2,3,7,8-TCDD 70 13C-1,2,3,7,8-PeCDD 69 13C-1,2,3,4,7,8-HxCDD 62 13C-1,2,3,6,7,8-HxCDD 62 3C-1,2,3,4,6,7,8-HpCDD 56 13C-OCDD 40 GERG/TAMU Date: 8/9/95 PCDD/PCDF Analysis Page 7 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. West Coast Samples LAB SAMPLE iD K9399 CLIENT SAMPLE ID PLLH INSTRUMENT DATA FILE 50719LCA01-Sl 1 WET WEIGHT 10.08 DRY WEIGHT 1.56 PERCENT SOLIDS 15.46 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX021 1 EXTRACTION DATE 6-7-95 ANALYSIS DATE 7-19-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 4.75 0.37 6.42 1 1,2,3,7,8-PeCDF 0.92 32.1 ND 2,3,4,7,8-PeCDF 2.55 32.1 ND 1,2,3,4,7,8-HxCDF 0.63 32.1 ND 1,2,3,6,7,8-HxCDF 1 *37 0,62 32,1 J 2,3,4,6,7,8-HxCDF 1.91 32.1 ND 1,2,3,7,8,9-HxCDF 4.17 32.1 ND 1,2,3,4,6,7,8-HpCDF 2.40 0.95 32.1 1 1,2,3,4,7,8,9-HpCDF 1.15 32.1 ND OCDF 0.80 64.2 ND 2,-3,7,&TCDD 0.44 6.42 ND 1,2,3,7,8-PeCDD 2.34 1.22 32.1 1 1,2,3,4,7,8-HxCDD 0.60 32.1 ND 1)2,3,6,7,8-HxCDD 0.58 32.1 ND 1,2,3,7,8,9-HxCDD 0.61 32.1 ND 1,2,1,4,6,7,8-HpCDD 10.8 32.1 ND OCDD 48*3 0,37 64*2 J Internal Standard % Recov DB Qual @/o Recoveries 13C-2,3,7,8-TCDF 70 13C-1,2,3,7,8-PeCDF 83 13C-2,3,4,7-18-PeCDF 89 13C-1,2,3,4,7,8-HxCDF 64 13C-1,2,3,6,7,8-HxCDF 66 13C-2,3,4,6,7,8-HxCDF 64 13C-1,2,3,7,8,9@HxCDF 66 13C-1,2,3,4,6,7,8-HpCDF 69 13C-1,2,3,4,7,8,9;HpCDF 81 13C-2,3,7,8-TCDD 88 13C-1,2,3,7,8-PeCDD 93 13C-1,2,3,4,7,8-HxCDD 73 13C-1,2,3,6,7,8-HxCDD 76 3C-1,2,3,4,6,7,8-HpCDD 70 13C-OCDD 53 GERGITAMU Date: 8/9/95 PCDD/PCDF Analysis Page 8 CLIENT NAME NOAA PROJECTNAME NS&TYear10 PURCHASE ORDER NO. West Coast Samples CAB SAMPLE ID K9401 CLIENT SAMPLE ID LJLJ INSTRUMENT DATA FILE 50719LCA01-S12 WET WEIGHT 10.34 DRY WEIGHT 2.29 PERCENT SOLIDS 22.11 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX021 1 EXTRACTION DATE 6-7-95 ANALYSIS DATE 7-19-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pgjg) (pg/g) 2,3,7,8-TCDF 1.46 0.33 4.37 1,2,3,7,8-PeCOF 0.23 21.9 ND 2,3,4,7,8-PeCDF 0.29 21.9 ND 1,2,3,4,7,8-HxCOF 0.60 21.9 ND 1,2,3,6,7,8-HxCDF 0.56 21.9 ND 2,3,4,6,7,8-HxCDF 0.77 21.9 ND 1,2,3,7,8,9-HxCOF 2.60 0.97 21.9 1,2,3,4,6,7,8-HpCDF 0.36 21.9 ND 1,2,3,4,7,8,9-HpCOF 0.39 21.9 ND OCOF 0.42 43.7 ND 2,3,7,8-tCDD 0.1 4.37 ND 1,2,3,7,8-PeCDD 0.82 21.9 ND 1,2,3,4,7,8-HxCDD 0.44 21.9 ND 1,@2,3,6,7,8-HxCDD 0.40 21.9 ND 1,2,3,7,8,9-HxCDD 0.43 21.9 ND .1,2,:S,4,6,7,8-HpCDD 4.67 0.3 21.9 1 OCDD 20.6 0.38 43.7 internal Standard % Recov DB Quaf .0/o Recoveries 13C-2,a,7,8-TCDF 60 13C-1,2,3,7,8-PeCDF 80 13C-2,3,4,7i8-PeCDF 80 13C-1,2,3,4,7,8-HxCDF 63 13C-1,2,3,6,7,8-HxCDF 62 13C-2,3,4,6,7,8-HxCDF 60 13C-1,2,3,7,8,9-HxCDF 65 13C-1,2,3,4,6,7,8-HpCDF 67 13C-1,2,3,4,7,8,9,@"pCDF 80 13C-2,3,7,8-TCDD 73 13C-1,2,3,7,8-PeCDD 83 13C-1,2,3,4,7,8-HxCDD 66 13C-1,2,3,6,7,8-HxCDD 67 3C-1,2,3,4,6,7,8-HpCDD 72 13C-OCDD 62 GERG/TAMU Date: 8/9/95 PCDD/PCDF Analysis Page 9 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. West Coast Samples LAB SAMPLE ID K9504 CLIENT SAMPLE'll) SFEM INSTRUMENT DATA FILE 50719LCA01-S13 WET WEIGHT 10.33 DRY WEIGHT 1.47 PERCENT SOLIDS 14,27 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX021 1 EXTRACTION DATE 6-7-95 ANALYSIS DATE 7-19-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 8.98 0.34 6.78 DB225 1,2,3,7,8-PeCDF 1.85 33.9 ND 2,3,4,7,8-PeCDF 2.78 33.9 ND 1,2,3,4,7,8-HxCDF 1.10 33.9 ND 1,2,3,6,7,8-HxCDF 1.05 33.9 ND 2,3,4,6,7,8-HxCDF 1.34 33.9 ND 1,2,3,7,8,9-HxCDF 1.83 33.9 ND 1,2,3,4,6,7,8-HpCDF 2.52 1.37 33.9 1 1,2,3,4,7,8,9-HpCDF 1.56 33.9 ND OCDF 4.15 0.81 67.8 1 2,3,7,8-TCDD 0.23 .6.78 ND 1,2,3,7,8-PecbD 0.54 33.9 ND 1,2,3,4,7,8-HxCDD. 0.49 33.9 ND 1 @ 2,3,6,7,8-H xC D D 0.46 33.9 N D 1,2,3,7,8,9-HxCDD 0.49 33.9 N D 1,2,1,4,6,7,8-HpCDD 12.2 0.36 33.9 1 OCDD 44*2 0"110 67*8 J Internal Standard % Recov DB Qual Recoveries 13C-2,3,7,8-TCDF 81 13C-1,2,3,7,8-PeCDF 100 13C-2,3,4,7-18-PeCDF 105 13C-1,2,3,4,7,8-HxCDF 73 13C-1,2,3,6,7,8-HxCDF 73 13C-2,3,4,6,7,8-HxCDF 73 13C-1,2,3,7,8,9-HxCDF 75 13C-1,2,3,4,6,7,8-HpCDF 84 13C-1,2,3,4,7,8,9;HpCDF 96 13C-2,3,7,8-TCDD 96 13C-1,2,3,7,8-PeCDD 101 13C-1,2,3,4,7,8-HxCDD 85 13C-1,2,3,6,7,8-HxCDD 88 3C-1,2,3,4,6,7,8-HpCDD 87 13C-OCDD 75 GERGITAMU Date: 8/9/95 PCDD/PCDF Analysis Page 10 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. West Coast Samples LAB SAMPLE ID K9506 CLIENT SAMPLE ID SFSM INSTRUMENT DATA FILE 50719LCA01-S14 WET WEIGHT 10.17 DRY WEIGHT 1.41 PERCENT SOLIDS 13..84 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX0211 EXTRACTION DATE 6-7-95 ANALYSIS DATE 7-19-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 2.28 7.10 ND 1,2,3,7,8-PeCDF 4.64 35.5 ND 2,3,4,7,8-PeCDF 4.53 35.5 ND 1,2,3,4,7,8-HxCDF 3.82 35.5 ND 1,2,3,6,7,8-HxCDF 3.72 35.5 ND 2,3,4,6,7,8-HxCDF 4.46 35.5 ND 1,2,3,7,8,9-HxCDF 6.10 35.5 ND 1,2,3,4i6,7,8-HpCDF 4.84 1.08 35.5 1 1,2,3,4,7,8,9-HpCDF 1.07 35.5 ND OCDF 0.71 71.0 ND 2,3,7,8-TCDD 1.60 7.10 ND 1,2,3,7,8-PeCDD 2.33 35.5 ND 1,2,3,4,7,8-HxCDD 1.15 35.5 ND 1,,2,3,6,7,8-HxCDD 1.15 35.5 ND 1,2,3,7,8,9-HxCDD 1.19 35.5 ND 1,2,1,4,6,7,8-HpCDD 8.89 35.5 ND OCDD 24.8 2.72 71.0 1 Internal Standard % Recov DB Qual Recoveries 13C-2,3,7,8-TCDF 66 13C-1,2,3,7,8-PeCDF MI 13C-2,3,4,718-PeCDF MI 13C-1,2,3,4,7,8-HxCDF 54 13C-1,2,3,6,7,8-HxCDF 56 13C-2,3,4,6,7,8-HxCDF 56 13C-1,2,3,7,8,9-HxCDF 60 13C-1,2,3,4,6,7,8-HpCDF 74 13C-1,2,3,4,7,8,,g.jipCDF 93 13C-2,3,7,8-TCDD 125 13C-1,2,3,7,8-PeCDD MI 13C-1,2,3,4,7,8-HxCDD 65 13C-1,2,3,6,7,8-HxCDO 69 3C-1,2,3,4,6,7,8-HpCDD 82 13C-OCDD 60 GERG/TAMU Date: 8/9/95 PCDD/PCDF Analysis Page 11 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. West Coast Samples LAB SAMPLE ID K9508 CLIENT SAMPLE ID SFDB INSTRUMENT DATA FILE 50719LCA01-Sl 5 WET WEIGHT 10.04 DRY WEIGHT 1.15 PERCENT SOLIDS 11,42 CALCULATION BASIS DRY SAMPLE TYPE SAMP MATRIX TISSUE QC BATCH DX021 1 EXTRACTION DATE 6-7-95 ANALYSIS DATE 7-19-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 8.43 0.50 8.72 1 1,2,3,7,8-PeCDF 1.48 43.6 ND 2,3,4,7,8-PeCDF 1.8 '0 43.6 ND 1,2,3,4,7,8-HxCDF 2.04 43.6 ND 1,2,3,6,7,8-HxCDF 1.96 43.6 ND 2,3,4,6,7,8-HxCDF 2.56 43.6 ND 1,2,3,7,8,9-HxCDF 5.38 3.52 43.6 1 1,2,3,4,6,7,8-HpCDF 0.75 43.6 ND 1,2,3,4,7,8,9-HpCDF 0.80 43.6 ND OCDF 1.44 87.2 ND 2,3,7,8-TCDD 0.47 8.72 ND 1,2,3,7,8-PeCDD 2.34 43.6 ND 1,2,3,4,7,8-HxCDD 1.52 43.6 ND 1)2,3,6,7,8-HxCDD 1.66 43.6 ND 1,2,3,7,8,9-HxCDD 1.66 43.6 ND 1,2,3,4,6,7,8-HpCDD 17.4 0.81 43.6 1 OCDD 44,4 87,2 ND Internal Standard % Recov DB Qual .'@/o Recoveries 13C-2,3,7,8-TCDF 68 13C-1,2,3,7,8-PeCDF 87 13C-2,3,4,7-18-PeCDF 89 13C-1,2,3,4,7,8-HxCDF 69 13C-1,2,3,6,7,8-HxCDF 69 13C-2,3,4,6,7,8-HxCDF 66 13C-1,2,3,7,8,9-HxCDF 68 13C-1,2,3,4,6,7,8-HpCDF 74 13C-1,2,3,4, 7,8,9.;HpCDF 90 13C-2,3,7,8-TCDD 87 13C-1,2,3,7,8-PeCDD 91 13C-1,2,3,4,7,8-HxCDD 77 13C-1,2,3,6,7,8-HxCDD 73 3C-1,2,3,4,6,7,8-HpCDD 77 13C-OCDD 57 GERGITAMU Date: 8/9/95 PCDD/PCDF Analysis Page 12 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 ORDER NO. West Coast Samples LAB SAMPLE ID Q10610 CLIENT SAMPLE ID INSTRUMENT DATA FILE 50719LCA01-S4 WET WEIGHT 1.00 DRY WEIGHT 1.00 PERCENT SOLIDS CALCULATION BASIS DRY SAMPLE TYPE BLANK MATRIX QC BATCH DX021 1 EXTRACTION DATE 6-7-95 ANALYSIS DATE 7-19-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 0.90 10.0 ND 1,2,3,7,8-PeCDF 1.09 50.0 ND 2,3,4,7,8-PeCDF 1.31 50.0 ND 1,2,3,4,7,8-HxCDF 1.26 50.0 ND 1,2,3,6,7,8-HxCDF 1.16 50.0 ND 2,3,4,6,7,8-HxCDF 1.40 1.49 50.0 1,2,3,7,8,9-HxCDF 2.30. 50.0 ND 1,2,3,4,6,7,8-HpCDF 1.46 50.0 ND 1,2,3,4,7,8,9-HpCDF 2.10 50.0 ND OCDF 5.49 100 ND 2,3,7,8-TCDD 0.93 10.0 ND 1,2,3,7,8-PeCDD 2.61 50.0 ND 1,2,3,4,7,8-HxCDD 2.09 50.0 ND 1;2,3,6,7,8-HxCDD 2.03 50.0 ND 1,2,3,7,8,9-HxCDD 2.11 50.0 ND 1,2,3,4,6,7,8-HpCDD 2.75 50.0 ND OCDD 3.52 100 ND Internal Standard % Recov DB Qual . 1@o Recoveries 13C-2,3,7,8-TCDF 86 13C-1,2,3,7,8-PeCDF 98 13C-2,3,4,7,8-PeCDF 98 13C-1,2,3,4,7,8-HxCDF 89 13C-1,2,3,6,7,8-HxCDF 103 13C-2,3,4,6,7,8-HxCDF 93 13C-1,2,3,7,8,9@HxCDF 89 13C-1,2,3,4,6,7,8-HpCDF 91 13C-1,2,3,4,7,8,9@;HpCDF 91 13C-2,3,7,8-TCDD 108 13C-1,2,3,7,8-PeCDD 98 13C-1,2,3,4,7,8-HxCDD 95 13C-1,2,3,6,7,8-HxCDD 108 3C-1,2,3,4,6,7,8-HpCDD 90 13C-OCDD 81 GERG/TAMIJ Date: 8/9/95 PCDD/PCDF Analysis Page 13 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. West Coast Samples LAB SAMPLE ID Q10611 CLIENT SAMPLE ID ABWJ INSTRUMENT DATA FILE 50719LCA01-S16 WET WEIGHT 10.15 DRY WEIGHT 2.33 PERCENT SOLIDS 22, 99 CALCULATION BASIS DRY SAMPLE TYPE DUP MATRIX TISSUE QC BATCH DX021 1 EXTRACTION DATE 6-7-95 ANALYSIS DATE 7-19-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg1g) (pg/g) 2,3,7,8-TCDF 7.86 0.20 4.29 DB225 1,2,3,7,8-PeCDF 0.73 21.4 ND 2,3,4,7,8-PeCDF 0.88 21.4 ND 1,2,3,4,7,8-HxCDF 0.36 21.4 ND 1,2,3,6,7,8-HxCDF 0.35 21.4 ND 2,3,4,6,7,8-HxCDF 0.43 21.4 ND 1,2,3,7,8,9-HxCDF 0.53 21.4 ND 1,2,3,4,6,7,8-HpCDF 0.37 21.4 ND 1,2,3,4,7,8,9-HpCDF 0.41 21.4 ND OCDF 0.58 42.9 ND 2,3,7,8-TCDD 0.74 4.29 ND 1,2,3,7,8-PeCDD 1.34 21.4 ND 1,2,3,4,7,8-HxCDD 0.52 21.4 ND 1,2,3,6,7,8-HxCDD 0.55 21.4 ND 1,2,3,7,8,9-HxCDD 0.56 21.4 ND 1,2,3@,4,6,7,8-HpCDD 11.2 0.52 21.4 1 OCDD 48.6 42.9 ND Internal Standard % Recov DB Qual % Recoveries 13C-2,3,7,8-TCDF 80 13C-1,2,3,7,8-PeCDF 95 13C-2,3,4,7,8-PeCDF 98 13C-1,2,3,4,7,9-HxCDF 73 13C-1,2,3,6,7,8-HxCDF 73 13C-2,3,4,6,7,8-HxCDF 72 13C-1,2,3,7,8,9-HxCDF 80 13C-1,2,3,4,6,7,8-HpCDF 85 13C-1,2,3,4,7,8,9- 102 ,VpCDF 13C-2,3,7,8-TCDD 42 13C-1,2,3,7,8-PeCDD 96 13C-1,2,3,4,7,8-HxCDD 84 13C-1,2,3,6,7,8-HxCDD 82 3C-1,2,3,4,6,7,8-HpCDD 90 13C-OCDD 78 GERG/TAMU Date: 8/9/95 PCDD/PCDF Analysis Page 14 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. West Coast Samples LAB SAMPLE ID K9387 Q10611 CLIENT SAMPLE ID ABWJ ABWJ INSTRUMENT DATA FILE 50719LCA01-S9 50719LCA01-S16 WET WEIGHT 10.60 10.15 DRY WEIGHT 2.42 2.33 PERCENT SOLIDS 22.8.1 22.99 CALCULATION BASIS DRY DRY SAMPLE TYPE SAMP DUP MATRIX TISSUE TISSUE QC BATCH DX021 1 DX021 1 EXTRACTION DATE 6-7-95 6-7-95 ANALYSIS DATE 7-19-95 7-19-95 Conc Conc RPD DB Compound Name (pg/g) (pg/g) M Qual . 2,3,7,8-TCDF 7.97 7.86 1 1,2,3,7,8-PeCDF 2,3,4,7,8-PeCDF 1.87 1,2,3,4,7,8-HxCDF 1,2,3,6,7,8-HxCDF 2,3,4,6,7,8-HxCDF 1,2,3,7,8,9-HxCDF 1.77 1,2,3,4,6,7,8-HpCDF 1,2,3,4,7,8,9-HpCDF OCDF 3.13 2,3,7,8-TCDD 0.63 1,2,3,7,8-PeCDD 1,2,3,4,7,8-HxCDD 1,2,3,6,7,8-HxCDD 1,2,3,7,8,9-HxCDD 1,2,3,4,6,7,8-HpCDD 9.36 11.2 17 OCDD 43.9 Internal Standard % Aecoveries 13C-2,3,7,,8-TCDF 13C-1,2,3,7,8-PeCDF 13C-2,3,4,7,8-PeCDF 13C-1,2,3,4,7,8-HxCDF 13C-1,2,3,6,7,8-HxCDF 13C-2,3,4,6,7,8-HxCDF 13C-1,2,3,7,8,9-HxCDF 13C-1,2,3,4,6,7,8-HpCDF 13C-1,2,3,4,7,8,9-),ApCDF 13C-2,3,7,8-TCDD 13C-1,2,3,7,8-PeCDD 13C-1,2,3,4,7,8-HxCDD 13C-1,2,3,6,7,8-HxCDD 3C-1,2,3,4,6,7,8-HpCDD 13C-OCDD GERG/TAMU Date: 819/95 PCDD/PCDF Analysis Page 15 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. West Coast Samples LAB SAMPLE ID Q1 0613 CLIENT SAMPLE ID ABWJ INSTRUMENT DATA FILE 50719LCA01 -S1 8 WET WEIGHT 10.22 DRY WEIGHT 2.44 PERCENT SOLIDS 23.83 CALCULATION BASIS DRY SAMPLE TYPE MS MATRIX TISSUE QC BATCH DX0211 EXTRACTION DATE 6-7-95 ANALYSIS DATE 7-19-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pg/g) (pg/g) I 2,3,7,8-TCDF 416 0.14 4.11 DB225 1,2,3,7,8-PeCDF 1979 8.26 20.5 2,3,4,7,8-.PeCDF 2184 9.66 20.5 1,2,3,4,7,8-HxCDF 1798 0.92 20.5 1,2,3,6,7,8-HxCDF 1857 0.89 20.5 2,3,4,6,7,8-HxCDF 1878 1.11 20.5 1,2,3,7,8,9-HxCDF 1782 1.37 20.5 1,2,3,4,6,7,8-HpCDF 1943 0.44 20.5 1,2,3,4,7,8,9-HpCDF 1890 0.43 20.5 OCDF 4105 0.39 41.1 2,3,7,8-TCDD 288 0.14 4.11 1,2,3,7,8-PeCDD 1887 1.23 20.5 1,2,3,4,7,8-HxCDD 1827 0.40 20.5 1@2,3,6,7,8-HxCDD 1824 0.42 20.5 1,2,3,7,8,9-HxCDD 1894 0.43 20.5 1,2A4,6,7,8-HpCDD 1687 0.23 20.5 OCDD 3103 0.47 41.1 Internal Standard % Recov DB Qual ' 61o Recoveries 13C-2,3,7,8-TCDF 71 13C-1,2,3,7,8-PeCDF 95 13C-2,3,4,7-18-PeCDF 98 13C-1,2,3,4,7,8-HxCDF 71 13C-1,2,3,6,7,8-HxCDF 67 13C-2,3,4,6,7,8-HxCDF 70 13C-1,2,3,7,8,9@HxCDF 76 13C-1,2,3,4,6,7,8-HpCDF 83 13C-1,2,3,4,7,8,9,;HpCDF 108 13C-2,3,7,8-TCDD 90 13C-1,2,3,7,8-PeCDD 91 13C-1,2,3,4,7,8-HxCDD 76 13C-1,2,3,6,7,8-HxCDD 75 3C-1,2,3,4,6,7,8-HpCDD 97 13C-OCDD 91 GERG/TAMU Date: 8/9/95 PCDD/PCDF Analysis Page 16 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. West Coast Samples LAB SAMPLE ID K9387 010613 CLIENT SAMPLE ID ABWJ ABWJI INSTRUMENT DATA FILE 50719LCA01-S9 50719LCAOI-SlS WET WEIGHT 10.60 10.22 DRY WEIGHT 2.42 2.44 PERCENT SOLIDS 22.8.1 23.83 CALCULATION BASIS DRY DRY SAMPLE TYPE SAMP IVIS MATRIX TISSUE TISSUE QC BATCH DX0211 DX0211 EXTRACTION DATE 6-7-95 6-7-95 ANALYSIS DATE 7-19-95 7-19-95 Conc Spike Amnt Conc Recov DB Compound Name fpg1g) (pg/g) (pg/g) (%) Qual 2,3,7,8-TCDF 7.97 329 416 124 1,2,3,7,8-PeCDF 1643 1979 120 2,3,4,7,8-PeCDF 1.87 1643 2184 133 Q 1,2,3,4,7,8-HxCDF 1643 1798 109 1,2,3,6,7,8-HxCDF 1643 1857 113 2,3,4,6,7,8-HxCDF 1643 1878 114 1,2,3,7,8,9-HxCDF 1.77 1643 1782 108 1643 1943 118 1,2,3,4,6,7,8-HpCDF 1,2,3,4,7,8,9-HpCDF 1643 1890 115 OCDF 3.13 3285 4105 125 2,3,7,8-TCDD 0.63 329 288 88 1,2,3,7,8-PeCDD 1643 1887 115 1,2,3,4,7,8-HxCDD 1643 1827 ill l,Z,3,6,7,8-HxCD[) 1643 1824 ill 1,2,3,7,8,9-HxCDD 1643 1894 115 1,2,3,4,6,7,8-HpCDD 9.36 1643 1687 102 OCDD 43.9 3285 3103 93 Internal, Standard -/.'kecoveries 13C-2,3,7,8-TCDF 13C-1,2,3,7,8-PeCDF 13C-2,3,4,7,8-PeCDF 13C- 1,2,3,4,7,8-HxCDF 13C-1,2,3,6,7,8-HxCDF 13C-2,3,4,6,7,8-HxCDF 13C-1,2,3,7,8,9-HxCDF 13C-1,2,3,4,6,7,8-HpCDF 13C- l,2,3,4,7,8,9-,@HjpCDF 13C-2,3,7,8-TCDD 13C-1,2,3,7,8-PeCDD l3C-l,2,3,4,7,8-HxCDD 13C-1,2,3,6,7,8-HxCDD 3C-1,2,3,4,6,7,8-HpCDD 13C-OCDD GERG/TAMLI Date: 819/95 PCDD/PCDF Analysis Page 17 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. West Coast Samples LAB SAMPLE ID Q1 0614 CLIENT SAMPLE ID ABWJ INSTRUMENT DATA FILE 50719LCA01-S19 WET WEIGHT 10.06 DRY WEIGHT 2.39 PERCENT SOLIDS 23.71 CALCULATION BASIS DRY SAMPLE TYPE MSD MATRIX TISSUE QC BATCH DX021 1 EXTRACTION DATE 6-7-95 ANALYSIS DATE 7-19-95 Conc EDL LMCL DBQual Compound Name (pg/g) (pgg) (pg/g) 2,3,7,8-TCDF 422 0.23 4.19 DB225 1,2,3,7,8-PeCDF 1988 6.59 21.0 2,3,4,7,8-PeCDF 2237 8.39 21.0 1,2,3,4,7,8-HxCDF 1864 0.99 21.0 1,2,3,6,7,8-HxCDF 1776 0.90 21.0 2,3,4,6,7,8-HxCDF 1858 1.14 21.0 1,2,3,7,8,9-HxCDF 1791 1.54 21.0 1,2,3,4,6,7,8-HpCDF 1920 0.81 21.0 1,2,3,4,7,8,9-HpCDF 1868 0.86 21.0 OCDF 4197 0.48 41.9 2,3,7,8-TCDD 306 0.34 4.19 1,2,3,7,8-PeCDD 1989 0.97 21.0 1,2,3,4,7,8-HxCDD 1812 0.75 21.0 1 12,3,6,7,8-HxCDD 1936 0.76 21.0 1,2,3,7,8,9-HxCDD 1932 0.78 21.0 1,2,1,4,6,7,8-HpCDD 1592 0.61 21.0 OCDD 3088 0*59 41*9 Internal Standard % Recov DB Qual A@ Recoveries 13C-2,3,7,8-TCDF 59 13C-1,2,3,7,8-PeCDF 84 13C-2,3,4,71-8-PeCDF 80 13C-1,2,3,4,7,8-HxCDF 59 13C-1,2,3,6,7,8-HxCDF 61 13C-2,3,4,6,7,8-HxCDF 60 13C-1,2,3,7,8,9@HxCDF 62 13C-1,2,3,4,6,7,8-HpCDF 69 13C-1,2,3,4,7,8,9-,HpCDF 82 13C-2,3,7,8-TCDD 68 13C-1,2,3,7,8-PeCDD 77 13C-1,2,3,4,7,8-HxCDD 63 13C-1,2,3,6,7,8-HxCDD 63 3C-1,2,3,4,6,7,8-HpCDD 78 13C-OCDD 66 GERGITAMU Date: 8/9/95 PCDD/PCDF Analysis Page 18 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. West Coast Samples LAB SAMPLE ID K9387 Ql 0614 CLIENT SAMPLE ID ABWJ ABWJ INSTRUMENT DATA FILE 50719LCA01-S9 507191-CA01-S19 WET WEIGHT 10.60 10.06 DRY WEIGHT 2.42 2.39 PERCENT SOLIDS 22.8.1 23.71 CALCULATION BASIS DRY DRY SAMPLE TYPE SAMP MSD MATRIX TISSUE TISSUE OC BATCH DX0211 DX0211 EXTRACTION DATE 6-7-95 6-7-95 ANALYSIS DATE 7-19-95 7-19-95 Conc Spike Amnt Conc Recov DB Compound Name (pg/g) (pg/g) (pg/g) M Qual 2,3,7,8-TCDF 7.97 335 422 123 1,2,3,7,8-PeCDF 1677 1988 119 2,3,4,7,87PeCDF 1.87 1677 2237 133 Q 1,2,3,4,7,8-HxCDF 1677 1864 ill 1,2,3,6,7,8-HxCDF 1677 1776 106 2,3,4,6,7,8-HxCDF 1677 1858 i'll 1,2,3,7,8,9-HxCDF 1.77 1677 1791 107 1,2,3,4,6,7,8-HpCDF 1677 1920 114 1,2,3,4,7,8,9-HpCDF 1677 1868 ill OCDF 3.13 3354 4197 125 2,3,7,8-TCDD 0.63 335 306 91 1,2,3,7,8-PeCDD 1677 1989 119 1,2,3,4,7,8-HxCDD 1677 1812 108 1,2,3,6,7,8-HxCDD 1677 1936 115 1,2,3,7,8,9-HxCDD 1677 1932 115 1,2,3,4,6,7,8-HpCDD 9.36 1677 1592 94 OCDD 43.9 3354 3088 91 Internal. Standard %'@ecoveries 13C-2,3,7,8-TCDF 13C-1,2,3,7,8-PeCDF 13C-2,3,4,7,8-PeCDF 13C-1,2,3,4,7,8-HxCDF 13C-1,2,3,6,7,8-HxCDF 13C-2,3,4,6,7,8-HxCDF 13C-1,2,3,7,8,9-HxCDF 13C-1,2,3,4,6,7,8-HpCDF 13C-1,2,3,4,7,8,9.HpCDF 13C-2,3,7,8-TCDD 13C-1,2,3,7,8-PeCDD 13C-1,2,3,4,7,8-HxCDD 13C-1,2,3,6,7,8-HxCDD 3C-1,2,3,4,6,7,8-HpCDD 13C-OCDD GERG/TAMU Date: 8/9/95 PCDD/PCDF Analysis Page 19 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. West Coast Samples LAB SAMPLE ID Q1 0613 Q10614 CLIENT SAMPLE ID ABWJ ABWJ INSTRUMENT DATA FILE 50719LCA01-S18 50719LCA01 -S 19 WET WEIGHT 10.22 10.06 DRY WEIGHT 2.44 2.39 PERCENT SOLIDS 23.83 23.71 CALCULATION BASIS DRY DRY SAMPLE TYPE MS MSD MATRIX TISSUE TISSUE QC BATCH DX021 1 DX021 1 EXTRACTION DATE 6-7-95 6-7-95 ANALYSIS DATE 7-19-95 7-19-95 Conc Conc RPD DB Compound Name (pg/g) (pg/g) M Qual 2,3,7,8-TCDF 416 422 1 1,2,3,7,8-PeCDF 1979 1988 0 2,3,4,7,8-PeCDF 2184 2237 2 1,2,3,4,7,8-HxCDF 1798 1864 4 1,2,3,6,7,8-HxCDF 1857 1776 4 2,3,4,6,7,8-HxCDF 1878 1858 1 1,2,3,7,8,9-HxCDF 1782 1791 1 1,2,3,4,6,7,8-HpCDF 1943 1920 1 1,2,3,4,7,8,9-HpCDF 1890 1868 1 OCDF 4105 4197 2 2,3,7,8-TCDD 288 306 6 1,2,3,7,8-PeCDD 1887 1989 5 1,2,3,4,7,8-HxCDD 1827 1812 1 1,21,3,6,7,8-HxCDD 1824 1936 6 1,2,3,7,8,9-HxCDD 1894 1932 2 1,2,3,-k,6,7,8-HpCDD 1687 1592 6 OCDD 3103 3088 0 Internal. Standard %'@ecoveries 13C-2,3,7,8-TCDF 13C-1,2,3,7,8-PeCDF 13C-2,3,4,7,8-PeCDF 13C-1,2,3,4,7,8-HxCDF 13C-1,2,3,6,7,8-HxCDF 13C-2,3,4,6,7,8-HxCDF 13C-1,2,3,7,8,9-HxCDF 13C-1,2,3,4,6,7,8-HpCDF 13C-1,2,3,4,7,8,9-;I.JpCDF '. I 13C-2,3,7,8-TCDD 13C-1,2,3,7,8-PeCDD 13C-1,2,3,4,7,8-HxCDD 13C-1,2,3,6,7,8-HxCDD 3C-1,2,3,4,6,7,8-HpCDD 13C-OCDD GERG/TAMU Date: 8/9/95 PCDD/PCDF Analysis Page 20 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. West Coast Samples LAB SAMPLE ID Q10533 CLIENT SAMPLE ID INSTRUMENT DATA FILE 50719LCA01-S17 WET WEIGHT 8.83 DRY WEIGHT PERCENT SOLIDS CALCULATION BASIS WET SAMPLE TYPE SRM CARP-1 MATRIX TISSUE QC BATCH DX021 1 EXTRACTION DATE 6-7-95 ANALYSIS DATE 7-19-95 Conc EDL LMCL DBOual Compound Name (pg/g) (pg/g) (pg/g) 2,3,7,8-TCDF 13.0 0.04 1.13 DB225 1,2,3,7,8-PeCDF 5.19 0.54 5.66 2,3,4,7,8-PeCDF 14.2 0.60 5.66 1,2,3,4,7,8-HxCDF 3.88 0.30 5.66 1,2,3,6,7,8-HxCDF 2.66 0.28 5.66 2,3,4,6,7,8-HxCDF 1.83 0.33 5.66 1,2,3,7,8,9-HxCDF 0.46 5.66 ND 1,2,3,4,6,7,8-HpCDF 5.42 0.26 5.66 1 1,2,3,4,7,8,9-HpCDF 0.27 5.66 ND OCDF 0.23 11.3 ND 2,3,7,8-TCDD 6.02 0.07 1.13 1,2,3,7,8-PeCDD 5.26 0.18 5.66 1,2,3,4,7,8-HxCDD 2.77 0.30 5.66 1)2,3,6,7,8-HxCDD 6.13 0.33 5.66 1,2,3,7,8,9-HxCDD 0.33 5.66 ND 1,2,J,4,6,7,8-HpCDD 6.29 0.15 5.66 OCDD 4.68 0.25 11.3 1 Internal Standard % Recov DB Qual O@o Recoveries 13C-2,3,7,8-TCDF 61 13C-1,2,3,7,8-PeCDF 73 13C-2,3,4,7;8-PeCDF 77 13C-1,2,3,4,7,8-HxCDF 56 13C-1,2,3,6,7,8-HxCDF 57 13C-2,3,4,6,7,8-HxCDF 60 13C-1,2,3,7,8,9-HxCDF 64 13C-1,2,3,4,6,7,8-HpCDF 68 13C-1,2,3,4,7,8,,9z;HpCDF 80 13C-2,3,7,8-TCDD 70 13C-1,2,3,7,8-PeCDD 73 13C-1,2,3,4,7,8-HxCDD 66 13C-1,2,3,6,7,8-HxCDD 62 3C-1,2,3,4,6,7,8-HpCDD 68 13C-OCDD 56 GERG/TAMU Date: 8/9/95 PCDD/PCDF Analysis Page 21 CLIENT NAME NOAA PROJECT NAME NS&T Year 10 PURCHASE ORDER NO. West Coast Samples LAB SAMPLE ID Q1 0533 CARP-1 CLIENT SAMPLE ID INSTRUMENT DATA FILE 50719LCA01-S17 WET WEIGHT 8.83 DRY WEIGHT PERCENT SOLIDS CALCULATION BASIS WET SAMPLE TYPE SRM CARP- I SRM MATRIX TISSUE TISSUE QC BATCH DX021 1 EXTRACTION DATE 6-7-95 ANALYSIS DATE 7-19-95 Conc Concensus Conc. Recy Compound Name (pg/g) (pg/g) M 2,3,7,8-TCDF 13.0 11.9 109 1,2,3,7,8-PeCDF 5.19 5.0 104 2,3,4,7,8-PeCDF 14.2 1,2,3,4,7,8-HxCDF 3.88 1,2,3,6,7,8-HxCDF 2.66 2,3,4,6,7,8-HxCDF 1.83 1,2,3,7,8,9-HxCDF 1,2,3,4,6,7,8-HpCDF 5.42 1, 2,3,4,7,8,9-HpCDF OCDF 2,3,7,8-TCDD 6.02 6.6 91 1,2,3,7,8-PeCDD 5.26 4.4 120 1,2,3,4,7,8-HxCDD 2.77 1.9 146 1,2,3,6,7,8-HxCDD 6.13 5.6 109 1,2,3,7,8,9-HxCDD 0.7 1,2,3,4,6,7,8-HpCDD 6.29 6.5 97 OCDD 4.68 6.3 74 Internal Standard % Recoveries .1 3C-2,3,7,8-TCDF 13C-1,2,3,7,8-PeCDF 13C-2,3,4,7,8-PeCDF 13C-1,2,3,4,7,8-HxCDF 13C-1,2,3,6,7,8-HxCDF 13C-2,3,4,6,7,8-HxCDF 13C-1,2,3,7,8,9-HxCDF 13C-1,2,3,4,6,7,8-HpCDF 13C-1,2,3,4,7,8,9-HpCDF 13C-2,3,7,8-TCDD 13C-1,2,3,7,8-PeCDD 13C-1,2,3,4,7,8-HxCDD 13C-1,2,3,6,7,8-HxCDD 3C-1,2,3,4,6,7,8-HpCDD 13C-OCDD GERG/TAMU Date: 8/9/95 I I I I I I I I I I I I I I I I I I " 1101811111mill I .1 3 6668 14101 8.699 r I